#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215614.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215614_Fobs loop_ _publ_author_name 'Wang, Qing-wei' 'Li, Xiu-mei' 'Wang, Xiu-yan' 'Zhang, Yue' _publ_section_title ; Bis{2-[tris(hydroxymethyl)methyliminomethyl]phenolato-{\k}^3^N,O,O'}nickel(II) methanol solvate ; _journal_coeditor_code NG2321 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2537 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1900 _cell_length_b 18.8378 _cell_length_c 22.4202 _exptl_crystal_F_000 2272.00 _reflns_d_resolution_high 0.8300 _[local]_cod_data_source_file ng2321Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 412.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 62351.65 58347.01 1659.47 o 4 0 0 15186.94 14536.97 398.27 o 6 0 0 40153.10 41088.51 1062.06 o 8 0 0 22940.49 24029.14 1194.82 o 10 0 0 6712.19 7832.70 796.55 o 12 0 0 2857.29 1858.61 862.92 o 2 1 0 761.08 929.30 66.38 o 4 1 0 2878.87 3186.18 199.14 o 6 1 0 3915.30 3849.97 265.52 o 8 1 0 927.66 862.93 398.27 o 10 1 0 123.59 -132.76 464.65 o 12 1 0 0.46 -331.89 597.41 o 2 2 0 46543.07 45336.76 597.41 o 4 2 0 6153.74 6040.48 199.14 o 6 2 0 30495.51 30600.65 531.03 o 8 2 0 15875.86 15599.03 531.03 o 10 2 0 4068.07 3717.22 531.03 o 12 2 0 2151.02 1593.09 531.03 o 2 3 0 13411.51 13076.63 199.14 o 4 3 0 3286.63 3451.70 132.76 o 6 3 0 615.65 796.55 265.52 o 8 3 0 5086.54 4712.90 398.27 o 10 3 0 442.15 398.27 398.27 o 12 3 0 708.48 796.55 531.03 o 0 4 0 1214.78 1393.96 132.76 o 2 4 0 83310.93 79455.48 862.92 o 4 4 0 34976.92 35446.30 531.03 o 6 4 0 55111.30 56355.64 929.30 o 8 4 0 1510.21 1792.23 331.89 o 10 4 0 3798.75 3783.59 464.65 o 12 4 0 1200.93 1128.44 531.03 o 2 5 0 724.61 730.17 66.38 o 4 5 0 6259.53 6903.40 199.14 o 6 5 0 2657.72 2787.91 199.14 o 8 5 0 1103.93 663.79 265.52 o 10 5 0 300.46 331.89 464.65 o 12 5 0 81.97 -132.76 862.92 o 0 6 0 9693.21 9558.55 265.52 o 2 6 0 9029.72 8961.14 132.76 o 4 6 0 33391.02 35180.79 464.65 o 6 6 0 1106.30 1327.58 199.14 o 8 6 0 2398.50 1991.37 331.89 o 10 6 0 2706.40 2522.40 398.27 o 12 6 0 56.78 -464.65 531.03 o 2 7 0 9865.82 9890.45 132.76 o 4 7 0 1236.17 1261.20 132.76 o 6 7 0 166.77 331.89 199.14 o 8 7 0 1605.50 1659.47 331.89 o 10 7 0 269.04 132.76 398.27 o 12 7 0 2.93 -331.89 597.41 o 0 8 0 8112.31 8230.98 331.89 o 2 8 0 30630.36 32127.36 331.89 o 4 8 0 683.56 862.93 132.76 o 6 8 0 768.00 730.17 199.14 o 8 8 0 203.61 66.38 199.14 o 10 8 0 189.51 331.89 398.27 o 12 8 0 0.87 -132.76 663.79 o 2 9 0 696.74 663.79 66.38 o 4 9 0 10688.83 10952.51 199.14 o 6 9 0 15.93 -66.38 199.14 o 8 9 0 105.58 199.14 265.52 o 10 9 0 33.61 -464.65 464.65 o 12 9 0 80.05 132.76 730.17 o 0 10 0 12093.67 12412.84 398.27 o 2 10 0 3251.28 3318.94 132.76 o 4 10 0 3362.42 3252.56 132.76 o 6 10 0 139.57 66.38 132.76 o 8 10 0 2016.25 1991.37 265.52 o 10 10 0 992.98 1062.06 464.65 o 12 10 0 522.69 1261.20 862.92 o 2 11 0 1695.46 1659.47 66.38 o 4 11 0 7859.31 8098.22 199.14 o 6 11 0 0.14 -66.38 199.14 o 8 11 0 766.25 331.89 265.52 o 10 11 0 606.15 398.27 531.03 o 0 12 0 5069.18 5111.17 398.27 o 2 12 0 20547.25 20710.20 331.89 o 4 12 0 9797.39 9890.45 265.52 o 6 12 0 848.71 796.55 199.14 o 8 12 0 3663.23 4248.25 398.27 o 10 12 0 3260.39 3053.43 597.41 o 2 13 0 118.20 132.76 66.38 o 4 13 0 172.14 199.14 132.76 o 6 13 0 171.74 66.38 199.14 o 8 13 0 956.22 597.41 398.27 o 10 13 0 6.50 929.30 862.92 o 0 14 0 12311.15 13342.15 730.17 o 2 14 0 17003.72 17723.15 796.55 o 4 14 0 4332.64 4248.25 199.14 o 6 14 0 3480.00 3717.22 398.27 o 8 14 0 4312.15 3916.35 464.65 o 10 14 0 1257.76 1593.09 862.92 o 2 15 0 757.18 862.93 398.27 o 4 15 0 630.72 398.27 132.76 o 6 15 0 714.21 66.38 331.89 o 8 15 0 3.58 66.38 398.27 o 10 15 0 28.11 1062.06 862.92 o 0 16 0 4346.80 5310.31 597.41 o 2 16 0 523.49 464.65 531.03 o 4 16 0 3836.45 3783.59 265.52 o 6 16 0 3686.03 3584.46 398.27 o 8 16 0 1712.46 1991.37 663.79 o 2 17 0 41.76 -663.79 663.79 o 4 17 0 476.57 464.65 199.14 o 6 17 0 102.76 -199.14 398.27 o 8 17 0 136.77 66.38 531.03 o 0 18 0 1935.17 1393.96 663.79 o 2 18 0 2172.73 1659.47 531.03 o 4 18 0 2774.19 2854.29 995.68 o 6 18 0 2423.33 2389.64 398.27 o 8 18 0 755.79 597.41 663.79 o 2 19 0 485.03 663.79 663.79 o 4 19 0 185.47 265.52 796.55 o 6 19 0 132.30 -464.65 663.79 o 0 20 0 105.27 995.68 1261.20 o 2 20 0 138.65 597.41 730.17 o 4 20 0 1.75 -331.89 929.30 o 6 20 0 536.32 862.93 862.92 o 2 21 0 149.06 66.38 730.17 o 4 21 0 259.61 -531.03 1194.82 o 0 22 0 331.29 -1261.20 1460.33 o 2 22 0 158.21 -1261.20 1261.20 o 2 1 1 2863.49 2887.86 93.87 o 3 1 1 18802.20 19089.18 298.70 o 4 1 1 1357.89 1120.39 165.95 o 5 1 1 1010.70 884.41 110.46 o 6 1 1 1789.77 1693.31 140.81 o 7 1 1 4.86 191.76 207.33 o 8 1 1 33.96 12.07 254.97 o 9 1 1 1437.40 1325.80 270.07 o 10 1 1 665.07 896.11 328.56 o 11 1 1 783.94 597.41 375.50 o 12 1 1 62.90 -139.08 491.16 o 13 1 1 0.49 -630.60 630.60 o 2 2 1 11354.80 11184.94 140.81 o 3 2 1 30656.09 30713.66 302.39 o 4 2 1 3593.25 3584.46 93.87 o 5 2 1 554.38 553.16 110.46 o 6 2 1 4381.86 4252.40 187.75 o 7 2 1 5282.71 4993.82 207.33 o 8 2 1 638.59 525.00 254.97 o 9 2 1 32.07 234.88 302.39 o 10 2 1 388.05 -61.27 302.39 o 11 2 1 1767.89 1970.62 380.66 o 12 2 1 56.84 431.46 469.37 o 13 2 1 117.13 -119.48 585.30 o 1 3 1 1608.39 1595.86 66.38 o 2 3 1 29182.70 28346.26 281.62 o 3 3 1 79522.29 77945.26 1062.06 o 4 3 1 2506.20 2434.19 165.95 o 5 3 1 12982.35 12775.19 207.33 o 6 3 1 404.94 610.69 140.81 o 7 3 1 2101.92 2161.06 207.33 o 8 3 1 2015.04 1840.81 220.92 o 9 3 1 6586.49 6414.34 302.39 o 10 3 1 21.23 -97.36 349.69 o 11 3 1 1430.08 1544.18 429.46 o 12 3 1 53.34 140.13 414.67 o 13 3 1 257.63 331.89 516.31 o 0 4 1 2439.60 2323.26 66.38 o 1 4 1 8707.13 8662.57 93.87 o 2 4 1 1956.79 2025.10 46.94 o 3 4 1 1826.56 1888.53 99.57 o 4 4 1 26350.70 26286.70 281.62 o 5 4 1 4160.77 4287.87 165.95 o 6 4 1 11379.92 11107.70 232.33 o 7 4 1 113.81 9.48 159.31 o 8 4 1 1797.44 1676.55 207.33 o 9 4 1 59.66 -165.95 234.68 o 10 4 1 1815.98 2146.62 302.39 o 11 4 1 641.42 564.22 375.50 o 12 4 1 251.47 -73.02 462.37 o 13 4 1 0.39 342.11 604.78 o 1 5 1 974.22 1062.06 46.94 o 2 5 1 8669.31 8695.63 93.87 o 3 5 1 32802.61 32459.39 281.62 o 4 5 1 528.04 531.03 93.87 o 5 5 1 58175.99 59071.23 663.79 o 6 5 1 39.11 -66.38 140.81 o 7 5 1 6192.73 5720.49 331.89 o 8 5 1 44.22 0.00 187.75 o 9 5 1 1557.12 1463.35 281.62 o 10 5 1 560.97 531.03 328.56 o 11 5 1 3010.50 2824.62 328.56 o 12 5 1 6.94 -24.46 464.65 o 13 5 1 626.39 54.93 679.37 o 0 6 1 2507.23 2456.02 66.38 o 1 6 1 607.46 698.56 46.94 o 2 6 1 25239.17 25354.52 207.33 o 3 6 1 2038.70 1924.99 93.87 o 4 6 1 48954.54 51410.44 469.37 o 5 6 1 3189.87 3324.25 140.81 o 6 6 1 8841.97 8596.19 187.75 o 7 6 1 71.64 132.76 140.81 o 8 6 1 2802.78 2794.04 265.52 o 9 6 1 294.34 165.95 234.68 o 10 6 1 1148.00 1270.05 349.69 o 11 6 1 87.08 296.49 349.69 o 12 6 1 619.29 603.44 509.94 o 1 7 1 10458.41 10560.14 110.46 o 2 7 1 129.31 66.38 46.94 o 3 7 1 51722.88 53103.08 444.05 o 4 7 1 2219.20 2190.50 93.87 o 5 7 1 11188.65 11157.97 265.52 o 6 7 1 149.18 99.57 140.81 o 7 7 1 4368.55 4385.03 187.75 o 8 7 1 156.50 265.52 187.75 o 9 7 1 5235.62 5415.20 302.39 o 10 7 1 403.81 229.31 254.97 o 11 7 1 2527.19 2231.52 396.90 o 12 7 1 54.13 265.52 469.37 o 0 8 1 3067.85 2987.05 66.38 o 1 8 1 2252.37 2356.92 46.94 o 2 8 1 40798.93 41322.99 328.56 o 3 8 1 1211.00 1463.35 93.87 o 4 8 1 21006.84 21444.83 207.33 o 5 8 1 888.33 802.08 93.87 o 6 8 1 1076.82 1066.21 140.81 o 7 8 1 273.79 331.89 140.81 o 8 8 1 5334.11 5178.40 234.68 o 9 8 1 10.67 -205.17 254.97 o 10 8 1 1096.02 857.82 302.39 o 11 8 1 0.22 -79.65 349.69 o 12 8 1 724.74 464.65 469.37 o 1 9 1 22463.91 22636.94 199.14 o 2 9 1 1316.24 1434.09 99.57 o 3 9 1 3776.09 3551.58 93.87 o 4 9 1 1857.31 1858.61 93.87 o 5 9 1 8958.97 8629.76 187.75 o 6 9 1 83.07 33.19 165.95 o 7 9 1 3180.63 3114.70 165.95 o 8 9 1 791.66 690.54 159.31 o 9 9 1 2450.55 1976.94 464.65 o 10 9 1 3.60 -99.57 328.56 o 11 9 1 2662.79 2618.32 464.65 o 12 9 1 1.82 -232.33 564.22 o 0 10 1 5391.14 5443.07 199.14 o 1 10 1 188.64 165.95 46.94 o 2 10 1 7703.60 7587.74 110.46 o 3 10 1 88.43 0.00 46.94 o 4 10 1 1481.86 1393.96 93.87 o 5 10 1 13.20 0.00 93.87 o 6 10 1 1729.12 1725.85 140.81 o 7 10 1 79.91 28.45 159.31 o 8 10 1 3440.01 3320.27 187.75 o 9 10 1 83.14 199.14 234.68 o 10 10 1 2696.36 2397.01 375.50 o 11 10 1 380.96 33.19 422.43 o 12 10 1 546.86 471.08 726.39 o 1 11 1 6117.57 5853.41 265.52 o 2 11 1 332.91 331.89 46.94 o 3 11 1 922.33 831.06 93.87 o 4 11 1 556.25 531.03 93.87 o 5 11 1 2621.19 2522.40 140.81 o 6 11 1 1318.55 1104.30 140.81 o 7 11 1 2225.56 2224.19 187.75 o 8 11 1 182.95 169.63 207.33 o 9 11 1 1641.01 1809.12 207.33 o 10 11 1 118.18 -168.16 349.69 o 11 11 1 1642.98 1715.23 574.14 o 0 12 1 9242.70 9359.42 265.52 o 1 12 1 2807.68 2890.91 187.75 o 2 12 1 3740.80 3783.59 46.94 o 3 12 1 402.57 365.08 93.87 o 4 12 1 205.90 199.14 93.87 o 5 12 1 297.49 232.33 140.81 o 6 12 1 1170.41 1237.30 159.31 o 7 12 1 0.05 95.88 207.33 o 8 12 1 139.99 199.14 234.68 o 9 12 1 6.93 -223.27 254.97 o 10 12 1 1035.69 1245.88 604.78 o 11 12 1 26.26 -531.03 622.00 o 1 13 1 2580.01 2642.74 398.27 o 2 13 1 3692.52 3589.37 132.76 o 3 13 1 449.71 199.14 93.87 o 4 13 1 228.64 232.33 93.87 o 5 13 1 931.97 934.05 140.81 o 6 13 1 314.03 232.33 165.95 o 7 13 1 1084.22 962.49 207.33 o 8 13 1 114.82 99.57 281.62 o 9 13 1 471.28 199.14 349.69 o 10 13 1 19.02 -401.16 538.25 o 11 13 1 100.97 103.00 650.75 o 0 14 1 612.02 597.41 331.89 o 1 14 1 1602.58 1487.60 254.97 o 2 14 1 157.59 331.89 281.62 o 3 14 1 654.15 632.35 46.94 o 4 14 1 40.73 66.38 93.87 o 5 14 1 295.80 298.70 93.87 o 6 14 1 12.01 66.38 281.62 o 7 14 1 27.26 42.24 265.52 o 8 14 1 6.94 -30.64 302.39 o 9 14 1 356.93 431.46 469.37 o 10 14 1 42.88 796.55 563.24 o 1 15 1 67.15 -121.69 270.07 o 2 15 1 6.26 132.76 331.38 o 3 15 1 1.26 -33.19 46.94 o 4 15 1 203.14 66.38 93.87 o 5 15 1 400.56 431.46 234.68 o 6 15 1 133.06 66.38 265.52 o 7 15 1 385.54 645.69 254.97 o 8 15 1 34.96 -185.86 331.38 o 9 15 1 4.56 -232.33 540.15 o 10 15 1 11.37 -526.13 526.13 o 0 16 1 2417.30 2588.78 398.27 o 1 16 1 47.89 10.21 302.39 o 2 16 1 1183.20 1464.40 375.50 o 3 16 1 4.13 22.13 59.37 o 4 16 1 2.63 -159.31 159.31 o 5 16 1 510.32 545.78 207.33 o 6 16 1 715.59 663.79 234.68 o 7 16 1 7.79 56.17 302.39 o 8 16 1 15.44 232.33 375.50 o 9 16 1 4.75 -469.37 469.37 o 1 17 1 203.57 365.08 328.56 o 2 17 1 870.94 862.92 414.67 o 3 17 1 23.08 99.57 375.50 o 4 17 1 159.24 165.95 140.81 o 5 17 1 805.10 796.55 207.33 o 6 17 1 0.68 -223.27 265.52 o 7 17 1 2215.24 1826.56 318.62 o 8 17 1 1.30 66.38 422.43 o 0 18 1 2010.02 1792.23 531.03 o 1 18 1 44.37 -258.14 414.67 o 2 18 1 51.64 -331.89 375.50 o 3 18 1 257.83 387.79 429.46 o 4 18 1 262.79 33.19 516.31 o 5 18 1 13.60 99.57 187.75 o 6 18 1 1250.98 995.68 281.62 o 7 18 1 98.77 161.21 318.62 o 8 18 1 509.96 265.52 516.31 o 1 19 1 447.71 862.93 444.05 o 2 19 1 727.31 702.22 444.05 o 3 19 1 118.73 167.53 491.16 o 4 19 1 99.70 63.22 491.16 o 5 19 1 343.47 -103.26 622.00 o 6 19 1 132.78 491.20 552.31 o 7 19 1 1113.71 694.77 531.03 o 0 20 1 3390.85 3119.81 796.55 o 1 20 1 43.54 -94.83 477.93 o 2 20 1 432.51 279.95 526.13 o 3 20 1 0.94 -99.57 469.37 o 4 20 1 1615.71 1221.37 585.30 o 5 20 1 0.03 188.92 604.78 o 6 20 1 605.41 1057.20 954.50 o 1 21 1 1778.26 1770.10 593.71 o 2 21 1 0.13 -199.14 552.31 o 3 21 1 847.50 698.42 538.25 o 4 21 1 53.73 -451.38 699.37 o 5 21 1 662.51 464.65 726.39 o 0 22 1 813.25 2721.53 995.68 o 1 22 1 144.35 927.09 631.91 o 2 22 1 415.09 663.79 995.68 o 3 22 1 16.39 419.61 1095.25 o 2 0 2 10462.67 10222.34 199.14 o 3 0 2 10984.84 10421.48 199.14 o 4 0 2 19965.85 19980.03 331.89 o 5 0 2 1948.99 1792.23 132.76 o 6 0 2 3286.20 3518.08 199.14 o 7 0 2 902.17 862.93 265.52 o 8 0 2 1258.89 796.55 265.52 o 9 0 2 0.66 597.41 398.27 o 10 0 2 219.42 -66.38 398.27 o 11 0 2 81.92 132.76 531.03 o 12 0 2 0.27 -199.14 597.41 o 13 0 2 98.97 66.38 1062.06 o 2 1 2 44.77 0.00 66.38 o 3 1 2 14445.44 13844.91 232.33 o 4 1 2 2918.02 2742.34 132.76 o 5 1 2 12194.80 11815.44 187.75 o 6 1 2 67.91 66.38 110.46 o 7 1 2 23675.92 23847.09 796.55 o 8 1 2 528.67 696.98 187.75 o 9 1 2 7625.28 7581.75 331.89 o 10 1 2 68.78 -153.18 302.39 o 11 1 2 2877.73 2784.00 366.77 o 12 1 2 27.56 116.95 491.16 o 13 1 2 3177.56 3196.05 652.10 o 2 2 2 7946.60 8098.76 93.87 o 3 2 2 1497.27 1460.33 59.37 o 4 2 2 9124.50 9117.91 159.31 o 5 2 2 0.23 66.38 93.87 o 6 2 2 11.15 -66.38 140.81 o 7 2 2 895.78 677.06 165.95 o 8 2 2 14.97 72.41 254.97 o 9 2 2 260.92 199.14 220.92 o 10 2 2 85.32 183.82 281.45 o 11 2 2 1.68 -150.46 349.69 o 12 2 2 41.33 398.27 469.37 o 13 2 2 6.38 262.63 829.74 o 1 3 2 15964.70 15532.94 140.81 o 2 3 2 36259.46 35446.80 328.56 o 3 3 2 21519.47 21505.15 331.89 o 4 3 2 3457.41 3648.05 110.46 o 5 3 2 13905.39 14011.05 207.33 o 6 3 2 1398.06 1295.24 140.81 o 7 3 2 14154.51 14661.21 349.69 o 8 3 2 1449.44 1434.89 207.33 o 9 3 2 2905.68 2810.84 270.07 o 10 3 2 218.51 362.53 302.39 o 11 3 2 2147.30 2341.37 366.77 o 12 3 2 19.00 -66.38 516.31 o 13 3 2 2099.17 2922.68 773.39 o 0 4 2 55576.48 53567.73 531.03 o 1 4 2 4661.75 4581.10 66.38 o 2 4 2 56880.11 55175.08 444.05 o 3 4 2 818.89 868.03 66.38 o 4 4 2 5625.92 5945.54 165.95 o 5 4 2 4375.23 4381.00 140.81 o 6 4 2 412.93 365.08 140.81 o 7 4 2 2911.85 2854.29 207.33 o 8 4 2 11.02 162.26 207.33 o 9 4 2 4.54 -230.53 230.53 o 10 4 2 194.75 189.65 318.62 o 11 4 2 0.24 -33.19 281.62 o 12 4 2 43.10 -165.95 516.31 o 13 4 2 57.72 -464.65 563.24 o 1 5 2 5374.23 5443.88 66.38 o 2 5 2 3598.32 3355.09 99.57 o 3 5 2 23179.80 23161.02 265.52 o 4 5 2 53.50 88.51 59.37 o 5 5 2 7775.27 7634.15 140.81 o 6 5 2 4500.15 4348.07 187.75 o 7 5 2 6724.25 6472.11 234.68 o 8 5 2 482.83 339.27 207.33 o 9 5 2 193.14 132.76 234.68 o 10 5 2 147.33 66.38 375.50 o 11 5 2 359.96 497.84 328.56 o 12 5 2 210.73 104.81 444.05 o 13 5 2 568.16 1016.11 604.78 o 0 6 2 16626.95 16395.58 199.14 o 1 6 2 17390.67 17759.38 232.33 o 2 6 2 787.76 730.17 46.94 o 3 6 2 642.48 597.41 46.94 o 4 6 2 5851.69 6411.77 165.95 o 5 6 2 1957.72 1892.38 93.87 o 6 6 2 768.73 682.75 140.81 o 7 6 2 39.19 -33.19 140.81 o 8 6 2 490.93 398.27 170.76 o 9 6 2 640.28 796.55 281.62 o 10 6 2 1905.15 1724.55 281.62 o 11 6 2 25.76 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