#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/56/2215601.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215601_Fobs loop_ _publ_author_name 'Betz, Richard' 'Kl\"ufers, Peter' _publ_section_title ; Cyclobutane-1,2-dione ; _journal_coeditor_code NC2049 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3981 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.3719 _cell_length_b 6.8819 _cell_length_c 10.8378 _exptl_crystal_F_000 176.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file nc2049Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ln359' _shelx_refln_list_code 4 _shelx_f_calc_maximum 43.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 681.44 637.38 15.65 o 4 0 0 314.33 351.63 30.60 o 6 0 0 24.37 23.33 5.42 o 1 1 0 1055.35 971.65 18.59 o 2 1 0 510.97 503.13 8.88 o 3 1 0 8.01 7.76 0.34 o 4 1 0 2.29 1.47 0.40 o 5 1 0 48.97 50.98 1.25 o 6 1 0 1.32 1.30 0.31 o 0 2 0 551.73 521.32 8.84 o 1 2 0 478.99 460.40 6.55 o 2 2 0 1.65 1.49 0.17 o 3 2 0 147.33 151.26 2.58 o 4 2 0 60.89 58.78 1.28 o 5 2 0 0.19 0.32 0.48 o 6 2 0 9.84 10.09 1.03 o 1 3 0 23.73 24.57 0.47 o 2 3 0 90.37 83.02 1.40 o 3 3 0 113.39 128.71 3.01 o 4 3 0 151.55 144.24 3.43 o 5 3 0 11.18 13.11 0.76 o 6 3 0 2.14 3.07 1.18 o 0 4 0 18.98 18.28 0.85 o 1 4 0 330.01 322.30 3.78 o 2 4 0 18.98 18.34 0.46 o 3 4 0 3.92 3.78 0.27 o 4 4 0 0.37 0.50 0.44 o 5 4 0 9.45 10.13 0.68 o 6 4 0 0.98 -0.17 0.83 o 1 5 0 2.51 2.54 0.28 o 2 5 0 0.25 0.21 0.14 o 3 5 0 0.63 0.55 0.23 o 4 5 0 0.16 0.21 0.29 o 5 5 0 2.74 3.24 1.15 o 0 6 0 77.60 77.63 1.92 o 1 6 0 3.60 3.52 0.39 o 2 6 0 39.40 40.85 0.90 o 3 6 0 10.27 12.75 0.42 o 4 6 0 1.71 1.99 0.48 o 5 6 0 2.96 4.74 0.99 o 1 7 0 0.11 0.09 0.16 o 2 7 0 12.33 10.99 0.93 o 3 7 0 0.37 1.26 0.69 o 4 7 0 10.26 6.08 1.17 o 0 8 0 84.51 93.99 7.01 o 1 8 0 1.71 1.74 0.74 o 2 8 0 0.36 -0.05 0.66 o 3 8 0 4.09 5.54 1.17 o 1 0 1 199.21 201.70 7.42 o 2 0 1 326.27 352.18 9.89 o 3 0 1 1.19 0.83 0.33 o 4 0 1 5.51 6.11 0.43 o 5 0 1 1.88 1.17 0.32 o 6 0 1 2.05 0.74 0.49 o 0 1 1 526.62 495.69 5.91 o 1 1 1 801.47 751.74 11.86 o 2 1 1 149.14 154.61 1.90 o 3 1 1 242.21 240.13 2.70 o 4 1 1 22.56 22.73 0.42 o 5 1 1 51.95 51.00 0.84 o 6 1 1 7.56 7.83 0.63 o 0 2 1 142.11 136.65 1.97 o 1 2 1 1033.35 1017.52 9.77 o 2 2 1 167.11 168.15 2.02 o 3 2 1 13.30 13.81 0.41 o 4 2 1 18.04 16.64 0.55 o 5 2 1 6.69 6.68 0.38 o 6 2 1 0.56 0.03 0.36 o 0 3 1 514.16 509.76 6.00 o 1 3 1 10.09 10.24 0.17 o 2 3 1 233.61 241.67 2.38 o 3 3 1 28.34 29.51 0.52 o 4 3 1 50.17 46.78 0.83 o 5 3 1 3.57 1.76 0.31 o 6 3 1 53.82 65.96 2.24 o 0 4 1 55.86 57.17 0.89 o 1 4 1 58.88 51.84 0.64 o 2 4 1 91.59 92.79 1.05 o 3 4 1 31.27 29.29 0.50 o 4 4 1 6.60 5.00 0.28 o 5 4 1 4.83 5.88 0.48 o 6 4 1 29.93 35.55 1.54 o 0 5 1 14.72 13.89 0.73 o 1 5 1 49.93 51.74 0.63 o 2 5 1 63.82 67.71 0.78 o 3 5 1 53.44 52.69 1.06 o 4 5 1 20.83 22.26 0.57 o 5 5 1 28.80 33.19 1.01 o 0 6 1 7.56 7.45 0.29 o 1 6 1 2.05 1.91 0.16 o 2 6 1 15.80 13.96 0.35 o 3 6 1 24.90 22.91 0.39 o 4 6 1 2.45 2.63 0.39 o 5 6 1 3.64 3.96 0.89 o 0 7 1 0.01 -0.17 0.20 o 1 7 1 17.16 16.45 0.43 o 2 7 1 20.47 20.93 0.53 o 3 7 1 7.83 7.07 0.62 o 4 7 1 0.25 -0.17 0.83 o 0 8 1 30.74 32.59 1.65 o 1 8 1 1.62 1.96 0.61 o 2 8 1 1.25 1.64 0.48 o 3 8 1 2.00 1.02 0.84 o 0 0 2 2.16 2.51 0.14 o 1 0 2 1492.92 1370.84 17.98 o 2 0 2 12.19 12.15 0.41 o 3 0 2 154.07 160.20 3.04 o 4 0 2 5.83 6.09 0.42 o 5 0 2 11.23 11.82 0.66 o 6 0 2 2.86 3.05 0.64 o 0 1 2 1778.59 1663.22 21.41 o 1 1 2 52.31 50.59 0.97 o 2 1 2 324.53 314.31 3.54 o 3 1 2 122.94 121.83 1.51 o 4 1 2 112.34 115.70 2.43 o 5 1 2 9.21 7.22 0.32 o 6 1 2 3.69 3.16 0.63 o 0 2 2 1882.72 1954.50 64.91 o 1 2 2 1074.69 1099.76 17.66 o 2 2 2 283.70 281.58 2.84 o 3 2 2 70.63 72.24 1.26 o 4 2 2 22.34 20.95 0.56 o 5 2 2 46.23 48.97 1.16 o 6 2 2 0.63 -0.07 0.43 o 0 3 2 2.32 1.84 0.11 o 1 3 2 12.04 13.50 0.33 o 2 3 2 91.76 96.93 1.03 o 3 3 2 47.12 49.06 0.73 o 4 3 2 1.62 1.23 0.18 o 5 3 2 22.41 22.13 0.79 o 6 3 2 4.81 6.40 0.76 o 0 4 2 92.31 87.14 1.17 o 1 4 2 201.96 216.18 2.59 o 2 4 2 63.99 67.81 0.75 o 3 4 2 58.64 57.70 1.11 o 4 4 2 0.59 1.19 0.20 o 5 4 2 12.64 13.24 0.53 o 6 4 2 10.02 10.03 0.90 o 0 5 2 0.04 0.16 0.09 o 1 5 2 8.84 9.22 0.26 o 2 5 2 39.30 41.85 0.70 o 3 5 2 33.37 29.15 0.55 o 4 5 2 17.15 15.37 0.53 o 5 5 2 9.70 9.01 0.81 o 0 6 2 65.37 68.09 1.42 o 1 6 2 98.95 104.51 1.37 o 2 6 2 1.49 1.06 0.19 o 3 6 2 8.30 8.05 0.35 o 4 6 2 12.41 13.18 0.74 o 5 6 2 7.68 7.30 1.01 o 0 7 2 7.99 7.18 0.36 o 1 7 2 10.09 9.63 0.31 o 2 7 2 10.90 9.82 0.37 o 3 7 2 7.25 5.72 0.47 o 4 7 2 5.99 4.41 0.88 o 0 8 2 8.75 8.97 1.48 o 1 8 2 23.80 25.48 1.41 o 2 8 2 1.23 1.20 0.53 o 1 0 3 276.71 273.36 3.08 o 2 0 3 221.20 215.72 6.13 o 3 0 3 12.67 14.40 0.80 o 4 0 3 8.36 6.98 0.27 o 5 0 3 26.49 25.35 1.30 o 6 0 3 4.20 3.87 2.01 o 0 1 3 81.07 76.45 0.95 o 1 1 3 818.50 825.17 7.68 o 2 1 3 97.25 102.76 1.13 o 3 1 3 58.85 54.76 0.94 o 4 1 3 137.55 131.72 1.67 o 5 1 3 84.87 85.63 1.32 o 6 1 3 14.24 15.27 0.92 o 0 2 3 4.10 4.50 0.23 o 1 2 3 735.05 749.37 6.61 o 2 2 3 74.43 77.88 1.46 o 3 2 3 101.44 98.12 1.14 o 4 2 3 0.16 0.25 0.14 o 5 2 3 26.90 27.20 0.64 o 6 2 3 14.04 14.70 1.04 o 0 3 3 44.46 54.43 1.20 o 1 3 3 57.97 62.20 1.21 o 2 3 3 36.68 40.12 0.57 o 3 3 3 155.18 174.87 2.89 o 4 3 3 0.06 0.05 0.25 o 5 3 3 34.35 35.66 1.36 o 6 3 3 6.37 6.61 1.88 o 0 4 3 68.23 68.05 0.99 o 1 4 3 44.14 45.73 0.62 o 2 4 3 53.42 54.32 1.15 o 3 4 3 55.66 53.58 0.73 o 4 4 3 1.27 1.21 0.19 o 5 4 3 11.48 11.73 0.60 o 6 4 3 2.23 1.13 0.67 o 0 5 3 23.42 25.59 0.76 o 1 5 3 41.92 40.49 0.60 o 2 5 3 0.67 0.44 0.15 o 3 5 3 2.82 2.28 0.15 o 4 5 3 1.68 1.39 0.28 o 5 5 3 3.23 2.91 0.45 o 0 6 3 3.85 4.44 0.21 o 1 6 3 5.84 5.43 0.21 o 2 6 3 22.23 21.16 0.46 o 4 6 3 5.37 4.81 0.69 o 0 7 3 46.84 49.31 1.68 o 1 7 3 35.96 37.94 0.70 o 2 7 3 16.27 15.36 0.73 o 3 7 3 0.76 0.46 0.32 o 4 7 3 25.79 25.15 2.10 o 0 8 3 16.93 18.68 2.78 o 1 8 3 6.78 6.24 0.85 o 2 8 3 0.47 -0.55 0.55 o 0 0 4 1797.47 1772.84 103.95 o 1 0 4 24.74 24.87 0.42 o 2 0 4 398.97 384.29 4.96 o 3 0 4 7.99 7.70 0.32 o 4 0 4 5.18 3.37 0.32 o 5 0 4 1.80 1.15 0.47 o 6 0 4 23.22 21.52 1.94 o 0 1 4 0.03 0.02 0.09 o 1 1 4 66.59 67.20 0.70 o 2 1 4 31.61 31.41 0.41 o 3 1 4 76.09 83.79 1.18 o 4 1 4 12.05 11.33 0.40 o 5 1 4 12.26 12.35 0.48 o 6 1 4 4.26 4.30 0.53 o 0 2 4 7.96 9.72 0.27 o 1 2 4 145.03 147.67 1.29 o 2 2 4 105.25 107.12 1.60 o 3 2 4 2.78 2.50 0.15 o 4 2 4 40.97 38.96 0.86 o 5 2 4 11.30 10.40 0.56 o 6 2 4 0.07 0.27 0.61 o 0 3 4 76.65 83.80 1.33 o 1 3 4 153.32 159.71 2.41 o 2 3 4 186.25 192.60 1.88 o 3 3 4 40.19 41.66 0.55 o 4 3 4 59.57 61.97 1.33 o 5 3 4 8.76 7.43 0.51 o 6 3 4 14.72 16.28 1.06 o 0 4 4 20.79 24.93 0.49 o 1 4 4 193.01 192.64 2.31 o 2 4 4 356.81 367.13 4.93 o 3 4 4 4.45 4.79 0.17 o 4 4 4 0.61 0.72 0.18 o 5 4 4 14.41 14.52 0.75 o 0 5 4 5.21 3.52 0.22 o 1 5 4 122.50 126.83 1.62 o 2 5 4 3.37 2.82 0.24 o 3 5 4 73.22 75.02 1.53 o 4 5 4 3.95 3.69 0.34 o 5 5 4 5.27 5.02 0.61 o 0 6 4 39.19 39.33 1.00 o 1 6 4 45.45 46.32 0.72 o 2 6 4 84.33 89.44 1.23 o 3 6 4 8.19 8.06 0.40 o 4 6 4 1.91 2.50 0.57 o 0 7 4 24.38 23.74 1.74 o 1 7 4 8.45 8.28 0.38 o 2 7 4 2.28 2.27 0.28 o 3 7 4 11.50 10.43 0.62 o 0 8 4 0.99 1.73 0.70 o 1 8 4 2.58 1.93 0.55 o 2 8 4 0.31 1.09 0.67 o 1 0 5 168.13 168.07 2.04 o 2 0 5 83.67 97.56 1.43 o 3 0 5 91.79 86.09 2.16 o 4 0 5 167.91 170.09 2.97 o 5 0 5 49.67 50.85 2.09 o 6 0 5 1.36 1.73 0.71 o 0 1 5 434.43 430.83 7.04 o 1 1 5 18.28 17.01 0.25 o 2 1 5 7.31 7.54 0.20 o 3 1 5 110.37 107.67 1.24 o 4 1 5 90.39 90.56 1.24 o 5 1 5 35.57 35.87 0.84 o 6 1 5 1.28 0.26 0.71 o 0 2 5 235.85 241.53 4.72 o 1 2 5 79.08 80.30 0.87 o 2 2 5 119.50 117.07 1.17 o 3 2 5 29.34 33.47 0.58 o 4 2 5 23.69 24.61 0.51 o 5 2 5 28.40 28.86 1.06 o 6 2 5 4.28 4.01 0.63 o 0 3 5 259.13 265.11 3.14 o 1 3 5 30.92 30.20 0.39 o 2 3 5 70.49 73.23 1.31 o 3 3 5 24.09 22.91 0.47 o 4 3 5 33.46 32.60 0.63 o 5 3 5 2.01 1.91 0.46 o 6 3 5 4.68 3.90 0.70 o 0 4 5 13.05 12.62 0.33 o 1 4 5 44.94 44.57 0.62 o 2 4 5 14.44 12.34 0.30 o 3 4 5 3.19 3.08 0.19 o 4 4 5 3.86 3.61 0.26 o 5 4 5 0.92 1.42 0.36 o 0 5 5 9.64 12.90 0.35 o 1 5 5 11.81 10.50 0.29 o 2 5 5 37.99 37.38 0.63 o 3 5 5 23.81 23.03 0.53 o 4 5 5 11.05 10.29 0.61 o 5 5 5 5.76 5.93 0.70 o 0 6 5 34.88 36.34 1.26 o 1 6 5 14.49 13.54 0.41 o 2 6 5 39.59 39.95 0.76 o 3 6 5 1.81 1.65 0.30 o 4 6 5 3.25 3.31 0.57 o 0 7 5 18.39 19.00 0.98 o 1 7 5 8.00 8.56 0.55 o 2 7 5 1.77 1.51 0.33 o 3 7 5 0.73 0.48 0.48 o 0 8 5 0.45 -0.28 0.87 o 1 8 5 8.94 8.67 0.80 o 0 0 6 2.66 2.87 0.28 o 1 0 6 300.42 306.77 3.99 o 2 0 6 0.01 -0.08 0.15 o 3 0 6 106.23 106.57 3.31 o 4 0 6 6.11 6.31 0.41 o 5 0 6 0.18 0.79 0.45 o 6 0 6 0.98 0.06 0.76 o 0 1 6 171.57 178.20 2.49 o 1 1 6 34.74 33.75 0.42 o 2 1 6 111.99 115.45 1.66 o 3 1 6 23.80 22.36 0.41 o 4 1 6 97.58 96.61 1.24 o 5 1 6 3.26 2.88 0.32 o 6 1 6 1.28 1.67 0.62 o 0 2 6 111.18 104.87 1.36 o 1 2 6 77.47 79.54 1.07 o 2 2 6 164.19 165.69 3.15 o 3 2 6 44.00 41.75 0.58 o 4 2 6 1.57 1.43 0.22 o 5 2 6 0.13 0.01 0.26 o 6 2 6 17.91 17.67 1.04 o 1 3 6 43.53 46.52 0.80 o 2 3 6 93.38 95.96 1.03 o 3 3 6 15.50 16.03 0.58 o 4 3 6 2.94 2.46 0.26 o 5 3 6 4.12 3.41 0.51 o 0 4 6 84.83 89.81 1.65 o 1 4 6 62.44 61.01 0.73 o 2 4 6 16.19 16.20 0.36 o 3 4 6 30.78 31.23 0.66 o 4 4 6 6.12 5.34 0.49 o 5 4 6 0.91 0.66 0.51 o 0 5 6 0.01 -0.13 0.13 o 1 5 6 31.13 29.08 0.91 o 2 5 6 152.15 152.92 2.12 o 3 5 6 35.57 33.76 0.92 o 4 5 6 3.42 3.91 0.77 o 0 6 6 12.99 18.14 0.84 o 1 6 6 1.22 1.17 0.26 o 2 6 6 4.91 5.38 0.35 o 3 6 6 15.98 18.35 1.01 o 4 6 6 2.00 0.25 1.03 o 0 7 6 2.85 0.32 0.52 o 1 7 6 10.21 9.64 0.71 o 2 7 6 0.18 0.01 0.39 o 3 7 6 3.47 0.86 0.82 o 0 8 6 0.00 0.62 1.13 o 1 0 7 151.43 153.26 2.01 o 2 0 7 32.22 34.64 0.84 o 3 0 7 27.41 28.81 1.00 o 4 0 7 65.38 71.70 1.52 o 5 0 7 10.99 9.15 1.01 o 6 0 7 0.19 0.12 0.85 o 0 1 7 3.77 4.24 0.23 o 1 1 7 46.81 48.36 0.56 o 2 1 7 14.77 13.10 0.28 o 3 1 7 8.50 7.66 0.28 o 4 1 7 3.96 3.22 0.29 o 5 1 7 9.92 8.79 0.66 o 6 1 7 0.59 -0.03 1.05 o 0 2 7 108.75 105.35 1.44 o 1 2 7 11.90 12.58 0.27 o 2 2 7 3.57 3.52 0.26 o 3 2 7 73.21 72.26 1.32 o 4 2 7 35.34 36.28 1.07 o 5 2 7 4.31 3.30 0.44 o 0 3 7 18.29 18.89 0.45 o 1 3 7 38.39 37.68 0.49 o 2 3 7 63.13 55.27 0.71 o 3 3 7 113.62 117.66 1.50 o 4 3 7 1.91 1.72 0.28 o 5 3 7 13.81 14.17 0.81 o 0 4 7 22.39 21.22 0.67 o 1 4 7 27.67 24.65 0.63 o 2 4 7 12.58 11.17 0.28 o 3 4 7 56.78 58.14 1.10 o 4 4 7 0.59 0.46 0.28 o 5 4 7 12.89 12.90 1.54 o 0 5 7 5.58 5.62 0.28 o 1 5 7 1.71 1.88 0.21 o 2 5 7 5.89 5.90 0.35 o 3 5 7 14.33 15.39 0.59 o 4 5 7 0.09 -0.19 0.44 o 0 6 7 22.42 20.89 1.07 o 1 6 7 12.99 13.01 0.51 o 2 6 7 11.28 10.02 0.50 o 3 6 7 5.48 5.13 0.49 o 0 7 7 2.19 5.64 1.00 o 1 7 7 7.78 7.06 0.58 o 2 7 7 2.35 2.71 0.57 o 0 0 8 58.59 61.47 1.39 o 1 0 8 10.63 11.02 0.37 o 2 0 8 68.47 78.55 1.29 o 3 0 8 17.11 15.20 0.58 o 4 0 8 36.13 35.12 1.18 o 5 0 8 0.93 1.14 0.68 o 0 1 8 1.84 1.79 0.20 o 1 1 8 223.13 234.35 2.02 o 2 1 8 14.04 12.26 0.35 o 3 1 8 125.12 124.69 2.46 o 4 1 8 18.68 20.11 0.57 o 5 1 8 0.85 1.62 0.44 o 0 2 8 119.09 120.12 1.94 o 1 2 8 3.54 2.75 0.17 o 2 2 8 23.86 23.06 0.44 o 3 2 8 33.06 32.94 0.58 o 4 2 8 12.95 11.62 0.47 o 5 2 8 7.98 7.62 0.74 o 0 3 8 3.56 3.46 0.31 o 1 3 8 6.64 6.18 0.20 o 2 3 8 88.32 88.13 1.11 o 3 3 8 1.49 1.17 0.22 o 4 3 8 7.74 6.80 0.39 o 5 3 8 1.31 1.03 0.64 o 0 4 8 4.43 5.95 0.31 o 1 4 8 26.26 24.41 0.45 o 2 4 8 0.99 1.02 0.17 o 3 4 8 0.52 0.28 0.19 o 4 4 8 2.65 2.31 0.48 o 0 5 8 8.20 7.13 0.35 o 1 5 8 0.99 0.57 0.20 o 2 5 8 1.60 0.97 0.24 o 3 5 8 0.93 0.13 0.34 o 4 5 8 0.18 -0.83 0.83 o 0 6 8 4.75 4.69 0.68 o 1 6 8 5.57 5.21 0.46 o 2 6 8 0.25 0.21 0.39 o 3 6 8 3.32 4.35 0.61 o 0 7 8 1.01 1.22 0.96 o 1 7 8 9.80 9.95 1.26 o 1 0 9 10.52 10.37 0.42 o 2 0 9 30.41 30.41 0.75 o 3 0 9 2.32 3.57 0.48 o 4 0 9 16.31 13.97 0.90 o 5 0 9 2.40 3.18 1.43 o 0 1 9 0.42 0.15 0.23 o 1 1 9 4.26 3.65 0.21 o 2 1 9 15.08 14.57 0.35 o 3 1 9 11.62 11.22 0.41 o 4 1 9 9.62 10.06 0.62 o 5 1 9 8.99 8.48 0.71 o 0 2 9 84.94 89.30 1.33 o 1 2 9 24.65 23.93 0.42 o 2 2 9 6.33 5.21 0.25 o 3 2 9 57.48 61.73 1.16 o 4 2 9 20.98 21.99 0.75 o 5 2 9 2.28 1.96 0.79 o 0 3 9 0.74 1.92 0.27 o 1 3 9 8.25 6.65 0.25 o 2 3 9 40.90 42.13 1.00 o 3 3 9 12.49 15.55 0.54 o 4 3 9 0.02 0.01 0.35 o 0 4 9 0.16 0.13 0.22 o 1 4 9 19.51 17.49 0.43 o 2 4 9 13.84 12.21 0.36 o 3 4 9 25.26 24.20 1.59 o 4 4 9 0.13 -0.21 0.62 o 0 5 9 0.37 -0.29 0.42 o 1 5 9 7.89 7.35 0.43 o 2 5 9 16.16 16.84 0.66 o 3 5 9 0.04 0.46 0.64 o 0 6 9 10.77 13.10 1.34 o 1 6 9 1.54 1.21 0.53 o 2 6 9 6.82 5.63 0.90 o 0 0 10 4.46 6.04 0.55 o 1 0 10 47.22 45.08 0.91 o 2 0 10 1.63 1.71 0.41 o 3 0 10 2.78 2.63 0.49 o 4 0 10 0.22 0.90 0.54 o 0 1 10 163.54 166.19 2.31 o 1 1 10 14.21 13.07 0.34 o 2 1 10 24.89 23.96 0.51 o 3 1 10 20.49 20.50 0.59 o 4 1 10 33.90 33.55 1.13 o 0 2 10 3.88 3.27 0.35 o 1 2 10 2.16 1.40 0.21 o 2 2 10 19.13 18.49 0.56 o 3 2 10 2.00 1.51 0.54 o 4 2 10 10.59 12.09 0.82 o 0 3 10 0.19 -0.10 0.37 o 1 3 10 19.39 18.93 0.87 o 2 3 10 26.28 27.12 0.72 o 3 3 10 2.23 1.92 0.35 o 4 3 10 1.63 0.99 0.48 o 0 4 10 17.36 17.43 0.69 o 1 4 10 21.52 20.29 1.03 o 2 4 10 5.76 5.36 0.40 o 3 4 10 7.88 7.27 0.73 o 0 5 10 0.07 -0.34 0.42 o 1 5 10 5.82 5.03 0.77 o 2 5 10 38.74 41.11 2.31 o 0 6 10 2.97 1.64 0.86 o 1 6 10 1.52 1.44 0.79 o 1 0 11 41.95 47.26 1.41 o 2 0 11 9.05 8.52 0.59 o 3 0 11 7.33 7.09 0.87 o 4 0 11 39.70 42.13 3.43 o 0 1 11 16.18 17.78 0.65 o 1 1 11 0.60 0.61 0.24 o 2 1 11 3.91 3.51 0.31 o 3 1 11 5.35 4.77 0.48 o 4 1 11 5.98 6.57 1.03 o 0 2 11 0.30 0.21 0.33 o 1 2 11 3.29 2.50 0.25 o 2 2 11 28.48 30.46 0.83 o 3 2 11 1.38 1.41 0.39 o 4 2 11 3.98 3.02 0.57 o 0 3 11 8.81 7.85 0.79 o 1 3 11 21.64 22.94 0.81 o 2 3 11 0.98 0.54 0.38 o 3 3 11 5.62 4.75 0.66 o 0 4 11 7.93 6.76 0.55 o 1 4 11 4.03 4.12 0.47 o 2 4 11 8.53 9.31 0.64 o 3 4 11 2.94 2.61 0.65 o 0 5 11 0.00 -1.10 1.10 o 1 5 11 1.05 2.61 0.78 o 0 0 12 29.62 32.57 2.42 o 1 0 12 1.22 1.08 0.44 o 2 0 12 2.78 2.42 0.64 o 3 0 12 2.00 1.25 0.78 o 0 1 12 7.84 7.21 0.79 o 1 1 12 4.82 4.10 0.53 o 2 1 12 2.13 0.62 0.38 o 3 1 12 5.00 5.76 0.64 o 0 2 12 2.99 3.24 0.45 o 1 2 12 4.34 3.33 0.36 o 2 2 12 1.03 1.01 0.45 o 3 2 12 1.97 1.93 0.80 o 0 3 12 15.60 17.47 1.66 o 1 3 12 30.80 33.62 1.51 o 2 3 12 6.65 5.74 0.55 o 0 4 12 0.01 -0.55 0.55 o 1 4 12 1.52 0.97 0.62 o 1 0 13 2.32 2.57 0.73 o 2 0 13 2.51 2.88 0.88 o 0 1 13 1.76 1.74 0.63 o 1 1 13 6.49 6.02 0.57 o 2 1 13 1.83 2.97 0.61 o 0 2 13 0.65 1.12 0.65 o 1 2 13 25.40 27.30 0.93 o 2 2 13 6.52 6.64 0.75 o 0 3 13 0.58 0.23 0.62 o 1 3 13 2.66 3.13 0.65 o 0 0 14 2.24 6.23 2.12 o