#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:35:19 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181073 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/53/2215389.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215389_Fobs loop_ _publ_author_name 'Sakthivel, P.' 'Joseph, P. S.' 'Sebastiyan, A.' 'Suvaikin, M. Yosuva' 'Ramesh, M.' _publ_section_title ; 1-(Morpholin-4-ylmethyl)pyrrolidine-2,5-dione ; _journal_coeditor_code BT2514 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4143 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.202 _cell_angle_gamma 90.000 _cell_length_a 6.1368 _cell_length_b 7.8038 _cell_length_c 20.9032 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8831 _cod_data_source_file bt2514Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MMS in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 123.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 184.21 173.16 3.19 o 4 0 0 40.04 35.46 3.47 o 6 0 0 26.23 32.55 4.68 o 1 1 0 941.00 882.51 5.99 o 2 1 0 38.26 33.28 0.76 o 3 1 0 226.15 235.24 3.76 o 4 1 0 104.34 115.81 3.19 o 5 1 0 91.82 99.52 3.29 o 6 1 0 169.53 171.69 4.89 o 0 2 0 7752.83 7317.40 83.33 o 1 2 0 444.79 427.19 4.05 o 2 2 0 180.97 182.14 2.37 o 3 2 0 223.53 229.78 2.91 o 4 2 0 24.98 28.62 1.34 o 5 2 0 14.90 21.13 1.88 o 6 2 0 2.80 0.37 1.88 o 1 3 0 1393.97 1417.72 14.59 o 2 3 0 0.34 -0.01 0.30 o 3 3 0 21.87 24.61 0.94 o 4 3 0 0.30 -0.52 0.87 o 5 3 0 0.81 1.27 1.59 o 6 3 0 2.71 2.07 1.90 o 0 4 0 1254.03 1404.98 24.93 o 1 4 0 101.17 100.54 2.01 o 2 4 0 88.22 76.25 1.79 o 3 4 0 31.73 37.52 1.00 o 4 4 0 2.70 2.20 0.75 o 5 4 0 8.31 8.34 2.07 o 6 4 0 0.14 -1.94 1.94 o 1 5 0 0.40 -0.70 0.70 o 2 5 0 278.49 290.88 4.60 o 3 5 0 108.95 113.53 2.85 o 4 5 0 107.68 107.68 2.01 o 5 5 0 32.57 31.05 2.03 o 0 6 0 24.59 24.44 4.05 o 1 6 0 38.46 36.76 1.41 o 2 6 0 254.48 248.75 4.86 o 3 6 0 49.02 47.10 2.78 o 4 6 0 32.06 30.72 2.86 o 5 6 0 0.00 0.40 1.85 o 1 7 0 0.03 2.90 2.48 o 2 7 0 11.87 13.94 1.58 o 3 7 0 56.86 53.48 3.18 o 4 7 0 0.10 -1.98 1.98 o 0 8 0 31.63 35.25 5.88 o 1 8 0 1.53 0.85 2.92 o 2 8 0 12.52 15.87 3.09 o -5 0 1 0.45 -0.23 1.62 o -3 0 1 406.01 415.95 10.78 o -1 0 1 1021.67 987.21 11.53 o 1 0 1 13985.76 12515.07 156.86 o 3 0 1 460.28 489.81 17.54 o 5 0 1 9.13 7.99 2.23 o -6 1 1 27.10 23.69 2.30 o -5 1 1 0.10 -0.88 1.24 o -4 1 1 98.14 106.86 2.22 o -3 1 1 1150.77 1174.02 11.80 o -2 1 1 831.78 846.66 7.13 o -1 1 1 28.18 30.74 0.46 o 0 1 1 307.18 296.90 3.03 o 1 1 1 148.81 152.18 1.29 o 2 1 1 143.58 139.57 1.52 o 3 1 1 1000.00 1026.69 9.59 o 4 1 1 308.72 306.67 5.09 o 5 1 1 101.27 99.45 3.30 o 6 1 1 4.43 1.78 1.64 o -6 2 1 7.39 4.23 2.09 o -5 2 1 0.11 0.82 1.25 o -4 2 1 2.03 1.16 0.66 o -3 2 1 48.28 50.19 1.22 o -2 2 1 217.31 206.04 2.25 o -1 2 1 2814.64 2780.84 23.22 o 0 2 1 1079.80 1091.87 8.78 o 1 2 1 92.76 100.79 1.23 o 2 2 1 148.73 164.49 1.91 o 3 2 1 72.40 69.95 1.38 o 4 2 1 1.88 2.22 0.79 o 5 2 1 16.42 13.13 1.70 o 6 2 1 18.91 15.49 2.55 o -6 3 1 1.55 -0.56 1.74 o -5 3 1 0.55 0.18 1.47 o -4 3 1 50.88 50.95 1.62 o -3 3 1 208.36 226.05 2.68 o -2 3 1 123.41 131.14 1.52 o -1 3 1 855.63 886.37 10.79 o 0 3 1 1401.78 1450.69 14.89 o 1 3 1 411.57 418.07 4.38 o 2 3 1 54.40 50.75 0.95 o 3 3 1 41.88 37.67 1.11 o 4 3 1 51.88 49.62 2.03 o 5 3 1 22.18 22.92 2.40 o 6 3 1 26.52 31.02 2.95 o -6 4 1 0.67 -1.23 2.03 o -5 4 1 3.19 3.03 2.11 o -4 4 1 79.11 77.58 2.22 o -3 4 1 0.19 0.40 0.41 o -2 4 1 40.66 47.84 2.45 o -1 4 1 1861.97 1902.38 21.27 o 0 4 1 38.20 36.08 1.15 o 1 4 1 313.91 332.99 4.04 o 2 4 1 22.03 24.32 1.13 o 3 4 1 4.57 6.14 0.61 o 4 4 1 73.93 82.98 2.05 o 5 4 1 32.09 30.35 2.01 o 6 4 1 25.89 26.83 2.25 o -5 5 1 16.90 19.91 2.42 o -4 5 1 25.05 22.56 1.37 o -3 5 1 74.87 70.49 2.68 o -2 5 1 5.54 2.89 1.00 o -1 5 1 28.41 26.66 1.18 o 0 5 1 58.64 49.90 3.10 o 1 5 1 311.18 315.52 3.70 o 2 5 1 196.59 196.13 3.59 o 3 5 1 358.24 362.04 5.62 o 4 5 1 75.70 76.44 1.84 o 5 5 1 20.00 20.53 1.84 o -5 6 1 0.67 -1.17 1.59 o -4 6 1 73.78 73.15 4.26 o -3 6 1 68.10 66.89 3.17 o -2 6 1 127.31 122.44 3.67 o -1 6 1 0.23 -0.19 0.75 o 0 6 1 5.94 6.90 2.33 o 1 6 1 2.28 3.21 0.73 o 2 6 1 10.80 13.90 1.51 o 3 6 1 106.99 110.08 3.93 o 4 6 1 17.39 13.71 2.25 o -4 7 1 28.28 27.64 4.67 o -3 7 1 4.34 2.75 2.06 o -2 7 1 77.37 75.89 2.74 o -1 7 1 0.39 2.00 3.29 o 0 7 1 34.04 26.31 3.22 o 1 7 1 67.35 65.92 4.37 o 2 7 1 9.19 10.65 1.55 o 3 7 1 4.20 0.46 1.95 o 4 7 1 4.53 2.12 2.50 o -2 8 1 11.51 13.46 2.17 o -1 8 1 3.84 1.22 3.07 o 0 8 1 1.42 -2.55 2.77 o 1 8 1 49.71 44.05 4.42 o 2 8 1 20.60 26.34 2.45 o -6 0 2 61.24 68.76 4.49 o -4 0 2 31.94 25.70 2.29 o -2 0 2 1443.38 1440.19 17.18 o 0 0 2 16.35 7.18 1.68 o 2 0 2 296.94 290.39 4.28 o 4 0 2 607.03 669.96 14.67 o 6 0 2 33.09 34.69 3.61 o -6 1 2 25.99 28.32 2.41 o -5 1 2 8.57 2.64 1.29 o -4 1 2 139.00 152.40 3.96 o -3 1 2 399.02 376.81 4.14 o -2 1 2 140.57 139.89 1.57 o -1 1 2 31.17 38.76 0.58 o 0 1 2 687.04 658.99 10.10 o 1 1 2 120.21 131.07 1.28 o 2 1 2 749.42 734.41 6.40 o 3 1 2 198.74 217.14 2.92 o 4 1 2 39.61 40.97 1.77 o 5 1 2 10.24 9.27 1.61 o 6 1 2 46.01 45.89 2.86 o -6 2 2 14.45 10.80 2.27 o -5 2 2 68.55 62.96 2.65 o -4 2 2 59.29 57.18 1.57 o -3 2 2 256.11 265.68 3.38 o -2 2 2 668.43 679.28 6.54 o -1 2 2 5080.96 4899.88 42.79 o 0 2 2 1180.70 1143.55 8.38 o 1 2 2 5.43 3.85 0.57 o 2 2 2 1610.11 1635.29 13.98 o 3 2 2 398.66 435.86 4.85 o 4 2 2 1.75 2.41 0.67 o 5 2 2 1.45 1.50 1.46 o 6 2 2 53.32 50.14 3.54 o -6 3 2 0.76 2.93 1.95 o -5 3 2 76.47 80.46 3.61 o -4 3 2 0.12 0.90 0.74 o -3 3 2 11.16 11.51 0.72 o -2 3 2 1.06 2.19 0.29 o -1 3 2 393.21 398.22 4.35 o 0 3 2 3251.95 3348.69 27.78 o 1 3 2 91.86 88.21 1.08 o 2 3 2 248.29 241.76 2.60 o 3 3 2 219.18 224.05 2.89 o 4 3 2 1.48 1.12 0.75 o 5 3 2 0.53 0.71 2.46 o 6 3 2 0.95 3.42 2.91 o -6 4 2 9.12 8.39 2.46 o -5 4 2 0.05 -1.20 1.20 o -4 4 2 17.50 19.78 1.56 o -3 4 2 7.29 8.82 0.87 o -2 4 2 26.67 27.99 1.47 o -1 4 2 11.69 10.55 0.87 o 0 4 2 56.26 64.17 1.08 o 1 4 2 306.30 302.81 3.51 o 2 4 2 38.65 39.04 1.08 o 3 4 2 0.08 -0.42 0.51 o 4 4 2 64.68 65.24 1.87 o 5 4 2 37.16 35.64 2.13 o 6 4 2 16.00 18.89 2.67 o -5 5 2 15.00 17.00 1.48 o -4 5 2 48.91 43.49 1.44 o -3 5 2 32.01 27.59 1.28 o -2 5 2 190.66 194.15 3.57 o -1 5 2 153.14 149.95 2.73 o 0 5 2 18.90 21.00 4.55 o 1 5 2 169.24 170.44 2.37 o 2 5 2 1.28 -0.89 0.89 o 3 5 2 267.68 268.08 3.54 o 4 5 2 76.65 74.65 2.06 o 5 5 2 3.79 -0.07 1.26 o -5 6 2 0.51 -1.38 1.38 o -4 6 2 16.94 14.35 3.38 o -3 6 2 145.16 146.89 4.55 o -2 6 2 98.71 100.28 2.96 o -1 6 2 0.86 1.07 0.80 o 0 6 2 152.25 148.70 5.55 o 1 6 2 1.11 0.87 0.68 o 2 6 2 43.90 42.03 2.27 o 3 6 2 6.97 6.88 1.92 o 4 6 2 0.06 -1.92 1.98 o -4 7 2 0.63 -1.50 2.50 o -3 7 2 0.96 -0.37 2.03 o -2 7 2 8.28 7.10 1.52 o -1 7 2 9.47 11.38 2.82 o 0 7 2 4.46 5.04 3.30 o 1 7 2 0.05 -3.02 3.55 o 2 7 2 16.22 17.32 1.97 o 3 7 2 79.50 77.15 8.01 o 4 7 2 3.05 3.87 2.58 o -2 8 2 34.77 35.36 2.65 o -1 8 2 42.74 34.91 3.96 o 0 8 2 18.47 14.55 3.47 o 1 8 2 12.14 6.79 7.33 o 2 8 2 10.54 12.73 2.19 o -5 0 3 56.80 55.80 3.58 o -3 0 3 0.04 0.39 0.73 o -1 0 3 10738.18 10384.96 108.81 o 1 0 3 88.31 110.80 2.39 o 3 0 3 2.16 0.29 1.09 o 5 0 3 509.09 483.06 12.16 o -6 1 3 5.73 2.19 1.59 o -5 1 3 1.25 0.75 1.20 o -4 1 3 0.00 0.56 0.59 o -3 1 3 2.39 0.58 0.45 o -2 1 3 0.85 0.10 0.40 o -1 1 3 15174.55 13886.55 117.66 o 0 1 3 31.16 29.25 0.56 o 1 1 3 170.44 206.82 2.32 o 2 1 3 57.53 62.02 1.09 o 3 1 3 526.33 552.59 6.13 o 4 1 3 34.32 37.56 1.75 o 5 1 3 125.32 122.07 3.82 o 6 1 3 1.36 -0.27 1.58 o -6 2 3 8.50 8.42 2.16 o -5 2 3 7.56 7.04 1.49 o -4 2 3 583.35 583.78 6.63 o -3 2 3 2.24 2.74 0.54 o -2 2 3 4.04 6.12 0.55 o -1 2 3 415.74 384.59 3.61 o 0 2 3 942.98 887.73 7.72 o 1 2 3 8.28 7.77 0.40 o 2 2 3 375.64 374.37 4.63 o 3 2 3 283.50 323.78 5.13 o 4 2 3 46.56 50.89 2.11 o 5 2 3 62.49 59.02 2.75 o 6 2 3 57.30 48.96 3.39 o -6 3 3 0.51 1.67 2.01 o -5 3 3 0.00 0.20 1.11 o -4 3 3 3.37 4.04 0.79 o -3 3 3 13.73 12.91 0.91 o -2 3 3 437.87 453.49 4.62 o -1 3 3 121.34 112.14 1.55 o 0 3 3 1099.70 1118.60 9.57 o 1 3 3 1.76 1.41 0.34 o 2 3 3 236.73 234.78 2.76 o 3 3 3 1.82 0.57 0.56 o 4 3 3 4.50 5.71 0.85 o 5 3 3 18.81 18.43 3.36 o 6 3 3 0.05 0.69 2.23 o -6 4 3 25.96 25.93 2.90 o -5 4 3 0.95 1.33 1.31 o -4 4 3 35.32 41.68 1.48 o -3 4 3 323.22 317.01 4.89 o -2 4 3 63.59 66.27 2.19 o -1 4 3 181.13 173.54 2.53 o 0 4 3 114.78 110.86 1.37 o 1 4 3 0.17 0.64 0.39 o 2 4 3 53.82 57.02 1.13 o 3 4 3 4.50 3.90 0.64 o 4 4 3 0.43 -0.77 0.77 o 5 4 3 8.61 9.53 1.32 o -5 5 3 21.01 22.66 3.48 o -4 5 3 34.37 38.46 1.86 o -3 5 3 19.49 17.49 1.68 o -2 5 3 6.64 6.55 1.11 o -1 5 3 2.74 3.71 1.30 o 0 5 3 141.10 128.91 6.53 o 1 5 3 347.87 343.40 4.47 o 2 5 3 98.29 105.02 2.61 o 3 5 3 84.18 92.83 2.18 o 4 5 3 21.83 27.82 1.27 o 5 5 3 27.67 28.58 1.86 o -5 6 3 1.50 1.74 2.50 o -4 6 3 0.93 4.17 2.50 o -3 6 3 128.04 124.31 4.90 o -2 6 3 17.07 20.28 1.75 o -1 6 3 51.37 47.52 1.66 o 0 6 3 51.77 48.86 3.46 o 1 6 3 16.02 23.23 2.28 o 2 6 3 60.87 51.39 2.89 o 3 6 3 42.39 46.39 3.35 o 4 6 3 0.03 -1.93 2.62 o -4 7 3 0.23 -0.04 2.49 o -3 7 3 4.46 4.58 2.60 o -2 7 3 14.47 14.90 1.66 o -1 7 3 2.62 2.84 1.19 o 0 7 3 3.51 6.63 2.74 o 1 7 3 14.44 11.86 3.31 o 2 7 3 69.60 71.95 3.42 o 3 7 3 5.82 2.14 2.27 o -2 8 3 0.00 -0.32 3.09 o -1 8 3 7.52 2.54 2.84 o 0 8 3 0.01 -1.64 3.07 o 1 8 3 26.87 29.48 4.42 o 2 8 3 26.28 28.17 2.80 o -6 0 4 0.45 0.02 2.20 o -4 0 4 537.46 560.15 10.47 o -2 0 4 2464.18 2392.15 30.98 o 0 0 4 7453.97 7041.88 65.69 o 2 0 4 60.00 64.76 3.36 o 4 0 4 1.09 1.51 1.61 o 6 0 4 55.94 42.66 3.99 o -6 1 4 0.91 1.06 1.57 o -5 1 4 3.55 2.85 1.31 o -4 1 4 30.05 34.32 1.35 o -3 1 4 87.38 83.11 1.76 o -2 1 4 320.64 307.89 3.16 o -1 1 4 374.17 371.98 3.40 o 0 1 4 6110.25 5693.45 40.75 o 1 1 4 173.37 175.46 1.83 o 2 1 4 1414.44 1449.46 15.22 o 3 1 4 101.66 115.85 1.81 o 4 1 4 19.07 18.74 1.05 o 5 1 4 0.34 0.84 1.32 o 6 1 4 83.24 78.66 4.20 o -6 2 4 5.36 7.38 2.12 o -5 2 4 1.13 4.29 0.95 o -4 2 4 289.21 295.91 3.97 o -3 2 4 189.72 196.06 2.98 o -2 2 4 225.99 211.35 2.44 o -1 2 4 1967.95 2029.48 15.49 o 0 2 4 0.78 0.73 0.53 o 1 2 4 105.60 96.45 1.24 o 2 2 4 4.91 3.59 0.56 o 3 2 4 122.54 120.39 1.93 o 4 2 4 77.22 84.23 1.70 o 5 2 4 76.03 68.33 2.95 o 6 2 4 0.04 -1.08 1.91 o -6 3 4 0.45 -0.64 1.81 o -5 3 4 89.05 92.27 2.50 o -4 3 4 98.81 91.17 2.01 o -3 3 4 0.30 0.31 0.58 o -2 3 4 97.11 104.26 2.36 o -1 3 4 1852.70 1876.42 22.16 o 0 3 4 805.47 864.40 7.15 o 1 3 4 123.47 123.45 1.71 o 2 3 4 11.85 9.95 0.63 o 3 3 4 57.42 59.04 1.90 o 4 3 4 26.70 25.85 1.58 o 5 3 4 67.17 66.75 3.39 o 6 3 4 22.77 24.30 2.86 o -6 4 4 9.97 7.39 2.31 o -5 4 4 3.44 4.48 1.14 o -4 4 4 3.26 2.47 0.87 o -3 4 4 28.09 29.02 1.01 o -2 4 4 361.35 363.09 5.67 o -1 4 4 1159.61 1136.67 13.17 o 0 4 4 1.00 1.57 0.39 o 1 4 4 22.13 18.42 0.64 o 2 4 4 4.13 3.38 0.51 o 3 4 4 33.76 34.45 1.12 o 4 4 4 7.92 6.74 0.99 o 5 4 4 35.66 33.33 1.84 o -5 5 4 89.34 87.92 3.50 o -4 5 4 4.62 5.10 0.91 o -3 5 4 147.57 153.17 3.22 o -2 5 4 195.57 193.21 4.01 o -1 5 4 87.73 89.80 1.76 o 0 5 4 568.03 572.23 7.20 o 1 5 4 22.30 22.78 1.04 o 2 5 4 1067.71 1077.28 14.81 o 3 5 4 109.00 109.08 2.06 o 4 5 4 19.09 19.81 1.62 o 5 5 4 40.71 44.36 3.25 o -5 6 4 0.03 -0.18 2.60 o -4 6 4 58.38 61.22 4.02 o -3 6 4 75.12 72.68 3.15 o -2 6 4 8.20 7.88 1.59 o -1 6 4 144.95 143.68 2.57 o 0 6 4 76.45 76.81 2.62 o 1 6 4 46.23 43.98 2.20 o 2 6 4 17.36 17.07 1.82 o 3 6 4 22.20 23.61 2.78 o 4 6 4 3.11 3.09 1.11 o -4 7 4 2.23 1.12 2.79 o -3 7 4 1.25 -0.42 2.74 o -2 7 4 4.51 2.42 2.22 o -1 7 4 1.72 3.74 1.04 o 0 7 4 110.38 107.11 5.29 o 1 7 4 0.06 0.09 0.90 o 2 7 4 24.33 18.73 3.87 o 3 7 4 0.87 2.65 2.29 o -2 8 4 10.99 9.81 2.43 o -1 8 4 3.50 4.70 4.07 o 0 8 4 0.08 6.89 4.29 o 1 8 4 5.95 3.59 4.10 o 2 8 4 1.12 1.20 2.08 o -5 0 5 0.15 0.71 1.61 o -3 0 5 10.55 9.23 1.62 o -1 0 5 4820.83 4427.88 50.13 o 1 0 5 9.29 9.51 0.70 o 3 0 5 1.86 0.74 0.64 o 5 0 5 451.30 445.51 20.28 o -6 1 5 22.00 21.18 2.52 o -5 1 5 0.31 -0.34 0.79 o -4 1 5 197.52 193.74 3.20 o -3 1 5 745.75 746.46 8.25 o -2 1 5 14.53 12.86 0.72 o -1 1 5 119.45 129.64 1.63 o 0 1 5 39.70 34.23 0.60 o 1 1 5 603.10 562.60 5.70 o 2 1 5 649.18 699.47 7.29 o 3 1 5 135.95 139.53 2.47 o 4 1 5 15.66 22.20 1.82 o 5 1 5 0.29 -0.98 1.34 o 6 1 5 1.64 0.79 2.05 o -6 2 5 2.96 3.04 1.96 o -5 2 5 9.43 10.79 1.10 o -4 2 5 21.02 21.83 1.66 o -3 2 5 40.04 39.88 1.24 o -2 2 5 210.15 225.10 2.44 o -1 2 5 1268.74 1219.43 9.55 o 0 2 5 13.03 14.08 0.53 o 1 2 5 2444.51 2392.24 20.04 o 2 2 5 6.89 9.16 0.66 o 3 2 5 199.53 200.99 2.94 o 4 2 5 0.04 0.25 0.52 o 5 2 5 98.06 111.57 4.29 o 6 2 5 1.58 4.33 2.22 o -6 3 5 1.12 2.86 1.85 o -5 3 5 0.09 0.54 1.01 o -4 3 5 20.07 21.10 1.13 o -3 3 5 249.57 244.99 3.41 o -2 3 5 332.07 346.65 3.55 o -1 3 5 150.60 146.85 1.74 o 0 3 5 379.99 387.83 3.40 o 1 3 5 32.46 31.94 0.80 o 2 3 5 320.76 317.20 3.61 o 3 3 5 21.17 27.51 1.11 o 4 3 5 96.67 96.32 2.22 o 5 3 5 37.68 32.83 1.76 o 6 3 5 23.63 25.71 2.48 o -6 4 5 0.31 -1.45 1.98 o -5 4 5 12.75 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