#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215666.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215666_Fobs loop_ _publ_author_name 'Diao, Yun-Peng' 'Li, Kun' _publ_section_title ; Aqua(azido)(\m-azido)bis{2-[(2-dimethylaminoethylimino)methyl]-6-methoxyphenolato}dicopper(II) monohydrate ; _journal_coeditor_code SJ2351 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2496 _journal_page_last m2497 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.821 _cell_angle_gamma 90.000 _cell_length_a 16.2320 _cell_length_b 13.5400 _cell_length_c 13.9970 _exptl_crystal_F_000 1432.00 _reflns_d_resolution_high 0.7492 _[local]_cod_data_source_file sj2351Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' b in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 333.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 32.61 -12.41 12.41 o 2 0 0 109880.37 116618.27 5006.05 o 3 0 0 1245.57 1774.23 76.35 o 4 0 0 5015.81 6166.05 234.59 o 5 0 0 1087.18 1044.22 61.78 o 6 0 0 2257.79 2177.96 103.01 o 7 0 0 482.41 580.20 86.40 o 8 0 0 869.08 1044.24 134.57 o 9 0 0 137.25 191.20 38.12 o 10 0 0 3183.49 2891.12 148.38 o 11 0 0 652.00 834.97 79.08 o 12 0 0 6726.74 6106.08 337.34 o 13 0 0 2485.37 2789.07 348.57 o 14 0 0 867.93 842.86 195.46 o 15 0 0 1058.86 992.54 195.94 o 16 0 0 268.20 423.28 97.58 o 17 0 0 167.42 208.20 79.80 o 18 0 0 246.94 413.40 155.64 o 19 0 0 556.39 463.91 186.58 o 20 0 0 422.23 466.57 179.33 o 1 1 0 8931.08 9602.75 295.88 o 2 1 0 3109.04 2951.69 80.08 o 3 1 0 2183.49 2252.20 66.16 o 4 1 0 5707.64 7513.86 199.03 o 5 1 0 2206.51 2309.51 73.74 o 6 1 0 3168.01 3045.06 105.74 o 7 1 0 639.64 705.01 72.06 o 8 1 0 7107.30 6805.66 194.09 o 9 1 0 52.88 55.16 21.00 o 10 1 0 5917.08 6226.26 185.07 o 11 1 0 40.82 14.41 27.13 o 12 1 0 335.13 328.62 53.88 o 13 1 0 97.67 90.82 42.74 o 14 1 0 535.22 462.20 63.40 o 15 1 0 26.32 44.93 51.16 o 16 1 0 14.67 57.84 45.24 o 17 1 0 1.88 -13.91 50.95 o 18 1 0 172.56 136.58 65.88 o 19 1 0 3.22 227.37 103.50 o 20 1 0 27.19 361.67 110.33 o 1 2 0 3159.87 3251.24 97.96 o 2 2 0 5121.53 4895.62 144.58 o 3 2 0 6318.77 6749.24 179.12 o 4 2 0 1165.00 1378.16 49.13 o 5 2 0 146.49 179.61 26.46 o 6 2 0 2231.86 2401.12 78.96 o 7 2 0 6.26 6.92 14.38 o 8 2 0 737.52 704.24 42.49 o 9 2 0 4.08 -3.66 17.28 o 10 2 0 185.16 258.47 39.51 o 11 2 0 300.29 230.35 38.68 o 12 2 0 413.78 493.04 53.35 o 13 2 0 7.03 10.21 30.17 o 14 2 0 1761.42 1805.96 123.40 o 15 2 0 142.44 97.92 59.60 o 16 2 0 144.41 153.48 64.35 o 17 2 0 105.29 163.37 66.48 o 18 2 0 5.69 40.85 60.60 o 19 2 0 206.54 242.89 77.37 o 20 2 0 0.31 27.22 94.07 o 1 3 0 626.08 756.80 41.82 o 2 3 0 12656.04 12621.21 401.39 o 3 3 0 3126.34 3581.15 102.32 o 4 3 0 13807.57 13293.90 344.16 o 5 3 0 3686.43 4632.26 132.76 o 6 3 0 23483.23 23141.39 594.36 o 7 3 0 3820.53 3804.07 116.44 o 8 3 0 15434.98 14659.59 390.18 o 9 3 0 3199.50 3112.16 136.89 o 10 3 0 9608.94 10256.07 319.69 o 11 3 0 580.36 696.28 60.09 o 12 3 0 1985.31 1906.16 127.80 o 13 3 0 35.26 86.02 52.64 o 14 3 0 175.00 192.78 56.12 o 15 3 0 151.75 185.04 60.99 o 16 3 0 0.48 34.69 52.84 o 17 3 0 119.29 63.64 58.87 o 18 3 0 7.91 67.27 64.82 o 19 3 0 51.15 33.22 67.37 o 20 3 0 90.74 49.42 111.29 o 0 4 0 34.62 175.51 28.51 o 1 4 0 1.84 17.99 12.84 o 2 4 0 2616.87 2440.79 85.54 o 3 4 0 240.39 360.84 31.36 o 4 4 0 25708.83 27637.21 771.17 o 5 4 0 391.24 420.70 31.79 o 6 4 0 6580.68 6485.54 182.26 o 7 4 0 541.24 649.99 36.70 o 8 4 0 247.15 312.47 27.96 o 9 4 0 3597.13 3607.76 134.68 o 10 4 0 1343.33 1321.51 80.77 o 11 4 0 471.21 425.19 57.94 o 12 4 0 580.45 549.69 65.61 o 13 4 0 106.20 172.72 47.64 o 14 4 0 381.51 270.75 55.59 o 15 4 0 1385.45 1203.15 203.35 o 16 4 0 1273.15 1337.16 228.30 o 17 4 0 502.43 708.29 177.91 o 18 4 0 98.17 149.95 69.34 o 19 4 0 55.16 31.94 66.92 o 1 5 0 612.71 673.98 38.19 o 2 5 0 47.01 40.98 14.26 o 3 5 0 1294.35 1298.20 62.93 o 4 5 0 986.07 998.42 59.97 o 5 5 0 1401.31 1359.17 67.21 o 6 5 0 2239.23 2089.49 76.15 o 7 5 0 1828.01 1832.77 99.17 o 8 5 0 2523.58 2490.92 105.20 o 9 5 0 3048.51 2822.82 182.73 o 10 5 0 384.17 416.29 72.92 o 11 5 0 778.19 680.11 79.85 o 12 5 0 1792.35 1922.39 127.59 o 13 5 0 3.74 15.37 38.90 o 14 5 0 309.01 458.87 91.95 o 15 5 0 6.52 17.07 42.03 o 16 5 0 685.79 631.16 100.20 o 17 5 0 26.29 -8.04 60.25 o 18 5 0 27.29 64.04 69.04 o 19 5 0 5.49 64.33 65.89 o 0 6 0 5770.89 5596.63 228.27 o 1 6 0 730.72 903.69 68.31 o 2 6 0 16697.19 14530.93 381.56 o 3 6 0 255.13 276.47 32.60 o 4 6 0 9097.97 7887.30 244.16 o 5 6 0 27.16 51.33 22.50 o 6 6 0 3315.60 2975.36 111.44 o 7 6 0 1.91 -4.46 20.45 o 8 6 0 151.02 97.53 45.78 o 9 6 0 92.44 93.63 36.81 o 10 6 0 436.54 487.46 61.37 o 11 6 0 25.33 50.41 36.83 o 12 6 0 99.75 64.14 39.72 o 13 6 0 559.03 524.05 70.46 o 14 6 0 1271.11 1405.77 115.52 o 15 6 0 126.86 161.21 67.15 o 16 6 0 1046.90 1179.88 131.83 o 17 6 0 501.60 562.81 97.94 o 18 6 0 1037.00 825.82 117.66 o 19 6 0 253.60 633.08 192.74 o 1 7 0 430.89 965.45 71.45 o 2 7 0 42.20 62.31 18.88 o 3 7 0 45.80 28.57 23.16 o 4 7 0 1468.40 1497.43 79.70 o 5 7 0 1589.32 1741.63 157.19 o 6 7 0 5891.05 5856.78 195.99 o 7 7 0 1518.00 1353.55 141.37 o 8 7 0 4044.05 3826.48 169.33 o 9 7 0 9.23 45.45 36.26 o 10 7 0 1424.40 1301.28 101.24 o 11 7 0 18.40 20.10 58.24 o 12 7 0 1722.13 1584.34 119.01 o 13 7 0 58.02 67.29 45.24 o 14 7 0 11.96 58.08 46.64 o 15 7 0 4.02 -39.08 39.08 o 16 7 0 195.88 225.25 59.84 o 17 7 0 468.37 571.30 101.81 o 18 7 0 9.16 91.18 69.32 o 0 8 0 11694.24 12778.92 491.01 o 1 8 0 2032.38 2274.26 88.68 o 2 8 0 2680.87 2759.80 111.06 o 3 8 0 3534.20 3285.59 125.49 o 4 8 0 2.84 6.97 26.95 o 5 8 0 1037.41 896.83 86.25 o 6 8 0 334.06 398.07 55.05 o 7 8 0 919.08 935.54 82.87 o 8 8 0 5.23 -9.72 49.05 o 9 8 0 194.72 205.99 66.91 o 10 8 0 469.33 551.80 69.03 o 11 8 0 88.84 -5.98 35.48 o 12 8 0 1493.58 1476.70 223.94 o 13 8 0 52.52 37.81 48.94 o 14 8 0 289.82 312.26 63.09 o 15 8 0 394.20 270.91 64.92 o 16 8 0 2.53 47.40 51.32 o 17 8 0 151.83 100.40 85.04 o 18 8 0 7.93 -90.15 114.56 o 1 9 0 569.66 490.54 41.62 o 2 9 0 50.85 5.44 25.81 o 3 9 0 59.52 82.99 32.71 o 4 9 0 1834.25 1556.63 107.42 o 5 9 0 769.04 743.65 70.76 o 6 9 0 3285.43 2934.68 187.22 o 7 9 0 109.74 135.76 41.91 o 8 9 0 4908.37 4537.87 285.16 o 9 9 0 528.74 508.42 68.58 o 10 9 0 3642.75 3310.35 180.95 o 11 9 0 853.85 909.84 92.73 o 12 9 0 2224.95 2090.62 157.78 o 13 9 0 583.53 507.99 72.73 o 14 9 0 210.97 295.00 63.87 o 15 9 0 149.80 90.31 52.00 o 16 9 0 107.02 21.33 58.82 o 17 9 0 81.43 27.63 64.22 o 0 10 0 4780.01 4758.11 279.82 o 1 10 0 8.78 -28.63 28.63 o 2 10 0 8678.48 8477.86 423.48 o 3 10 0 31.80 8.49 31.90 o 4 10 0 3706.28 3548.91 156.16 o 5 10 0 2.73 -19.34 36.82 o 6 10 0 973.14 939.85 85.58 o 7 10 0 26.15 82.71 40.12 o 8 10 0 253.84 316.50 58.02 o 9 10 0 1107.76 802.57 85.63 o 10 10 0 22.72 80.36 45.34 o 11 10 0 1556.30 1564.39 125.54 o 12 10 0 690.67 850.77 92.97 o 13 10 0 228.70 179.85 57.34 o 14 10 0 347.49 242.81 99.89 o 15 10 0 190.56 310.28 69.29 o 16 10 0 117.83 185.60 67.22 o 17 10 0 160.58 133.17 129.42 o 1 11 0 823.98 936.54 89.39 o 2 11 0 82.55 100.65 41.01 o 3 11 0 1201.39 1281.24 99.76 o 4 11 0 513.06 398.26 56.27 o 5 11 0 1.49 -6.86 37.28 o 6 11 0 560.85 478.79 63.61 o 7 11 0 305.44 344.27 83.56 o 8 11 0 672.15 590.52 75.80 o 9 11 0 119.74 98.85 63.00 o 10 11 0 227.47 221.25 54.02 o 11 11 0 261.79 249.43 59.77 o 12 11 0 109.16 77.86 57.09 o 13 11 0 202.51 264.87 64.14 o 14 11 0 4.26 20.38 53.90 o 15 11 0 81.91 126.08 69.02 o 16 11 0 54.72 3.19 138.60 o 0 12 0 7535.02 7305.17 408.96 o 1 12 0 57.24 -8.34 44.96 o 2 12 0 4196.02 3792.57 193.53 o 3 12 0 1.21 -28.75 43.60 o 4 12 0 1328.22 1296.07 106.40 o 5 12 0 189.25 252.99 74.49 o 6 12 0 113.92 70.39 41.88 o 7 12 0 374.67 273.05 68.48 o 8 12 0 320.63 226.30 55.89 o 9 12 0 0.30 26.47 42.52 o 10 12 0 511.86 497.71 74.19 o 11 12 0 188.10 149.04 52.56 o 12 12 0 450.03 393.49 71.68 o 13 12 0 22.45 157.87 63.19 o 14 12 0 185.98 255.89 72.84 o 15 12 0 103.65 180.29 139.33 o 1 13 0 1227.49 1139.59 111.96 o 2 13 0 409.30 387.85 107.79 o 3 13 0 412.45 394.81 89.82 o 4 13 0 1091.96 1161.95 140.58 o 5 13 0 160.21 282.06 81.44 o 6 13 0 642.33 584.12 76.77 o 7 13 0 153.41 161.78 53.22 o 8 13 0 1040.45 907.99 95.74 o 9 13 0 135.74 139.57 72.80 o 10 13 0 969.98 819.61 95.00 o 11 13 0 88.10 101.54 71.02 o 12 13 0 192.06 169.96 66.19 o 13 13 0 101.04 36.98 64.36 o 0 14 0 89.30 122.71 101.20 o 1 14 0 0.34 -18.73 59.88 o 2 14 0 3.83 -27.17 54.85 o 3 14 0 28.76 17.87 66.48 o 4 14 0 19.37 40.48 69.12 o 5 14 0 498.63 472.35 97.47 o 6 14 0 114.05 39.51 62.00 o 7 14 0 395.33 437.39 105.69 o 8 14 0 273.14 191.24 71.60 o 9 14 0 238.74 363.35 73.40 o 10 14 0 93.02 129.40 56.63 o 11 14 0 276.08 190.58 65.39 o 12 14 0 1.20 -21.62 71.48 o 1 15 0 4.85 29.68 64.32 o 2 15 0 624.08 584.71 111.34 o 3 15 0 40.33 156.29 84.22 o 4 15 0 2016.00 1986.59 337.62 o 5 15 0 50.92 49.71 80.69 o 6 15 0 1490.76 1626.56 200.71 o 7 15 0 214.47 260.77 82.83 o 8 15 0 710.56 978.27 171.91 o 9 15 0 93.01 224.06 88.25 o 10 15 0 275.84 437.81 147.18 o 11 15 0 46.95 59.33 105.01 o 0 16 0 389.07 441.83 134.66 o 1 16 0 24.07 9.97 80.86 o 2 16 0 358.76 484.15 111.42 o 3 16 0 4.18 -15.15 78.91 o 4 16 0 147.61 305.68 100.01 o 5 16 0 80.58 -85.29 85.29 o 6 16 0 206.23 159.72 90.44 o 7 16 0 285.75 189.29 84.35 o 8 16 0 95.90 441.67 150.81 o 1 17 0 590.26 618.49 163.95 o 2 17 0 34.75 162.12 97.18 o 3 17 0 250.51 184.68 94.55 o 4 17 0 29.30 -71.96 83.20 o 5 17 0 24.33 60.06 170.51 o -20 1 1 1.82 83.59 86.16 o -19 1 1 1000.55 1104.79 153.59 o -18 1 1 19.68 243.96 68.89 o -17 1 1 976.13 949.55 110.88 o -16 1 1 195.10 123.27 67.31 o -15 1 1 722.41 739.19 83.98 o -14 1 1 237.00 229.92 51.01 o -13 1 1 1092.34 1133.57 79.31 o -12 1 1 88.53 84.81 32.00 o -11 1 1 155.84 157.73 36.50 o -10 1 1 641.52 711.51 48.23 o -9 1 1 3.55 4.21 17.99 o -8 1 1 817.29 860.92 48.68 o -7 1 1 2382.99 2195.21 76.05 o -6 1 1 1686.67 1563.63 65.00 o -5 1 1 29391.01 29714.47 751.55 o -4 1 1 31821.39 34266.41 861.99 o -3 1 1 11879.36 11542.76 296.25 o -2 1 1 34801.33 40028.75 999.13 o -1 1 1 18211.63 19987.16 547.47 o 1 1 1 22523.69 27535.29 691.54 o 2 1 1 2494.49 2453.15 77.46 o 3 1 1 12.25 22.09 8.90 o 4 1 1 1728.36 1423.87 63.03 o 5 1 1 141.49 108.94 17.32 o 6 1 1 610.77 827.91 49.01 o 7 1 1 6.10 31.02 15.45 o 8 1 1 4206.17 3866.76 121.38 o 9 1 1 741.85 806.80 49.26 o 10 1 1 7136.59 6326.16 210.27 o 11 1 1 886.98 998.79 71.15 o 12 1 1 4384.70 4104.21 177.83 o 13 1 1 459.57 415.78 59.65 o 14 1 1 2566.31 2503.61 149.87 o 15 1 1 0.32 -28.35 38.90 o 16 1 1 1226.38 1292.07 129.19 o 17 1 1 20.42 86.05 63.26 o 18 1 1 6.14 95.67 66.99 o 19 1 1 26.57 159.77 184.58 o -20 2 1 0.07 24.36 67.18 o -19 2 1 67.82 95.24 67.14 o -18 2 1 12.18 22.27 55.74 o -17 2 1 229.77 149.59 62.41 o -16 2 1 49.30 70.15 53.73 o -15 2 1 520.78 529.39 134.18 o -14 2 1 136.80 106.09 66.35 o -13 2 1 1913.51 1874.49 104.04 o -12 2 1 392.88 432.49 49.29 o -11 2 1 7118.17 6918.04 230.04 o -10 2 1 5837.40 5941.64 179.17 o -9 2 1 10180.93 9710.04 269.89 o -8 2 1 13.10 28.75 17.48 o -7 2 1 1871.31 1707.55 65.63 o -6 2 1 333.97 482.86 33.75 o -5 2 1 1679.23 1487.56 55.13 o -4 2 1 3827.96 4714.87 130.89 o -3 2 1 4506.54 5069.35 137.39 o -2 2 1 6533.68 7756.79 202.00 o -1 2 1 5154.60 4714.67 125.44 o 1 2 1 24830.86 27619.08 692.58 o 2 2 1 55420.66 60575.43 1512.50 o 3 2 1 32007.43 35100.45 967.17 o 4 2 1 2377.28 1889.90 70.36 o 5 2 1 4241.23 4264.07 138.35 o 6 2 1 14768.07 14095.09 369.92 o 7 2 1 4162.80 4156.05 125.02 o 8 2 1 12244.88 11503.63 310.85 o 9 2 1 1676.32 1694.18 78.76 o 10 2 1 3583.50 3538.27 136.72 o 11 2 1 82.66 84.97 32.71 o 12 2 1 93.03 105.88 39.92 o 13 2 1 15.64 37.22 41.23 o 14 2 1 0.94 41.65 40.53 o 15 2 1 672.83 773.14 101.23 o 16 2 1 399.05 419.27 79.59 o 17 2 1 103.06 29.97 108.35 o 18 2 1 494.69 484.89 92.99 o 19 2 1 18.81 40.83 68.11 o 20 2 1 249.61 439.38 167.24 o -20 3 1 5.07 4.22 83.77 o -19 3 1 4.42 89.64 91.24 o -18 3 1 0.41 30.71 55.86 o -17 3 1 126.40 153.59 59.96 o -16 3 1 15.93 116.76 53.96 o -15 3 1 593.79 666.83 89.92 o -14 3 1 777.61 603.06 97.71 o -13 3 1 125.69 100.74 39.43 o -12 3 1 99.31 34.81 31.14 o -11 3 1 82.72 74.78 30.33 o -10 3 1 44.49 83.26 28.76 o -9 3 1 159.62 161.65 25.81 o -8 3 1 3074.15 3375.54 110.03 o -7 3 1 2679.03 3178.36 101.93 o -6 3 1 2883.10 3328.33 102.53 o -5 3 1 1685.18 2087.49 69.19 o -4 3 1 18629.10 20903.98 533.44 o -3 3 1 1802.63 2085.80 65.20 o -2 3 1 55.81 6.65 8.65 o -1 3 1 1143.11 1257.95 43.13 o 0 3 1 559.22 501.25 37.69 o 1 3 1 1385.81 1229.97 42.84 o 2 3 1 8524.20 8860.42 232.93 o 3 3 1 14.60 4.18 10.43 o 4 3 1 302.02 455.54 43.69 o 5 3 1 163.11 281.65 36.45 o 6 3 1 171.07 153.62 27.34 o 7 3 1 298.54 371.79 44.51 o 8 3 1 336.29 438.81 46.24 o 9 3 1 168.65 263.59 38.05 o 10 3 1 888.83 829.21 63.86 o 11 3 1 65.65 59.56 32.69 o 12 3 1 28.09 95.78 33.78 o 13 3 1 80.40 85.66 41.27 o 14 3 1 3.54 115.20 53.63 o 15 3 1 63.31 79.31 52.46 o 16 3 1 1304.95 1080.33 122.90 o 17 3 1 36.20 172.58 66.03 o 18 3 1 89.22 85.28 69.37 o 19 3 1 4.56 34.60 65.07 o 20 3 1 2.58 27.31 122.77 o -19 4 1 38.11 131.39 97.91 o -18 4 1 88.40 158.32 65.19 o -17 4 1 252.61 370.32 80.99 o -16 4 1 6.90 36.59 52.50 o -15 4 1 134.90 184.30 48.98 o -14 4 1 134.71 187.38 47.61 o -13 4 1 705.61 670.60 73.11 o -12 4 1 547.52 482.09 61.33 o -11 4 1 8294.25 7573.23 281.95 o -10 4 1 307.79 338.34 42.63 o -9 4 1 6572.69 6205.38 184.01 o -8 4 1 6999.52 7017.91 201.12 o -7 4 1 3191.02 2893.74 94.95 o -6 4 1 15064.82 16570.12 433.36 o -5 4 1 491.00 463.69 34.74 o -4 4 1 156.30 169.19 23.32 o -3 4 1 1572.68 1762.19 69.08 o -2 4 1 3344.09 3435.95 100.88 o -1 4 1 2067.49 2505.84 77.56 o 0 4 1 9550.15 11167.41 321.02 o 1 4 1 7679.23 6833.47 184.76 o 2 4 1 5496.53 5854.14 161.55 o 3 4 1 10393.69 10407.64 275.32 o 4 4 1 34330.46 36211.09 915.99 o 5 4 1 5434.73 5724.99 161.70 o 6 4 1 15786.53 16046.54 465.19 o 7 4 1 981.62 1060.58 62.32 o 8 4 1 9463.98 8898.98 277.68 o 9 4 1 132.45 113.04 31.41 o 10 4 1 586.44 703.52 75.17 o 11 4 1 9.07 23.46 34.03 o 12 4 1 1038.75 878.12 84.53 o 13 4 1 117.98 162.35 46.32 o 14 4 1 33.03 71.98 52.35 o 15 4 1 8.64 45.81 65.59 o 16 4 1 783.84 810.84 236.86 o 17 4 1 205.92 256.60 75.43 o 18 4 1 244.65 270.60 82.54 o 19 4 1 17.99 22.18 67.33 o -19 5 1 377.20 527.39 101.10 o -18 5 1 49.41 114.34 63.20 o -17 5 1 853.85 965.35 118.16 o -16 5 1 3.26 -43.99 52.52 o -15 5 1 2240.00 2157.37 145.21 o -14 5 1 67.92 137.12 44.76 o -13 5 1 2140.29 1875.33 144.45 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