#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215578.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215578_Fobs loop_ _publ_author_name 'Zewge, Daniel' 'Brunskill, Andrew P. J.' 'Thompson, Hugh W.' 'Lalancette, Roger A.' _publ_section_title ; (+/-)-4-(2-Oxo-1,2,3,4,4a,5,6,7-octahydroquinolin-8-yl)butan-2-one. A Michael-reaction adduct from acid-catalyzed alkylation of a bicyclic enamide ; _journal_coeditor_code LH2489 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4007 _journal_page_last o4008 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 104.694 _cell_angle_beta 97.764 _cell_angle_gamma 91.147 _cell_length_a 5.4984 _cell_length_b 10.4062 _cell_length_c 10.7217 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.8306 _[local]_cod_data_source_file lh2489Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 052606RAL in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1339.90 1254.29 21.40 o 2 0 0 316.51 307.37 3.42 o 3 0 0 1.46 2.00 0.23 o 4 0 0 29.32 26.84 0.77 o -5 1 0 54.93 52.48 1.27 o -4 1 0 15.45 19.37 0.46 o -3 1 0 9.38 10.96 0.26 o -2 1 0 482.20 463.90 5.17 o -1 1 0 99.21 87.95 1.67 o 0 1 0 567.70 514.42 36.29 o 1 1 0 566.44 525.27 6.57 o 2 1 0 333.60 371.80 4.31 o 3 1 0 65.97 66.92 1.68 o 4 1 0 159.85 156.76 3.53 o -6 2 0 25.44 23.39 1.78 o -5 2 0 18.02 15.12 0.46 o -4 2 0 88.85 90.44 1.23 o -3 2 0 176.09 184.06 1.99 o -2 2 0 18.81 26.86 0.47 o -1 2 0 6.41 3.96 0.16 o 0 2 0 2486.78 2432.07 36.39 o 1 2 0 71.33 73.24 1.57 o 2 2 0 39.56 51.86 0.91 o 3 2 0 9.18 8.51 0.43 o -6 3 0 27.15 22.13 1.77 o -5 3 0 52.94 46.90 0.83 o -4 3 0 7.79 8.67 0.51 o -3 3 0 0.04 0.24 0.15 o -2 3 0 139.37 139.11 1.29 o -1 3 0 971.50 945.26 9.97 o 0 3 0 134.84 128.05 1.34 o 1 3 0 630.92 598.50 8.64 o 2 3 0 33.40 33.93 0.63 o 3 3 0 0.09 0.13 0.09 o 4 3 0 157.71 158.24 2.39 o -6 4 0 7.01 8.26 0.77 o -5 4 0 49.08 50.92 1.19 o -4 4 0 0.03 0.02 0.15 o -3 4 0 63.22 59.07 0.92 o -2 4 0 96.00 91.90 1.00 o -1 4 0 280.29 326.34 3.86 o 0 4 0 1054.61 1178.53 9.55 o 1 4 0 0.09 1.39 0.15 o 2 4 0 0.56 1.03 0.13 o 3 4 0 16.81 11.38 0.41 o 4 4 0 1.44 3.58 0.60 o -6 5 0 0.11 0.40 0.72 o -5 5 0 36.55 35.37 0.77 o -4 5 0 339.80 332.29 2.58 o -3 5 0 18.05 18.32 0.52 o -2 5 0 29.71 26.29 1.72 o -1 5 0 299.20 332.39 4.32 o 0 5 0 3.65 4.96 0.28 o 1 5 0 434.70 425.84 3.44 o 2 5 0 9.89 8.76 0.27 o 3 5 0 19.97 14.88 0.42 o 4 5 0 13.60 10.70 0.95 o 5 5 0 9.68 7.81 0.68 o -5 6 0 109.61 108.62 1.58 o -4 6 0 397.08 401.63 3.26 o -3 6 0 69.43 60.41 0.90 o -2 6 0 26.57 26.14 1.10 o -1 6 0 31.88 37.71 0.90 o 0 6 0 341.88 362.44 3.44 o 1 6 0 180.44 177.08 1.54 o 2 6 0 6.76 6.02 0.26 o 3 6 0 71.41 68.86 0.89 o 4 6 0 3.19 3.35 0.28 o 5 6 0 21.85 21.10 0.83 o -5 7 0 72.78 82.36 1.32 o -4 7 0 2.06 1.41 0.21 o -3 7 0 98.54 81.95 1.88 o -2 7 0 8.88 6.77 0.58 o -1 7 0 43.44 44.47 1.07 o 0 7 0 13.36 13.71 0.77 o 1 7 0 42.92 37.43 0.74 o 2 7 0 300.99 281.34 2.59 o 3 7 0 1.69 1.84 0.20 o 4 7 0 107.84 116.36 1.70 o 5 7 0 44.58 47.07 1.28 o -5 8 0 2.22 1.52 0.27 o -4 8 0 35.31 11.96 2.18 o -3 8 0 139.43 140.98 1.41 o -2 8 0 0.51 0.29 0.12 o -1 8 0 83.33 70.44 1.00 o 0 8 0 0.19 0.54 0.16 o 1 8 0 0.66 0.26 0.14 o 2 8 0 327.09 317.62 2.18 o 3 8 0 101.49 103.81 1.12 o 4 8 0 99.10 92.04 1.18 o -4 9 0 86.47 92.28 1.02 o -3 9 0 11.18 11.76 0.29 o -2 9 0 0.11 0.01 0.08 o -1 9 0 8.46 6.72 0.48 o 0 9 0 0.11 0.23 0.10 o 1 9 0 30.23 27.52 0.45 o 2 9 0 37.60 36.71 0.60 o 3 9 0 53.81 52.77 0.68 o 4 9 0 12.80 12.31 0.59 o -4 10 0 0.00 0.30 0.20 o -3 10 0 12.03 12.26 0.25 o -2 10 0 0.12 0.17 0.10 o -1 10 0 77.06 62.82 0.63 o 0 10 0 0.13 0.54 0.09 o 1 10 0 0.35 0.53 0.12 o 2 10 0 0.55 1.07 0.18 o 3 10 0 4.79 5.11 0.21 o -3 11 0 49.85 58.41 0.79 o -2 11 0 0.40 0.20 0.08 o -1 11 0 2.89 2.98 0.17 o 0 11 0 2.99 3.91 0.18 o 1 11 0 18.25 18.03 0.61 o 2 11 0 30.30 29.78 0.58 o -1 12 0 4.48 6.74 0.52 o 0 12 0 45.11 43.58 0.58 o 0 -12 1 2.54 1.44 0.14 o 1 -12 1 23.75 26.29 0.53 o -2 -11 1 1.85 1.66 0.13 o -1 -11 1 0.31 0.10 0.11 o 0 -11 1 14.97 12.96 0.30 o 1 -11 1 24.75 20.32 0.29 o 2 -11 1 10.02 12.99 0.34 o 3 -11 1 13.61 15.96 0.43 o -3 -10 1 31.37 36.48 0.50 o -2 -10 1 23.61 22.94 0.54 o -1 -10 1 6.52 6.17 0.23 o 0 -10 1 1.54 1.51 0.25 o 1 -10 1 2.33 1.80 0.14 o 2 -10 1 22.86 20.32 0.31 o 3 -10 1 12.09 13.81 0.27 o 4 -10 1 20.47 22.63 0.52 o -4 -9 1 0.13 0.17 0.11 o -3 -9 1 91.62 90.18 0.97 o -2 -9 1 51.37 48.35 0.62 o -1 -9 1 6.14 5.48 0.20 o 0 -9 1 35.01 30.64 0.46 o 1 -9 1 26.13 10.84 0.19 o 2 -9 1 36.98 26.13 0.33 o 3 -9 1 1.11 1.25 0.14 o 4 -9 1 11.53 12.30 0.38 o -4 -8 1 123.12 125.57 1.19 o -3 -8 1 40.32 42.88 0.60 o -2 -8 1 109.51 109.01 0.96 o -1 -8 1 24.32 26.74 0.55 o 0 -8 1 20.55 18.43 0.55 o 1 -8 1 37.13 38.23 0.76 o 2 -8 1 22.47 28.22 0.39 o 3 -8 1 0.71 0.83 0.41 o 4 -8 1 5.49 5.90 1.87 o 5 -8 1 62.59 69.45 1.15 o -5 -7 1 2.10 1.50 0.22 o -4 -7 1 24.44 28.49 0.64 o -3 -7 1 20.02 20.15 0.49 o -2 -7 1 4.61 3.73 0.22 o -1 -7 1 425.22 401.94 3.89 o 0 -7 1 9.38 13.09 0.48 o 1 -7 1 3.04 2.20 0.41 o 2 -7 1 82.83 78.73 1.89 o 3 -7 1 98.36 91.02 2.69 o 4 -7 1 3.48 3.12 0.43 o 5 -7 1 28.85 27.15 0.79 o -5 -6 1 65.19 71.21 1.28 o -4 -6 1 59.29 59.14 0.90 o -3 -6 1 199.68 189.88 2.08 o -2 -6 1 24.00 25.26 0.49 o -1 -6 1 180.04 192.59 1.63 o 0 -6 1 296.87 295.08 2.85 o 1 -6 1 5.10 4.58 0.36 o 2 -6 1 1.16 1.65 0.32 o 3 -6 1 94.66 88.66 1.17 o 4 -6 1 30.06 31.62 0.71 o 5 -6 1 0.00 -0.07 0.38 o -5 -5 1 107.08 104.92 1.73 o -4 -5 1 0.07 0.12 0.15 o -3 -5 1 34.71 40.11 0.64 o -2 -5 1 0.26 1.29 0.14 o -1 -5 1 48.04 47.76 0.59 o 0 -5 1 1789.50 1917.20 16.91 o 1 -5 1 559.37 665.92 7.77 o 2 -5 1 69.45 59.07 1.29 o 3 -5 1 0.04 0.12 0.13 o 4 -5 1 12.23 10.84 0.35 o 5 -5 1 256.55 237.96 3.66 o 6 -5 1 6.97 2.51 0.97 o -5 -4 1 74.36 72.65 1.39 o -4 -4 1 3.62 4.75 0.28 o -3 -4 1 191.80 208.90 1.91 o -2 -4 1 16.77 15.92 0.36 o -1 -4 1 50.92 43.28 0.61 o 0 -4 1 2602.52 2680.92 28.97 o 1 -4 1 22.02 38.72 0.66 o 2 -4 1 172.03 168.08 2.04 o 3 -4 1 1.04 0.78 0.15 o 4 -4 1 0.08 0.35 0.23 o 5 -4 1 178.00 179.63 3.32 o 6 -4 1 16.64 14.09 1.10 o -5 -3 1 80.69 88.01 2.48 o -4 -3 1 20.05 16.00 0.42 o -3 -3 1 315.00 373.03 4.28 o -2 -3 1 93.72 102.44 1.21 o -1 -3 1 383.91 365.70 4.25 o 0 -3 1 125.24 119.68 1.52 o 1 -3 1 881.58 925.63 8.96 o 2 -3 1 213.70 220.79 2.02 o 3 -3 1 14.75 14.93 0.39 o 4 -3 1 9.51 7.70 0.37 o 5 -3 1 11.45 11.85 0.41 o 6 -3 1 9.54 12.05 1.67 o -5 -2 1 108.33 113.45 2.98 o -4 -2 1 8.25 9.29 0.52 o -3 -2 1 39.39 32.70 0.81 o -2 -2 1 91.91 93.54 1.54 o -1 -2 1 22.85 12.60 0.95 o 0 -2 1 222.70 228.78 13.04 o 1 -2 1 217.26 222.90 2.30 o 2 -2 1 56.00 71.48 0.92 o 3 -2 1 129.22 139.98 1.44 o 4 -2 1 1.11 1.22 0.17 o 5 -2 1 64.12 59.11 0.96 o 6 -2 1 0.00 -0.71 0.75 o -5 -1 1 141.93 150.42 3.81 o -4 -1 1 142.84 148.92 1.93 o -3 -1 1 15.78 13.67 0.71 o -2 -1 1 14.29 17.10 0.56 o -1 -1 1 8.64 4.16 0.27 o 0 -1 1 379.91 261.31 8.02 o 1 -1 1 1901.29 1913.16 18.07 o 2 -1 1 129.20 123.96 1.38 o 3 -1 1 0.07 0.12 0.12 o 4 -1 1 10.02 7.33 0.44 o -5 0 1 0.17 0.63 0.26 o -4 0 1 38.34 41.57 0.90 o -3 0 1 52.07 56.86 0.87 o -2 0 1 87.03 94.43 1.32 o -1 0 1 464.34 449.34 5.38 o 1 0 1 4224.15 4215.29 45.24 o 2 0 1 201.41 216.24 1.93 o 3 0 1 0.02 0.49 0.17 o -6 1 1 7.94 8.38 1.17 o -5 1 1 9.84 7.08 0.51 o -4 1 1 942.48 914.30 8.48 o -3 1 1 0.29 0.76 0.13 o -2 1 1 146.18 165.43 2.43 o -1 1 1 150.97 142.32 2.03 o 0 1 1 63.04 61.98 0.96 o 1 1 1 10235.82 9945.30 93.35 o 2 1 1 28.33 34.37 0.58 o -6 2 1 0.09 -0.34 0.47 o -5 2 1 18.33 18.36 0.50 o -4 2 1 26.24 33.49 0.67 o -3 2 1 230.62 232.67 2.17 o -2 2 1 56.07 61.88 0.69 o -1 2 1 10.99 7.09 0.26 o 0 2 1 184.36 186.08 2.21 o 1 2 1 115.90 94.20 0.95 o 2 2 1 724.06 707.68 6.15 o 3 2 1 0.41 0.86 0.26 o -6 3 1 7.87 6.67 1.33 o -5 3 1 9.49 10.44 0.41 o -4 3 1 15.22 14.66 0.51 o -3 3 1 90.30 81.45 1.11 o -2 3 1 0.00 -0.08 0.08 o -1 3 1 223.80 221.60 2.61 o 0 3 1 1079.96 1132.56 11.16 o 1 3 1 0.06 0.95 0.11 o 2 3 1 536.58 554.18 4.32 o 3 3 1 16.91 16.88 0.50 o -6 4 1 22.65 19.57 0.80 o -5 4 1 28.04 25.65 0.63 o -4 4 1 11.72 15.85 0.45 o -3 4 1 24.01 24.24 0.55 o -2 4 1 32.88 33.21 0.49 o -1 4 1 840.76 858.40 9.62 o 0 4 1 0.00 0.61 0.11 o 1 4 1 576.56 613.35 4.92 o 2 4 1 40.12 43.39 0.54 o 3 4 1 4.34 2.86 0.22 o 4 4 1 174.51 165.17 2.41 o -6 5 1 12.86 13.35 2.01 o -5 5 1 25.28 21.94 0.60 o -4 5 1 382.56 366.04 3.80 o -3 5 1 91.79 97.25 1.34 o -2 5 1 59.81 63.35 1.28 o -1 5 1 7.54 14.25 0.74 o 0 5 1 1214.41 1303.64 11.03 o 1 5 1 1005.03 988.56 6.90 o 2 5 1 180.59 175.73 1.54 o 3 5 1 139.46 128.37 1.65 o 4 5 1 25.71 28.23 1.79 o -5 6 1 1.67 1.71 0.34 o -4 6 1 23.40 22.89 0.41 o -3 6 1 775.36 744.46 10.02 o -2 6 1 32.44 31.24 0.90 o -1 6 1 78.44 86.45 1.79 o 0 6 1 31.75 43.61 0.74 o 1 6 1 351.87 325.12 2.57 o 2 6 1 177.42 166.36 1.65 o 3 6 1 13.55 10.66 0.44 o 4 6 1 218.47 221.74 3.11 o 5 6 1 3.66 5.33 0.54 o -5 7 1 5.00 8.59 1.10 o -4 7 1 110.69 115.64 1.38 o -3 7 1 313.25 331.15 2.66 o -2 7 1 10.66 9.62 0.62 o -1 7 1 31.86 31.90 0.75 o 0 7 1 18.36 17.02 0.54 o 1 7 1 5.60 7.48 0.31 o 2 7 1 0.69 1.26 0.14 o 3 7 1 10.60 8.72 0.39 o 4 7 1 21.13 20.81 0.52 o -4 8 1 0.70 0.65 0.13 o -3 8 1 49.83 56.95 0.55 o -2 8 1 90.40 82.24 0.68 o -1 8 1 4.12 5.55 0.22 o 0 8 1 166.42 139.84 1.47 o 1 8 1 274.37 243.93 1.69 o 2 8 1 102.43 98.35 0.89 o 3 8 1 40.45 38.40 0.65 o 4 8 1 7.70 8.70 0.28 o -4 9 1 49.34 57.17 0.71 o -3 9 1 31.92 30.06 0.43 o -2 9 1 48.31 44.55 0.41 o -1 9 1 18.60 22.80 0.29 o 0 9 1 7.87 7.18 0.26 o 1 9 1 41.06 37.44 0.52 o 2 9 1 0.02 0.17 0.11 o 3 9 1 9.80 11.36 0.33 o -3 10 1 37.19 44.26 0.65 o -2 10 1 0.77 1.24 0.17 o -1 10 1 8.92 8.27 0.23 o 0 10 1 1.75 1.07 0.10 o 1 10 1 0.61 0.29 0.10 o 2 10 1 11.68 10.80 0.34 o -2 11 1 3.56 3.40 0.16 o -1 11 1 8.74 6.52 0.19 o 0 11 1 8.70 6.62 0.32 o 1 11 1 63.84 73.84 1.27 o 0 -12 2 24.01 26.95 0.43 o 1 -12 2 2.93 2.43 0.31 o 2 -12 2 0.78 0.58 0.28 o -2 -11 2 2.41 2.06 0.14 o -1 -11 2 2.99 5.28 0.20 o 0 -11 2 2.62 1.18 0.11 o 1 -11 2 38.64 34.12 0.40 o 2 -11 2 3.08 4.29 0.30 o 3 -11 2 60.49 70.06 1.06 o -3 -10 2 120.46 119.74 1.25 o -2 -10 2 0.09 0.14 0.11 o -1 -10 2 10.03 8.33 0.35 o 0 -10 2 81.26 75.71 0.63 o 1 -10 2 2.39 1.32 0.13 o 2 -10 2 197.03 176.10 1.41 o 3 -10 2 1.63 1.34 0.13 o 4 -10 2 2.38 3.08 0.32 o -4 -9 2 11.32 11.52 0.33 o -3 -9 2 1.36 1.74 0.16 o -2 -9 2 39.75 37.34 0.54 o -1 -9 2 9.92 9.36 0.24 o 0 -9 2 39.65 46.26 0.53 o 1 -9 2 0.03 0.72 0.10 o 2 -9 2 22.89 20.33 0.33 o 3 -9 2 12.72 10.65 0.33 o 4 -9 2 0.85 0.76 0.19 o -4 -8 2 0.76 0.81 0.21 o -3 -8 2 436.57 435.98 3.17 o -2 -8 2 373.37 376.93 2.92 o -1 -8 2 0.05 0.01 0.24 o 0 -8 2 0.01 -0.24 0.24 o 1 -8 2 17.07 19.88 0.39 o 2 -8 2 361.46 309.35 1.99 o 3 -8 2 30.39 28.34 0.64 o 4 -8 2 4.97 6.18 0.60 o 5 -8 2 36.21 41.52 1.15 o -5 -7 2 2.12 2.67 0.25 o -4 -7 2 4.89 5.06 0.33 o -3 -7 2 193.46 187.58 1.73 o -2 -7 2 139.52 130.72 1.45 o -1 -7 2 48.15 42.95 0.89 o 0 -7 2 18.83 18.27 0.95 o 1 -7 2 125.48 104.19 1.72 o 2 -7 2 15.44 11.35 0.85 o 3 -7 2 30.11 34.21 1.19 o 4 -7 2 47.26 49.49 1.06 o 5 -7 2 0.79 2.10 1.19 o -5 -6 2 73.81 73.03 1.33 o -4 -6 2 30.91 29.22 0.61 o -3 -6 2 1.51 1.09 0.18 o -2 -6 2 100.68 96.02 1.09 o -1 -6 2 3.14 4.02 0.41 o 0 -6 2 276.87 287.26 3.09 o 1 -6 2 310.53 370.34 4.52 o 2 -6 2 122.65 145.48 5.48 o 3 -6 2 65.74 63.81 1.11 o 4 -6 2 18.18 18.41 0.64 o 5 -6 2 36.16 33.28 1.09 o -5 -5 2 29.85 26.21 0.66 o -4 -5 2 0.17 0.33 0.16 o -3 -5 2 24.09 26.57 0.55 o -2 -5 2 179.43 175.37 1.64 o -1 -5 2 26.36 24.11 0.43 o 0 -5 2 239.68 243.54 2.54 o 1 -5 2 7.29 9.73 0.40 o 2 -5 2 165.44 182.32 3.05 o 3 -5 2 12.20 11.81 0.47 o 4 -5 2 1.44 0.53 0.14 o 5 -5 2 37.78 40.14 0.97 o -5 -4 2 0.39 0.84 0.22 o -4 -4 2 109.05 91.31 1.05 o -3 -4 2 2.94 0.55 0.13 o -2 -4 2 93.73 74.05 0.91 o 0 -4 2 102.31 102.07 1.20 o 1 -4 2 731.41 836.76 7.73 o 2 -4 2 132.16 157.56 1.58 o 3 -4 2 0.07 0.33 0.15 o 4 -4 2 56.84 53.95 0.80 o 5 -4 2 6.56 5.20 0.51 o 6 -4 2 69.77 60.17 1.41 o -5 -3 2 15.03 18.14 0.76 o -4 -3 2 13.21 19.49 0.52 o -3 -3 2 481.61 479.54 9.91 o -2 -3 2 440.67 499.86 7.61 o -1 -3 2 14.56 13.10 0.41 o 0 -3 2 476.82 463.76 12.61 o 1 -3 2 356.16 321.13 4.00 o 2 -3 2 749.42 786.30 5.86 o 3 -3 2 63.93 62.32 0.83 o 4 -3 2 0.09 0.27 0.17 o 5 -3 2 0.18 0.71 0.27 o 6 -3 2 7.61 5.60 1.75 o -5 -2 2 0.26 0.42 0.25 o -4 -2 2 7.22 5.93 0.38 o -3 -2 2 63.93 55.78 0.84 o -2 -2 2 387.57 398.81 4.33 o -1 -2 2 1.13 3.18 0.25 o 0 -2 2 23.16 25.51 0.81 o 1 -2 2 259.62 292.52 2.99 o 2 -2 2 1439.17 1454.01 10.40 o 3 -2 2 4.63 3.85 0.25 o 4 -2 2 33.39 32.32 0.65 o 5 -2 2 13.65 9.65 0.40 o -5 -1 2 18.25 20.69 1.14 o -4 -1 2 166.57 156.26 2.29 o -3 -1 2 63.64 47.07 0.74 o -2 -1 2 96.89 87.95 1.66 o -1 -1 2 3692.76 3538.55 38.21 o 0 -1 2 75.38 54.62 5.10 o 1 -1 2 34.38 29.30 0.46 o 2 -1 2 245.65 272.65 2.49 o 3 -1 2 16.38 21.12 0.66 o 4 -1 2 97.24 93.28 2.55 o -6 0 2 1.31 0.89 0.56 o -5 0 2 43.11 44.14 1.25 o -4 0 2 93.82 88.42 1.34 o -3 0 2 928.16 889.23 8.09 o -2 0 2 379.14 356.69 6.91 o -1 0 2 733.64 763.88 6.96 o 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