#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/57/2215708.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215708_Fobs loop_ _publ_author_name 'Zhu, Li-Na' 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; Bis(\m-N,2-di-3-pyridylisoindoline-1-imine-\k^2^N,N')bis[aqua(perchlorato-\kO)cadmium(II)] bis(perchlorate) methanol disolvate ; _journal_coeditor_code XU2328 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2618 _journal_volume 63 _journal_year 2007 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.0869 _cell_length_b 14.8065 _cell_length_c 24.5650 _exptl_crystal_F_000 3792.00 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file xu2328Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 684.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2238.76 2521.55 106.34 o 6 0 0 91556.90 81954.33 1037.14 o 8 0 0 65.28 56.08 70.48 o 10 0 0 193.21 336.27 81.33 o 12 0 0 9622.47 12213.91 292.58 o 14 0 0 17024.15 17106.79 365.83 o 16 0 0 109.12 195.77 120.58 o 18 0 0 12958.47 12927.14 431.33 o 20 0 0 12.43 -6.02 112.87 o 22 0 0 5010.41 5916.95 469.46 o 24 0 0 65.13 91.92 166.73 o 26 0 0 1694.96 2325.70 297.25 o 3 1 0 51403.60 53770.13 430.69 o 5 1 0 69181.66 71668.91 625.51 o 7 1 0 24.59 -36.63 54.25 o 9 1 0 22557.57 19975.37 239.81 o 11 1 0 3815.56 2512.95 110.11 o 13 1 0 14988.46 14372.24 249.55 o 15 1 0 3849.33 3270.64 136.64 o 17 1 0 281.36 404.54 110.25 o 19 1 0 1805.54 1838.89 149.61 o 21 1 0 1399.23 1423.78 202.51 o 23 1 0 258.80 333.51 130.72 o 25 1 0 61.28 271.46 162.39 o 27 1 0 264.84 168.22 165.36 o 2 2 0 9685.26 11783.72 127.21 o 4 2 0 15705.16 12510.70 142.44 o 6 2 0 79044.39 78868.73 728.47 o 8 2 0 7445.04 7571.54 128.91 o 10 2 0 7214.75 7306.94 143.71 o 12 2 0 11815.47 10689.38 208.17 o 14 2 0 7947.19 7409.17 197.00 o 16 2 0 63.48 30.69 84.69 o 18 2 0 502.99 733.85 123.83 o 20 2 0 1.60 -69.33 95.15 o 22 2 0 641.84 909.94 411.63 o 24 2 0 25.76 87.50 125.72 o 26 2 0 253.71 66.57 148.29 o 1 3 0 83579.65 95573.30 1128.47 o 3 3 0 9155.44 9443.31 138.80 o 5 3 0 100.82 109.40 46.36 o 7 3 0 120280.98 116464.34 1109.46 o 9 3 0 272.52 296.84 62.11 o 11 3 0 36391.60 36604.61 427.11 o 13 3 0 882.53 672.46 115.35 o 15 3 0 51276.12 50519.19 664.79 o 17 3 0 22.36 63.05 166.51 o 19 3 0 3864.66 4110.82 188.26 o 21 3 0 921.89 987.44 172.20 o 23 3 0 1379.08 1635.27 358.78 o 25 3 0 1743.49 2454.33 211.79 o 27 3 0 394.38 691.17 268.74 o 0 4 0 34768.09 32551.94 622.89 o 2 4 0 322892.00 393855.31 3678.88 o 4 4 0 78288.96 79886.98 1347.03 o 6 4 0 5377.32 4483.36 110.47 o 8 4 0 15569.53 14274.74 210.76 o 10 4 0 26452.22 28566.29 349.58 o 12 4 0 10355.67 9890.27 197.03 o 14 4 0 6684.12 7011.33 176.14 o 16 4 0 6.68 -59.51 91.15 o 18 4 0 1762.15 1936.04 157.90 o 20 4 0 854.12 986.52 139.40 o 22 4 0 2488.20 2878.42 194.14 o 24 4 0 13.57 -116.62 137.92 o 26 4 0 448.19 550.03 204.81 o 1 5 0 99939.30 101329.52 1273.64 o 3 5 0 3964.70 3579.16 108.96 o 5 5 0 9660.14 10166.52 152.71 o 7 5 0 21602.17 18981.89 275.85 o 9 5 0 2036.01 1953.90 112.09 o 11 5 0 2127.62 2173.76 124.28 o 13 5 0 1666.24 1441.38 120.59 o 15 5 0 1627.38 1761.35 151.79 o 17 5 0 132.96 -25.08 80.67 o 19 5 0 3112.35 3205.22 179.42 o 21 5 0 9.09 -1.64 95.69 o 23 5 0 1.22 -64.12 124.58 o 25 5 0 4.15 169.05 150.93 o 0 6 0 69866.01 63237.67 1224.22 o 2 6 0 24368.77 23273.46 262.06 o 4 6 0 62534.59 62698.89 730.97 o 6 6 0 1629.42 1815.19 101.09 o 8 6 0 19608.46 19201.17 267.35 o 10 6 0 15772.44 14569.97 245.81 o 12 6 0 18129.33 18415.32 321.61 o 14 6 0 3361.09 4029.28 168.91 o 16 6 0 996.51 1453.84 193.09 o 18 6 0 9544.37 11456.71 331.43 o 20 6 0 756.28 407.53 154.07 o 22 6 0 3228.73 4213.86 256.86 o 24 6 0 35.51 -134.30 134.30 o 1 7 0 25075.79 22764.18 377.75 o 3 7 0 15926.34 14858.21 319.68 o 5 7 0 105.22 113.39 71.78 o 7 7 0 19248.57 19474.19 339.82 o 9 7 0 493.14 525.18 55.88 o 11 7 0 21019.15 21452.11 337.47 o 13 7 0 107.22 351.25 96.57 o 15 7 0 8596.31 9485.65 256.94 o 17 7 0 585.57 814.81 142.91 o 19 7 0 2153.09 2491.68 500.47 o 21 7 0 198.67 157.62 146.73 o 23 7 0 96.78 60.64 133.24 o 25 7 0 672.59 710.72 257.89 o 0 8 0 3932.42 3832.85 220.26 o 2 8 0 379.09 293.38 87.47 o 4 8 0 10577.89 10923.39 253.73 o 6 8 0 113.97 57.41 108.70 o 8 8 0 3457.11 3833.57 145.92 o 10 8 0 540.70 515.89 103.24 o 12 8 0 5704.00 5163.66 244.08 o 14 8 0 1274.23 1594.69 139.21 o 16 8 0 5248.39 5665.88 220.36 o 18 8 0 10.20 -34.45 105.41 o 20 8 0 92.50 5.09 122.36 o 22 8 0 341.68 256.71 169.89 o 24 8 0 13.63 38.65 170.81 o 1 9 0 8085.75 8790.05 236.79 o 3 9 0 51458.98 51558.01 547.49 o 5 9 0 2506.13 2545.58 159.12 o 7 9 0 17865.38 18880.12 328.81 o 9 9 0 3716.36 3669.86 207.43 o 11 9 0 3870.32 4126.06 203.86 o 13 9 0 42.10 14.80 32.56 o 15 9 0 5590.29 5896.80 263.83 o 17 9 0 1030.23 990.71 254.61 o 19 9 0 503.96 301.97 141.23 o 21 9 0 380.46 -0.71 111.88 o 23 9 0 88.89 40.47 172.34 o 0 10 0 10205.65 9713.86 548.89 o 2 10 0 644.81 627.94 69.05 o 4 10 0 17346.12 18308.19 301.67 o 6 10 0 12.59 85.17 84.90 o 8 10 0 9445.45 10434.70 253.10 o 10 10 0 457.44 529.14 118.52 o 12 10 0 237.84 349.04 128.90 o 14 10 0 2188.53 2765.65 242.18 o 16 10 0 1735.64 1748.13 404.95 o 18 10 0 841.02 485.12 174.11 o 20 10 0 45.07 -0.18 103.35 o 22 10 0 544.46 32.67 175.12 o 1 11 0 1750.99 1856.70 164.32 o 3 11 0 148.73 125.09 38.64 o 5 11 0 968.67 1006.71 111.23 o 7 11 0 2.57 118.29 99.35 o 9 11 0 877.77 810.26 179.28 o 11 11 0 353.88 430.86 170.71 o 13 11 0 1547.93 2142.91 201.10 o 15 11 0 1026.62 1707.19 184.51 o 17 11 0 6.53 54.44 135.56 o 19 11 0 24.73 -9.54 136.80 o 21 11 0 19.05 10.63 180.36 o 0 12 0 2273.84 3135.03 300.75 o 2 12 0 2310.13 2238.01 98.60 o 4 12 0 3054.72 3210.02 186.41 o 6 12 0 4157.11 4981.32 181.99 o 8 12 0 2676.11 3050.89 228.08 o 10 12 0 2213.39 2116.63 171.66 o 12 12 0 697.71 946.26 157.43 o 14 12 0 694.73 680.47 259.85 o 16 12 0 344.76 195.29 190.79 o 18 12 0 1006.59 20.90 133.16 o 20 12 0 117.28 0.24 124.54 o 1 13 0 1321.26 1571.69 111.59 o 3 13 0 1918.37 1648.30 208.59 o 5 13 0 1373.10 1661.11 185.75 o 7 13 0 8573.45 10366.41 342.19 o 9 13 0 0.21 -134.49 134.49 o 11 13 0 3154.64 4039.11 340.62 o 13 13 0 0.01 -48.69 191.80 o 15 13 0 628.07 362.39 223.98 o 17 13 0 307.40 45.77 157.83 o 19 13 0 606.82 58.43 155.43 o 0 14 0 1325.07 1642.15 291.74 o 2 14 0 24.86 -17.53 104.87 o 4 14 0 1526.00 2067.28 208.61 o 6 14 0 16.34 13.75 105.31 o 8 14 0 11.99 84.58 165.65 o 10 14 0 4.10 -29.36 113.39 o 12 14 0 0.10 15.51 133.15 o 14 14 0 448.48 95.96 146.71 o 16 14 0 20.11 7.06 172.41 o 18 14 0 10.66 3.24 128.82 o 1 15 0 985.04 886.41 110.60 o 3 15 0 2810.00 3552.79 418.52 o 5 15 0 265.96 246.60 162.25 o 7 15 0 827.96 31.57 164.20 o 9 15 0 85.42 3.17 129.22 o 11 15 0 1365.57 1473.70 592.38 o 13 15 0 2.67 -25.13 143.21 o 15 15 0 635.69 84.89 176.15 o 17 15 0 69.00 40.98 171.44 o 0 16 0 1479.44 1280.24 505.13 o 2 16 0 479.75 297.18 288.13 o 4 16 0 1265.42 0.15 249.34 o 6 16 0 72.06 -3.48 126.97 o 8 16 0 1107.94 1355.88 860.97 o 10 16 0 426.55 22.05 140.33 o 12 16 0 277.19 -32.10 175.53 o 14 16 0 394.51 44.99 156.81 o 1 17 0 224.20 78.04 147.18 o 3 17 0 17.93 -0.22 74.78 o 5 17 0 31.33 -5.06 158.37 o 7 17 0 5.19 -30.37 155.61 o 9 17 0 6.60 -5.39 147.73 o 11 17 0 87.04 25.18 172.17 o 0 18 0 3.93 108.63 234.31 o 2 18 0 35.95 6.51 128.75 o 4 18 0 667.31 -9.99 169.87 o 6 18 0 4.65 -29.14 219.13 o 8 18 0 80.10 14.93 147.22 o 1 19 0 427.28 585.58 464.16 o 3 19 0 167.10 105.27 165.25 o 3 1 1 101470.60 115399.76 659.81 o 4 1 1 30936.31 30047.17 193.46 o 5 1 1 11850.19 12400.45 108.79 o 6 1 1 6130.30 4843.45 75.66 o 7 1 1 23242.82 19334.84 152.78 o 8 1 1 18527.48 17244.31 154.34 o 9 1 1 8665.24 8684.38 100.53 o 10 1 1 586.70 418.92 47.72 o 11 1 1 14401.91 14143.78 141.21 o 12 1 1 4964.02 5203.72 96.26 o 13 1 1 2095.90 2165.76 87.68 o 14 1 1 2992.32 3573.02 101.91 o 15 1 1 12433.36 12199.40 169.25 o 16 1 1 7584.24 6928.50 135.70 o 17 1 1 537.09 552.45 91.77 o 18 1 1 3119.54 3046.56 114.74 o 19 1 1 198.01 362.58 79.11 o 20 1 1 1901.05 2044.59 115.86 o 21 1 1 1416.44 1370.90 113.47 o 22 1 1 102.79 179.55 97.76 o 23 1 1 286.52 343.38 101.99 o 24 1 1 863.07 427.15 175.04 o 25 1 1 562.06 378.84 140.30 o 26 1 1 18.83 49.01 107.77 o 27 1 1 68.13 152.48 114.74 o 1 2 1 7254.85 6948.34 46.01 o 2 2 1 196.69 134.87 15.53 o 3 2 1 1721.87 1653.60 47.23 o 4 2 1 22967.93 20032.05 150.61 o 5 2 1 93240.15 90115.38 574.62 o 6 2 1 31802.28 31142.33 223.49 o 7 2 1 4473.57 3965.53 65.32 o 8 2 1 8509.52 7963.44 91.94 o 9 2 1 15588.35 14069.95 136.96 o 10 2 1 3681.89 2787.83 70.55 o 11 2 1 273.60 580.32 54.45 o 12 2 1 19707.74 18236.76 190.17 o 13 2 1 16662.89 15296.11 200.17 o 14 2 1 4983.85 4831.34 113.67 o 15 2 1 2963.74 3194.99 108.41 o 16 2 1 1286.20 1373.71 90.52 o 17 2 1 8553.06 9251.78 175.59 o 18 2 1 1319.65 1565.18 98.21 o 19 2 1 74.63 93.28 71.31 o 20 2 1 278.12 254.84 87.49 o 21 2 1 257.98 276.71 91.47 o 22 2 1 2338.71 2565.85 143.55 o 23 2 1 1360.22 1729.30 148.68 o 24 2 1 49.71 39.07 90.45 o 25 2 1 306.28 219.97 106.69 o 26 2 1 711.62 446.06 166.71 o 27 2 1 562.45 362.39 144.20 o 1 3 1 5714.18 5614.79 61.46 o 2 3 1 83.33 77.10 17.61 o 3 3 1 7274.44 7903.69 75.29 o 4 3 1 1047.36 712.25 37.67 o 5 3 1 5026.41 4276.63 71.67 o 6 3 1 62.54 59.54 37.14 o 7 3 1 6164.83 5933.96 86.38 o 8 3 1 19.11 -31.02 31.02 o 9 3 1 723.69 786.54 49.80 o 10 3 1 1773.02 1735.38 62.88 o 11 3 1 566.69 659.53 60.53 o 12 3 1 48.74 120.51 50.60 o 13 3 1 4372.01 4616.52 97.04 o 14 3 1 653.22 598.79 70.63 o 15 3 1 2.42 -44.99 55.51 o 16 3 1 5357.05 5426.59 127.90 o 17 3 1 494.49 409.34 77.11 o 18 3 1 35.17 -63.25 64.99 o 19 3 1 107.15 99.40 80.61 o 20 3 1 4.28 57.04 84.46 o 21 3 1 20.84 187.71 95.25 o 22 3 1 15.41 49.81 82.57 o 23 3 1 131.89 179.70 89.13 o 24 3 1 84.22 154.45 102.50 o 25 3 1 40.84 133.84 103.81 o 26 3 1 13.03 -77.62 106.74 o 27 3 1 30.62 -153.69 214.52 o 0 4 1 24594.82 21407.73 312.49 o 1 4 1 287799.25 344984.91 2658.76 o 2 4 1 1467.97 1083.22 38.96 o 3 4 1 1272.03 1306.70 34.59 o 4 4 1 5364.21 5536.41 67.76 o 5 4 1 4293.32 4145.51 65.95 o 6 4 1 5652.52 6078.34 83.30 o 7 4 1 14043.92 12073.92 120.40 o 8 4 1 10733.91 9479.38 105.77 o 9 4 1 12886.67 13194.21 150.78 o 10 4 1 21229.91 19173.43 183.25 o 11 4 1 192.83 105.35 50.77 o 12 4 1 6759.09 5985.93 109.89 o 13 4 1 8681.17 7986.58 134.93 o 14 4 1 1038.99 1359.18 82.98 o 15 4 1 4.55 48.52 53.94 o 16 4 1 624.06 732.72 90.47 o 17 4 1 433.66 612.11 91.98 o 18 4 1 4622.39 4889.63 156.32 o 19 4 1 576.36 587.27 104.30 o 20 4 1 998.08 896.27 106.22 o 21 4 1 396.23 348.26 96.20 o 22 4 1 1190.90 1288.97 213.26 o 23 4 1 515.62 365.96 112.06 o 24 4 1 2.26 -62.77 92.22 o 25 4 1 171.16 353.40 107.54 o 26 4 1 287.71 257.07 136.26 o 1 5 1 4542.67 4778.43 75.51 o 2 5 1 45532.78 44058.99 337.98 o 3 5 1 15315.77 13735.31 116.86 o 4 5 1 6730.13 6355.52 74.88 o 5 5 1 24687.10 23666.15 178.07 o 6 5 1 24764.25 25182.22 184.32 o 7 5 1 37153.05 36209.43 287.53 o 8 5 1 7460.07 6535.58 98.80 o 9 5 1 91.76 8.58 33.08 o 10 5 1 20524.19 18715.50 190.64 o 11 5 1 13003.00 12556.46 167.22 o 12 5 1 8092.30 8374.22 124.79 o 13 5 1 1371.74 1172.81 79.95 o 14 5 1 831.10 1137.59 104.41 o 15 5 1 4670.24 5190.61 130.43 o 16 5 1 2371.76 2336.95 114.17 o 17 5 1 706.08 701.24 93.91 o 18 5 1 953.52 1561.20 155.75 o 19 5 1 4587.92 5307.14 209.68 o 20 5 1 2024.57 2352.92 166.72 o 21 5 1 967.99 939.62 160.25 o 22 5 1 11.25 7.07 68.32 o 23 5 1 637.98 598.65 120.29 o 24 5 1 317.75 287.04 109.89 o 25 5 1 285.33 177.69 114.63 o 26 5 1 5.13 -9.27 102.62 o 0 6 1 550.09 828.35 136.08 o 1 6 1 5168.87 4426.51 78.24 o 2 6 1 54.19 150.47 22.83 o 3 6 1 2307.17 2213.32 52.58 o 4 6 1 450.33 433.67 51.64 o 5 6 1 651.90 594.81 56.50 o 6 6 1 275.25 230.46 25.66 o 7 6 1 296.06 260.76 28.40 o 8 6 1 12008.98 11415.00 134.16 o 9 6 1 2166.71 2050.03 73.33 o 10 6 1 15972.72 17066.80 185.01 o 11 6 1 2065.83 2243.08 85.59 o 12 6 1 146.18 132.96 58.68 o 13 6 1 24.65 -19.19 52.59 o 14 6 1 81.39 115.32 67.44 o 15 6 1 948.22 1204.88 103.76 o 16 6 1 1227.75 1402.51 112.11 o 17 6 1 1417.32 1483.61 117.84 o 18 6 1 136.77 77.16 75.20 o 19 6 1 530.84 467.88 93.38 o 20 6 1 707.37 612.81 123.08 o 21 6 1 14.23 55.52 82.96 o 22 6 1 0.22 71.99 92.61 o 23 6 1 9.00 0.40 60.15 o 24 6 1 9.19 -15.26 79.46 o 25 6 1 0.99 155.07 124.76 o 1 7 1 6958.49 7411.32 112.76 o 2 7 1 85.80 204.43 46.73 o 3 7 1 14587.67 13763.46 103.81 o 4 7 1 865.93 1253.06 67.21 o 5 7 1 22761.17 22553.95 237.79 o 6 7 1 443.63 671.30 66.52 o 7 7 1 2995.94 2440.22 134.62 o 8 7 1 5235.83 4870.58 72.45 o 9 7 1 329.59 223.53 20.46 o 10 7 1 8303.04 8453.88 105.40 o 11 7 1 993.04 1110.81 82.97 o 12 7 1 1059.55 1428.68 84.17 o 13 7 1 6.54 -35.20 60.26 o 14 7 1 3514.41 3925.95 132.41 o 15 7 1 4483.55 5141.54 136.55 o 16 7 1 2660.16 2783.76 121.61 o 17 7 1 1794.95 1959.02 121.75 o 18 7 1 409.18 469.42 108.19 o 19 7 1 244.56 248.96 97.70 o 20 7 1 1386.43 1508.93 263.52 o 21 7 1 84.35 48.84 84.73 o 22 7 1 131.47 129.90 90.97 o 23 7 1 292.35 259.82 107.39 o 24 7 1 319.11 274.77 119.70 o 25 7 1 135.66 -15.39 97.42 o 0 8 1 50157.96 52046.46 781.43 o 1 8 1 219.91 341.58 54.92 o 2 8 1 156.21 145.79 43.42 o 3 8 1 20796.15 20688.72 150.25 o 4 8 1 31295.96 30722.45 300.44 o 5 8 1 21632.49 19852.96 225.64 o 6 8 1 3477.38 3338.36 96.23 o 7 8 1 608.83 806.85 70.66 o 8 8 1 2371.61 2633.14 92.38 o 9 8 1 5652.37 5771.08 122.47 o 10 8 1 1933.01 1988.04 69.12 o 11 8 1 6.17 -1.58 17.42 o 12 8 1 5398.72 5542.06 94.93 o 13 8 1 8039.63 8979.36 164.54 o 14 8 1 6188.74 7325.21 168.30 o 15 8 1 2.02 -42.01 70.11 o 16 8 1 343.71 335.52 87.87 o 17 8 1 657.73 781.78 97.42 o 18 8 1 1512.47 1506.20 260.04 o 19 8 1 293.42 261.76 96.76 o 20 8 1 480.57 184.16 103.67 o 21 8 1 1073.37 360.68 162.28 o 22 8 1 502.51 348.63 151.68 o 23 8 1 535.76 609.43 124.33 o 24 8 1 114.43 69.76 101.50 o 1 9 1 1745.19 1535.05 81.42 o 2 9 1 18277.04 19021.46 208.93 o 3 9 1 3058.83 3265.80 59.79 o 4 9 1 69.41 69.38 51.16 o 5 9 1 44.74 40.85 49.35 o 6 9 1 473.95 613.16 69.54 o 7 9 1 2.56 9.55 46.48 o 8 9 1 194.50 200.80 82.18 o 9 9 1 257.30 192.27 78.98 o 10 9 1 194.79 188.56 83.12 o 11 9 1 113.03 127.72 78.66 o 12 9 1 244.38 360.80 86.60 o 13 9 1 3.88 24.29 39.95 o 14 9 1 591.61 508.67 43.64 o 15 9 1 1944.87 1965.04 118.22 o 16 9 1 811.64 855.56 70.00 o 17 9 1 25.80 81.79 53.76 o 18 9 1 9.00 -37.67 75.90 o 19 9 1 860.44 677.06 204.78 o 20 9 1 33.84 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350.74 154.98 86.20 o 2 1 28 182.99 90.39 70.85 o 3 1 28 129.48 78.37 66.92 o 4 1 28 38.81 48.40 65.03 o 5 1 28 0.79 7.28 58.11 o 6 1 28 123.71 139.19 83.01 o 7 1 28 351.65 246.67 92.41 o 8 1 28 4.22 -64.54 87.20 o 9 1 28 0.30 143.79 100.54 o 10 1 28 0.40 20.60 74.19 o 11 1 28 434.76 394.35 140.34 o 12 1 28 127.77 35.85 94.31 o 0 2 28 553.76 314.59 139.03 o 1 2 28 0.17 -40.08 53.00 o 2 2 28 122.27 64.67 67.55 o 3 2 28 5.93 -51.74 59.67 o 4 2 28 555.84 353.21 94.75 o 5 2 28 109.40 -1.88 65.88 o 6 2 28 10.90 -48.58 72.39 o 7 2 28 4.47 4.23 64.44 o 8 2 28 290.13 132.97 106.57 o 9 2 28 24.49 60.15 87.66 o 10 2 28 86.53 39.32 87.21 o 11 2 28 0.26 39.49 102.15 o 12 2 28 3.14 125.64 112.65 o 1 3 28 811.94 590.96 129.15 o 2 3 28 423.99 295.94 98.99 o 3 3 28 621.31 687.94 123.94 o 4 3 28 81.43 169.06 74.70 o 5 3 28 110.09 97.10 77.99 o 6 3 28 236.32 214.69 82.28 o 7 3 28 1056.30 553.67 186.39 o 8 3 28 325.70 128.98 102.30 o 9 3 28 50.58 18.14 83.39 o 10 3 28 32.40 73.24 98.15 o 11 3 28 886.02 566.03 228.91 o 12 3 28 117.37 58.40 111.84 o 0 4 28 446.38 502.79 112.02 o 1 4 28 33.57 10.06 65.47 o 2 4 28 13.84 77.42 85.74 o 3 4 28 67.13 131.58 68.97 o 4 4 28 326.46 226.55 98.94 o 5 4 28 226.67 173.15 62.50 o 6 4 28 33.73 -29.27 70.87 o 7 4 28 4.86 40.32 87.37 o 8 4 28 531.22 251.14 92.61 o 9 4 28 46.42 112.00 101.75 o 10 4 28 85.82 94.17 97.98 o 11 4 28 0.64 50.73 101.90 o 1 5 28 22.55 126.71 103.87 o 2 5 28 23.54 82.86 96.10 o 3 5 28 30.51 143.56 92.09 o 4 5 28 0.22 -50.38 83.89 o 5 5 28 0.33 -5.74 58.75 o 6 5 28 2.34 37.88 67.27 o 7 5 28 93.69 83.23 69.10 o 8 5 28 99.69 87.03 99.82 o 9 5 28 0.72 -85.38 85.38 o 10 5 28 28.07 117.24 106.38 o 0 6 28 485.49 542.58 156.36 o 1 6 28 4.99 -2.64 80.56 o 2 6 28 8.68 26.16 81.63 o 3 6 28 7.78 -40.14 97.56 o 4 6 28 1288.68 1465.04 214.32 o 5 6 28 183.16 236.41 94.19 o 6 6 28 282.36 188.48 100.95 o 7 6 28 62.26 -17.29 50.36 o 8 6 28 858.28 409.37 161.55 o 9 6 28 122.05 75.63 97.88 o 1 7 28 171.11 366.89 110.40 o 2 7 28 78.78 69.27 102.84 o 3 7 28 515.24 650.61 123.39 o 4 7 28 33.48 124.21 115.17 o 5 7 28 200.30 187.39 98.81 o 6 7 28 45.89 51.71 96.17 o 7 7 28 493.50 433.76 190.86 o 8 7 28 9.82 -27.56 70.75 o 0 8 28 15.43 -1.99 134.68 o 1 8 28 25.77 145.36 107.39 o 2 8 28 9.95 117.77 107.63 o 3 8 28 0.38 26.71 93.03 o 4 8 28 48.69 14.10 104.80 o 5 8 28 0.30 -82.55 90.20 o 6 8 28 2.83 49.65 97.65 o 1 9 28 485.58 482.16 150.22 o 2 9 28 128.11 126.83 126.47 o 1 1 29 494.22 208.69 93.11 o 2 1 29 79.24 85.72 65.15 o 3 1 29 1638.87 1558.50 333.78 o 4 1 29 31.95 -35.26 64.28 o 5 1 29 377.13 124.81 76.51 o 6 1 29 157.34 70.29 78.52 o 7 1 29 683.82 512.17 135.59 o 8 1 29 49.70 53.62 87.23 o 9 1 29 14.14 -37.99 85.77 o 10 1 29 39.43 70.15 100.63 o 11 1 29 461.65 386.87 128.94 o 0 2 29 604.30 178.83 166.32 o 1 2 29 186.89 96.31 89.76 o 2 2 29 3.73 -24.19 97.08 o 3 2 29 82.55 15.12 87.52 o 4 2 29 905.58 540.46 135.31 o 5 2 29 26.01 -6.13 54.16 o 6 2 29 113.49 20.03 85.46 o 7 2 29 8.11 32.61 84.91 o 8 2 29 385.09 402.97 108.10 o 9 2 29 213.30 181.80 105.99 o 10 2 29 524.62 319.73 155.38 o 11 2 29 68.96 43.28 391.17 o 1 3 29 21.71 107.86 79.00 o 2 3 29 29.80 65.43 76.74 o 3 3 29 0.50 40.37 77.76 o 4 3 29 0.04 -5.72 58.43 o 5 3 29 13.96 -52.78 100.73 o 6 3 29 11.31 48.09 75.39 o 7 3 29 6.42 26.34 70.10 o 8 3 29 0.06 -14.35 76.06 o 9 3 29 0.20 -19.93 78.48 o 10 3 29 5.38 15.43 79.69 o 0 4 29 392.02 400.37 219.55 o 1 4 29 29.17 -37.20 88.52 o 2 4 29 1.33 65.00 89.13 o 3 4 29 73.11 100.67 92.47 o 4 4 29 411.94 330.48 98.10 o 5 4 29 43.80 21.93 81.00 o 6 4 29 160.69 194.83 90.84 o 7 4 29 8.16 -59.72 88.10 o 8 4 29 300.80 99.24 88.82 o 9 4 29 155.38 76.81 88.74 o 1 5 29 262.17 216.76 104.04 o 2 5 29 52.52 -39.09 89.80 o 3 5 29 856.95 910.30 113.00 o 4 5 29 0.03 55.53 94.22 o 5 5 29 154.12 222.05 119.96 o 6 5 29 144.00 278.19 117.77 o 7 5 29 758.83 703.51 167.93 o 8 5 29 42.57 -37.98 72.80 o 0 6 29 189.24 321.57 173.63 o 1 6 29 64.20 264.07 116.58 o 2 6 29 45.20 -10.42 79.10 o 3 6 29 0.01 70.40 103.07 o 4 6 29 211.60 124.47 105.28 o 5 6 29 18.05 101.42 88.29 o 6 6 29 0.16 109.17 91.89 o 7 6 29 4.88 27.25 101.71 o 1 7 29 153.07 291.89 132.86 o 2 7 29 108.53 -29.46 90.99 o 3 7 29 273.53 330.36 130.09 o 4 7 29 25.97 -36.24 99.78 o 5 7 29 31.26 156.01 107.19 o 0 0 30 576.37 39.36 290.32 o 1 0 30 365.07 -21.43 189.64 o 2 0 30 6.41 -6.89 172.75 o 3 0 30 356.35 213.68 177.72 o 4 0 30 546.80 389.59 208.99 o 5 0 30 899.38 1242.93 287.21 o 6 0 30 36.17 100.99 126.44 o 7 0 30 4.73 -65.91 116.87 o 8 0 30 49.10 129.84 134.91 o 9 0 30 410.78 515.56 219.64 o 1 1 30 9.77 -19.28 118.14 o 2 1 30 254.94 31.52 120.45 o 3 1 30 60.40 -23.95 106.29 o 4 1 30 146.73 10.00 83.27 o 5 1 30 15.29 45.43 78.65 o 6 1 30 345.70 147.97 82.36 o 7 1 30 51.21 69.39 92.67 o 8 1 30 58.27 30.38 92.73 o 9 1 30 11.31 173.43 118.77 o 0 2 30 228.44 85.89 126.15 o 1 2 30 51.97 62.31 110.49 o 2 2 30 12.64 58.09 108.50 o 3 2 30 146.93 34.71 80.55 o 4 2 30 106.63 -84.51 110.12 o 5 2 30 18.64 75.74 102.07 o 6 2 30 78.21 22.27 74.05 o 7 2 30 0.11 51.95 84.44 o 8 2 30 0.06 44.53 86.04 o 1 3 30 52.56 61.93 116.04 o 2 3 30 978.52 786.79 193.45 o 3 3 30 120.16 157.57 127.56 o 4 3 30 148.31 90.33 103.98 o 5 3 30 1.32 -5.91 128.61 o 6 3 30 963.01 807.68 236.92 o 7 3 30 122.39 211.23 119.94 o 8 3 30 58.87 103.36 87.50 o 0 4 30 9.02 38.18 134.99 o 1 4 30 265.75 379.55 111.16 o 2 4 30 1.67 -74.54 92.66 o 3 4 30 111.60 45.35 95.33 o 4 4 30 118.96 94.96 104.63 o 5 4 30 204.92 271.15 154.76 o 6 4 30 0.71 157.13 122.33 o 7 4 30 195.61 247.75 144.63 o 1 5 30 5.43 57.70 88.03 o 2 5 30 105.37 -19.88 85.92 o 3 5 30 0.34 38.12 86.87 o 4 5 30 38.38 40.90 105.36 o 5 5 30 22.53 22.10 110.68 o 0 6 30 143.74 174.39 154.06 o 1 6 30 276.00 375.94 129.16 o 2 6 30 2.55 190.46 131.67 o 3 6 30 217.18 363.19 110.70 o 1 1 31 63.94 4.96 129.62 o 2 1 31 667.12 -11.05 144.98 o 3 1 31 8.82 -36.75 106.65 o 4 1 31 64.38 63.46 109.44 o 5 1 31 6.50 31.14 91.95 o 6 1 31 98.50 -43.36 95.13 o 0 2 31 36.71 17.11 248.74 o 1 2 31 440.33 -4.37 130.20 o 2 2 31 24.13 37.99 138.14 o 3 2 31 299.63 63.26 123.34 o 4 2 31 131.43 62.39 111.37 o 5 2 31 716.28 599.40 202.57 o 1 3 31 8.74 -32.72 115.35 o 2 3 31 26.76 128.07 131.95 o 3 3 31 0.12 43.80 125.97 o 4 3 31 4.05 -3.38 92.89 o 0 4 31 13.13 39.93 174.82 o 1 4 31 252.83 300.11 154.27 o 2 4 31 32.80 92.89 99.33 o