#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/56/2215605.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215605_Fobs loop_ _publ_author_name 'Xie, Ming-Jin' 'Yu, Yao' 'Liu, Wei-Ping' 'Hou, Shu-Qian' 'Chen, Xi-Zhu' _publ_section_title ; cis-(Malonato-\k^2^O,O')bis(2-methylpyridine-\kN)platinum(II) ; _journal_coeditor_code NC2058 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2627 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.748 _cell_angle_gamma 90.000 _cell_length_a 8.5790 _cell_length_b 15.8079 _cell_length_c 11.5595 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.7505 _[local]_cod_data_source_file nc2058Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070629C in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 345.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1603.39 1817.03 80.24 o 4 0 0 53172.90 52641.56 671.94 o 6 0 0 4474.24 4606.03 112.84 o 8 0 0 5701.28 5879.33 202.58 o 10 0 0 1992.07 2260.34 190.66 o 1 1 0 37068.84 36174.50 517.61 o 2 1 0 7729.13 8289.79 86.85 o 3 1 0 40168.86 39760.96 358.41 o 4 1 0 81.85 78.27 13.30 o 5 1 0 7441.01 7401.97 100.14 o 6 1 0 4399.90 4488.86 85.39 o 7 1 0 14988.62 14779.29 236.17 o 8 1 0 211.73 216.47 40.98 o 9 1 0 67.03 19.73 61.77 o 10 1 0 358.08 356.21 99.44 o 0 2 0 70770.58 59994.40 1709.84 o 1 2 0 14643.29 15214.07 141.00 o 2 2 0 8151.74 8639.51 100.67 o 3 2 0 4011.73 4053.18 57.13 o 4 2 0 24271.87 24275.68 320.36 o 5 2 0 18357.47 18332.75 215.47 o 6 2 0 5554.62 5527.44 102.81 o 7 2 0 1671.67 1632.94 59.56 o 8 2 0 6318.64 6069.27 175.89 o 9 2 0 3573.85 3520.33 135.23 o 10 2 0 1148.13 1123.71 107.14 o 1 3 0 518.73 516.59 15.65 o 2 3 0 26658.25 26635.03 246.23 o 3 3 0 12704.74 13267.84 141.21 o 4 3 0 12695.64 13376.81 162.20 o 5 3 0 734.53 745.55 35.51 o 6 3 0 18323.61 18250.31 233.60 o 7 3 0 4073.71 4129.18 107.01 o 8 3 0 2961.69 2952.09 100.84 o 9 3 0 115.14 103.84 40.11 o 10 3 0 2110.55 2197.12 205.21 o 0 4 0 1654.55 1750.72 40.25 o 1 4 0 35763.24 35066.01 423.04 o 2 4 0 3956.58 4222.13 97.91 o 3 4 0 17606.92 17653.85 281.18 o 4 4 0 2357.21 2332.42 48.03 o 5 4 0 23058.38 22461.91 298.75 o 6 4 0 482.09 490.54 35.45 o 7 4 0 1375.23 1462.82 59.12 o 8 4 0 89.58 44.05 32.06 o 9 4 0 7488.49 7246.24 260.84 o 10 4 0 47.73 1.44 65.55 o 1 5 0 624.84 709.87 28.34 o 2 5 0 46837.02 45663.30 472.58 o 3 5 0 326.74 363.17 37.10 o 4 5 0 450.56 490.17 24.08 o 5 5 0 341.38 390.70 31.25 o 6 5 0 14099.38 14130.09 198.16 o 7 5 0 1231.73 1162.86 54.31 o 8 5 0 3325.85 3178.33 104.24 o 9 5 0 15.00 2.01 41.84 o 10 5 0 2167.80 2533.32 215.77 o 0 6 0 23085.30 23253.52 520.79 o 1 6 0 20188.16 20508.44 200.34 o 2 6 0 242.08 260.20 17.88 o 3 6 0 15485.92 16354.91 190.03 o 4 6 0 6123.04 6174.05 86.63 o 5 6 0 10324.34 10034.65 150.67 o 6 6 0 730.03 741.90 42.72 o 7 6 0 572.08 629.82 51.07 o 8 6 0 967.29 1078.24 67.27 o 9 6 0 4917.60 4927.58 218.01 o 10 6 0 519.45 770.30 142.55 o 1 7 0 16607.42 16951.59 174.19 o 2 7 0 14243.82 14162.66 153.60 o 3 7 0 12958.95 13190.47 266.53 o 4 7 0 1559.44 1560.03 117.33 o 5 7 0 2641.69 2695.94 70.80 o 6 7 0 4601.83 4601.30 136.31 o 7 7 0 6257.24 6373.12 148.90 o 8 7 0 1253.31 1220.29 86.13 o 9 7 0 3.50 -12.96 36.88 o 0 8 0 7875.27 7213.29 130.57 o 1 8 0 1788.75 1882.52 39.95 o 2 8 0 2648.54 2697.53 50.48 o 3 8 0 667.50 677.34 29.93 o 4 8 0 19469.13 19124.79 335.78 o 5 8 0 1409.98 1454.11 63.24 o 6 8 0 2316.21 2399.94 133.41 o 7 8 0 4.65 6.76 27.68 o 8 8 0 5180.74 5349.44 168.55 o 9 8 0 726.96 852.22 82.30 o 1 9 0 11422.33 11305.36 133.36 o 2 9 0 11.42 37.27 15.50 o 3 9 0 19927.00 19349.37 329.45 o 4 9 0 128.75 107.31 24.84 o 5 9 0 1694.67 1726.94 71.34 o 6 9 0 13.37 0.22 23.56 o 7 9 0 11416.50 11099.14 218.73 o 8 9 0 3.89 40.02 37.91 o 9 9 0 89.96 181.02 54.96 o 0 10 0 24482.07 23383.44 342.82 o 1 10 0 3002.05 2986.44 89.68 o 2 10 0 367.19 376.46 27.12 o 3 10 0 608.38 585.17 43.04 o 4 10 0 16904.78 16627.40 260.16 o 5 10 0 2078.13 2035.67 79.58 o 6 10 0 2344.46 2252.14 89.07 o 7 10 0 30.08 45.15 32.44 o 8 10 0 4392.18 4255.38 156.27 o 9 10 0 522.94 527.92 76.48 o 1 11 0 9079.38 9324.97 140.86 o 2 11 0 13299.69 13407.37 184.13 o 3 11 0 12677.24 12314.51 209.71 o 4 11 0 68.15 19.24 22.25 o 5 11 0 902.30 958.37 64.96 o 6 11 0 3614.60 3452.29 123.77 o 7 11 0 4383.87 4490.07 154.82 o 8 11 0 684.64 683.05 107.49 o 9 11 0 26.27 92.26 59.28 o 0 12 0 5789.55 6101.35 208.16 o 1 12 0 10396.45 10985.32 162.75 o 2 12 0 179.24 168.68 36.83 o 3 12 0 3832.63 3885.09 126.82 o 4 12 0 4027.72 3920.08 113.25 o 5 12 0 9031.25 9053.41 190.66 o 6 12 0 127.90 128.05 36.75 o 7 12 0 258.45 259.70 54.99 o 8 12 0 1306.83 1507.30 106.29 o 1 13 0 222.86 195.68 26.56 o 2 13 0 18759.83 18807.28 291.41 o 3 13 0 899.58 816.58 55.91 o 4 13 0 905.08 885.35 61.38 o 5 13 0 254.43 262.91 43.15 o 6 13 0 8426.39 8385.25 193.92 o 7 13 0 77.37 43.73 42.92 o 8 13 0 1306.74 1291.55 103.92 o 0 14 0 357.05 461.11 62.42 o 1 14 0 10196.83 10584.59 198.08 o 2 14 0 132.96 95.60 30.17 o 3 14 0 2948.77 2796.70 96.81 o 4 14 0 365.45 466.40 57.54 o 5 14 0 9639.88 9377.90 204.67 o 6 14 0 91.28 45.34 36.15 o 7 14 0 325.11 400.93 68.29 o 1 15 0 2074.29 2044.31 107.64 o 2 15 0 9081.50 9199.01 236.26 o 3 15 0 1974.41 2121.32 112.50 o 4 15 0 236.19 237.10 43.66 o 5 15 0 435.63 466.46 59.96 o 6 15 0 4147.29 4154.08 156.29 o 7 15 0 986.40 973.64 118.19 o 0 16 0 8935.33 9101.72 375.20 o 1 16 0 2744.67 2918.44 140.87 o 2 16 0 119.27 156.95 45.06 o 3 16 0 1667.00 1793.55 107.77 o 4 16 0 4857.97 4755.47 176.31 o 5 16 0 1864.99 1912.13 98.38 o 6 16 0 588.25 577.90 75.19 o 7 16 0 96.95 20.33 91.88 o 1 17 0 3716.57 3939.36 155.30 o 2 17 0 666.60 557.19 73.03 o 3 17 0 5841.77 5910.28 198.65 o 4 17 0 101.18 93.25 48.95 o 5 17 0 679.81 590.35 81.00 o 6 17 0 385.80 260.32 103.11 o 0 18 0 4974.65 4654.33 357.76 o 1 18 0 0.07 -27.53 50.84 o 2 18 0 374.51 356.72 80.49 o 3 18 0 8.91 49.98 45.20 o 4 18 0 4457.27 4519.67 182.46 o 5 18 0 10.00 167.33 125.44 o 1 19 0 1863.50 1910.60 182.17 o 2 19 0 497.70 548.52 78.27 o 3 19 0 2688.64 2713.34 202.02 o 4 19 0 150.03 235.33 73.20 o 0 20 0 2920.01 3195.29 330.76 o 1 20 0 1104.57 1410.32 214.66 o 2 20 0 59.83 134.32 64.27 o 3 20 0 460.89 464.34 92.55 o -11 0 1 966.78 740.63 133.44 o -9 0 1 8815.12 8893.99 297.65 o -7 0 1 1449.46 1433.38 129.99 o -5 0 1 50757.62 49345.09 640.55 o -3 0 1 336.84 367.68 29.89 o -1 0 1 83379.83 65332.61 917.11 o 1 0 1 21542.17 21100.54 272.02 o 3 0 1 35203.79 34119.39 446.80 o 5 0 1 10065.29 10307.24 184.87 o 7 0 1 6280.26 6196.97 150.57 o 9 0 1 6894.78 7314.54 349.21 o -11 1 1 339.36 266.65 94.88 o -10 1 1 980.90 1041.77 98.40 o -9 1 1 549.87 522.91 53.81 o -8 1 1 8471.59 8365.65 173.39 o -7 1 1 1443.38 1404.49 62.04 o -6 1 1 13921.43 13651.85 197.24 o -5 1 1 104.71 79.04 14.72 o -4 1 1 25558.00 25705.37 245.93 o -3 1 1 34669.66 35576.18 360.30 o -2 1 1 70297.53 66106.40 682.53 o -1 1 1 789.78 871.30 39.23 o 0 1 1 23219.11 23604.29 237.19 o 1 1 1 19035.30 19587.24 217.93 o 2 1 1 42729.84 41633.72 371.60 o 3 1 1 466.31 506.40 20.22 o 4 1 1 3460.76 3680.88 77.80 o 5 1 1 2956.86 3012.63 61.99 o 6 1 1 24620.55 24160.26 261.26 o 7 1 1 70.34 83.16 28.49 o 8 1 1 26.93 30.22 53.00 o 9 1 1 118.50 101.22 74.11 o 10 1 1 4970.59 4958.49 211.88 o -10 2 1 2659.76 2880.64 238.21 o -9 2 1 5238.11 5171.60 141.64 o -8 2 1 1566.15 1504.09 71.13 o -7 2 1 2791.23 2900.23 81.68 o -6 2 1 8169.18 8239.87 145.40 o -5 2 1 26259.71 26494.50 262.69 o -4 2 1 6100.00 6093.31 99.74 o -3 2 1 1632.52 1661.35 42.09 o -2 2 1 26663.10 27240.85 271.62 o -1 2 1 31456.45 31028.05 342.08 o 0 2 1 26251.30 26596.04 293.43 o 1 2 1 50133.64 49506.29 1021.54 o 2 2 1 17540.30 18250.80 354.15 o 3 2 1 16164.73 16232.04 168.74 o 4 2 1 17263.81 17543.74 187.32 o 5 2 1 7987.52 7965.49 110.61 o 6 2 1 24.59 27.24 15.91 o 7 2 1 3623.81 3563.70 98.96 o 8 2 1 4355.99 4056.39 166.55 o 9 2 1 3138.09 3030.86 222.10 o 10 2 1 104.75 81.99 55.11 o -10 3 1 175.13 154.28 82.00 o -9 3 1 1255.04 1323.79 76.04 o -8 3 1 2200.86 2120.41 83.32 o -7 3 1 12541.05 12395.75 207.12 o -6 3 1 1767.65 1708.35 53.75 o -5 3 1 146.56 143.78 15.40 o -4 3 1 1927.30 1920.63 41.12 o -3 3 1 50610.45 48919.28 579.17 o -2 3 1 21525.14 21965.75 226.68 o -1 3 1 441.45 491.18 27.04 o 0 3 1 163.50 169.99 12.90 o 1 3 1 33842.45 34907.11 313.38 o 2 3 1 18822.76 19175.75 189.25 o 3 3 1 10610.80 10713.38 183.54 o 4 3 1 445.43 513.47 39.66 o 5 3 1 22385.65 22261.34 238.87 o 6 3 1 7596.97 7528.42 130.23 o 7 3 1 4471.50 4256.63 111.84 o 8 3 1 53.77 80.10 30.47 o 9 3 1 2275.76 2363.24 141.52 o 10 3 1 1244.31 1036.40 160.55 o -10 4 1 4848.00 4533.00 210.79 o -9 4 1 200.24 301.58 58.04 o -8 4 1 2864.80 2888.89 83.18 o -7 4 1 34.28 59.61 24.23 o -6 4 1 14556.03 14655.29 196.84 o -5 4 1 1753.69 1808.26 51.27 o -4 4 1 8813.61 8661.50 103.19 o -3 4 1 3539.22 3989.18 71.77 o -2 4 1 22316.29 22430.50 234.95 o -1 4 1 7280.71 7427.60 119.45 o 0 4 1 40239.35 39380.12 465.11 o 1 4 1 492.76 590.72 19.21 o 2 4 1 8200.87 8583.41 141.70 o 3 4 1 141.01 189.73 23.48 o 4 4 1 41966.86 41762.03 397.86 o 5 4 1 49.01 37.24 18.25 o 6 4 1 71.95 98.71 54.96 o 7 4 1 6.32 -17.32 23.91 o 8 4 1 11345.80 11255.40 212.61 o 9 4 1 320.00 233.54 87.33 o 10 4 1 273.52 150.33 86.22 o -10 5 1 1.44 -31.06 48.45 o -9 5 1 845.20 814.81 106.39 o -8 5 1 756.37 756.14 65.93 o -7 5 1 15464.63 15311.38 247.78 o -6 5 1 19.08 21.12 15.84 o -5 5 1 82.67 58.43 16.36 o -4 5 1 309.91 340.02 51.47 o -3 5 1 63451.55 62055.65 612.60 o -2 5 1 651.09 688.74 44.29 o -1 5 1 3060.92 3111.66 43.80 o 0 5 1 196.65 225.99 24.13 o 1 5 1 50994.16 50122.71 447.61 o 2 5 1 2295.70 2416.07 44.92 o 3 5 1 10869.03 11355.29 146.28 o 4 5 1 199.66 218.21 20.34 o 5 5 1 9909.69 9936.71 169.29 o 6 5 1 410.04 446.25 42.31 o 7 5 1 7111.41 7008.10 151.10 o 8 5 1 40.13 35.78 31.74 o 9 5 1 2025.26 2490.99 210.88 o -10 6 1 2749.41 2802.12 244.60 o -9 6 1 1430.93 1411.51 99.53 o -8 6 1 1154.25 1225.54 87.06 o -7 6 1 26.33 23.77 23.34 o -6 6 1 8145.67 8032.27 192.31 o -5 6 1 4683.76 4441.13 86.81 o -4 6 1 9750.68 9379.49 148.77 o -3 6 1 97.39 167.38 12.71 o -2 6 1 12025.17 12109.40 128.79 o -1 6 1 20681.76 20751.12 201.19 o 0 6 1 32170.83 31623.20 293.56 o 1 6 1 1051.48 1259.64 30.18 o 2 6 1 2592.68 2701.75 49.40 o 3 6 1 9266.54 9565.61 119.67 o 4 6 1 22779.32 22764.07 240.97 o 5 6 1 1783.65 1779.20 58.08 o 6 6 1 7.90 -0.09 18.17 o 7 6 1 1740.93 1791.37 127.17 o 8 6 1 5438.34 5984.95 233.19 o 9 6 1 1014.11 976.96 95.35 o -10 7 1 308.70 254.22 78.23 o -9 7 1 224.56 255.11 47.62 o -8 7 1 5380.84 5170.34 139.11 o -7 7 1 5231.09 5204.51 131.32 o -6 7 1 4328.69 4579.72 114.52 o -5 7 1 117.57 123.20 28.21 o -4 7 1 6564.62 6556.17 168.26 o -3 7 1 6836.46 6865.20 87.29 o -2 7 1 16857.58 17026.88 175.06 o -1 7 1 158.84 149.33 16.06 o 0 7 1 6072.70 6239.96 80.57 o 1 7 1 15954.95 16311.83 210.93 o 2 7 1 18386.56 18220.92 192.62 o 3 7 1 5201.87 5327.94 82.05 o 4 7 1 960.47 922.96 42.52 o 5 7 1 5774.34 5931.69 114.20 o 6 7 1 7675.23 7730.67 160.87 o 7 7 1 3507.44 3413.47 243.17 o 8 7 1 190.60 147.80 70.28 o 9 7 1 930.98 795.81 93.24 o -10 8 1 359.55 116.66 109.22 o -9 8 1 4959.59 4976.80 221.40 o -8 8 1 104.65 84.89 34.85 o -7 8 1 503.27 602.65 69.21 o -6 8 1 1643.53 1629.99 70.32 o -5 8 1 18109.95 17817.92 268.25 o -4 8 1 755.84 775.40 45.58 o -3 8 1 211.75 217.41 22.29 o -2 8 1 1394.20 1366.58 33.42 o -1 8 1 36918.71 35358.27 333.88 o 0 8 1 1782.73 1743.43 45.14 o 1 8 1 4110.70 3909.20 66.66 o 2 8 1 567.51 580.31 26.01 o 3 8 1 21263.67 21086.82 249.19 o 4 8 1 1400.68 1344.65 51.65 o 5 8 1 6407.77 6490.92 141.41 o 6 8 1 9.62 -2.60 23.66 o 7 8 1 4007.42 3969.32 157.80 o 8 8 1 928.65 932.26 80.54 o 9 8 1 2911.72 2629.99 223.43 o -10 9 1 293.93 380.20 147.55 o -9 9 1 81.32 13.42 38.66 o -8 9 1 7920.51 7835.20 183.39 o -7 9 1 54.44 51.73 30.30 o -6 9 1 4345.75 4499.15 138.11 o -5 9 1 8.12 12.73 19.97 o -4 9 1 11807.22 11982.11 200.58 o -3 9 1 539.23 495.95 37.50 o -2 9 1 20394.35 19955.16 236.61 o -1 9 1 525.89 548.47 23.29 o 0 9 1 2876.98 2787.07 64.26 o 1 9 1 388.53 388.14 21.94 o 2 9 1 32262.97 31231.09 310.04 o 3 9 1 5.67 31.40 13.75 o 4 9 1 482.35 512.95 42.32 o 5 9 1 2.24 6.74 21.27 o 6 9 1 11376.45 11294.28 213.31 o 7 9 1 55.11 44.58 36.47 o 8 9 1 64.50 56.98 40.62 o 9 9 1 9.02 54.78 79.22 o -9 10 1 3693.02 3796.46 168.24 o -8 10 1 337.15 375.59 85.49 o -7 10 1 237.17 271.44 43.61 o -6 10 1 306.17 320.16 42.86 o -5 10 1 10532.77 10372.54 193.93 o -4 10 1 2508.35 2338.95 91.47 o -3 10 1 319.68 378.36 40.40 o -2 10 1 1607.05 1643.10 49.50 o -1 10 1 22966.56 22702.52 235.82 o 0 10 1 1801.74 1741.42 46.57 o 1 10 1 1752.22 1787.26 58.56 o 2 10 1 45.49 85.23 16.14 o 3 10 1 23038.18 22684.60 325.83 o 4 10 1 5161.26 5139.95 124.19 o 5 10 1 4294.76 4328.68 119.05 o 6 10 1 41.80 32.76 28.65 o 7 10 1 4360.90 4163.04 184.38 o 8 10 1 960.37 959.92 88.56 o 9 10 1 2532.00 2639.54 207.10 o -9 11 1 132.76 90.28 97.77 o -8 11 1 2835.64 2934.61 116.54 o -7 11 1 3856.99 3758.20 123.04 o -6 11 1 3223.55 3117.42 106.57 o -5 11 1 57.22 72.15 27.02 o -4 11 1 6919.65 6779.57 184.87 o -3 11 1 8892.18 8912.59 235.51 o -2 11 1 9334.42 9782.30 149.94 o -1 11 1 750.56 713.57 36.36 o 0 11 1 4727.25 4733.50 79.07 o 1 11 1 7521.12 7435.97 107.36 o 2 11 1 10731.41 10815.45 159.55 o 3 11 1 3085.27 3214.87 94.50 o 4 11 1 164.42 219.96 58.10 o 5 11 1 1929.19 1987.60 146.15 o 6 11 1 5729.99 5807.25 236.49 o 7 11 1 3461.18 3167.52 217.18 o 8 11 1 16.99 -19.83 43.02 o 9 11 1 735.65 920.96 185.21 o -8 12 1 893.13 1118.06 93.75 o -7 12 1 19.53 43.75 33.14 o -6 12 1 4532.68 4484.63 131.07 o -5 12 1 4461.46 4310.00 122.47 o -4 12 1 11156.62 11104.08 206.98 o -3 12 1 174.61 151.33 34.05 o -2 12 1 10040.21 10060.54 183.41 o -1 12 1 3812.49 3827.97 117.80 o 0 12 1 15609.49 15545.54 208.77 o 1 12 1 326.63 305.53 28.45 o 2 12 1 1169.68 1205.57 49.33 o 3 12 1 3108.40 3120.16 96.20 o 4 12 1 10970.98 10629.15 223.65 o 5 12 1 1605.61 1618.77 94.42 o 6 12 1 0.67 20.98 33.53 o 7 12 1 1104.69 982.29 85.75 o 8 12 1 3419.12 3462.93 151.97 o -8 13 1 65.29 126.16 52.58 o -7 13 1 6001.21 6022.50 166.11 o -6 13 1 277.78 228.65 47.31 o -5 13 1 155.58 130.96 34.47 o -4 13 1 640.34 686.73 55.98 o -3 13 1 10399.11 10515.08 199.46 o -2 13 1 517.66 444.75 42.61 o -1 13 1 819.29 868.45 44.24 o 0 13 1 459.23 387.08 43.62 o 1 13 1 19960.47 20829.49 341.95 o 2 13 1 200.54 197.50 47.13 o 3 13 1 3604.09 3480.65 160.70 o 4 13 1 83.68 94.71 30.45 o 5 13 1 7959.23 8047.62 221.42 o 6 13 1 310.29 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