#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:35:37 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181074 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/54/2215461.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215461_Fobs loop_ _publ_author_name 'Pearsal, Matthew' 'Gembicky, Milan' 'Dominiak, Paulina' 'Larsen, Anna' 'Coppens, Philip' _publ_section_title ; Di-\m-nitrosyl-bis[(\h^5^-pentamethylcyclopentadienyl)ruthenium(0)](Ru{---Ru}) ; _journal_coeditor_code ER2041 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2596 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.209 _cell_angle_beta 89.220 _cell_angle_gamma 85.373 _cell_length_a 10.7181 _cell_length_b 10.7364 _cell_length_c 17.9238 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7496 _cod_data_source_file er2041Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ru2 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 683.30 471.91 30.42 o 2 0 0 69061.47 66174.34 1582.62 o 3 0 0 270.97 271.14 11.74 o 4 0 0 16072.04 14774.29 537.25 o 5 0 0 5178.31 5529.54 181.90 o 6 0 0 222.87 195.74 14.47 o 7 0 0 4387.17 5003.85 190.67 o 8 0 0 2762.96 2704.08 95.67 o 9 0 0 776.63 870.72 73.08 o 10 0 0 3372.95 3505.05 123.94 o 11 0 0 484.53 559.73 47.34 o 12 0 0 6048.27 6031.58 287.75 o 13 0 0 670.37 395.78 69.13 o 14 0 0 2343.04 2616.39 146.97 o -14 1 0 1603.15 1933.38 351.03 o -13 1 0 8.82 11.50 19.95 o -12 1 0 1124.28 1264.00 163.22 o -11 1 0 108.29 75.92 25.63 o -10 1 0 50.73 61.92 12.66 o -9 1 0 10136.93 10274.69 337.16 o -8 1 0 1037.51 1073.82 44.76 o -7 1 0 32263.81 32881.95 1050.07 o -6 1 0 1922.32 1863.09 81.76 o -5 1 0 40254.78 41213.20 1311.47 o -4 1 0 20.08 26.35 6.59 o -3 1 0 24719.93 24963.66 714.27 o -2 1 0 61.93 69.87 4.83 o -1 1 0 1.83 -2.08 2.08 o 0 1 0 325.49 202.29 24.80 o 1 1 0 1.16 -2.22 2.22 o 2 1 0 311.01 391.01 17.95 o 3 1 0 13704.82 13218.98 421.89 o 4 1 0 250.58 255.85 16.58 o 5 1 0 19978.45 17808.02 566.22 o 6 1 0 4297.07 3986.36 153.53 o 7 1 0 27390.54 25916.26 1036.68 o 8 1 0 1947.03 1856.64 82.73 o 9 1 0 11239.62 10863.07 352.69 o 10 1 0 306.97 79.80 26.88 o 11 1 0 556.99 594.14 80.30 o 12 1 0 1498.91 2627.20 219.01 o 13 1 0 557.75 596.01 65.82 o 14 1 0 1896.66 2794.34 506.94 o -13 2 0 1020.44 1122.29 79.92 o -12 2 0 2048.75 2061.40 119.69 o -11 2 0 230.86 232.61 33.53 o -10 2 0 1257.02 1264.71 53.98 o -9 2 0 1717.18 1705.83 74.50 o -8 2 0 751.78 729.19 34.59 o -7 2 0 2845.20 2781.17 98.56 o -6 2 0 403.52 381.38 21.50 o -5 2 0 323.07 337.75 18.77 o -4 2 0 142.40 169.64 15.11 o -3 2 0 6047.38 5753.68 215.11 o -2 2 0 33743.83 31151.79 990.03 o -1 2 0 70.96 68.67 4.11 o 0 2 0 69431.56 65933.62 1872.96 o 1 2 0 725.21 619.92 33.09 o 2 2 0 30317.51 24146.95 2604.53 o 3 2 0 1486.62 1096.24 84.49 o 4 2 0 3477.92 3186.02 105.92 o 5 2 0 605.35 630.48 47.26 o 6 2 0 915.05 1033.00 48.66 o 7 2 0 4762.75 4650.17 208.92 o 8 2 0 15.22 0.46 8.22 o 9 2 0 1283.01 1229.91 153.62 o 10 2 0 2803.87 2689.38 98.12 o 11 2 0 530.62 563.28 31.94 o 12 2 0 4822.03 5342.76 290.75 o 13 2 0 1628.86 1742.00 103.72 o 14 2 0 1505.99 1654.20 103.53 o -13 3 0 1587.49 1845.05 114.24 o -12 3 0 1242.46 1170.82 81.29 o -11 3 0 726.89 773.93 60.25 o -10 3 0 131.60 133.79 16.84 o -9 3 0 455.34 404.41 26.18 o -8 3 0 998.92 1267.18 99.58 o -7 3 0 6011.56 6074.21 203.37 o -6 3 0 1055.77 1141.79 46.17 o -5 3 0 13435.28 13304.44 485.00 o -4 3 0 88.08 114.88 11.28 o -3 3 0 51.18 52.60 8.47 o -2 3 0 2618.96 2947.08 108.80 o -1 3 0 22581.78 22667.84 718.50 o 0 3 0 135.97 218.10 18.11 o 1 3 0 13488.81 11844.16 549.37 o 2 3 0 3424.58 3146.18 207.89 o 3 3 0 39.58 21.11 6.51 o 4 3 0 1284.51 1195.47 43.75 o 5 3 0 11418.58 11052.09 354.15 o 6 3 0 4767.13 4537.05 182.86 o 7 3 0 16466.40 16386.32 525.78 o 8 3 0 4297.90 4285.60 196.19 o 9 3 0 2928.92 2749.82 162.80 o 10 3 0 667.22 680.76 34.50 o 11 3 0 466.38 542.06 42.79 o 13 3 0 195.01 209.86 34.47 o 14 3 0 1795.37 2700.48 231.28 o -13 4 0 1070.62 1309.84 173.57 o -12 4 0 63.68 109.17 29.85 o -11 4 0 1807.58 2058.21 119.37 o -10 4 0 909.67 1044.31 48.79 o -9 4 0 599.65 712.27 67.49 o -8 4 0 9051.70 9055.95 300.60 o -7 4 0 664.77 845.78 86.30 o -6 4 0 26001.90 25886.99 940.20 o -5 4 0 371.75 387.50 24.48 o -4 4 0 13709.78 13607.83 437.05 o -3 4 0 140.36 145.42 12.29 o -2 4 0 184.98 195.77 13.21 o -1 4 0 47.28 42.77 6.56 o 0 4 0 13996.45 13661.20 685.74 o 1 4 0 114.26 49.98 16.22 o 2 4 0 2883.29 2779.48 106.24 o 3 4 0 550.94 283.02 33.18 o 4 4 0 245.32 311.81 20.02 o 5 4 0 1037.14 909.58 54.77 o 6 4 0 6135.35 5997.67 300.24 o 7 4 0 4220.55 3887.44 160.83 o 8 4 0 3093.29 2841.56 131.30 o 9 4 0 2068.91 1874.99 153.46 o 10 4 0 2.61 -3.28 9.21 o 11 4 0 90.76 80.09 15.77 o 12 4 0 149.50 184.26 29.82 o 13 4 0 1386.28 1528.94 92.55 o 14 4 0 905.61 1208.79 131.11 o -12 5 0 354.63 332.03 44.85 o -11 5 0 6905.21 7177.03 341.62 o -10 5 0 14.15 20.02 18.22 o -9 5 0 1237.04 1415.30 60.89 o -8 5 0 5523.10 4878.84 296.90 o -7 5 0 311.90 252.44 20.66 o -6 5 0 1231.23 1190.21 49.01 o -5 5 0 141.94 170.74 17.42 o -4 5 0 865.86 780.94 33.58 o -3 5 0 11508.57 11909.38 383.83 o -2 5 0 193.54 240.09 18.31 o -1 5 0 40423.50 40239.00 1439.48 o 0 5 0 6877.68 6377.16 207.59 o 1 5 0 18746.51 16113.39 850.18 o 2 5 0 1397.57 1314.62 75.19 o 3 5 0 10873.78 9943.32 604.98 o 4 5 0 1194.90 1014.71 47.98 o 5 5 0 39.57 29.52 7.78 o 6 5 0 2709.30 3072.33 174.26 o 7 5 0 1411.51 806.77 52.49 o 8 5 0 1887.64 1237.00 91.74 o 9 5 0 449.23 459.81 26.78 o 10 5 0 513.68 425.27 66.52 o 11 5 0 36.27 21.36 12.06 o 12 5 0 263.51 271.89 34.91 o 13 5 0 253.66 248.32 62.41 o -12 6 0 214.24 250.62 41.88 o -11 6 0 1620.99 1606.65 101.17 o -10 6 0 1937.15 2135.73 147.48 o -9 6 0 222.70 241.38 22.97 o -8 6 0 13452.24 13642.58 447.38 o -7 6 0 674.73 913.59 89.05 o -6 6 0 21988.58 21296.97 684.93 o -5 6 0 969.54 1014.16 42.88 o -4 6 0 25244.69 25098.73 800.39 o -3 6 0 1481.55 1398.04 53.53 o -2 6 0 324.58 319.40 18.74 o -1 6 0 1123.60 1404.68 121.26 o 0 6 0 243.84 181.28 13.72 o 2 6 0 1314.65 1202.32 45.79 o 4 6 0 6058.54 5442.74 238.88 o 5 6 0 4011.96 4261.07 143.60 o 6 6 0 12112.20 10732.03 346.31 o 7 6 0 3085.81 3269.24 114.11 o 8 6 0 4674.27 4499.76 221.90 o 9 6 0 4578.60 5224.41 180.22 o 10 6 0 1120.20 1247.28 53.46 o 11 6 0 366.24 334.36 25.43 o 12 6 0 371.57 358.31 39.21 o -11 7 0 5781.54 5761.29 282.52 o -10 7 0 104.89 100.07 27.48 o -9 7 0 1232.54 1297.45 59.48 o -8 7 0 2242.18 2054.04 81.87 o -7 7 0 4.62 -2.93 12.04 o -6 7 0 1579.48 1441.56 67.05 o -5 7 0 194.97 166.53 16.71 o -4 7 0 1550.61 1409.54 55.67 o -3 7 0 5879.73 6003.64 226.51 o -2 7 0 2596.13 2654.96 93.81 o -1 7 0 32432.03 32333.76 1027.08 o 0 7 0 6736.47 6517.13 215.09 o 1 7 0 27742.44 26290.13 908.86 o 2 7 0 7190.71 7015.67 304.62 o 3 7 0 17698.24 16515.18 571.38 o 4 7 0 5157.15 5206.40 174.36 o 5 7 0 2339.99 2406.00 100.50 o 7 7 0 598.98 506.32 27.51 o 8 7 0 2694.18 1449.78 146.24 o 9 7 0 807.01 950.09 43.79 o 11 7 0 523.19 611.00 36.03 o 12 7 0 1097.55 1315.77 81.35 o -11 8 0 927.96 977.52 74.66 o -10 8 0 792.30 851.37 66.68 o -9 8 0 227.89 286.82 26.68 o -8 8 0 6112.42 6051.15 210.02 o -7 8 0 1570.74 1757.13 81.96 o -6 8 0 14302.88 14330.02 465.39 o -5 8 0 3226.36 3370.50 144.65 o -4 8 0 8969.30 8987.13 336.30 o -3 8 0 1952.31 1723.31 105.71 o -2 8 0 569.91 581.45 29.93 o -1 8 0 1092.09 1045.85 43.86 o 0 8 0 1891.24 2099.73 88.86 o 1 8 0 877.34 1243.07 97.72 o 2 8 0 34.26 21.19 8.12 o 4 8 0 3262.07 2876.49 156.47 o 5 8 0 3048.57 3120.94 112.44 o 6 8 0 4169.30 4055.56 265.07 o 7 8 0 5590.33 6429.23 374.32 o 8 8 0 3006.39 2961.99 106.48 o 9 8 0 3209.93 3999.81 160.77 o 10 8 0 1021.73 1089.68 50.20 o 11 8 0 1225.24 1314.36 58.81 o 12 8 0 438.57 590.97 49.96 o -10 9 0 55.71 25.75 20.85 o -9 9 0 20.32 18.77 19.88 o -8 9 0 249.15 256.27 29.76 o -7 9 0 1551.05 1442.95 143.06 o -6 9 0 340.47 316.54 30.94 o -5 9 0 1752.55 1648.29 67.82 o -4 9 0 1211.91 973.94 60.67 o -3 9 0 260.48 310.60 40.22 o -2 9 0 883.24 1053.65 113.00 o -1 9 0 9010.86 9298.84 305.55 o 0 9 0 1828.23 1870.06 84.38 o 1 9 0 10821.97 11076.71 359.96 o 2 9 0 2479.17 2544.44 126.06 o 3 9 0 3274.40 3408.09 119.09 o 4 9 0 2859.55 2941.45 105.29 o 5 9 0 210.70 224.18 32.58 o 6 9 0 1958.30 340.95 56.11 o 8 9 0 1416.31 529.56 73.50 o 9 9 0 297.62 323.99 25.50 o 10 9 0 1180.39 322.37 54.52 o 11 9 0 327.15 433.83 34.97 o -9 10 0 62.72 94.52 46.09 o -8 10 0 1142.09 957.30 64.16 o -7 10 0 97.07 117.44 20.63 o -6 10 0 2765.40 2495.54 131.91 o -5 10 0 10.01 6.43 10.65 o -4 10 0 1134.05 1115.42 50.82 o -3 10 0 78.15 98.61 14.72 o -2 10 0 902.42 965.32 44.47 o -1 10 0 56.30 73.52 12.69 o 0 10 0 2281.22 2525.99 132.44 o 1 10 0 701.39 833.97 58.56 o 2 10 0 2265.99 2264.52 198.65 o 3 10 0 639.68 702.29 33.89 o 4 10 0 2.88 5.01 8.23 o 5 10 0 741.06 759.13 36.91 o 6 10 0 758.12 907.18 55.18 o 7 10 0 2565.97 3435.47 187.25 o 8 10 0 798.47 728.85 62.69 o 9 10 0 2774.45 3787.82 328.36 o 10 10 0 453.56 547.20 86.04 o 11 10 0 1070.76 1366.24 129.62 o -8 11 0 721.44 856.38 56.39 o -7 11 0 5635.34 5736.21 205.39 o -6 11 0 1397.05 1434.31 64.87 o -5 11 0 7318.85 7302.37 249.66 o -4 11 0 2370.24 2350.93 91.82 o -3 11 0 705.08 762.24 48.84 o -2 11 0 418.81 440.06 36.09 o -1 11 0 73.82 42.97 19.71 o 0 11 0 476.60 572.34 40.94 o 1 11 0 312.53 330.01 51.21 o 2 11 0 548.23 599.91 56.27 o 3 11 0 232.29 246.43 54.30 o 4 11 0 84.67 44.66 23.75 o 5 11 0 48.69 32.17 20.41 o 6 11 0 513.65 587.28 54.20 o 7 11 0 250.14 296.68 55.69 o 8 11 0 1107.65 1304.39 173.99 o 9 11 0 140.99 14.51 28.80 o 10 11 0 798.23 1022.89 132.60 o -6 12 0 372.62 373.51 86.94 o -5 12 0 354.37 346.79 48.84 o -4 12 0 142.83 165.95 36.30 o -3 12 0 893.67 1015.74 79.32 o -2 12 0 1915.36 1928.16 122.73 o -1 12 0 1451.95 1392.57 97.11 o 0 12 0 4941.17 5131.64 559.11 o 1 12 0 3296.41 3718.55 542.84 o 2 12 0 4706.54 5028.49 636.77 o 3 12 0 1653.16 2015.67 300.20 o 4 12 0 226.66 248.34 39.78 o 5 12 0 191.18 227.26 54.14 o 6 12 0 166.61 102.84 72.70 o 7 12 0 824.48 999.54 163.97 o 8 12 0 202.60 18.35 29.87 o -4 13 0 1850.08 1710.83 116.09 o -3 13 0 1638.49 1680.84 115.40 o -2 13 0 1109.81 1094.60 87.22 o -1 13 0 17.75 19.59 25.99 o 0 13 0 287.47 394.07 74.36 o 1 13 0 338.57 374.54 110.25 o 3 13 0 83.23 8.89 44.75 o 4 13 0 613.09 23.58 30.72 o 5 13 0 335.30 316.18 47.59 o 6 13 0 1488.82 2070.71 248.30 o 7 13 0 707.39 850.92 115.11 o -1 14 0 2402.05 2571.42 205.52 o 0 14 0 2041.05 2320.36 148.79 o 1 14 0 3628.14 4490.43 452.37 o 2 14 0 1420.58 1482.62 196.66 o 3 14 0 3172.82 3836.00 452.80 o 4 14 0 961.46 1101.86 88.67 o -4 -14 1 116.15 8.53 34.35 o -3 -14 1 687.12 40.32 34.03 o -2 -14 1 122.09 78.66 68.81 o 0 -14 1 105.05 78.55 34.11 o 1 -14 1 911.22 946.19 176.45 o -6 -13 1 513.91 578.25 63.42 o -5 -13 1 189.22 213.42 41.02 o -4 -13 1 1942.52 2514.16 248.56 o -3 -13 1 1591.10 1260.63 131.32 o -2 -13 1 2804.88 3300.13 494.14 o -1 -13 1 2066.93 1458.20 143.91 o 0 -13 1 1330.41 1430.41 102.12 o 1 -13 1 388.41 368.37 55.05 o 2 -13 1 589.28 664.00 68.43 o 3 -13 1 69.28 98.28 32.65 o 4 -13 1 202.03 210.63 70.73 o -8 -12 1 167.77 221.36 53.66 o -7 -12 1 456.85 582.97 71.21 o -6 -12 1 44.11 48.15 24.27 o -5 -12 1 142.60 186.11 36.94 o -4 -12 1 382.05 255.39 56.65 o -3 -12 1 1102.23 1270.17 91.31 o -2 -12 1 1133.62 1324.94 195.17 o -1 -12 1 486.64 571.16 57.13 o 0 -12 1 79.64 88.50 33.50 o 1 -12 1 63.46 49.87 25.33 o 2 -12 1 614.96 713.92 63.78 o 3 -12 1 806.34 758.02 126.52 o 4 -12 1 3977.05 4186.78 230.50 o 5 -12 1 1530.85 1489.45 103.64 o 6 -12 1 3773.72 3834.52 215.49 o -9 -11 1 759.10 428.74 69.02 o -8 -11 1 1829.80 2354.62 344.36 o -7 -11 1 555.59 387.78 64.22 o -6 -11 1 856.93 897.67 69.86 o -5 -11 1 56.83 25.31 18.96 o -4 -11 1 414.95 228.08 51.53 o -3 -11 1 858.42 912.44 161.46 o -2 -11 1 712.19 855.42 144.39 o -1 -11 1 1523.48 1902.01 101.15 o 0 -11 1 332.97 378.87 29.46 o 1 -11 1 751.61 817.50 47.48 o 2 -11 1 180.13 211.45 22.34 o 3 -11 1 540.45 539.24 32.36 o 4 -11 1 79.91 110.08 17.30 o 5 -11 1 2299.14 2342.20 93.21 o 6 -11 1 20.96 36.44 15.13 o 7 -11 1 462.08 403.30 46.37 o 8 -11 1 82.03 38.12 23.05 o -10 -10 1 295.32 306.48 41.30 o -9 -10 1 1644.53 395.78 63.69 o -8 -10 1 365.58 419.99 31.84 o -7 -10 1 1358.55 232.60 33.61 o -6 -10 1 103.74 116.41 17.16 o -5 -10 1 1814.21 1975.90 164.85 o -4 -10 1 1079.91 1201.06 50.96 o -3 -10 1 4062.57 4242.41 261.68 o -2 -10 1 10508.62 11262.26 662.66 o -1 -10 1 1272.91 1473.81 111.79 o 0 -10 1 5162.76 5562.93 188.56 o 1 -10 1 304.39 310.50 22.41 o 2 -10 1 307.97 319.73 23.30 o 3 -10 1 93.99 86.15 14.83 o 4 -10 1 1457.12 1416.42 60.56 o 5 -10 1 39.42 54.74 17.25 o 6 -10 1 3062.72 2957.56 128.96 o 7 -10 1 45.95 94.84 21.37 o 8 -10 1 117.11 112.55 21.59 o 9 -10 1 15.54 13.98 31.79 o -11 -9 1 1200.62 1316.55 79.23 o -10 -9 1 3754.56 5265.05 207.58 o -9 -9 1 1802.18 1741.87 70.40 o -8 -9 1 4664.57 5779.28 297.47 o -7 -9 1 2113.87 2139.14 89.05 o -6 -9 1 3070.48 3125.67 125.65 o -5 -9 1 1674.42 1592.46 62.81 o -4 -9 1 2116.30 2946.08 250.32 o -3 -9 1 151.44 70.47 41.93 o -1 -9 1 516.87 593.41 53.38 o 0 -9 1 234.39 344.20 30.80 o 1 -9 1 583.24 561.12 29.76 o 2 -9 1 2842.14 2571.93 119.98 o 3 -9 1 4560.39 4736.20 163.24 o 4 -9 1 3373.69 3662.62 188.83 o 5 -9 1 10784.17 10556.42 396.77 o 6 -9 1 2779.45 2650.45 114.96 o 7 -9 1 6076.33 6024.93 252.95 o 8 -9 1 876.49 910.23 47.68 o 9 -9 1 421.31 381.90 43.99 o 10 -9 1 784.23 642.01 79.53 o -12 -8 1 353.30 469.60 53.23 o -11 -8 1 781.14 163.12 31.57 o -10 -8 1 289.47 248.58 23.16 o -9 -8 1 2087.50 673.38 54.32 o -8 -8 1 185.00 167.68 17.91 o -7 -8 1 1174.33 299.88 50.99 o -6 -8 1 870.21 869.19 49.41 o -5 -8 1 2228.07 2140.04 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