#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/57/2215712.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215712_Fobs loop_ _publ_author_name 'Morris, J. Jacob' 'Noll, Bruce C.' 'Henderson, Kenneth W.' _publ_section_title ; A polymeric mixed-metal hexamethyldisilazide ; _journal_coeditor_code ZL2045 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2477 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.657 _cell_angle_gamma 90.000 _cell_length_a 11.3154 _cell_length_b 17.5465 _cell_length_c 12.6528 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.8179 _[local]_cod_data_source_file zl2045Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JJM67 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 330.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 109524.28 108856.79 1000.05 o 4 0 0 10496.78 9930.04 98.16 o 6 0 0 9004.82 8922.67 95.79 o 8 0 0 3345.83 3329.02 44.92 o 10 0 0 341.21 324.17 10.58 o 12 0 0 277.48 316.44 13.07 o 1 1 0 576.27 597.81 4.00 o 3 1 0 5.63 11.41 1.18 o 5 1 0 940.76 912.93 8.63 o 7 1 0 1691.10 1577.89 14.52 o 9 1 0 1178.17 1128.76 13.89 o 11 1 0 246.97 238.86 10.12 o 13 1 0 270.72 278.56 12.52 o 0 2 0 6864.90 6840.12 178.17 o 2 2 0 3095.98 3172.37 19.35 o 4 2 0 2221.64 2188.52 18.58 o 6 2 0 285.90 290.83 4.64 o 8 2 0 5.34 -1.46 2.64 o 10 2 0 62.84 63.45 4.67 o 12 2 0 78.84 79.59 6.26 o 1 3 0 102.23 132.86 1.66 o 3 3 0 2381.50 2969.31 19.09 o 5 3 0 3808.79 4246.77 29.00 o 7 3 0 226.03 236.29 4.60 o 9 3 0 48.44 50.58 3.72 o 11 3 0 38.58 38.05 4.75 o 0 4 0 17420.90 17607.12 226.10 o 2 4 0 2134.95 2015.69 13.03 o 4 4 0 1114.27 1014.69 8.28 o 6 4 0 4731.63 4618.93 32.62 o 8 4 0 749.29 729.97 9.74 o 10 4 0 89.66 84.34 6.34 o 12 4 0 13.79 5.39 4.79 o 1 5 0 3382.17 3552.84 26.83 o 3 5 0 1788.68 1967.20 12.79 o 5 5 0 21.07 17.92 1.64 o 7 5 0 5.06 2.62 1.99 o 9 5 0 170.01 174.18 5.61 o 11 5 0 124.82 127.71 6.55 o 0 6 0 2412.30 2040.35 28.51 o 2 6 0 986.22 765.20 5.70 o 4 6 0 1026.38 935.37 7.51 o 6 6 0 3489.54 3358.12 23.44 o 8 6 0 1624.79 1543.46 14.85 o 10 6 0 564.03 569.30 10.79 o 12 6 0 26.53 20.19 5.48 o 3 7 0 1717.68 1697.54 12.75 o 5 7 0 3001.89 2887.80 20.39 o 7 7 0 3559.22 3382.99 25.09 o 9 7 0 1721.69 1696.48 19.17 o 11 7 0 1479.13 1535.04 22.38 o 0 8 0 707.30 717.58 12.58 o 2 8 0 3123.21 3141.97 23.28 o 4 8 0 2254.71 2321.42 16.92 o 6 8 0 1130.97 1098.14 9.94 o 8 8 0 681.95 658.55 9.17 o 10 8 0 197.44 208.07 7.35 o 12 8 0 7.52 3.53 5.74 o 1 9 0 14.28 12.82 1.30 o 3 9 0 24.14 35.52 1.70 o 5 9 0 332.39 371.53 5.30 o 7 9 0 336.21 345.29 6.78 o 9 9 0 123.71 135.02 10.10 o 11 9 0 5.02 -1.95 3.78 o 0 10 0 331.29 397.16 8.51 o 2 10 0 9.95 11.61 1.65 o 4 10 0 5.44 7.64 1.79 o 6 10 0 47.18 49.38 2.76 o 8 10 0 21.59 11.65 3.98 o 10 10 0 1.78 -0.94 3.43 o 1 11 0 283.03 284.43 4.93 o 3 11 0 326.39 353.20 5.21 o 5 11 0 50.35 48.98 2.98 o 7 11 0 60.17 63.57 4.22 o 9 11 0 17.51 20.33 4.75 o 11 11 0 15.45 19.31 6.09 o 0 12 0 321.65 346.06 8.43 o 2 12 0 110.15 146.66 4.24 o 4 12 0 9.98 29.94 2.43 o 6 12 0 20.54 38.61 3.74 o 8 12 0 15.09 12.01 4.34 o 10 12 0 1.57 -2.19 4.91 o 1 13 0 0.45 -1.01 1.79 o 3 13 0 0.01 0.36 1.82 o 5 13 0 47.21 32.60 2.69 o 7 13 0 18.03 18.23 4.93 o 9 13 0 45.52 42.04 5.80 o 0 14 0 3238.13 3143.39 39.08 o 2 14 0 1828.48 1774.85 21.84 o 4 14 0 429.78 425.62 7.71 o 6 14 0 0.02 4.24 4.23 o 8 14 0 11.76 15.08 5.39 o 1 15 0 12.72 11.05 2.56 o 3 15 0 99.89 113.69 3.90 o 5 15 0 451.49 463.68 10.48 o 7 15 0 674.11 675.67 17.02 o 9 15 0 496.66 491.62 18.13 o 0 16 0 584.09 579.76 12.40 o 2 16 0 849.97 856.74 14.08 o 4 16 0 915.31 920.68 18.84 o 6 16 0 710.40 641.31 19.82 o 8 16 0 236.52 240.71 12.73 o 1 17 0 31.51 33.74 6.73 o 3 17 0 57.11 65.91 5.53 o 5 17 0 88.83 90.34 7.50 o 7 17 0 13.41 11.17 8.17 o 0 18 0 87.26 76.52 11.21 o 2 18 0 43.40 31.82 5.17 o 4 18 0 48.30 42.62 6.26 o 6 18 0 33.56 17.60 6.95 o 1 19 0 13.99 18.04 5.04 o 3 19 0 22.09 26.29 5.59 o 5 19 0 0.99 -5.98 9.34 o 2 20 0 32.64 45.41 16.98 o 4 20 0 17.51 18.24 6.80 o 1 21 0 0.00 10.64 9.06 o -13 1 1 489.15 514.60 16.64 o -11 1 1 849.39 859.29 15.31 o -9 1 1 4387.12 4281.96 43.95 o -7 1 1 6106.75 5898.56 43.63 o -5 1 1 4695.00 4455.58 30.21 o -3 1 1 5807.15 6018.47 37.20 o -1 1 1 12896.29 12994.48 74.71 o 1 1 1 2147.80 2027.02 13.80 o 3 1 1 3014.80 2959.47 21.22 o 5 1 1 234.75 238.41 4.19 o 7 1 1 738.78 705.57 8.97 o 9 1 1 301.14 303.98 7.23 o 11 1 1 79.52 78.91 5.88 o -12 2 1 14.63 16.30 4.61 o -10 2 1 0.38 9.08 3.35 o -8 2 1 6.16 5.39 2.44 o -6 2 1 80.34 81.58 2.79 o -4 2 1 1200.65 1164.43 9.00 o -2 2 1 10192.66 10763.63 59.06 o 0 2 1 29948.65 30433.94 215.66 o 2 2 1 15382.01 16402.19 106.14 o 4 2 1 10217.28 10594.79 73.63 o 6 2 1 2677.83 2599.23 21.09 o 8 2 1 792.77 741.83 10.02 o 10 2 1 42.00 36.39 4.32 o 12 2 1 95.44 89.29 9.08 o -13 3 1 2.11 -1.30 6.06 o -11 3 1 13.85 7.73 3.71 o -9 3 1 26.15 18.68 3.02 o -7 3 1 16.98 19.06 2.16 o -5 3 1 204.23 226.12 3.64 o -3 3 1 685.10 727.62 5.62 o -1 3 1 4243.73 4457.28 28.67 o 1 3 1 2243.76 2484.03 16.32 o 3 3 1 5902.40 6376.84 41.33 o 5 3 1 287.67 315.10 4.74 o 7 3 1 660.51 636.73 8.16 o 9 3 1 12.44 12.85 3.03 o 11 3 1 17.43 14.72 4.39 o -12 4 1 163.52 155.32 7.63 o -10 4 1 247.82 231.86 6.79 o -8 4 1 999.10 930.74 10.82 o -6 4 1 954.95 954.31 9.22 o -4 4 1 608.89 626.59 5.61 o -2 4 1 289.58 318.14 3.41 o 0 4 1 832.11 991.38 8.42 o 2 4 1 2540.88 3030.13 19.30 o 4 4 1 700.38 742.79 6.74 o 6 4 1 1206.31 1139.81 10.77 o 8 4 1 1497.65 1395.41 15.47 o 10 4 1 644.99 625.79 11.86 o 12 4 1 245.18 252.87 10.93 o -11 5 1 739.57 723.62 13.46 o -9 5 1 2957.18 2828.18 25.18 o -7 5 1 5998.96 5667.73 37.95 o -5 5 1 1727.27 1652.89 12.38 o -3 5 1 4948.91 4662.74 28.46 o -1 5 1 17063.66 17134.21 125.72 o 1 5 1 11945.18 12784.67 99.74 o 3 5 1 4805.54 5468.44 35.55 o 5 5 1 2755.90 2940.06 20.95 o 7 5 1 140.20 176.46 4.14 o 9 5 1 8.33 11.30 3.13 o 11 5 1 75.66 70.52 5.87 o -12 6 1 32.65 27.01 5.68 o -10 6 1 10.80 4.98 3.48 o -8 6 1 470.22 466.56 6.96 o -6 6 1 4523.11 4476.65 30.74 o -4 6 1 6115.63 6305.59 43.21 o -2 6 1 1638.52 1497.16 10.41 o 0 6 1 360.16 244.31 3.52 o 2 6 1 3183.09 3127.31 22.58 o 4 6 1 3356.66 3395.88 23.22 o 6 6 1 3853.84 3724.63 27.11 o 8 6 1 1577.22 1530.90 15.36 o 10 6 1 290.77 264.43 7.99 o 12 6 1 0.70 0.39 5.30 o -11 7 1 53.69 50.79 6.09 o -9 7 1 1.20 -2.86 2.86 o -7 7 1 29.02 18.02 2.19 o -5 7 1 3.03 -0.26 1.16 o -3 7 1 915.34 961.76 7.79 o -1 7 1 777.12 757.70 6.91 o 1 7 1 1887.56 1919.43 17.06 o 3 7 1 4192.11 4428.56 30.87 o 5 7 1 1739.17 1899.61 14.04 o 7 7 1 638.31 700.58 7.81 o 9 7 1 814.27 864.41 12.38 o 11 7 1 278.66 280.40 9.22 o -12 8 1 74.57 87.55 8.55 o -10 8 1 76.55 79.79 5.34 o -8 8 1 604.06 575.25 8.02 o -6 8 1 1958.76 1859.87 13.95 o -4 8 1 2938.05 2982.68 21.69 o -2 8 1 3126.05 3169.11 23.24 o 0 8 1 379.64 497.26 5.74 o 2 8 1 20.16 47.32 2.35 o 4 8 1 1521.35 1396.19 11.80 o 6 8 1 1965.65 1894.46 17.79 o 8 8 1 306.19 307.93 6.73 o 10 8 1 85.45 94.27 5.51 o -11 9 1 775.93 795.88 14.04 o -9 9 1 868.62 898.15 12.92 o -7 9 1 746.53 794.89 8.79 o -5 9 1 116.13 129.38 3.39 o -3 9 1 0.36 2.38 1.28 o -1 9 1 188.22 199.32 3.00 o 1 9 1 25.85 24.12 2.43 o 3 9 1 534.95 554.06 5.45 o 5 9 1 965.81 1026.33 10.18 o 7 9 1 847.84 940.50 12.11 o 9 9 1 573.24 572.40 9.81 o 11 9 1 759.58 768.83 14.26 o -10 10 1 0.01 -3.03 3.03 o -8 10 1 14.68 8.62 3.89 o -6 10 1 57.74 50.68 2.87 o -4 10 1 209.15 234.82 4.31 o -2 10 1 2640.22 2613.60 21.73 o 0 10 1 1739.27 1731.68 17.63 o 2 10 1 792.25 755.85 8.59 o 4 10 1 1277.72 1271.66 11.65 o 6 10 1 1556.33 1613.03 17.24 o 8 10 1 625.90 633.57 11.48 o 10 10 1 272.66 283.66 10.92 o -11 11 1 0.61 -1.45 5.23 o -9 11 1 65.84 59.83 5.58 o -7 11 1 198.25 200.93 6.06 o -5 11 1 1459.05 1464.42 14.85 o -3 11 1 4367.21 4335.37 34.45 o -1 11 1 5072.84 5131.71 46.34 o 1 11 1 2953.19 2948.75 28.12 o 3 11 1 2307.14 2273.88 20.78 o 5 11 1 911.87 914.34 10.91 o 7 11 1 919.72 960.10 17.48 o 9 11 1 743.89 744.02 16.48 o -10 12 1 99.24 93.65 7.32 o -8 12 1 208.83 198.03 8.22 o -6 12 1 428.44 436.30 8.28 o -4 12 1 2.08 3.48 1.84 o -2 12 1 65.42 63.29 2.50 o 0 12 1 496.94 446.63 5.70 o 2 12 1 797.83 750.84 9.18 o 4 12 1 1080.04 1039.02 11.65 o 6 12 1 221.20 207.83 5.99 o 8 12 1 92.55 98.06 6.57 o 10 12 1 32.40 35.54 6.54 o -9 13 1 245.26 259.63 10.96 o -7 13 1 256.08 270.36 8.58 o -5 13 1 464.36 474.38 7.58 o -3 13 1 170.78 182.07 3.91 o -1 13 1 32.27 31.97 2.28 o 1 13 1 6.48 4.33 1.67 o 3 13 1 1.20 3.62 1.79 o 5 13 1 291.11 309.69 7.65 o 7 13 1 291.06 327.14 9.92 o 9 13 1 216.12 233.02 9.49 o -10 14 1 26.95 25.72 7.02 o -8 14 1 241.92 243.73 10.00 o -6 14 1 643.19 601.24 15.94 o -4 14 1 759.68 717.69 10.34 o -2 14 1 1035.22 991.48 11.66 o 0 14 1 1083.87 1077.33 12.89 o 2 14 1 947.93 937.50 11.81 o 4 14 1 583.52 603.75 9.49 o 6 14 1 417.34 442.03 12.71 o 8 14 1 231.96 226.91 11.58 o -9 15 1 0.08 -7.52 7.52 o -7 15 1 1.50 1.23 5.00 o -5 15 1 12.25 6.74 3.87 o -3 15 1 63.76 65.55 3.40 o -1 15 1 2.78 -0.03 1.79 o 1 15 1 21.35 21.43 2.99 o 3 15 1 142.65 146.20 4.37 o 5 15 1 284.28 283.80 8.93 o 7 15 1 54.74 71.50 14.94 o -8 16 1 9.26 8.95 7.45 o -6 16 1 2.52 0.54 4.62 o -4 16 1 142.51 127.91 6.52 o -2 16 1 633.54 605.43 11.29 o 0 16 1 1095.31 1043.96 18.00 o 2 16 1 491.91 465.10 12.06 o 4 16 1 411.91 410.01 16.94 o 6 16 1 233.15 234.07 12.11 o 8 16 1 69.35 64.44 10.65 o -7 17 1 303.24 304.04 20.52 o -5 17 1 403.11 418.76 16.23 o -3 17 1 523.73 508.29 13.65 o -1 17 1 407.60 402.48 12.69 o 1 17 1 150.06 154.70 6.97 o 3 17 1 35.43 32.41 6.13 o 5 17 1 1.84 5.93 4.97 o 7 17 1 0.40 -6.17 6.17 o -6 18 1 4.40 4.16 9.10 o -4 18 1 0.21 3.04 5.15 o -2 18 1 0.39 -0.02 5.73 o 0 18 1 27.92 30.89 8.66 o 2 18 1 1.40 -1.19 5.50 o 4 18 1 13.67 6.11 4.70 o 6 18 1 109.99 107.22 9.45 o -5 19 1 11.72 4.47 7.87 o -3 19 1 8.94 7.46 7.44 o -1 19 1 19.81 31.92 10.41 o 1 19 1 164.14 167.43 11.47 o 3 19 1 182.61 169.53 12.29 o 5 19 1 84.11 64.05 8.60 o -4 20 1 2.91 -4.99 6.53 o -2 20 1 28.70 24.83 7.37 o 0 20 1 50.98 62.26 12.68 o 2 20 1 72.42 91.22 9.37 o 4 20 1 101.74 136.29 14.49 o -1 21 1 63.04 67.80 13.13 o -12 0 2 1.72 2.39 5.40 o -10 0 2 299.65 274.78 8.81 o -8 0 2 961.09 970.76 15.59 o -6 0 2 3158.44 3200.56 33.22 o -4 0 2 152.72 192.75 4.01 o -2 0 2 2554.05 2602.17 22.08 o 0 0 2 4949.58 5279.89 46.94 o 2 0 2 12925.35 14149.06 136.91 o 4 0 2 8297.58 8917.19 97.24 o 6 0 2 0.53 2.89 2.79 o 8 0 2 1.77 2.38 2.81 o 10 0 2 53.29 51.59 6.70 o 12 0 2 51.17 35.68 10.46 o -13 1 2 92.59 96.77 8.21 o -11 1 2 94.31 102.19 5.79 o -9 1 2 175.66 184.52 5.02 o -7 1 2 682.37 682.03 8.09 o -5 1 2 4225.38 4261.15 29.12 o -3 1 2 4849.98 4929.62 30.95 o -1 1 2 14255.48 14992.50 88.92 o 1 1 2 6390.98 6624.01 47.48 o 3 1 2 664.75 572.56 6.22 o 5 1 2 810.06 787.82 8.49 o 7 1 2 1170.81 1112.05 13.00 o 9 1 2 44.49 55.07 4.74 o 11 1 2 0.06 -0.52 4.20 o -12 2 2 173.85 170.52 6.89 o -10 2 2 446.47 443.30 8.88 o -8 2 2 1707.78 1562.99 15.44 o -6 2 2 22.42 42.79 2.18 o -4 2 2 5205.31 5655.49 35.51 o -2 2 2 6376.79 6602.21 38.86 o 0 2 2 4099.70 4344.49 26.38 o 2 2 2 5760.47 6298.95 44.07 o 4 2 2 311.02 311.19 4.84 o 6 2 2 350.27 331.58 6.36 o 8 2 2 922.66 896.74 11.82 o 10 2 2 535.71 499.18 10.47 o 12 2 2 305.20 281.17 14.19 o -13 3 2 162.58 168.67 10.73 o -11 3 2 96.00 98.57 5.36 o -9 3 2 178.17 180.87 5.00 o -7 3 2 10.00 6.44 1.91 o -5 3 2 394.65 414.88 4.87 o -3 3 2 1558.60 1863.03 12.24 o -1 3 2 3992.77 3841.99 24.56 o 1 3 2 24005.14 24570.23 152.37 o 3 3 2 9377.33 9872.26 68.53 o 5 3 2 6232.75 6095.73 45.52 o 7 3 2 2556.89 2459.29 22.49 o 9 3 2 911.85 919.50 13.06 o 11 3 2 87.93 98.71 6.72 o -12 4 2 58.88 58.62 5.10 o -10 4 2 10.55 4.45 3.06 o -8 4 2 0.67 3.56 2.37 o -6 4 2 251.24 236.86 4.00 o -4 4 2 593.12 730.23 6.48 o -2 4 2 4417.68 4901.01 30.94 o 0 4 2 88.98 107.81 2.07 o 2 4 2 4070.23 4484.21 30.38 o 4 4 2 2643.95 2616.25 19.15 o 6 4 2 574.37 603.10 7.44 o 8 4 2 77.40 84.18 4.07 o 10 4 2 8.46 7.05 4.29 o 12 4 2 77.62 84.90 7.93 o -13 5 2 272.46 284.92 12.99 o -11 5 2 150.17 140.46 6.15 o -9 5 2 40.96 33.72 3.14 o -7 5 2 154.90 141.61 3.45 o -5 5 2 1.32 4.58 1.40 o -3 5 2 1942.05 2142.48 14.52 o -1 5 2 3193.92 3221.08 21.82 o 1 5 2 1251.36 1078.68 8.57 o 3 5 2 5854.65 5868.02 40.51 o 5 5 2 5027.28 4946.82 35.36 o 7 5 2 1975.34 1879.63 16.69 o 9 5 2 960.69 951.94 14.61 o 11 5 2 556.37 581.89 13.01 o -12 6 2 739.71 767.96 15.81 o -10 6 2 1344.65 1349.66 17.33 o -8 6 2 1627.86 1626.64 15.57 o -6 6 2 2192.83 2307.56 19.87 o -4 6 2 4738.73 5101.97 32.96 o -2 6 2 2793.07 2959.88 20.08 o 0 6 2 16911.02 18511.87 144.33 o 2 6 2 11415.69 12662.70 82.57 o 4 6 2 395.52 425.33 5.08 o 6 6 2 37.25 35.47 2.48 o 8 6 2 11.99 11.88 3.09 o 10 6 2 374.08 377.31 10.02 o -11 7 2 914.34 940.73 15.95 o -9 7 2 1169.27 1174.59 13.65 o -7 7 2 1528.27 1590.81 13.21 o -5 7 2 2620.25 2722.54 19.04 o -3 7 2 7411.22 7596.66 47.59 o -1 7 2 951.82 902.12 8.81 o 1 7 2 0.19 1.20 1.02 o 3 7 2 12.51 14.79 1.32 o 5 7 2 492.08 506.94 6.16 o 7 7 2 78.48 77.64 3.45 o 9 7 2 30.36 30.87 3.83 o 11 7 2 246.24 256.92 9.35 o -12 8 2 55.91 55.38 6.27 o -10 8 2 6.34 3.73 3.78 o -8 8 2 0.42 2.10 2.30 o -6 8 2 796.67 834.66 8.93 o -4 8 2 2968.37 2943.40 21.07 o -2 8 2 2222.74 2057.18 16.41 o 0 8 2 1131.63 966.30 11.30 o 2 8 2 3462.08 3506.44 29.19 o 4 8 2 3416.24 3422.31 25.24 o 6 8 2 2917.83 2991.00 32.44 o 8 8 2 1337.09 1357.87 16.71 o 10 8 2 535.96 534.82 11.09 o -11 9 2 0.35 -1.61 3.85 o -9 9 2 37.11 37.20 3.94 o -7 9 2 94.15 98.68 3.00 o -5 9 2 598.55 551.40 6.67 o -3 9 2 1463.85 1436.99 12.36 o -1 9 2 2653.52 2820.53 44.05 o 1 9 2 2420.83 2424.56 25.16 o 3 9 2 1620.70 1622.67 13.53 o 5 9 2 556.59 495.35 6.40 o 7 9 2 409.12 401.67 8.12 o 9 9 2 327.16 310.57 6.79 o 11 9 2 193.76 225.31 8.79 o -12 10 2 75.74 79.20 12.23 o -10 10 2 505.28 500.79 10.03 o -8 10 2 1410.99 1346.16 16.97 o -6 10 2 5749.00 5655.51 51.93 o -4 10 2 8574.59 8597.45 64.85 o -2 10 2 7446.42 7677.18 69.13 o 0 10 2 3460.32 3638.06 40.13 o 2 10 2 1813.37 1855.30 19.49 o 4 10 2 84.91 106.56 2.85 o 6 10 2 118.22 135.22 4.71 o 8 10 2 41.47 40.99 4.42 o 10 10 2 2.19 -1.43 5.14 o -11 11 2 29.71 29.12 3.80 o -9 11 2 75.65 82.59 9.14 o -7 11 2 4.58 7.71 3.25 o -5 11 2 384.37 331.75 5.30 o -3 11 2 119.58 110.85 2.85 o -1 11 2 10.28 10.39 1.61 o 1 11 2 0.11 -1.61 2.28 o 3 11 2 19.81 9.72 1.64 o 5 11 2 140.32 120.89 3.73 o 7 11 2 7.49 8.29 3.72 o 9 11 2 17.86 16.39 5.41 o -10 12 2 398.97 379.27 13.46 o -8 12 2 712.70 693.19 14.91 o -6 12 2 1074.72 1085.75 15.76 o -4 12 2 1873.21 1850.76 17.33 o -2 12 2 2238.02 2193.30 21.67 o 0 12 2 2161.33 2160.98 25.98 o 2 12 2 1118.23 1155.45 12.98 o 4 12 2 147.75 149.86 4.02 o 6 12 2 72.32 73.39 4.55 o 8 12 2 102.80 96.08 7.26 o 10 12 2 4.96 -0.83 6.53 o -9 13 2 80.57 81.88 7.60 o -7 13 2 82.33 97.21 5.64 o -5 13 2 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