#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/53/2215391.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215391_Fobs loop_ _publ_author_name 'Chen, Peng-Gang' 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; Diaquatetrakis(2,3,5-triiodobenzoato-\k^2^O:O')dicopper(II)(Cu{--Cu}) bis(methanol-\kO)tetrakis(2,3,5-triiodobenzoato-\k^2^O:O')dicopper(II)(Cu{--Cu}) methanol disolvate ; _journal_coeditor_code BT2517 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2617 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 96.799 _cell_angle_beta 103.136 _cell_angle_gamma 91.532 _cell_length_a 11.9321 _cell_length_b 11.9345 _cell_length_c 17.9212 _exptl_crystal_F_000 1960.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file bt2517Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 628.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 403.38 617.09 33.73 o 3 0 0 20081.10 20292.92 738.97 o 4 0 0 151978.28 188247.23 14951.01 o 5 0 0 60875.44 73312.97 3909.24 o 6 0 0 4529.82 4881.50 225.43 o 7 0 0 2048.25 2615.74 96.04 o 8 0 0 26854.45 29940.45 1032.16 o 9 0 0 543.81 616.49 52.27 o 10 0 0 587.64 779.13 48.87 o 11 0 0 2901.11 2956.35 125.83 o 12 0 0 3718.78 3441.80 217.10 o 13 0 0 38.74 75.57 25.26 o 14 0 0 279.75 302.40 55.72 o 15 0 0 27.96 26.80 22.45 o -15 1 0 70.41 76.15 37.67 o -14 1 0 0.25 58.41 27.51 o 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