#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/56/2215615.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215615_Fobs loop_ _publ_author_name 'Li, Xiu-Ling' 'Niu, De-Zhong' 'Lu, Zai-Sheng' _publ_section_title ; Tetraaquabis(thiocyanato-{\kN})cobalt(II) hexamethylenetetramine (1/2) cocrystal ; _journal_coeditor_code NG2324 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2478 _journal_volume 63 _journal_year 2007 _space_group_IT_number 136 _symmetry_space_group_name_Hall '-P 4n 2n' _symmetry_space_group_name_H-M 'P 42/m n m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4846 _cell_length_b 9.4846 _cell_length_c 13.7339 _exptl_crystal_F_000 554.00 _reflns_d_resolution_high 0.8393 _[local]_cod_data_source_file ng2324Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lxl in P4(2)/mnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-y+1/2, x+1/2, z+1/2' 'y+1/2, -x+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'y, x, -z' '-y, -x, -z' '-x, -y, -z' 'x, y, -z' 'y-1/2, -x-1/2, -z-1/2' '-y-1/2, x-1/2, -z-1/2' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' '-y, -x, z' 'y, x, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 2412.30 2163.32 38.51 o 0 2 0 11621.25 11479.42 203.45 o 1 2 0 2510.09 2527.65 33.69 o 2 2 0 6752.45 6502.13 208.14 o 1 3 0 70.67 85.64 3.66 o 2 3 0 3956.28 4146.52 123.76 o 3 3 0 8323.07 8683.91 154.32 o 0 4 0 1746.46 2037.60 48.17 o 1 4 0 1.28 4.03 1.12 o 2 4 0 801.80 716.34 9.47 o 3 4 0 2.32 5.08 0.73 o 4 4 0 7871.80 7503.14 133.67 o 1 5 0 87.60 74.57 1.86 o 2 5 0 805.77 845.65 11.22 o 3 5 0 1336.39 1314.13 23.66 o 4 5 0 4.37 8.26 1.11 o 5 5 0 1074.44 987.95 24.13 o 0 6 0 1492.70 1650.69 52.40 o 1 6 0 254.54 254.40 4.06 o 2 6 0 1847.92 1895.67 24.48 o 3 6 0 14.21 10.36 1.29 o 4 6 0 240.54 223.26 6.14 o 5 6 0 517.27 479.56 10.20 o 6 6 0 497.89 427.60 13.44 o 1 7 0 716.62 742.10 10.26 o 2 7 0 1408.06 1389.51 26.81 o 3 7 0 344.52 347.74 11.78 o 4 7 0 67.53 45.55 2.93 o 5 7 0 119.55 96.03 3.96 o 6 7 0 85.87 78.96 3.78 o 7 7 0 1201.02 1151.46 32.09 o 0 8 0 2120.56 2348.01 43.13 o 1 8 0 120.79 121.86 5.35 o 2 8 0 518.68 528.60 12.29 o 3 8 0 193.18 173.21 5.19 o 4 8 0 237.98 218.79 6.18 o 5 8 0 0.41 3.99 2.37 o 6 8 0 258.35 223.49 8.75 o 7 8 0 25.71 25.57 5.55 o 1 9 0 329.48 313.77 6.22 o 2 9 0 16.91 10.33 2.84 o 3 9 0 5.67 7.93 2.72 o 4 9 0 0.06 1.43 2.45 o 5 9 0 27.90 36.13 8.89 o 6 9 0 16.65 20.46 3.56 o 0 10 0 1.93 -3.14 3.14 o 1 10 0 73.53 72.10 5.29 o 2 10 0 358.11 366.72 9.14 o 3 10 0 7.32 14.30 3.19 o 4 10 0 455.45 451.33 11.00 o 5 10 0 261.70 271.06 8.00 o 1 11 0 38.01 42.23 5.39 o 2 11 0 47.06 48.85 6.07 o 0 1 1 5237.02 5044.01 56.57 o 1 1 1 1730.90 1827.61 34.21 o 1 2 1 1821.09 1923.23 17.19 o 2 2 1 1350.20 1357.73 33.70 o 0 3 1 2955.31 3029.83 38.26 o 1 3 1 450.04 476.82 6.16 o 2 3 1 2644.00 2522.71 22.60 o 3 3 1 51.75 79.58 1.92 o 1 4 1 632.68 512.79 6.64 o 2 4 1 231.38 250.91 3.78 o 3 4 1 469.66 476.55 7.28 o 4 4 1 0.07 1.19 0.70 o 0 5 1 1499.25 1462.18 18.92 o 1 5 1 435.97 431.90 4.29 o 2 5 1 746.74 765.34 7.23 o 3 5 1 571.05 511.21 5.00 o 4 5 1 820.29 769.89 12.83 o 5 5 1 663.32 601.56 9.74 o 1 6 1 334.60 339.27 3.60 o 2 6 1 128.66 112.08 3.20 o 3 6 1 583.12 555.73 8.47 o 4 6 1 36.24 24.64 2.04 o 5 6 1 910.77 777.27 12.39 o 6 6 1 5.06 7.05 2.16 o 0 7 1 37.85 41.52 2.08 o 1 7 1 16.08 16.21 1.29 o 2 7 1 428.70 427.63 5.02 o 3 7 1 101.31 86.94 1.95 o 4 7 1 835.07 754.32 9.48 o 5 7 1 1.54 -1.24 1.86 o 6 7 1 300.85 275.66 5.03 o 7 7 1 10.71 -1.52 7.51 o 1 8 1 306.15 309.06 3.61 o 2 8 1 325.37 323.27 5.01 o 3 8 1 661.49 631.19 10.95 o 4 8 1 0.05 -0.57 1.39 o 5 8 1 220.63 218.95 4.45 o 6 8 1 138.63 112.65 3.37 o 7 8 1 10.57 0.93 3.76 o 0 9 1 174.43 190.63 4.64 o 1 9 1 163.12 158.40 7.73 o 2 9 1 257.12 247.67 5.71 o 3 9 1 1.17 3.20 1.74 o 4 9 1 212.26 222.62 5.29 o 5 9 1 76.86 64.86 5.46 o 6 9 1 7.17 9.02 2.22 o 1 10 1 348.38 372.06 6.40 o 2 10 1 32.91 31.79 3.90 o 3 10 1 93.43 105.49 3.56 o 4 10 1 5.05 8.02 4.37 o 5 10 1 3.95 9.63 4.03 o 0 11 1 270.19 274.66 11.23 o 1 11 1 32.93 31.51 5.61 o 2 11 1 130.23 142.19 10.58 o 0 0 2 67.87 59.11 1.89 o 1 1 2 27876.86 24682.17 308.99 o 0 2 2 188.65 234.14 4.45 o 1 2 2 1326.39 1307.96 12.79 o 2 2 2 6165.90 6060.06 88.05 o 1 3 2 759.25 893.32 8.17 o 2 3 2 120.15 128.46 2.10 o 3 3 2 3531.14 3506.48 44.34 o 0 4 2 662.84 626.00 13.30 o 1 4 2 286.93 308.40 3.57 o 2 4 2 2482.80 2439.57 21.95 o 3 4 2 8.47 9.37 0.56 o 4 4 2 4904.58 4932.57 62.34 o 1 5 2 228.44 240.91 3.18 o 2 5 2 483.70 461.91 6.81 o 3 5 2 1739.87 1648.42 17.62 o 4 5 2 22.41 26.78 1.09 o 5 5 2 429.54 403.68 11.29 o 0 6 2 1494.14 1591.91 18.54 o 1 6 2 548.23 598.34 5.88 o 2 6 2 474.49 444.60 6.66 o 3 6 2 410.33 390.95 5.01 o 4 6 2 2.20 2.79 2.09 o 5 6 2 141.89 127.47 3.26 o 6 6 2 1174.50 1042.19 20.35 o 1 7 2 2048.63 2174.89 19.90 o 2 7 2 36.27 34.56 1.45 o 3 7 2 124.04 114.46 2.66 o 4 7 2 248.60 235.26 4.40 o 5 7 2 36.43 28.25 1.91 o 6 7 2 36.81 35.15 2.59 o 7 7 2 359.36 345.22 9.90 o 0 8 2 1793.23 1813.78 23.81 o 1 8 2 15.14 13.70 1.24 o 2 8 2 24.97 20.63 1.44 o 3 8 2 29.06 25.65 2.78 o 4 8 2 3.71 0.44 3.53 o 5 8 2 1.85 1.25 1.69 o 6 8 2 353.95 341.36 8.20 o 7 8 2 19.35 26.37 2.58 o 1 9 2 117.52 116.06 2.88 o 2 9 2 296.64 316.29 4.50 o 3 9 2 342.04 330.19 7.49 o 4 9 2 2.15 3.78 1.87 o 5 9 2 291.59 283.15 5.63 o 6 9 2 145.25 144.03 4.18 o 0 10 2 34.77 33.56 3.61 o 1 10 2 35.79 38.99 2.59 o 2 10 2 270.19 317.17 11.07 o 3 10 2 83.90 91.35 3.52 o 4 10 2 163.66 177.19 8.88 o 5 10 2 2.45 -3.57 3.94 o 1 11 2 8.08 -1.75 3.96 o 2 11 2 0.83 -2.78 3.82 o 0 1 3 2.70 5.37 0.41 o 1 1 3 6131.23 6182.36 69.44 o 1 2 3 3007.07 3094.24 27.60 o 2 2 3 1699.33 1606.33 27.72 o 0 3 3 495.20 472.21 6.33 o 1 3 3 1283.67 1441.50 13.05 o 2 3 3 611.89 627.15 6.31 o 3 3 3 2520.20 2678.59 39.44 o 1 4 3 7476.65 8044.72 71.54 o 2 4 3 1061.43 1143.66 10.50 o 3 4 3 483.35 507.16 8.18 o 4 4 3 3.98 2.54 2.12 o 0 5 3 1491.27 1476.76 19.14 o 1 5 3 24.72 20.23 1.45 o 2 5 3 149.91 134.89 2.53 o 3 5 3 207.21 235.06 5.25 o 4 5 3 95.18 80.26 2.70 o 5 5 3 263.16 214.69 8.43 o 1 6 3 968.82 969.56 9.21 o 2 6 3 961.05 989.85 10.02 o 3 6 3 651.83 620.66 7.32 o 4 6 3 134.93 113.86 3.65 o 5 6 3 527.79 468.26 7.68 o 6 6 3 466.96 384.75 11.72 o 0 7 3 327.71 366.57 7.59 o 1 7 3 40.96 38.77 1.95 o 2 7 3 733.43 737.38 9.89 o 3 7 3 3.59 4.41 1.19 o 4 7 3 664.39 624.80 9.54 o 5 7 3 73.01 68.60 1.88 o 6 7 3 160.40 136.41 3.38 o 7 7 3 19.42 16.69 7.02 o 1 8 3 8.17 9.32 2.51 o 2 8 3 9.55 8.38 1.37 o 3 8 3 644.45 620.45 10.14 o 4 8 3 26.34 30.59 3.58 o 5 8 3 338.64 322.25 5.81 o 6 8 3 33.23 30.41 2.50 o 7 8 3 2.70 5.35 4.21 o 0 9 3 296.87 327.96 8.37 o 1 9 3 244.36 256.43 4.90 o 2 9 3 390.22 382.37 10.06 o 3 9 3 27.10 24.18 2.29 o 4 9 3 287.76 286.89 7.50 o 5 9 3 52.21 52.87 2.96 o 6 9 3 14.27 7.24 2.13 o 1 10 3 107.57 110.86 5.31 o 2 10 3 1.01 -2.23 3.11 o 3 10 3 131.83 134.48 4.67 o 4 10 3 74.28 75.92 4.64 o 0 11 3 218.27 248.75 11.49 o 1 11 3 5.39 -0.43 5.71 o 0 0 4 12547.36 13246.04 332.17 o 1 1 4 2474.16 2456.56 31.09 o 0 2 4 526.57 630.20 8.94 o 1 2 4 250.49 288.63 2.84 o 2 2 4 72.25 91.28 13.36 o 1 3 4 3979.75 4073.76 34.31 o 2 3 4 83.95 70.49 1.90 o 3 3 4 6088.90 6241.35 91.00 o 0 4 4 72.19 64.93 1.52 o 1 4 4 450.16 476.23 4.38 o 2 4 4 202.20 203.61 2.78 o 3 4 4 484.55 513.19 8.09 o 4 4 4 2028.70 1910.05 28.61 o 1 5 4 2375.02 2524.14 21.53 o 2 5 4 14.53 26.29 1.78 o 3 5 4 774.53 736.51 11.92 o 4 5 4 5.60 5.03 0.99 o 5 5 4 356.62 343.22 11.64 o 0 6 4 1441.63 1461.11 19.13 o 1 6 4 130.28 137.20 2.34 o 2 6 4 1027.06 1038.37 14.99 o 3 6 4 1.48 4.72 1.87 o 4 6 4 7.73 6.41 1.17 o 5 6 4 93.45 91.26 2.02 o 6 6 4 31.19 34.45 2.22 o 1 7 4 1555.00 1667.67 16.63 o 2 7 4 4.00 6.77 1.56 o 3 7 4 5.86 11.68 1.57 o 4 7 4 36.12 30.64 1.97 o 5 7 4 312.48 277.95 4.01 o 6 7 4 1.65 -0.81 1.81 o 7 7 4 867.26 810.79 20.49 o 0 8 4 410.46 500.53 8.82 o 1 8 4 116.02 134.52 2.97 o 2 8 4 56.17 58.21 1.99 o 3 8 4 190.99 188.19 3.25 o 4 8 4 100.17 82.46 2.89 o 5 8 4 1.97 3.15 3.06 o 6 8 4 91.23 84.58 3.27 o 7 8 4 62.95 55.24 3.02 o 1 9 4 349.81 382.45 7.70 o 2 9 4 52.09 56.54 2.33 o 3 9 4 296.09 309.21 5.47 o 4 9 4 15.42 15.65 3.00 o 5 9 4 316.24 307.69 5.93 o 6 9 4 17.50 24.18 6.74 o 0 10 4 84.77 91.30 5.28 o 1 10 4 23.07 37.82 2.95 o 2 10 4 96.80 107.42 3.89 o 3 10 4 2.16 1.33 2.85 o 4 10 4 242.65 240.37 11.73 o 0 1 5 17.34 10.31 0.67 o 1 1 5 2780.07 2735.63 34.67 o 1 2 5 480.76 369.07 4.28 o 2 2 5 7817.43 8195.77 103.04 o 0 3 5 8007.49 8207.72 103.24 o 1 3 5 1.30 1.28 0.47 o 2 3 5 2592.34 2663.22 23.94 o 3 3 5 64.88 56.13 6.18 o 1 4 5 1015.43 949.67 9.55 o 2 4 5 77.35 93.61 1.51 o 3 4 5 6.15 9.07 0.96 o 4 4 5 15.68 17.08 1.54 o 0 5 5 4473.80 4768.96 60.40 o 1 5 5 871.70 894.47 8.44 o 2 5 5 1144.52 1207.44 13.09 o 3 5 5 576.03 560.89 7.09 o 4 5 5 116.27 116.27 4.23 o 5 5 5 1232.05 1210.95 37.23 o 1 6 5 639.55 664.84 7.03 o 2 6 5 547.71 531.46 7.43 o 3 6 5 287.82 297.98 4.03 o 4 6 5 15.55 9.03 1.24 o 5 6 5 309.48 288.59 4.07 o 6 6 5 1.42 11.05 7.17 o 0 7 5 2.83 1.18 2.14 o 1 7 5 218.88 212.63 3.40 o 2 7 5 286.64 283.82 3.73 o 3 7 5 1.34 0.32 1.16 o 4 7 5 769.44 750.75 11.98 o 5 7 5 53.85 47.54 3.18 o 6 7 5 174.56 154.87 2.94 o 7 7 5 71.47 53.20 3.85 o 1 8 5 217.63 243.82 4.19 o 2 8 5 90.89 99.81 2.91 o 3 8 5 790.23 811.50 15.60 o 4 8 5 32.23 33.54 2.89 o 5 8 5 297.65 268.73 4.25 o 6 8 5 110.12 123.25 3.80 o 7 8 5 2.00 1.30 6.07 o 0 9 5 2.08 0.77 3.10 o 1 9 5 94.21 106.24 4.09 o 2 9 5 95.70 107.56 3.14 o 3 9 5 2.74 3.56 1.79 o 4 9 5 344.24 327.56 6.82 o 5 9 5 77.58 78.47 3.31 o 1 10 5 216.07 240.56 5.55 o 2 10 5 82.36 87.18 5.10 o 3 10 5 99.62 104.60 5.59 o 0 0 6 4971.19 5166.68 130.34 o 1 1 6 1412.70 1415.83 29.13 o 0 2 6 935.75 844.73 11.12 o 1 2 6 15.63 16.47 0.64 o 2 2 6 3156.27 3134.46 39.79 o 1 3 6 53.66 44.87 1.64 o 2 3 6 110.94 127.33 1.97 o 3 3 6 2423.66 2359.91 35.07 o 0 4 6 766.53 842.15 11.23 o 1 4 6 505.22 566.94 5.51 o 2 4 6 477.93 493.71 6.65 o 3 4 6 106.80 105.46 2.02 o 4 4 6 762.32 821.33 13.08 o 1 5 6 923.71 895.34 9.56 o 2 5 6 643.87 692.29 7.33 o 3 5 6 1278.55 1295.12 14.52 o 4 5 6 22.96 31.68 1.54 o 5 5 6 256.32 259.69 5.66 o 0 6 6 685.20 749.07 13.06 o 1 6 6 25.16 25.54 1.85 o 2 6 6 256.10 278.46 3.91 o 3 6 6 134.01 120.71 2.40 o 4 6 6 4.93 4.86 1.19 o 5 6 6 52.22 39.04 1.73 o 6 6 6 746.87 676.35 12.68 o 1 7 6 635.38 700.58 10.26 o 2 7 6 12.75 13.99 1.45 o 3 7 6 68.33 71.31 3.38 o 4 7 6 24.26 22.16 2.48 o 5 7 6 38.36 38.12 1.92 o 6 7 6 2.88 0.58 1.47 o 7 7 6 231.56 225.18 6.97 o 0 8 6 939.74 1058.19 21.04 o 1 8 6 1.41 -0.73 1.70 o 2 8 6 146.42 163.62 4.80 o 3 8 6 4.72 3.48 2.36 o 4 8 6 235.78 234.15 3.90 o 5 8 6 2.27 7.05 3.17 o 6 8 6 255.18 229.99 5.87 o 1 9 6 7.82 9.64 2.44 o 2 9 6 51.68 50.38 3.16 o 3 9 6 102.30 113.55 3.00 o 4 9 6 0.09 0.61 2.83 o 5 9 6 156.11 145.19 6.50 o 0 10 6 15.30 19.71 4.10 o 1 10 6 1.63 -2.38 2.38 o 2 10 6 238.21 278.58 6.01 o 3 10 6 6.95 6.97 3.58 o 0 1 7 639.67 679.78 9.13 o 1 1 7 1101.75 1159.92 15.13 o 1 2 7 1363.76 1405.42 12.88 o 2 2 7 644.41 596.28 8.15 o 0 3 7 1201.30 1184.76 15.50 o 1 3 7 53.70 41.11 1.00 o 2 3 7 614.25 590.21 6.19 o 3 3 7 112.56 109.70 3.95 o 1 4 7 1729.27 1736.31 15.92 o 2 4 7 424.85 463.32 5.54 o 3 4 7 166.53 164.52 4.28 o 4 4 7 8.38 14.88 4.26 o 0 5 7 1002.20 997.64 18.60 o 1 5 7 127.32 136.24 2.34 o 2 5 7 226.35 221.26 3.26 o 3 5 7 409.93 418.69 5.05 o 4 5 7 172.18 182.30 3.03 o 5 5 7 109.30 111.96 4.47 o 1 6 7 102.78 103.57 2.87 o 2 6 7 326.38 323.22 7.78 o 3 6 7 374.24 385.69 4.71 o 4 6 7 110.08 113.78 3.89 o 5 6 7 480.46 481.80 6.66 o 6 6 7 194.53 174.65 5.19 o 0 7 7 80.93 75.52 3.98 o 1 7 7 16.77 15.61 1.81 o 2 7 7 392.79 435.03 6.28 o 3 7 7 4.31 0.98 1.32 o 4 7 7 529.37 564.89 7.61 o 5 7 7 31.06 31.71 3.17 o 6 7 7 164.74 157.09 3.30 o 7 7 7 5.47 2.38 8.79 o 1 8 7 11.04 7.79 2.32 o 2 8 7 90.25 108.94 3.06 o 3 8 7 396.29 426.97 6.47 o 4 8 7 0.09 0.08 1.41 o 5 8 7 228.13 249.70 4.79 o 6 8 7 38.95 49.81 2.36 o 0 9 7 145.53 168.00 6.55 o 1 9 7 160.47 188.48 5.96 o 2 9 7 197.39 223.13 5.24 o 3 9 7 18.72 15.82 2.77 o 4 9 7 176.68 176.93 3.81 o 1 10 7 144.70 198.23 5.41 o 2 10 7 20.85 22.64 3.77 o 0 0 8 6225.21 6509.11 164.29 o 1 1 8 2091.99 2229.38 28.60 o 0 2 8 411.16 403.99 5.83 o 1 2 8 48.62 40.62 1.07 o 2 2 8 1619.25 1647.70 21.35 o 1 3 8 28.66 26.27 0.97 o 2 3 8 661.35 723.95 8.18 o 3 3 8 499.94 472.49 8.06 o 0 4 8 225.99 219.25 3.70 o 1 4 8 94.69 93.52 1.93 o 2 4 8 1246.93 1247.95 13.60 o 3 4 8 107.21 98.66 2.23 o 4 4 8 3306.79 3379.61 43.46 o 1 5 8 2.33 4.03 1.21 o 2 5 8 306.98 339.09 5.12 o 3 5 8 43.14 39.54 2.07 o 4 5 8 49.06 50.23 1.80 o 5 5 8 177.61 162.41 5.97 o 0 6 8 713.66 713.24 14.65 o 1 6 8 319.29 300.22 7.51 o 2 6 8 1017.80 1071.28 12.01 o 3 6 8 239.53 211.97 5.47 o 4 6 8 228.70 224.47 3.37 o 5 6 8 18.10 13.97 1.55 o 6 6 8 275.26 285.56 6.32 o 1 7 8 289.58 270.19 5.18 o 2 7 8 4.72 0.54 1.78 o 3 7 8 2.59 8.13 4.51 o 4 7 8 12.86 9.06 1.63 o 5 7 8 141.91 152.60 3.16 o 6 7 8 14.34 14.94 1.92 o 0 8 8 426.51 448.41 22.11 o 1 8 8 0.12 3.12 2.04 o 2 8 8 65.19 67.40 4.65 o 3 8 8 0.01 0.96 1.86 o 4 8 8 69.73 70.91 2.92 o 5 8 8 11.33 9.25 3.34 o 1 9 8 200.25 222.13 5.72 o 2 9 8 0.05 -0.75 3.23 o 3 9 8 124.43 138.88 4.45 o 4 9 8 0.67 -2.11 2.23 o 0 1 9 729.99 750.26 10.18 o 1 1 9 344.99 360.09 5.40 o 1 2 9 827.89 855.04 8.16 o 2 2 9 40.55 39.93 2.02 o 0 3 9 315.96 331.12 6.33 o 1 3 9 2.80 6.10 1.03 o 2 3 9 428.65 428.43 6.09 o 3 3 9 35.02 32.15 3.87 o 1 4 9 747.28 772.99 8.79 o 2 4 9 175.05 182.78 3.29 o 3 4 9 235.66 229.29 3.55 o 4 4 9 3.87 2.86 2.09 o 0 5 9 137.60 144.98 11.32 o 1 5 9 52.58 52.60 2.01 o 2 5 9 128.42 116.99 2.50 o 3 5 9 65.54 84.92 2.35 o 4 5 9 306.86 279.50 4.19 o 5 5 9 156.30 144.25 3.64 o 1 6 9 247.79 240.41 5.21 o 2 6 9 44.93 62.96 2.10 o 3 6 9 275.37 286.84 4.32 o 4 6 9 22.72 20.90 1.74 o 5 6 9 297.99 308.67 5.48 o 6 6 9 29.77 32.72 3.14 o 0 7 9 53.34 42.19 5.12 o 1 7 9 0.47 -2.69 2.69 o 2 7 9 223.29 203.66 4.59 o 3 7 9 45.92 39.59 2.59 o 4 7 9 295.73 311.81 6.67 o 5 7 9 29.90 22.89 2.17 o 6 7 9 113.47 123.85 3.59 o 1 8 9 70.82 72.93 3.37 o 2 8 9 77.86 82.75 4.99 o 3 8 9 187.20 218.77 5.49 o 4 8 9 0.01 -1.74 1.74 o 5 8 9 88.24 104.69 5.93 o 0 9 9 232.19 257.49 8.60 o 1 9 9 65.37 70.93 4.35 o 2 9 9 167.43 173.79 5.01 o 0 0 10 3331.09 3323.89 84.85 o 1 1 10 900.80 839.84 11.40 o 0 2 10 246.54 248.60 4.12 o 1 2 10 111.49 101.05 1.70 o 2 2 10 711.22 725.37 11.70 o 1 3 10 52.84 61.69 3.05 o 2 3 10 7.34 3.50 1.62 o 3 3 10 1299.46 1384.54 21.40 o 0 4 10 13.48 14.40 2.35 o 1 4 10 169.60 155.85 2.98 o 2 4 10 125.09 125.24 2.54 o 3 4 10 40.42 39.34 1.79 o 4 4 10 683.36 653.32 11.23 o 1 5 10 275.41 318.63 5.55 o 2 5 10 431.81 422.13 6.08 o 3 5 10 753.30 752.73 17.42 o 4 5 10 26.51 17.32 2.26 o 5 5 10 251.23 216.26 5.59 o 0 6 10 205.48 211.93 6.35 o 1 6 10 2.53 -0.08 1.94 o 2 6 10 147.20 141.10 3.69 o 3 6 10 3.70 3.55 1.73 o 4 6 10 23.98 28.51 2.62 o 5 6 10 31.10 34.19 2.72 o 6 6 10 307.07 358.79 10.25 o 1 7 10 401.44 397.23 7.68 o 2 7 10 61.94 39.94 2.90 o 3 7 10 29.13 22.33 2.19 o 4 7 10 6.69 9.81 1.89 o 5 7 10 15.90 11.54 1.82 o 0 8 10 593.79 665.88 33.81 o 1 8 10 2.00 4.18 2.48 o 2 8 10 88.46 86.71 3.99 o 3 8 10 2.80 0.63 2.48 o 4 8 10 55.64 83.74 7.12 o 0 1 11 396.01 342.51 5.39 o 1 1 11 74.90 74.76 3.11 o 1 2 11 174.74 156.19 2.66 o 2 2 11 314.02 351.83 6.52 o 0 3 11 741.93 726.45 16.22 o 1 3 11 31.85 24.10 2.22 o 2 3 11 495.67 500.51 7.25 o 3 3 11 1.53 1.31 3.20 o 1 4 11 87.04 101.50 3.90 o 2 4 11 0.78 2.43 1.31 o 3 4 11 142.78 132.90 3.01 o 4 4 11 9.62 4.86 2.38 o 0 5 11 642.49 670.58 14.05 o 1 5 11 15.95 12.47 1.94 o 2 5 11 283.77 279.63 6.26 o 3 5 11 34.49 30.49 2.21 o 4 5 11 156.36 150.15 3.27 o 5 5 11 144.45 134.22 4.64 o 1 6 11 159.35 176.05 7.80 o 2 6 11 8.18 12.15 2.25 o 3 6 11 138.80 127.72 6.51 o 4 6 11 0.83 -0.63 1.81 o 5 6 11 116.86 103.09 3.04 o 0 7 11 59.78 67.76 4.81 o 1 7 11 5.38 10.15 2.40 o 2 7 11 101.85 109.83 3.77 o 3 7 11 10.84 2.45 3.29 o 4 7 11 92.16 103.11 3.94 o 1 8 11 217.84 232.13 10.20 o 2 8 11 17.03 9.73 2.67 o 0 0 12 1045.27 994.06 27.08 o 1 1 12 559.16 492.42 8.52 o 0 2 12 13.01 9.92 2.10 o 1 2 12 0.78 2.66 1.33 o 2 2 12 144.13 123.00 5.21 o 1 3 12 302.49 286.23 4.90 o 2 3 12 32.52 22.90 2.40 o 3 3 12 899.97 908.33 15.86 o 0 4 12 1.27 2.10 2.21 o 1 4 12 23.06 26.59 2.11 o 2 4 12 49.58 61.29 2.38 o 3 4 12 43.42 49.12 2.29 o 4 4 12 306.16 307.91 8.73 o 1 5 12 351.23 359.69 6.31 o 2 5 12 2.90 3.44 3.05 o 3 5 12 300.30 306.72 5.68 o 4 5 12 1.36 -1.11 1.70 o 5 5 12 198.35 205.26 5.84 o 0 6 12 136.08 161.55 6.05 o 1 6 12 32.12 35.59 3.39 o 2 6 12 126.94 130.09 4.09 o 3 6 12 3.31 7.21 2.98 o 4 6 12 1.92 4.74 3.67 o 1 7 12 359.12 432.72 7.73 o 2 7 12 8.49 4.43 7.40 o 3 7 12 35.79 44.28 3.23 o 0 1 13 109.43 93.70 2.72 o 1 1 13 144.16 136.18 3.68 o 1 2 13 279.71 258.66 4.77 o 2 2 13 5.69 -0.11 3.67 o 0 3 13 47.58 43.29 7.96 o 1 3 13 22.77 29.93 2.29 o 2 3 13 137.67 133.57 3.17 o 3 3 13 118.04 117.39 4.08 o 1 4 13 471.73 471.65 7.67 o 2 4 13 35.84 28.20 2.49 o 3 4 13 126.69 125.98 3.39 o 4 4 13 0.09 0.24 2.68 o 0 5 13 138.71 147.35 5.78 o 1 5 13 0.00 1.84 2.10 o 2 5 13 64.50 68.51 3.12 o 3 5 13 17.50 11.20 2.40 o 4 5 13 50.23 58.58 5.55 o 1 6 13 138.00 141.43 4.27 o 2 6 13 31.20 19.67 2.90 o 3 6 13 60.39 59.19 6.35 o 0 0 14 128.00 141.51 6.80 o 1 1 14 419.81 414.75 7.67 o 0 2 14 28.47 30.18 3.15 o 1 2 14 0.06 -0.21 3.64 o 2 2 14 292.47 302.72 7.15 o 1 3 14 28.80 30.29 4.31 o 2 3 14 0.56 1.51 1.86 o 3 3 14 116.32 123.46 6.94 o 0 4 14 215.04 179.49 6.08 o 1 4 14 5.41 0.13 2.06 o 2 4 14 198.88 180.79 5.25 o 3 4 14 0.00 -2.15 2.30 o 4 4 14 286.44 291.47 8.09 o 1 5 14 52.44 56.98 3.29 o 2 5 14 1.02 2.31 3.68 o 3 5 14 48.99 55.28 3.65 o 0 1 15 112.77 132.25 8.43 o 1 1 15 23.22 25.57 4.61 o 1 2 15 83.77 81.73 3.15 o 2 2 15 69.53 55.77 5.31 o 0 3 15 175.25 174.54 17.54 o 1 3 15 5.06 7.51 2.07 o 2 3 15 139.20 127.63 3.82 o 3 3 15 0.78 0.52 3.86 o 1 4 15 80.60 59.79 4.96 o 2 4 15 0.61 -0.73 2.17 o 1 1 16 0.83 -1.18 4.45 o 0 2 16 200.68 187.34 6.36 o 1 2 16 0.25 -0.55 2.64 o