#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215679.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215679_Fobs loop_ _publ_author_name 'Du, Jianquan' 'Li, Jikun' 'Ma, Chunlin' 'He, Guofang' _publ_section_title ; [4-(2-Hydroxybenzylideneamino)benzenethiolato]triphenyltin(IV) ; _journal_coeditor_code TK2196 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2599 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.064 _cell_angle_beta 95.430 _cell_angle_gamma 104.936 _cell_length_a 9.5561 _cell_length_b 9.6073 _cell_length_c 30.1104 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file tk2196Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070616c in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 373.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8239.75 6780.19 418.46 o 2 0 0 133792.03 123986.73 7347.71 o 3 0 0 2544.83 2201.71 147.64 o 4 0 0 1959.61 1834.74 131.42 o 5 0 0 7688.68 7975.85 501.23 o 6 0 0 8118.44 8682.25 550.01 o 7 0 0 39.12 56.63 50.20 o 8 0 0 2057.52 2032.45 171.45 o 9 0 0 535.62 580.21 104.12 o 10 0 0 201.52 152.00 83.91 o -10 1 0 332.73 402.47 72.23 o -9 1 0 471.01 639.93 107.34 o -8 1 0 1166.18 1198.90 119.95 o -7 1 0 558.36 505.31 80.82 o -6 1 0 1078.06 1042.39 96.53 o -5 1 0 5648.51 6256.19 396.84 o -4 1 0 761.38 895.67 74.27 o -3 1 0 10967.86 11360.73 686.19 o -2 1 0 23845.76 25703.74 1070.53 o -1 1 0 8.87 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