#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215636.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215636_Fobs loop_ _publ_author_name 'S\/lota, Rudolf' 'Mele, Giuseppe' 'Ejsmont, Krzysztof' 'Doma\'nski, Andrzej A.' 'del Sole, Roberta' _publ_section_title ; [5,10,15,20-Tetrakis(4-tert-butylphenyl)porphyrinato-\k^4^N]zinc(II) toluene solvate ; _journal_coeditor_code PV2028 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2582 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.892 _cell_angle_gamma 90.000 _cell_length_a 16.0277 _cell_length_b 9.5884 _cell_length_c 16.8714 _exptl_crystal_F_000 1040.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file pv2028Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 444.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 20466.34 23400.04 158.24 o 6 0 0 20763.38 22023.26 54.92 o 8 0 0 9773.02 10672.01 183.58 o 10 0 0 6570.35 6644.94 121.84 o 12 0 0 196.01 181.18 20.10 o 14 0 0 112.12 133.57 28.29 o 16 0 0 817.23 962.65 67.73 o 18 0 0 14.23 4.67 29.58 o 2 1 0 239.87 171.80 11.86 o 3 1 0 16151.09 17415.15 364.81 o 4 1 0 13.70 53.80 8.34 o 5 1 0 1319.79 1170.21 28.54 o 6 1 0 1774.04 2091.01 64.84 o 7 1 0 5651.10 5722.13 50.02 o 8 1 0 347.63 280.26 16.16 o 9 1 0 186.28 128.99 11.21 o 10 1 0 206.58 225.95 14.25 o 11 1 0 324.89 289.24 15.31 o 12 1 0 6.95 12.69 8.17 o 13 1 0 166.12 130.55 18.43 o 14 1 0 42.66 52.11 16.86 o 15 1 0 5.27 13.83 16.42 o 16 1 0 105.69 94.72 31.76 o 17 1 0 14.64 42.04 27.11 o 18 1 0 0.00 33.37 30.21 o 0 2 0 197237.64 208291.75 6494.62 o 1 2 0 804.28 831.57 26.23 o 2 2 0 781.16 600.09 11.39 o 3 2 0 521.73 524.38 24.00 o 4 2 0 4871.01 5007.88 73.03 o 5 2 0 2138.41 2062.97 32.42 o 6 2 0 3114.48 3164.93 95.18 o 7 2 0 352.87 380.64 22.76 o 8 2 0 9309.59 9977.25 62.94 o 9 2 0 66.84 90.56 16.30 o 10 2 0 3467.27 3693.52 45.92 o 11 2 0 179.97 179.32 31.28 o 12 2 0 1028.14 1009.33 26.77 o 13 2 0 527.87 526.00 29.93 o 14 2 0 426.97 435.27 32.47 o 15 2 0 522.92 504.51 31.74 o 16 2 0 437.94 536.36 35.69 o 17 2 0 0.52 -2.34 16.74 o 18 2 0 460.51 463.22 71.24 o 1 3 0 43612.70 46585.23 1080.91 o 2 3 0 1.19 7.49 4.51 o 3 3 0 79.30 34.61 7.36 o 4 3 0 128.97 163.74 9.74 o 5 3 0 4381.77 4406.45 170.75 o 6 3 0 489.60 472.49 15.13 o 7 3 0 4597.52 4727.79 193.39 o 8 3 0 714.16 748.26 24.75 o 9 3 0 3843.55 3975.48 191.93 o 10 3 0 35.08 30.69 19.78 o 11 3 0 179.50 184.40 18.38 o 12 3 0 0.44 3.32 7.94 o 13 3 0 1446.01 1426.36 43.33 o 14 3 0 493.40 484.79 38.46 o 15 3 0 493.56 519.67 58.78 o 16 3 0 36.10 42.43 44.38 o 17 3 0 4.40 23.36 22.96 o 18 3 0 12.72 6.62 28.42 o 0 4 0 16425.12 17059.04 329.12 o 1 4 0 399.16 643.09 58.54 o 2 4 0 3992.56 4116.26 78.11 o 3 4 0 30.28 45.03 9.47 o 4 4 0 2256.87 2397.74 75.61 o 5 4 0 118.07 114.89 10.62 o 6 4 0 41.72 12.42 7.22 o 7 4 0 143.86 151.00 13.66 o 8 4 0 6966.27 7285.77 60.50 o 9 4 0 16.47 19.31 8.13 o 10 4 0 1066.57 1095.08 24.64 o 11 4 0 191.58 199.80 21.43 o 12 4 0 997.74 1009.32 46.99 o 13 4 0 366.31 394.62 39.40 o 14 4 0 41.83 54.18 24.20 o 15 4 0 34.00 31.53 35.81 o 16 4 0 12.43 12.07 38.54 o 17 4 0 3.72 12.07 25.69 o 1 5 0 18563.42 19890.90 788.43 o 2 5 0 60.89 51.73 12.14 o 3 5 0 56.13 32.65 10.04 o 4 5 0 207.80 189.29 16.46 o 5 5 0 2116.03 2259.51 57.04 o 6 5 0 0.06 7.17 5.26 o 7 5 0 3461.51 3723.94 51.68 o 8 5 0 330.32 328.84 20.71 o 9 5 0 2360.06 2471.99 57.75 o 10 5 0 21.84 17.21 12.77 o 11 5 0 534.77 514.99 35.05 o 12 5 0 296.61 278.51 30.96 o 13 5 0 454.81 386.07 34.89 o 14 5 0 47.94 57.11 28.76 o 15 5 0 1110.80 1241.98 92.06 o 16 5 0 186.13 172.44 59.95 o 17 5 0 142.22 90.31 43.21 o 0 6 0 24860.94 25180.61 1105.71 o 1 6 0 342.64 1436.71 414.40 o 2 6 0 378.52 425.51 20.92 o 3 6 0 209.75 193.31 16.01 o 4 6 0 1494.78 1593.12 25.97 o 5 6 0 255.51 228.53 18.64 o 6 6 0 836.38 888.44 27.22 o 7 6 0 29.65 36.13 13.56 o 8 6 0 3475.94 3672.34 38.83 o 9 6 0 275.01 247.76 23.01 o 10 6 0 1117.39 1151.80 44.18 o 11 6 0 1.13 8.95 11.29 o 12 6 0 428.10 390.88 33.56 o 13 6 0 55.71 69.80 30.99 o 14 6 0 167.85 82.48 34.30 o 15 6 0 12.72 10.51 29.58 o 16 6 0 42.07 73.57 48.27 o 1 7 0 5891.38 6363.29 262.33 o 2 7 0 441.20 436.47 25.43 o 3 7 0 186.36 188.09 17.04 o 4 7 0 981.65 1064.15 27.40 o 5 7 0 1060.22 1096.09 30.82 o 6 7 0 121.77 118.52 17.56 o 7 7 0 2143.53 2271.14 57.47 o 8 7 0 341.91 371.19 31.65 o 9 7 0 354.77 331.95 32.30 o 10 7 0 0.28 16.89 19.32 o 11 7 0 719.71 716.72 58.61 o 12 7 0 175.66 143.01 35.99 o 13 7 0 4.21 8.40 17.19 o 14 7 0 6.51 9.51 19.17 o 15 7 0 137.11 128.02 32.09 o 0 8 0 28219.30 29109.22 2427.26 o 1 8 0 218.89 1457.43 430.10 o 2 8 0 44.10 320.07 98.28 o 3 8 0 723.39 693.14 28.68 o 4 8 0 1139.85 1104.83 59.76 o 5 8 0 30.47 10.30 9.28 o 6 8 0 1228.92 1223.02 39.41 o 7 8 0 34.21 59.32 15.81 o 8 8 0 1332.93 1405.70 65.17 o 9 8 0 41.18 56.31 28.32 o 10 8 0 1532.74 1488.82 65.92 o 11 8 0 111.48 130.86 46.16 o 12 8 0 26.21 18.45 21.57 o 13 8 0 0.47 10.90 15.61 o 1 9 0 1999.39 1799.75 64.22 o 2 9 0 803.71 916.37 46.10 o 3 9 0 108.69 100.27 20.77 o 4 9 0 221.85 162.86 28.74 o 5 9 0 580.06 600.43 34.87 o 6 9 0 94.61 86.78 20.69 o 7 9 0 968.83 913.12 39.85 o 8 9 0 0.68 16.73 17.73 o 9 9 0 287.65 375.10 43.28 o 10 9 0 0.05 6.15 18.33 o 11 9 0 686.57 720.82 59.97 o 0 10 0 9600.63 9712.15 152.59 o 1 10 0 56.78 77.62 67.93 o 2 10 0 12.77 34.27 23.18 o 3 10 0 483.65 427.77 49.68 o 4 10 0 745.72 787.59 49.37 o 5 10 0 131.93 122.12 27.43 o 6 10 0 237.62 196.53 29.88 o 7 10 0 0.13 21.75 18.06 o 8 10 0 752.62 682.32 47.62 o 9 10 0 46.87 50.21 20.19 o 1 11 0 2205.71 2326.06 87.70 o 2 11 0 16.88 16.57 23.20 o 3 11 0 18.46 22.45 24.03 o 4 11 0 94.96 84.49 35.81 o 5 11 0 652.44 549.18 57.86 o -19 0 1 105.30 62.28 47.88 o -17 0 1 483.09 546.92 76.69 o -15 0 1 179.17 229.89 32.69 o -13 0 1 29.08 8.30 11.60 o -11 0 1 9028.83 8510.27 118.92 o -9 0 1 643.95 567.94 21.54 o -7 0 1 742.80 613.26 26.38 o -5 0 1 262.46 131.34 11.71 o -3 0 1 13897.83 10363.28 848.40 o 3 0 1 475.99 217.99 26.47 o 5 0 1 1889.51 2510.55 27.05 o 7 0 1 9557.72 9910.61 57.22 o 9 0 1 68.49 80.73 13.25 o 11 0 1 37.27 32.00 10.08 o 13 0 1 404.96 378.07 30.59 o 15 0 1 1877.60 2093.85 88.75 o 17 0 1 116.00 99.65 30.36 o -18 1 1 632.61 672.20 53.58 o -17 1 1 4.62 8.99 14.68 o -16 1 1 749.73 835.31 56.69 o -15 1 1 55.93 43.29 16.55 o -14 1 1 184.12 148.75 24.92 o -13 1 1 748.03 794.97 29.82 o -12 1 1 2063.02 1953.21 53.71 o -11 1 1 47.23 61.96 12.69 o -10 1 1 1635.20 1510.30 40.02 o -9 1 1 1139.16 1194.51 20.01 o -8 1 1 8384.54 8599.28 207.47 o -7 1 1 1138.46 1328.42 62.37 o -6 1 1 3623.76 3816.88 141.31 o -5 1 1 4925.95 5292.54 227.94 o -4 1 1 22214.94 23787.46 57.83 o -3 1 1 1.82 40.16 14.72 o -2 1 1 13.79 14.85 6.57 o 2 1 1 29960.91 30940.70 1186.79 o 3 1 1 158.47 282.30 19.05 o 4 1 1 2103.91 2067.42 40.60 o 5 1 1 2913.69 3364.58 41.42 o 6 1 1 3902.01 4163.36 77.11 o 7 1 1 594.78 555.85 24.95 o 8 1 1 4187.92 4513.81 73.28 o 9 1 1 779.15 781.20 42.70 o 10 1 1 2126.21 2301.72 70.96 o 11 1 1 276.73 261.02 16.33 o 12 1 1 996.39 947.31 20.12 o 13 1 1 58.64 31.49 12.05 o 14 1 1 245.90 202.79 22.79 o 15 1 1 67.05 68.33 30.03 o 16 1 1 2970.95 3262.54 75.00 o 17 1 1 165.95 163.87 39.21 o 18 1 1 272.08 278.26 44.80 o -18 2 1 5.87 22.19 43.21 o -17 2 1 245.94 254.08 38.35 o -16 2 1 45.29 51.27 29.86 o -15 2 1 201.43 361.25 35.50 o -14 2 1 1356.06 1476.43 37.04 o -13 2 1 8.56 21.62 16.39 o -12 2 1 0.21 6.12 8.51 o -11 2 1 5017.00 5281.35 98.68 o -10 2 1 1035.35 1070.16 37.31 o -9 2 1 238.22 218.55 17.41 o -8 2 1 1922.69 2071.36 25.59 o -7 2 1 5963.09 6437.44 191.48 o -6 2 1 200.91 227.77 14.15 o -5 2 1 1255.76 1335.69 22.38 o -4 2 1 3233.26 3389.10 35.47 o -3 2 1 4410.56 4735.85 106.95 o -2 2 1 196.85 173.12 9.37 o -1 2 1 17130.16 19340.79 550.08 o 0 2 1 2101.20 2120.83 56.86 o 1 2 1 13603.83 14627.87 427.87 o 2 2 1 2548.36 2431.85 101.18 o 3 2 1 255.24 277.25 13.44 o 4 2 1 46.10 50.02 9.35 o 5 2 1 66.43 37.34 7.00 o 6 2 1 22.21 9.59 5.49 o 7 2 1 5887.24 5878.97 51.19 o 8 2 1 1368.60 1461.86 25.84 o 9 2 1 315.15 283.38 17.28 o 10 2 1 7.00 10.47 7.18 o 11 2 1 747.11 631.90 21.36 o 12 2 1 284.82 278.56 20.87 o 13 2 1 800.17 774.38 39.01 o 14 2 1 32.44 36.30 21.63 o 15 2 1 857.37 895.29 38.03 o 16 2 1 41.58 60.49 31.09 o 17 2 1 212.18 290.15 42.28 o 18 2 1 122.90 151.42 66.56 o -18 3 1 300.65 282.04 49.49 o -17 3 1 3.60 23.10 22.67 o -16 3 1 756.00 817.69 50.21 o -15 3 1 0.86 1.17 18.30 o -14 3 1 1102.95 898.42 66.56 o -13 3 1 372.38 400.61 25.11 o -12 3 1 3648.64 3722.10 41.55 o -11 3 1 12.24 13.42 10.59 o -10 3 1 849.72 749.17 31.07 o -9 3 1 393.28 446.94 21.76 o -8 3 1 4768.96 4882.19 80.95 o -7 3 1 196.86 265.35 15.91 o -6 3 1 4099.58 4197.57 98.28 o -5 3 1 1033.10 1054.67 22.47 o -4 3 1 995.38 865.60 16.59 o -3 3 1 169.84 168.16 14.25 o -2 3 1 3852.61 3954.62 83.01 o -1 3 1 245.65 558.24 106.33 o 0 3 1 44918.18 48567.82 316.18 o 1 3 1 82.14 187.03 40.85 o 2 3 1 2234.36 2239.41 84.12 o 3 3 1 63.41 82.85 9.75 o 4 3 1 7149.27 7446.28 166.20 o 5 3 1 974.10 836.72 14.52 o 6 3 1 1565.68 1672.45 72.62 o 7 3 1 1100.43 1164.85 28.09 o 8 3 1 2227.64 2235.81 36.82 o 9 3 1 0.56 4.66 5.25 o 10 3 1 685.97 701.50 22.96 o 11 3 1 145.96 135.80 14.74 o 12 3 1 18.44 14.87 11.04 o 13 3 1 151.22 138.33 26.15 o 14 3 1 1053.35 1030.02 37.72 o 15 3 1 21.53 43.28 28.51 o 16 3 1 2527.48 2661.01 105.88 o 17 3 1 290.76 305.18 74.74 o 18 3 1 70.64 57.22 42.04 o -17 4 1 325.80 284.55 53.72 o -16 4 1 91.30 58.39 37.37 o -15 4 1 686.29 651.24 72.01 o -14 4 1 54.88 38.09 25.13 o -13 4 1 468.97 558.84 42.27 o -12 4 1 116.83 84.60 21.25 o -11 4 1 2923.08 2879.47 77.42 o -10 4 1 55.63 40.33 13.45 o -9 4 1 24.42 19.55 9.85 o -8 4 1 189.82 235.74 16.95 o -7 4 1 8167.60 8906.23 43.31 o -6 4 1 219.71 270.36 15.65 o -5 4 1 2522.91 2674.78 87.01 o -4 4 1 325.55 277.97 14.75 o -3 4 1 290.68 265.24 13.24 o -2 4 1 660.60 686.20 18.19 o -1 4 1 6323.59 6942.07 197.08 o 0 4 1 567.27 731.13 93.04 o 1 4 1 5818.66 5672.48 184.50 o 2 4 1 1374.36 1512.41 50.24 o 3 4 1 234.45 234.82 13.12 o 4 4 1 12.89 18.25 7.40 o 5 4 1 23.69 34.33 10.19 o 6 4 1 256.61 217.39 101.66 o 7 4 1 2597.88 2719.10 35.65 o 8 4 1 30.16 29.89 9.04 o 9 4 1 1047.70 1132.11 31.54 o 10 4 1 55.49 59.46 15.06 o 11 4 1 2217.39 2491.70 56.51 o 12 4 1 0.20 5.30 12.29 o 13 4 1 514.92 474.27 43.67 o 14 4 1 9.56 21.43 17.66 o 15 4 1 867.24 950.19 104.32 o 16 4 1 3.40 17.52 43.99 o 17 4 1 660.25 662.53 86.81 o -17 5 1 27.17 17.82 21.73 o -16 5 1 403.52 411.62 54.42 o -15 5 1 152.56 121.08 32.42 o -14 5 1 1180.58 952.41 50.08 o -13 5 1 236.89 224.27 27.57 o -12 5 1 2509.52 2641.55 71.75 o -11 5 1 18.43 19.44 12.56 o -10 5 1 451.85 385.84 23.08 o -9 5 1 0.07 9.11 8.38 o -8 5 1 2577.36 2720.59 37.07 o -7 5 1 120.45 126.28 18.75 o -6 5 1 3074.68 3138.09 38.55 o -5 5 1 345.40 329.75 13.12 o -4 5 1 360.33 283.66 16.68 o -3 5 1 12.75 20.09 8.18 o -2 5 1 1562.78 1563.03 61.67 o -1 5 1 3.32 61.18 23.17 o 0 5 1 24592.75 25385.70 331.44 o 1 5 1 154.40 1129.95 332.58 o 2 5 1 7.38 103.63 37.53 o 3 5 1 65.02 71.81 11.18 o 4 5 1 5067.62 5582.53 124.79 o 5 5 1 39.98 33.86 12.96 o 6 5 1 963.19 928.72 34.50 o 7 5 1 33.21 19.25 7.01 o 8 5 1 2213.86 2344.13 41.37 o 9 5 1 364.63 456.54 33.29 o 10 5 1 149.92 123.71 20.49 o 11 5 1 90.34 91.53 23.46 o 12 5 1 66.22 36.29 17.25 o 13 5 1 847.36 840.80 39.95 o 14 5 1 1036.05 1050.66 116.39 o 15 5 1 27.88 25.76 22.52 o 16 5 1 1011.43 966.93 88.36 o 17 5 1 34.67 43.99 42.43 o -16 6 1 124.06 116.39 58.39 o -15 6 1 169.41 230.44 82.52 o -14 6 1 202.82 163.49 35.35 o -13 6 1 82.74 93.07 28.79 o -12 6 1 3.98 8.30 13.48 o -11 6 1 2863.12 2909.23 139.89 o -10 6 1 56.68 62.19 15.81 o -9 6 1 84.42 78.38 20.97 o -8 6 1 581.43 587.92 34.33 o -7 6 1 3646.31 3785.01 78.69 o -6 6 1 119.35 105.56 14.55 o -5 6 1 3091.38 3322.41 77.98 o -4 6 1 683.25 819.45 50.57 o -3 6 1 1384.48 1249.18 41.77 o -2 6 1 3.20 4.50 6.16 o -1 6 1 5841.51 6246.35 244.80 o 0 6 1 1809.54 1976.91 38.66 o 1 6 1 4444.45 4636.65 43.69 o 2 6 1 445.06 536.58 21.49 o 3 6 1 97.85 67.12 13.86 o 4 6 1 2.62 3.92 5.97 o 5 6 1 26.56 17.37 8.01 o 6 6 1 303.50 276.15 22.33 o 7 6 1 3317.42 3309.03 145.35 o 8 6 1 4.18 17.67 8.28 o 9 6 1 1509.70 1584.33 38.12 o 10 6 1 571.04 568.89 33.65 o 11 6 1 347.33 309.77 41.82 o 12 6 1 6.50 5.16 15.78 o 13 6 1 61.31 11.40 17.24 o 14 6 1 37.25 206.48 213.32 o 15 6 1 1580.15 1627.67 83.11 o 16 6 1 0.03 17.13 37.76 o -15 7 1 177.64 180.62 76.69 o -14 7 1 35.55 33.82 25.63 o -13 7 1 190.73 136.63 37.45 o -12 7 1 947.04 1023.17 61.79 o -11 7 1 37.65 32.08 20.73 o -10 7 1 425.23 374.09 28.86 o -9 7 1 53.58 26.42 13.11 o -8 7 1 1012.55 978.13 38.20 o -7 7 1 14.83 12.80 9.94 o -6 7 1 977.89 963.32 28.24 o -5 7 1 133.03 87.15 16.62 o -4 7 1 534.40 525.25 23.54 o -3 7 1 43.38 37.04 12.05 o -2 7 1 155.76 118.56 16.77 o -1 7 1 21.37 18.18 9.87 o 0 7 1 4834.46 5305.26 120.41 o 1 7 1 341.20 324.73 21.65 o 2 7 1 1801.23 1839.30 43.79 o 3 7 1 478.85 436.70 22.79 o 4 7 1 26.68 23.55 10.42 o 5 7 1 163.19 160.71 18.04 o 6 7 1 488.25 504.65 25.35 o 7 7 1 52.34 43.59 22.69 o 8 7 1 1492.41 1592.55 52.96 o 9 7 1 17.70 44.04 20.38 o 10 7 1 99.24 88.65 31.33 o 11 7 1 12.93 11.24 14.56 o 12 7 1 10.14 16.39 17.76 o 13 7 1 463.12 495.06 58.19 o 14 7 1 350.63 337.26 52.85 o -13 8 1 8.47 19.01 18.29 o -12 8 1 13.26 16.23 22.53 o -11 8 1 2301.00 2274.86 307.71 o -10 8 1 118.67 120.13 42.04 o -9 8 1 210.92 224.53 48.58 o -8 8 1 545.34 554.24 44.22 o -7 8 1 1776.73 1867.78 49.39 o -6 8 1 29.38 23.49 11.90 o -5 8 1 1587.37 1850.83 53.01 o -4 8 1 88.73 71.45 16.72 o -3 8 1 1507.04 1765.61 41.96 o -2 8 1 68.37 81.48 21.28 o -1 8 1 5125.19 5762.63 366.89 o 0 8 1 4747.21 5685.35 58.18 o 1 8 1 2536.66 3308.68 255.08 o 2 8 1 16.47 15.27 9.40 o 3 8 1 246.32 254.78 20.84 o 4 8 1 160.82 120.33 24.24 o 5 8 1 154.29 212.15 26.97 o 6 8 1 1152.15 1277.85 40.70 o 7 8 1 2897.05 2980.28 109.02 o 8 8 1 0.28 17.93 17.43 o 9 8 1 769.75 929.39 68.59 o 10 8 1 289.82 280.81 46.43 o 11 8 1 30.13 31.81 22.68 o 12 8 1 13.33 2.62 14.63 o 13 8 1 7.80 12.04 20.08 o -11 9 1 246.44 278.78 46.52 o -10 9 1 108.39 106.66 39.65 o -9 9 1 69.51 39.51 25.52 o -8 9 1 1154.34 1045.67 104.85 o -7 9 1 22.74 27.18 14.67 o -6 9 1 431.15 336.51 40.13 o -5 9 1 67.83 26.25 17.58 o -4 9 1 780.31 753.22 32.69 o -3 9 1 48.72 39.87 15.80 o -2 9 1 41.40 29.74 13.31 o -1 9 1 47.33 49.16 18.60 o 0 9 1 2772.30 2548.61 122.10 o 1 9 1 450.46 439.98 41.86 o 2 9 1 1230.65 1218.98 50.14 o 3 9 1 548.55 544.98 43.71 o 4 9 1 60.10 45.81 16.42 o 5 9 1 16.66 18.94 14.33 o 6 9 1 767.94 770.61 41.55 o 7 9 1 115.33 139.36 29.54 o 8 9 1 418.22 388.98 39.80 o 9 9 1 625.29 655.68 60.56 o 10 9 1 216.19 228.54 49.08 o 11 9 1 53.90 20.07 21.03 o -9 10 1 83.38 141.64 46.39 o -8 10 1 201.34 152.25 32.70 o -7 10 1 964.04 894.51 43.63 o -6 10 1 33.31 15.51 13.99 o -5 10 1 230.65 185.22 26.22 o -4 10 1 100.24 77.16 35.30 o -3 10 1 179.38 185.45 37.28 o -2 10 1 34.27 231.15 93.42 o -1 10 1 2063.64 2150.22 73.99 o 0 10 1 1879.00 2233.34 85.18 o 1 10 1 1208.74 1317.61 70.18 o 2 10 1 17.13 22.33 15.25 o 3 10 1 27.36 27.35 18.76 o 4 10 1 1.84 11.48 13.63 o 5 10 1 265.63 258.29 46.37 o 6 10 1 283.93 249.72 41.65 o 7 10 1 1301.52 1326.33 89.53 o 8 10 1 88.80 76.77 27.17 o 9 10 1 113.50 81.82 23.97 o -4 11 1 500.81 537.92 55.66 o -3 11 1 0.47 4.78 18.01 o -2 11 1 267.07 366.69 55.70 o -1 11 1 376.61 384.23 53.70 o 0 11 1 3020.45 3249.78 87.38 o 1 11 1 144.11 133.67 47.88 o 2 11 1 5.72 28.34 34.84 o 3 11 1 40.90 20.38 22.00 o 4 11 1 396.31 511.85 48.86 o -18 0 2 28.31 7.01 23.36 o -16 0 2 1092.25 989.01 51.44 o -14 0 2 394.99 387.18 36.98 o -12 0 2 3966.59 3957.43 237.26 o -10 0 2 506.36 470.85 28.54 o -8 0 2 3565.47 3482.48 92.60 o -6 0 2 10582.49 11347.01 269.18 o -4 0 2 24552.65 24958.81 339.05 o -2 0 2 12.02 64.04 9.71 o 2 0 2 1912.01 1585.72 55.28 o 4 0 2 43104.26 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