#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/54/2215480.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215480_Fobs loop_ _publ_author_name 'Dutkiewicz, Grzegorz' 'Borowiak, Teresa' 'Pietraszkiewicz, Marek' 'Pietraszkiewicz, Oksana' _publ_section_title ; Tetraammonium benzene-1,2,4,5-tetracarboxylate dihydrate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4101 _journal_volume 63 _journal_year 2007 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.821 _cell_angle_gamma 90.000 _cell_length_a 11.6054 _cell_length_b 6.7122 _cell_length_c 10.5718 _exptl_crystal_F_000 380.00 _reflns_d_resolution_high 0.7308 _[local]_cod_data_source_file gg2029Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pirom in C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 968.70 921.27 2.95 o 4 0 0 1425.27 1365.57 10.44 o 6 0 0 1828.83 1892.61 7.59 o 8 0 0 376.71 415.44 4.16 o 10 0 0 490.89 474.64 11.24 o 12 0 0 162.89 150.02 5.00 o 1 1 0 3668.14 3770.99 6.10 o 3 1 0 266.85 335.94 1.81 o 5 1 0 324.62 389.22 2.00 o 7 1 0 644.79 632.42 4.18 o 9 1 0 633.15 607.18 7.34 o 11 1 0 114.06 105.75 2.99 o 13 1 0 132.31 130.26 5.08 o 0 2 0 9864.78 9593.69 34.55 o 2 2 0 102.57 80.02 0.91 o 4 2 0 678.47 674.11 3.00 o 6 2 0 601.01 630.35 2.56 o 8 2 0 212.20 208.90 2.12 o 10 2 0 1125.80 1119.78 6.68 o 12 2 0 84.96 88.80 3.31 o 14 2 0 22.50 22.96 3.34 o 1 3 0 346.08 354.56 1.70 o 3 3 0 2045.84 2073.94 6.01 o 5 3 0 467.68 504.61 3.76 o 7 3 0 120.55 117.18 1.81 o 9 3 0 630.35 630.62 5.24 o 11 3 0 14.84 13.74 1.91 o 13 3 0 22.73 22.24 3.29 o 0 4 0 4771.14 5069.29 18.49 o 2 4 0 228.44 228.23 1.88 o 4 4 0 313.35 316.07 2.56 o 6 4 0 257.07 264.86 3.35 o 8 4 0 11.87 9.76 1.31 o 10 4 0 1159.36 1171.95 10.26 o 12 4 0 51.48 48.04 2.96 o 1 5 0 704.57 745.61 3.51 o 3 5 0 64.23 60.19 1.37 o 5 5 0 116.34 118.79 2.58 o 7 5 0 47.05 45.99 2.62 o 9 5 0 399.73 389.32 7.22 o 11 5 0 16.80 14.48 2.39 o 0 6 0 3618.88 3644.91 15.41 o 2 6 0 619.03 626.10 4.16 o 4 6 0 101.17 99.59 3.32 o 6 6 0 40.09 42.15 2.11 o 8 6 0 29.50 28.65 2.52 o 10 6 0 51.31 50.27 3.23 o 1 7 0 224.14 226.61 3.23 o 3 7 0 305.56 312.10 3.89 o 5 7 0 124.17 122.84 3.93 o 7 7 0 99.73 103.21 4.16 o 9 7 0 118.35 116.24 4.51 o 0 8 0 713.51 703.79 12.48 o 2 8 0 40.91 41.51 2.39 o 4 8 0 6.15 5.15 2.05 o 6 8 0 66.34 77.83 3.73 o -12 0 1 81.58 73.77 4.05 o -10 0 1 2427.39 2411.18 11.54 o -8 0 1 2131.22 2130.40 9.53 o -6 0 1 161.58 175.93 2.56 o -4 0 1 11785.23 11291.20 106.68 o -2 0 1 40.71 68.03 1.01 o 2 0 1 16.79 30.87 0.65 o 4 0 1 7428.56 7572.63 54.11 o 6 0 1 923.08 973.11 5.17 o 8 0 1 445.92 470.97 4.73 o 10 0 1 281.31 261.17 7.24 o 12 0 1 186.88 195.63 6.14 o -11 1 1 122.57 114.00 3.31 o -9 1 1 1778.63 1753.25 8.76 o -7 1 1 217.95 228.52 1.90 o -5 1 1 1129.78 1269.89 9.19 o -3 1 1 681.96 768.50 5.88 o -1 1 1 113.71 122.61 0.94 o 1 1 1 929.98 952.51 5.99 o 3 1 1 4594.91 4435.37 6.75 o 5 1 1 970.88 1109.15 3.70 o 7 1 1 0.59 2.56 1.51 o 9 1 1 225.16 215.63 2.47 o 11 1 1 148.55 151.07 3.50 o 13 1 1 16.78 16.16 2.63 o -14 2 1 11.32 5.96 2.98 o -12 2 1 167.24 174.86 4.07 o -10 2 1 923.35 911.84 6.33 o -8 2 1 291.65 289.65 4.90 o -6 2 1 59.53 67.52 1.13 o -4 2 1 132.78 126.74 1.89 o -2 2 1 78.28 83.44 0.67 o 0 2 1 19288.86 18232.14 59.84 o 2 2 1 830.28 765.07 6.69 o 4 2 1 164.03 181.50 1.51 o 6 2 1 970.40 986.72 3.82 o 8 2 1 792.71 826.51 4.72 o 10 2 1 373.40 374.40 3.58 o 12 2 1 294.71 307.88 7.41 o -13 3 1 23.20 24.72 2.43 o -11 3 1 38.70 36.30 2.50 o -9 3 1 567.92 580.92 5.15 o -7 3 1 780.12 763.04 8.05 o -5 3 1 740.95 759.41 4.29 o -3 3 1 514.70 539.13 2.01 o -1 3 1 646.00 604.20 3.39 o 1 3 1 3448.60 3750.72 6.03 o 3 3 1 511.47 507.89 4.51 o 5 3 1 46.83 48.42 2.09 o 7 3 1 13.73 12.86 1.07 o 9 3 1 218.15 197.95 3.15 o 11 3 1 6.78 6.61 1.78 o 13 3 1 90.40 98.45 5.11 o -14 4 1 111.82 113.64 5.95 o -12 4 1 54.06 58.19 3.14 o -10 4 1 431.02 442.61 6.46 o -8 4 1 517.35 522.00 5.59 o -6 4 1 377.61 372.70 3.80 o -4 4 1 214.96 228.67 3.55 o -2 4 1 187.14 194.26 1.78 o 0 4 1 3183.17 3353.38 8.91 o 2 4 1 320.37 353.49 2.22 o 4 4 1 204.86 215.18 2.31 o 6 4 1 139.86 130.22 2.51 o 8 4 1 195.00 219.93 5.12 o 10 4 1 18.04 16.64 1.75 o 12 4 1 128.03 125.57 4.01 o -11 5 1 0.33 -0.14 2.21 o -9 5 1 723.85 746.23 8.51 o -7 5 1 28.05 28.25 1.66 o -5 5 1 68.33 68.87 2.43 o -3 5 1 309.43 298.85 4.15 o -1 5 1 68.80 57.23 1.33 o 1 5 1 261.66 280.96 2.47 o 3 5 1 653.55 686.72 6.05 o 5 5 1 627.77 648.67 5.56 o 7 5 1 57.77 59.89 2.46 o 9 5 1 192.12 194.70 3.66 o 11 5 1 6.30 5.31 2.06 o -10 6 1 825.70 854.19 18.04 o -8 6 1 308.42 319.87 5.94 o -6 6 1 349.54 362.86 4.61 o -4 6 1 403.52 409.58 4.03 o -2 6 1 69.18 69.72 1.65 o 0 6 1 363.34 389.04 3.22 o 2 6 1 298.62 284.51 3.95 o 4 6 1 376.99 391.00 4.70 o 6 6 1 213.36 219.68 4.27 o 8 6 1 132.00 139.21 3.33 o 10 6 1 183.51 188.52 5.13 o -9 7 1 297.89 298.44 9.12 o -7 7 1 109.61 111.05 5.29 o -5 7 1 11.06 10.34 1.60 o -3 7 1 61.71 62.57 2.09 o -1 7 1 140.39 136.82 2.59 o 1 7 1 100.45 99.07 2.87 o 3 7 1 332.21 341.85 5.74 o 5 7 1 57.10 58.54 3.25 o 7 7 1 26.93 27.38 2.88 o -6 8 1 27.70 31.01 2.82 o -4 8 1 40.46 36.71 2.20 o -2 8 1 29.50 25.33 2.06 o 0 8 1 264.51 265.77 4.62 o 2 8 1 19.59 22.65 2.58 o 4 8 1 41.35 40.15 2.79 o 6 8 1 65.26 66.51 2.92 o -3 9 1 5.10 4.65 2.27 o -1 9 1 20.35 19.20 3.82 o -14 0 2 0.78 0.59 2.73 o -12 0 2 415.36 438.75 8.52 o -10 0 2 29.18 20.94 1.80 o -8 0 2 153.36 138.79 2.83 o -6 0 2 1533.70 1558.09 7.43 o -4 0 2 12472.14 11756.10 99.91 o -2 0 2 1898.74 1909.24 6.95 o 0 0 2 98.15 77.12 1.96 o 2 0 2 6870.91 6282.07 14.54 o 4 0 2 69.35 70.92 2.33 o 6 0 2 542.58 493.70 3.63 o 8 0 2 272.51 258.86 3.66 o 10 0 2 262.87 280.87 6.85 o 12 0 2 18.04 17.29 3.49 o -15 1 2 178.76 194.79 7.12 o -13 1 2 198.66 204.05 4.50 o -11 1 2 5.11 3.97 1.37 o -9 1 2 570.26 574.87 3.99 o -7 1 2 132.22 134.13 1.52 o -5 1 2 4395.90 4540.75 13.30 o -3 1 2 934.19 926.26 3.15 o -1 1 2 3434.56 3404.02 5.04 o 1 1 2 1308.78 1258.59 8.66 o 3 1 2 691.42 720.50 3.48 o 5 1 2 570.90 651.71 2.20 o 7 1 2 1260.45 1289.74 5.26 o 9 1 2 380.44 366.68 3.32 o 11 1 2 38.23 33.96 2.58 o 13 1 2 19.54 14.84 2.76 o -14 2 2 5.97 10.27 2.99 o -12 2 2 222.58 214.97 3.71 o -10 2 2 177.96 180.04 3.15 o -8 2 2 232.74 223.15 4.33 o -6 2 2 293.83 300.95 3.61 o -4 2 2 369.91 389.38 1.52 o -2 2 2 431.92 395.64 2.47 o 0 2 2 271.59 282.92 1.55 o 2 2 2 1668.37 1780.69 8.20 o 4 2 2 3779.08 4038.37 7.21 o 6 2 2 155.75 166.43 2.08 o 8 2 2 293.72 299.31 4.91 o 10 2 2 75.03 76.45 1.92 o 12 2 2 72.79 75.09 4.34 o -13 3 2 49.47 51.70 2.98 o -11 3 2 208.66 204.01 3.59 o -9 3 2 446.69 433.43 4.94 o -7 3 2 394.92 369.93 5.00 o -5 3 2 919.02 956.82 8.61 o -3 3 2 3403.23 3441.03 7.91 o -1 3 2 363.59 381.01 2.03 o 1 3 2 146.51 180.43 1.71 o 3 3 2 218.08 229.77 2.32 o 5 3 2 733.06 818.12 5.32 o 7 3 2 6.04 4.59 1.03 o 9 3 2 51.33 55.01 1.69 o 11 3 2 68.08 69.26 2.37 o -14 4 2 57.34 59.02 4.56 o -12 4 2 183.11 181.08 4.71 o -10 4 2 250.73 256.68 5.06 o -8 4 2 30.65 29.80 1.83 o -6 4 2 107.91 103.96 2.13 o -4 4 2 70.92 75.20 1.41 o -2 4 2 267.95 270.62 2.04 o 0 4 2 265.65 272.35 1.98 o 2 4 2 296.33 336.82 3.49 o 4 4 2 982.38 1083.11 6.73 o 6 4 2 231.91 244.28 2.82 o 8 4 2 224.42 225.19 3.65 o 10 4 2 64.20 65.05 2.89 o 12 4 2 165.74 172.81 6.55 o -11 5 2 21.34 20.69 2.33 o -9 5 2 97.99 104.43 3.61 o -7 5 2 65.78 66.37 2.85 o -5 5 2 791.42 787.97 5.03 o -3 5 2 186.61 190.30 2.02 o -1 5 2 454.98 464.54 2.92 o 1 5 2 133.42 131.82 2.00 o 3 5 2 1.03 3.49 0.95 o 5 5 2 390.34 380.11 6.46 o 7 5 2 157.03 161.13 4.20 o 9 5 2 126.84 121.48 3.04 o 11 5 2 51.86 49.46 3.10 o -10 6 2 114.50 111.77 5.64 o -8 6 2 177.51 172.93 5.68 o -6 6 2 578.82 586.08 14.49 o -4 6 2 532.73 541.27 4.56 o -2 6 2 422.64 405.56 3.10 o 0 6 2 59.50 62.40 1.57 o 2 6 2 207.74 206.71 4.31 o 4 6 2 147.46 159.33 3.26 o 6 6 2 74.22 76.04 2.61 o 8 6 2 12.62 13.61 1.81 o 10 6 2 42.72 43.24 3.78 o -9 7 2 106.27 109.72 5.17 o -7 7 2 126.76 127.25 6.48 o -5 7 2 200.86 200.50 3.87 o -3 7 2 7.04 7.15 1.29 o -1 7 2 189.01 197.26 3.08 o 1 7 2 110.65 108.70 3.55 o 3 7 2 6.79 4.32 3.13 o 5 7 2 28.52 33.31 2.89 o 7 7 2 105.43 103.95 3.23 o -6 8 2 4.56 1.94 2.13 o -4 8 2 31.12 29.10 2.17 o -2 8 2 11.50 11.73 2.40 o 0 8 2 49.39 42.80 2.95 o 2 8 2 227.09 225.49 5.29 o 4 8 2 86.10 82.39 4.52 o 6 8 2 30.73 30.15 3.83 o 1 9 2 16.96 14.52 3.57 o -14 0 3 509.81 552.00 10.73 o -12 0 3 4.50 4.94 1.78 o -10 0 3 337.37 314.46 6.20 o -8 0 3 1881.95 1904.75 19.55 o -6 0 3 90.25 111.57 2.43 o -4 0 3 393.45 406.67 3.33 o -2 0 3 159.77 136.82 1.67 o 0 0 3 1761.14 1803.00 5.67 o 2 0 3 1175.59 1148.08 4.84 o 4 0 3 547.34 667.72 3.63 o 6 0 3 15.41 15.63 0.94 o 8 0 3 60.80 49.77 3.89 o 10 0 3 175.05 166.32 5.78 o 12 0 3 70.69 61.69 3.29 o 14 0 3 13.92 21.09 3.32 o -15 1 3 100.19 105.33 5.66 o -13 1 3 22.36 22.57 1.88 o -11 1 3 128.02 121.03 2.35 o -9 1 3 473.23 473.99 3.79 o -7 1 3 62.33 53.27 2.57 o -5 1 3 1594.75 1688.40 7.03 o -3 1 3 5839.93 5575.21 6.45 o -1 1 3 2070.41 1993.95 4.12 o 1 1 3 580.57 508.53 2.52 o 3 1 3 2296.17 2406.37 7.94 o 5 1 3 390.03 422.91 2.36 o 7 1 3 158.63 162.21 2.14 o 9 1 3 40.31 32.96 1.74 o 11 1 3 68.37 67.93 3.28 o 13 1 3 6.43 8.54 2.10 o -14 2 3 396.37 432.31 6.91 o -12 2 3 45.97 44.46 2.21 o -10 2 3 102.03 100.49 2.54 o -8 2 3 149.46 155.36 2.77 o -6 2 3 313.51 351.24 2.94 o -4 2 3 5305.87 5461.80 8.06 o -2 2 3 996.90 1046.27 6.18 o 0 2 3 1222.21 1198.52 8.18 o 2 2 3 3228.95 3434.17 8.81 o 4 2 3 28.43 23.63 1.00 o 6 2 3 321.42 316.01 2.89 o 8 2 3 142.01 115.86 2.11 o 10 2 3 85.87 91.44 2.47 o 12 2 3 58.16 56.32 5.10 o -15 3 3 179.17 179.73 7.18 o -13 3 3 26.63 27.73 2.56 o -11 3 3 50.52 49.49 2.26 o -9 3 3 14.46 14.80 2.49 o -7 3 3 154.23 134.63 3.11 o -5 3 3 511.56 521.88 4.45 o -3 3 3 89.92 100.94 1.31 o -1 3 3 1060.67 1177.32 3.98 o 1 3 3 79.30 83.69 1.22 o 3 3 3 35.95 27.94 1.13 o 5 3 3 520.37 536.10 3.78 o 7 3 3 546.72 587.80 4.32 o 9 3 3 92.70 91.00 2.11 o 11 3 3 20.27 19.05 2.07 o -12 4 3 33.42 34.95 3.44 o -10 4 3 1.18 -0.52 2.41 o -8 4 3 19.82 20.03 1.95 o -6 4 3 568.02 576.39 4.97 o -4 4 3 641.64 689.56 3.69 o -2 4 3 263.65 311.41 2.21 o 0 4 3 658.18 702.49 6.43 o 2 4 3 690.90 733.90 8.22 o 4 4 3 90.24 104.52 1.97 o 6 4 3 21.77 21.64 1.31 o 8 4 3 187.95 183.31 3.34 o 10 4 3 33.70 33.73 2.01 o 12 4 3 1.28 -0.59 6.91 o -11 5 3 77.36 76.17 3.52 o -9 5 3 6.35 6.24 1.69 o -7 5 3 198.43 197.27 4.31 o -5 5 3 232.91 245.75 2.62 o -3 5 3 506.61 494.89 3.15 o -1 5 3 194.46 180.99 1.94 o 1 5 3 821.21 812.72 5.68 o 3 5 3 257.81 251.82 3.37 o 5 5 3 109.32 115.03 2.79 o 7 5 3 97.09 103.50 2.77 o 9 5 3 47.56 47.24 2.27 o 11 5 3 13.28 10.76 3.05 o -10 6 3 166.69 174.24 4.83 o -8 6 3 240.45 248.97 5.23 o -6 6 3 78.54 82.31 3.19 o -4 6 3 151.16 150.16 2.31 o -2 6 3 10.46 9.19 0.95 o 0 6 3 266.19 262.24 3.73 o 2 6 3 10.58 8.64 1.41 o 4 6 3 16.91 17.62 2.18 o 6 6 3 21.23 21.34 1.94 o 8 6 3 133.06 139.13 3.52 o 10 6 3 11.53 11.80 2.65 o -9 7 3 23.73 24.01 3.24 o -7 7 3 12.74 13.21 2.21 o -5 7 3 185.22 179.14 4.01 o -3 7 3 205.96 190.08 3.18 o -1 7 3 129.08 126.63 2.99 o 1 7 3 64.27 58.54 3.09 o 3 7 3 47.19 47.69 2.95 o 5 7 3 88.27 92.91 4.18 o 7 7 3 6.91 5.39 1.76 o -6 8 3 216.52 228.55 8.98 o -4 8 3 67.41 66.19 2.76 o -2 8 3 213.55 231.49 8.54 o 0 8 3 40.72 37.79 2.93 o 2 8 3 28.95 26.35 2.86 o 4 8 3 165.94 166.84 5.04 o -14 0 4 552.53 576.20 11.12 o -12 0 4 18.67 17.81 2.25 o -10 0 4 27.71 31.48 2.36 o -8 0 4 0.12 4.65 2.92 o -6 0 4 597.33 587.94 9.43 o -4 0 4 155.28 168.78 1.43 o -2 0 4 146.14 143.03 1.44 o 0 0 4 1848.78 1753.85 20.19 o 2 0 4 5032.21 5316.23 14.57 o 4 0 4 80.60 68.80 1.16 o 6 0 4 720.98 761.62 7.95 o 8 0 4 398.64 309.34 5.12 o 10 0 4 151.61 165.44 4.44 o 12 0 4 48.06 43.09 3.22 o -15 1 4 21.91 26.03 2.72 o -13 1 4 168.10 178.66 3.64 o -11 1 4 30.47 27.95 1.62 o -9 1 4 148.28 145.08 2.42 o -7 1 4 662.83 661.59 4.90 o -5 1 4 331.37 328.61 1.87 o -3 1 4 527.64 517.70 4.00 o -1 1 4 426.35 413.62 2.17 o 1 1 4 156.92 165.51 1.36 o 3 1 4 424.39 420.58 3.78 o 5 1 4 1122.74 1132.90 6.58 o 7 1 4 97.91 81.47 1.72 o 9 1 4 336.30 320.18 5.23 o 11 1 4 281.44 293.57 4.68 o 13 1 4 0.91 -0.44 1.26 o -14 2 4 325.59 361.72 5.30 o -12 2 4 72.66 74.13 2.60 o -10 2 4 53.87 43.22 2.15 o -8 2 4 1033.89 1012.69 9.49 o -6 2 4 353.45 350.06 3.49 o -4 2 4 289.52 295.83 3.09 o -2 2 4 834.74 980.51 5.50 o 0 2 4 786.69 763.95 3.99 o 2 2 4 83.13 79.38 1.71 o 4 2 4 81.25 76.94 1.55 o 6 2 4 256.73 245.44 2.68 o 8 2 4 285.25 260.17 4.40 o 10 2 4 13.58 10.65 2.22 o 12 2 4 27.70 23.03 2.72 o -13 3 4 21.93 23.63 2.13 o -11 3 4 32.50 29.51 2.18 o -9 3 4 34.93 31.83 1.90 o -7 3 4 293.45 298.79 3.94 o -5 3 4 432.23 450.93 2.67 o -3 3 4 816.62 826.51 4.15 o -1 3 4 228.12 219.29 1.59 o 1 3 4 565.23 580.25 2.61 o 3 3 4 1067.63 1093.04 11.27 o 5 3 4 30.36 28.03 1.43 o 7 3 4 148.18 141.80 2.38 o 9 3 4 322.26 298.46 4.55 o 11 3 4 128.31 133.24 5.59 o 13 3 4 69.88 77.58 5.20 o -12 4 4 8.86 8.57 1.88 o -10 4 4 278.89 259.04 4.24 o -8 4 4 318.12 322.80 5.19 o -6 4 4 27.52 24.26 1.35 o -4 4 4 868.83 851.30 6.69 o -2 4 4 52.56 52.68 1.26 o 0 4 4 177.31 178.60 2.47 o 2 4 4 82.14 83.31 2.02 o 4 4 4 137.09 124.26 2.24 o 6 4 4 127.81 121.88 2.32 o 8 4 4 163.81 153.64 2.75 o 10 4 4 17.13 17.44 1.78 o 12 4 4 81.79 75.22 5.11 o -11 5 4 45.95 46.26 2.53 o -9 5 4 52.34 48.93 2.44 o -7 5 4 166.99 170.96 3.23 o -5 5 4 30.68 27.30 1.42 o -3 5 4 489.67 470.75 3.40 o -1 5 4 42.92 37.67 1.31 o 1 5 4 168.72 158.75 2.86 o 3 5 4 88.71 82.99 2.40 o 5 5 4 309.03 306.26 3.53 o 7 5 4 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3 12 372.06 383.67 9.56 o 1 3 12 237.89 259.62 5.73 o -6 4 12 3.96 2.94 2.37 o -4 4 12 19.76 18.45 3.69 o -2 4 12 63.88 62.41 5.12 o 0 4 12 16.93 10.98 2.37 o -1 5 12 62.90 70.85 4.79 o -8 0 13 12.25 12.19 3.81 o -2 0 13 1.86 2.63 2.83 o 0 0 13 98.50 85.68 5.24 o 2 0 13 260.92 291.00 8.61 o -9 1 13 4.49 2.49 3.66 o -5 1 13 60.38 61.38 4.54 o -3 1 13 33.15 35.66 3.71 o -1 1 13 16.03 13.28 3.43 o 1 1 13 10.36 11.24 2.52 o 3 1 13 85.81 94.37 5.41 o -8 2 13 139.08 147.45 5.14 o -6 2 13 53.60 56.88 2.90 o -4 2 13 54.39 50.83 4.83 o -2 2 13 2.48 0.90 2.99 o 0 2 13 31.62 37.18 4.35 o 2 2 13 53.73 64.64 4.69 o -7 3 13 391.73 455.35 10.76 o -5 3 13 54.98 65.42 4.57 o -3 3 13 0.81 -0.08 3.50 o 0 0 14 32.11 32.78 4.52 o -3 1 14 156.82 190.06 7.21 o