#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/54/2215468.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2215468_Fobs
loop_
_publ_author_name
'Lee, Chang-Ho'
'Jang, Gyung-Joo'
'Yun, Hoseop'
_publ_section_title
;
 Stoichiometric ZrGeTe~4~
;
_journal_coeditor_code           FI2044
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i183
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           36
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   3.9794
_cell_length_b                   15.9296
_cell_length_c                   10.9957
_exptl_crystal_F_000             1119.77
_reflns_d_resolution_high        0.7706
_[local]_cod_data_source_file    fi2044Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
' N-24 (L-35 again) with IBERS HfGeTe4 COORDINATE, 150K'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            779.10
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 -13 7541.29 6415.64 775.11 o
0 2 -13 17671.82 15290.50 1907.96 o
2 2 -13 14557.18 12949.54 1481.16 o
1 3 -13 24144.36 19767.55 2474.66 o
0 4 -13 6751.40 5781.05 798.14 o
1 5 -13 5269.20 4268.72 451.49 o
0 6 -13 7158.65 5706.42 783.17 o
1 7 -13 9992.53 8179.82 801.14 o
0 8 -13 22211.43 17594.23 2417.33 o
2 0 -12 4273.38 3976.25 409.89 o
1 1 -12 11563.59 10460.14 1218.52 o
0 2 -12 38702.83 32181.41 4355.41 o
2 2 -12 31022.39 27065.38 3254.72 o
1 3 -12 21290.76 18744.59 2468.44 o
0 4 -12 1298.00 1205.15 290.35 o
2 4 -12 1029.67 1026.15 227.59 o
1 5 -12 59763.26 51839.84 5202.35 o
0 6 -12 24211.72 20639.53 2685.71 o
2 6 -12 19405.26 16766.52 1483.76 o
1 7 -12 1419.05 1487.08 223.53 o
1 9 -12 12278.07 11471.58 1210.34 o
0 10 -12 3941.48 4465.37 672.35 o
1 1 -11 8494.79 7968.36 601.18 o
0 2 -11 41525.20 35534.11 4600.82 o
2 2 -11 33100.09 31411.21 3859.37 o
1 3 -11 1163.44 1014.31 158.19 o
3 3 -11 879.23 908.76 226.34 o
0 4 -11 8582.09 7145.52 900.25 o
2 4 -11 6703.41 5815.93 511.90 o
1 5 -11 8109.28 7670.20 723.89 o
3 5 -11 5529.62 4247.74 397.19 o
0 6 -11 96380.20 82483.74 12263.65 o
2 6 -11 76929.13 71354.57 7269.16 o
1 7 -11 8844.00 8632.52 834.42 o
0 8 -11 539.91 683.66 143.54 o
2 8 -11 424.08 462.38 142.80 o
1 9 -11 32652.57 31045.30 2693.11 o
0 10 -11 24772.39 26078.44 3798.06 o
2 10 -11 19956.40 17082.18 1314.33 o
1 11 -11 38.00 205.42 74.41 o
0 12 -11 10784.60 11332.98 1516.50 o
0 0 -10 29138.19 26965.78 3234.89 o
2 0 -10 22379.19 21392.92 2346.29 o
1 1 -10 64606.76 65236.00 6022.88 o
3 1 -10 40312.55 38744.67 4606.92 o
0 2 -10 37853.15 31952.64 4000.36 o
2 2 -10 29217.25 29201.42 2376.58 o
1 3 -10 3922.22 3755.68 378.79 o
3 3 -10 2557.10 2308.22 220.33 o
0 4 -10 13357.63 11756.06 1376.11 o
2 4 -10 10564.13 9770.55 824.65 o
1 5 -10 7200.89 6984.92 638.06 o
3 5 -10 4610.93 3880.39 362.69 o
0 6 -10 6883.73 7792.91 1216.69 o
2 6 -10 5309.60 4832.98 396.00 o
1 7 -10 15022.78 13701.23 1079.90 o
3 7 -10 9481.66 8244.70 942.85 o
0 8 -10 1102.21 1291.20 189.26 o
2 8 -10 861.00 788.07 149.83 o
1 9 -10 101037.70 108211.53 11408.33 o
0 10 -10 2863.08 3049.21 380.75 o
2 10 -10 2290.68 2126.87 245.00 o
1 11 -10 3288.76 3692.70 315.43 o
0 12 -10 27013.04 27459.54 3982.00 o
2 12 -10 22142.78 19473.81 1597.00 o
1 13 -10 3151.17 3359.84 384.58 o
0 14 -10 1746.02 1839.42 268.55 o
1 1 -9 14239.29 14186.81 1121.23 o
3 1 -9 8322.89 7583.77 856.07 o
0 2 -9 30973.03 27152.08 3286.13 o
2 2 -9 23519.29 23274.75 1517.95 o
1 3 -9 63951.40 65735.09 5028.62 o
3 3 -9 38056.02 33522.68 2992.46 o
0 4 -9 22292.02 21318.23 2552.13 o
2 4 -9 17042.79 16533.78 1366.52 o
1 5 -9 2408.77 2264.09 214.77 o
3 5 -9 1421.12 1317.81 184.99 o
0 6 -9 16830.21 17979.66 1828.69 o
2 6 -9 13078.32 11416.08 818.21 o
1 7 -9 9137.33 8545.16 596.95 o
3 7 -9 5830.61 5047.09 477.07 o
0 8 -9 9928.77 10355.94 1105.28 o
2 8 -9 7943.67 6817.27 522.88 o
1 9 -9 238.77 294.45 56.88 o
3 9 -9 153.74 53.68 103.73 o
0 10 -9 17935.90 18326.98 2281.89 o
2 10 -9 14436.93 12628.22 999.92 o
1 11 -9 12450.20 12919.44 939.01 o
0 12 -9 47364.09 48551.86 6347.27 o
2 12 -9 38033.75 33633.79 2797.96 o
1 13 -9 43235.47 44018.58 3150.69 o
0 14 -9 19727.09 19879.60 2010.54 o
1 15 -9 20497.61 20383.35 1335.87 o
0 16 -9 4287.81 4622.38 524.37 o
0 0 -8 48824.35 44866.25 5525.93 o
2 0 -8 35797.63 35775.02 4264.45 o
1 1 -8 27353.21 27295.29 1802.57 o
3 1 -8 15845.84 14402.01 907.36 o
0 2 -8 49837.91 45058.50 5604.92 o
2 2 -8 37012.52 37657.45 2552.27 o
4 2 -8 18191.32 16906.15 2081.89 o
1 3 -8 34675.56 34306.18 2389.55 o
3 3 -8 20346.43 18962.85 1577.99 o
0 4 -8 19638.34 21507.36 2229.41 o
2 4 -8 14795.26 14147.93 1120.89 o
4 4 -8 7564.31 7017.87 626.56 o
1 5 -8 91174.04 86965.40 7222.92 o
3 5 -8 54477.61 52524.45 5081.86 o
0 6 -8 66915.44 69783.83 6720.81 o
2 6 -8 50480.27 46525.74 3589.24 o
4 6 -8 25480.32 22031.77 2897.40 o
1 7 -8 5917.89 6435.32 469.72 o
3 7 -8 3852.56 3643.22 391.26 o
0 8 -8 26344.72 26973.54 2657.29 o
2 8 -8 20263.74 17701.28 1271.58 o
1 9 -8 4369.65 4621.60 289.43 o
3 9 -8 2470.51 2231.09 309.68 o
0 10 -8 27925.36 28302.14 2493.71 o
2 10 -8 21956.78 18948.13 1395.40 o
1 11 -8 1295.39 1281.43 138.45 o
3 11 -8 893.60 912.99 171.60 o
0 12 -8 444.94 454.10 123.37 o
2 12 -8 360.94 332.62 166.48 o
1 13 -8 19915.52 19621.31 1262.80 o
0 14 -8 4806.93 4800.00 479.40 o
2 14 -8 3955.48 3537.24 368.06 o
1 15 -8 9417.32 9330.24 613.36 o
0 16 -8 24309.79 24184.46 2265.42 o
1 1 -7 66029.78 71792.10 4566.67 o
3 1 -7 37699.36 36035.09 2460.60 o
0 2 -7 62512.86 61535.50 7884.42 o
2 2 -7 45413.76 46873.98 3162.09 o
4 2 -7 22222.38 20606.88 1799.74 o
1 3 -7 9087.96 8803.30 576.53 o
3 3 -7 4933.87 4757.57 512.55 o
0 4 -7 31669.97 32625.22 2778.59 o
2 4 -7 22998.41 20945.24 1706.15 o
4 4 -7 10929.72 10165.14 893.34 o
1 5 -7 14456.89 13744.69 977.02 o
3 5 -7 8198.93 7428.28 651.30 o
0 6 -7 70180.24 71839.13 6737.89 o
2 6 -7 52006.13 47405.38 3561.72 o
4 6 -7 25373.82 23079.74 2100.61 o
1 7 -7 24414.70 24944.31 1449.40 o
3 7 -7 14564.88 12693.53 1095.95 o
0 8 -7 13033.27 13331.21 1105.65 o
2 8 -7 9823.39 8690.24 667.02 o
4 8 -7 5021.18 4590.42 508.95 o
1 9 -7 30742.42 31667.04 1927.49 o
3 9 -7 18680.36 16613.46 1665.25 o
0 10 -7 62575.38 60590.45 5899.29 o
2 10 -7 47936.85 47063.92 3914.20 o
1 11 -7 8001.83 7257.12 456.11 o
3 11 -7 5052.06 4039.77 366.40 o
0 12 -7 25448.41 23673.68 2152.65 o
2 12 -7 19838.09 18800.04 1129.56 o
1 13 -7 6685.89 5738.97 388.43 o
3 13 -7 4430.56 3537.71 439.08 o
0 14 -7 17713.83 16362.74 1472.94 o
2 14 -7 14029.32 12424.73 1078.63 o
1 15 -7 2221.30 2108.87 181.51 o
0 16 -7 9568.51 9475.82 889.54 o
2 16 -7 7861.53 7537.52 855.75 o
1 17 -7 27321.02 26179.01 1746.49 o
0 18 -7 14897.97 14695.01 1468.63 o
0 0 -6 22905.33 21012.35 2194.74 o
2 0 -6 15816.66 15754.47 1126.92 o
4 0 -6 6980.91 6601.35 721.34 o
1 1 -6 43785.31 46694.11 2742.39 o
3 1 -6 23703.57 22964.41 1487.65 o
0 2 -6 29712.78 31129.80 2483.98 o
2 2 -6 20756.78 20442.30 1242.17 o
4 2 -6 9177.86 8698.70 841.84 o
1 3 -6 15153.52 14520.71 910.70 o
3 3 -6 7923.12 7166.46 592.42 o
0 4 -6 74002.05 75132.91 6771.30 o
2 4 -6 53045.39 49381.70 3599.81 o
4 4 -6 25449.09 23736.06 2096.93 o
1 5 -6 2183.57 2469.28 154.68 o
3 5 -6 1163.65 1078.91 188.63 o
0 6 -6 54702.67 55891.36 5072.90 o
2 6 -6 39462.57 35068.33 2514.13 o
4 6 -6 18474.12 16616.98 1530.50 o
1 7 -6 83467.30 84725.71 5796.11 o
3 7 -6 47574.72 41211.24 3837.78 o
0 8 -6 4238.73 4258.24 354.46 o
2 8 -6 3165.33 2956.48 270.79 o
4 8 -6 1575.82 1570.66 304.10 o
1 9 -6 127259.59 126700.59 9366.71 o
3 9 -6 75740.04 71620.75 7399.20 o
0 10 -6 2028.12 2022.11 235.59 o
2 10 -6 1582.83 1594.30 107.50 o
1 11 -6 2289.57 2097.63 172.11 o
3 11 -6 1312.47 1249.32 175.44 o
0 12 -6 35490.60 32764.53 2952.99 o
2 12 -6 27722.67 25052.22 1524.36 o
1 13 -6 6363.71 5785.16 389.26 o
3 13 -6 4037.94 3651.70 398.94 o
0 14 -6 11858.95 10840.13 957.84 o
2 14 -6 9440.93 8395.48 545.22 o
1 15 -6 21592.66 19864.70 1128.48 o
0 16 -6 5661.74 5222.83 408.89 o
2 16 -6 4601.81 3985.39 513.52 o
1 17 -6 10469.04 10138.96 595.35 o
0 18 -6 10115.76 9259.87 742.46 o
1 1 -5 15953.55 16060.58 824.83 o
3 1 -5 7794.51 7562.12 420.30 o
0 2 -5 47724.63 49152.94 4118.84 o
2 2 -5 31756.82 30569.18 1957.06 o
4 2 -5 13963.78 13109.12 1247.99 o
1 3 -5 134804.75 126628.94 10533.06 o
3 3 -5 70087.61 69402.42 5120.27 o
0 4 -5 31818.97 33411.99 2685.72 o
2 4 -5 22077.15 19921.03 1299.26 o
4 4 -5 9953.24 8824.19 822.91 o
1 5 -5 20927.61 21880.47 1201.66 o
3 5 -5 11206.56 9874.64 849.32 o
0 6 -5 31161.24 30390.09 2445.15 o
2 6 -5 22436.90 20397.29 1352.38 o
4 6 -5 10720.93 9763.89 940.09 o
1 7 -5 17674.14 17092.25 920.75 o
3 7 -5 10157.96 9267.37 799.54 o
0 8 -5 10846.29 10049.87 774.04 o
2 8 -5 7847.11 7348.00 511.01 o
4 8 -5 3665.76 3555.29 408.17 o
1 9 -5 2474.74 2265.66 172.49 o
3 9 -5 1414.08 1397.26 243.42 o
0 10 -5 2827.32 2756.40 196.12 o
2 10 -5 2128.13 2018.54 130.16 o
4 10 -5 1093.25 1138.09 422.88 o
1 11 -5 46397.23 41773.09 2425.16 o
3 11 -5 28135.15 24815.30 2353.54 o
0 12 -5 53363.85 48721.36 3704.91 o
2 12 -5 40919.35 37094.84 2113.79 o
1 13 -5 43075.96 39462.21 2041.40 o
3 13 -5 26749.55 23020.32 3114.24 o
0 14 -5 36158.58 32331.08 2389.47 o
2 14 -5 28828.18 25547.36 1427.57 o
1 15 -5 51237.41 45720.22 2500.09 o
3 15 -5 33767.64 34140.89 3523.08 o
0 16 -5 8243.43 7747.93 547.11 o
2 16 -5 6551.16 6100.52 419.54 o
1 17 -5 9806.45 8695.61 443.78 o
0 18 -5 22971.55 21918.69 1595.01 o
0 0 -4 501888.97 434789.34 65765.01 o
2 0 -4 317896.53 281580.72 31710.39 o
4 0 -4 132527.83 112375.32 31590.89 o
1 1 -4 24680.55 26226.02 1355.77 o
3 1 -4 11795.26 10631.07 575.19 o
0 2 -4 25707.96 26392.27 1995.90 o
2 2 -4 16770.28 15402.32 1005.55 o
4 2 -4 7101.80 7108.02 391.48 o
1 3 -4 83239.83 81634.69 8933.84 o
3 3 -4 41268.05 40113.13 2554.60 o
0 4 -4 26453.34 27339.95 2100.33 o
2 4 -4 17663.37 15638.50 2241.84 o
4 4 -4 7980.33 7588.79 649.99 o
1 5 -4 53496.22 53332.35 3863.49 o
3 5 -4 27766.47 25753.31 2335.13 o
0 6 -4 59534.19 55623.97 4784.50 o
2 6 -4 41008.96 38801.89 2920.91 o
4 6 -4 18420.96 17601.36 1541.08 o
1 7 -4 13145.40 11705.71 549.11 o
3 7 -4 7187.19 6766.19 607.87 o
0 8 -4 86062.18 78066.40 5938.82 o
2 8 -4 61754.92 58219.02 3252.02 o
4 8 -4 28919.87 27082.93 2510.03 o
1 9 -4 6019.38 5621.43 285.44 o
3 9 -4 3111.40 2988.95 355.23 o
0 10 -4 42125.39 37989.84 3279.15 o
2 10 -4 31231.20 29438.63 1857.59 o
4 10 -4 15445.36 14761.65 2061.88 o
1 11 -4 32873.70 29692.50 1619.78 o
3 11 -4 19860.69 17711.34 1167.90 o
0 12 -4 3569.46 3063.68 341.60 o
2 12 -4 2759.29 2558.24 215.48 o
1 13 -4 5094.03 4688.81 284.18 o
3 13 -4 3054.39 2791.71 273.46 o
0 14 -4 132.89 490.62 104.10 o
2 14 -4 99.80 114.54 83.52 o
1 15 -4 10039.54 9147.53 514.07 o
3 15 -4 6262.54 6349.52 616.99 o
0 16 -4 19193.35 17850.29 1560.20 o
2 16 -4 15149.60 13195.25 1392.81 o
1 17 -4 2088.40 1963.68 172.63 o
0 18 -4 21030.89 20863.64 2682.12 o
2 18 -4 17085.25 15751.78 1801.24 o
1 19 -4 1563.60 1530.01 195.11 o
1 1 -3 81827.00 85233.62 4717.16 o
3 1 -3 38167.99 35977.07 2144.80 o
5 1 -3 15697.14 14764.15 1708.58 o
0 2 -3 30529.42 32825.50 2511.51 o
2 2 -3 18723.16 16104.97 1210.64 o
4 2 -3 8047.70 7936.68 416.79 o
1 3 -3 90460.12 87161.72 13724.94 o
3 3 -3 42937.27 40836.07 2823.76 o
0 4 -3 49159.07 46310.25 4254.67 o
2 4 -3 31194.83 29690.07 4204.34 o
4 4 -3 12928.54 12515.28 662.07 o
1 5 -3 75341.22 71052.96 6932.99 o
3 5 -3 37155.80 35841.18 2068.89 o
0 6 -3 6818.64 6071.08 338.79 o
2 6 -3 4598.83 4578.63 204.64 o
4 6 -3 1757.78 1763.62 285.48 o
1 7 -3 43130.33 40079.54 2046.25 o
3 7 -3 23158.17 22128.65 2003.02 o
0 8 -3 91544.72 80456.18 7499.76 o
2 8 -3 64038.21 60402.62 4016.82 o
4 8 -3 29407.45 29076.21 2936.85 o
1 9 -3 9516.68 8889.97 431.97 o
3 9 -3 5230.92 4988.52 267.52 o
0 10 -3 72366.42 65701.09 6177.87 o
2 10 -3 52917.14 48929.41 2777.06 o
4 10 -3 25212.46 27664.45 3900.45 o
1 11 -3 50765.73 46390.79 2965.24 o
3 11 -3 29716.41 27024.72 1516.29 o
0 12 -3 38349.91 36492.94 3241.34 o
2 12 -3 28638.12 26413.31 1410.83 o
4 12 -3 14041.20 14577.57 2127.01 o
1 13 -3 64.14 95.70 39.01 o
3 13 -3 47.16 65.05 28.28 o
0 14 -3 11631.67 11264.19 950.96 o
2 14 -3 9012.72 8281.72 471.73 o
1 15 -3 9328.27 8494.00 513.48 o
3 15 -3 5801.49 5879.49 527.26 o
0 16 -3 18865.87 19053.21 1895.89 o
2 16 -3 14969.05 15230.79 1263.70 o
1 17 -3 14769.53 14110.69 900.02 o
0 18 -3 17274.82 17250.50 2041.65 o
2 18 -3 13914.46 15181.59 1294.93 o
1 19 -3 36948.54 37035.43 2478.20 o
0 20 -3 5733.30 5659.87 923.68 o
0 0 -2 3015.03 3764.07 296.02 o
2 0 -2 1700.94 1683.30 116.75 o
4 0 -2 684.22 732.38 112.16 o
1 1 -2 8486.59 7729.26 804.57 o
3 1 -2 3871.14 3850.80 211.61 o
5 1 -2 1480.58 1555.26 122.93 o
0 2 -2 4749.85 4891.31 319.34 o
2 2 -2 2659.15 2686.03 171.81 o
4 2 -2 975.55 1023.68 102.41 o
1 3 -2 102184.56 95239.21 10323.33 o
3 3 -2 45156.70 47004.96 2856.98 o
5 3 -2 16666.73 17175.97 1492.08 o
0 4 -2 169018.72 145787.23 19387.22 o
2 4 -2 103460.68 103708.15 5522.70 o
4 4 -2 43689.99 43023.13 2661.91 o
1 5 -2 600.69 652.45 70.19 o
3 5 -2 340.69 388.57 28.84 o
0 6 -2 136625.31 117942.05 11118.71 o
2 6 -2 88902.36 91593.55 4528.85 o
4 6 -2 37560.27 36240.09 2189.58 o
1 7 -2 122432.97 112152.42 7702.94 o
3 7 -2 63431.08 63499.38 3296.99 o
0 8 -2 6213.65 5611.68 592.78 o
2 8 -2 4437.53 4196.92 208.27 o
4 8 -2 2058.47 1977.15 297.46 o
1 9 -2 30908.26 28266.70 1596.32 o
3 9 -2 16965.70 16293.71 698.61 o
0 10 -2 17213.05 15343.82 1304.56 o
2 10 -2 12457.62 11659.20 596.40 o
4 10 -2 6176.15 5485.08 939.57 o
1 11 -2 15861.63 14874.85 882.94 o
3 11 -2 8872.89 8500.23 365.29 o
0 12 -2 13623.31 12658.18 1062.81 o
2 12 -2 10291.15 9373.38 487.91 o
4 12 -2 5316.96 5324.66 668.97 o
1 13 -2 47392.67 43991.81 2909.12 o
3 13 -2 28790.09 25456.85 1442.97 o
0 14 -2 59100.98 57422.39 5553.92 o
2 14 -2 45827.73 40541.15 2618.66 o
1 15 -2 40590.71 39737.40 2632.73 o
3 15 -2 25309.70 21026.84 2631.85 o
0 16 -2 10298.14 9540.83 923.25 o
2 16 -2 8384.59 8025.46 504.45 o
1 17 -2 12324.24 11433.41 735.55 o
0 18 -2 4161.39 4273.09 892.16 o
2 18 -2 3336.05 3631.14 415.38 o
1 19 -2 11205.72 11108.66 747.97 o
0 20 -2 4407.28 4522.18 954.95 o
1 1 -1 8278.07 8380.12 330.11 o
3 1 -1 3565.09 3803.22 205.17 o
5 1 -1 1376.31 1526.72 115.33 o
0 2 -1 18822.53 18391.85 1319.23 o
2 2 -1 9613.66 9270.10 354.84 o
4 2 -1 3687.85 3728.19 209.19 o
1 3 -1 185137.03 191221.47 16480.04 o
3 3 -1 81797.31 85896.67 5133.70 o
5 3 -1 30376.18 29798.72 1852.07 o
0 4 -1 27047.96 24592.92 1861.12 o
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