#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/57/2215716.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215716_Fobs loop_ _publ_author_name 'Song, Wen-Dong' 'Hong, Peng-Zhi' 'Wu, Zao-He' _publ_section_title ; 4-(2,2':6',2''-Terpyridyl)benzyltriphenylphosphonium bromide ; _journal_coeditor_code ZL2064 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4047 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.874 _cell_angle_gamma 90.000 _cell_length_a 12.7721 _cell_length_b 12.5364 _cell_length_c 23.3622 _exptl_crystal_F_000 1368.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file zl2064Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31297.92 31619.86 1059.34 o 4 0 0 4071.88 4054.78 75.43 o 6 0 0 4505.32 4638.05 149.35 o 8 0 0 1383.98 1345.49 89.70 o 10 0 0 18.17 2.15 101.47 o 12 0 0 556.25 510.79 163.95 o 14 0 0 1409.75 1527.21 261.86 o 1 1 0 3744.70 3557.67 38.02 o 2 1 0 3375.81 3173.28 53.96 o 3 1 0 15187.21 14729.98 191.06 o 4 1 0 97.89 72.89 18.23 o 5 1 0 156.53 221.93 23.10 o 6 1 0 1656.85 1769.00 46.17 o 7 1 0 1919.47 1885.58 54.94 o 8 1 0 64.06 61.97 39.22 o 9 1 0 1581.24 1465.48 136.27 o 10 1 0 156.40 74.03 86.56 o 11 1 0 1305.96 1351.12 156.08 o 12 1 0 15.82 2.14 92.76 o 13 1 0 11.65 64.19 99.26 o 14 1 0 1.86 3.49 105.93 o 0 2 0 4037.59 4052.67 25.73 o 1 2 0 198.11 150.25 19.42 o 2 2 0 226.12 177.58 26.64 o 3 2 0 2675.64 2814.98 51.80 o 4 2 0 3741.27 3568.94 61.33 o 5 2 0 26.33 18.09 17.84 o 6 2 0 5141.64 5137.08 112.10 o 7 2 0 11.02 38.16 26.84 o 8 2 0 2393.03 2571.85 97.84 o 9 2 0 79.05 124.88 57.64 o 10 2 0 1118.94 1169.53 135.90 o 11 2 0 488.90 656.01 188.61 o 12 2 0 19.60 7.73 90.28 o 13 2 0 0.88 0.33 95.90 o 14 2 0 254.74 335.23 132.15 o 1 3 0 16625.10 17333.77 297.81 o 2 3 0 3915.10 4142.63 60.82 o 3 3 0 9421.21 9033.67 120.70 o 4 3 0 1926.32 1939.44 48.35 o 5 3 0 9.31 20.80 21.22 o 6 3 0 987.56 1042.64 46.34 o 7 3 0 190.13 206.13 35.42 o 8 3 0 558.62 484.89 59.70 o 9 3 0 596.44 594.38 78.92 o 10 3 0 26.45 95.66 63.11 o 11 3 0 8.86 0.97 90.81 o 12 3 0 218.08 130.27 110.84 o 13 3 0 488.28 460.36 129.19 o 14 3 0 62.34 42.47 109.44 o 0 4 0 5745.18 6358.46 228.20 o 1 4 0 1658.51 1938.31 58.00 o 2 4 0 7080.96 7159.32 80.88 o 3 4 0 1411.34 1468.55 34.71 o 4 4 0 3817.79 3893.07 62.06 o 5 4 0 2410.92 2282.43 71.03 o 6 4 0 241.46 221.42 34.29 o 7 4 0 628.73 654.67 41.95 o 8 4 0 55.12 58.61 38.92 o 9 4 0 1155.24 1130.66 100.03 o 10 4 0 1160.39 1206.89 101.57 o 11 4 0 12.04 58.68 92.72 o 12 4 0 0.12 32.13 104.67 o 13 4 0 14.85 79.44 110.44 o 14 4 0 6.14 109.24 128.00 o 1 5 0 3173.74 3137.95 99.16 o 2 5 0 3028.34 2818.44 49.48 o 3 5 0 10.29 5.46 13.07 o 4 5 0 326.71 409.27 25.83 o 5 5 0 223.98 151.38 25.31 o 6 5 0 9.57 14.80 24.84 o 7 5 0 2337.34 2851.35 93.53 o 8 5 0 1351.48 1497.72 72.66 o 9 5 0 108.90 201.26 68.36 o 10 5 0 1.19 0.22 62.51 o 11 5 0 3.44 112.21 77.96 o 12 5 0 201.88 244.78 120.55 o 13 5 0 169.93 187.05 126.39 o 0 6 0 1112.85 983.82 74.76 o 1 6 0 1326.75 1234.53 53.43 o 2 6 0 120.68 169.14 46.35 o 3 6 0 94.67 108.99 24.13 o 4 6 0 2772.80 2897.71 60.28 o 5 6 0 6860.24 7015.28 103.01 o 6 6 0 11.35 31.10 23.90 o 7 6 0 1061.94 1166.28 70.74 o 8 6 0 38.29 19.64 55.62 o 9 6 0 693.87 598.71 88.72 o 10 6 0 157.82 324.86 79.19 o 11 6 0 95.73 261.07 115.67 o 12 6 0 45.13 81.43 159.42 o 13 6 0 70.44 195.40 185.38 o 1 7 0 1.50 29.82 25.87 o 2 7 0 3218.29 3384.29 82.79 o 3 7 0 631.90 680.50 47.14 o 4 7 0 802.79 871.43 88.88 o 5 7 0 66.15 74.46 51.15 o 6 7 0 326.73 396.04 62.56 o 7 7 0 221.28 235.87 94.31 o 8 7 0 1034.86 1020.38 134.16 o 9 7 0 43.35 174.55 147.36 o 10 7 0 58.94 8.64 93.17 o 11 7 0 9.23 1.98 89.91 o 12 7 0 62.76 10.09 100.05 o 13 7 0 5.03 1.62 161.47 o 0 8 0 1292.41 1267.84 70.85 o 1 8 0 479.78 534.30 42.02 o 2 8 0 83.75 161.39 39.16 o 3 8 0 1169.32 1376.71 60.80 o 4 8 0 316.78 357.69 52.63 o 5 8 0 81.22 116.77 50.77 o 6 8 0 221.72 81.49 79.25 o 7 8 0 0.74 5.15 75.49 o 8 8 0 0.16 33.38 83.05 o 9 8 0 248.73 315.10 105.44 o 10 8 0 43.84 205.37 107.85 o 11 8 0 69.82 194.80 159.42 o 12 8 0 23.09 77.30 113.44 o 1 9 0 835.26 913.66 105.76 o 2 9 0 503.13 561.66 98.83 o 3 9 0 2.21 7.29 71.66 o 4 9 0 732.70 701.02 152.31 o 5 9 0 298.69 453.17 152.20 o 6 9 0 531.91 191.74 133.89 o 7 9 0 183.94 44.35 73.62 o 8 9 0 333.25 267.74 129.91 o 9 9 0 38.02 3.69 83.37 o 10 9 0 1.73 2.55 87.55 o 11 9 0 27.72 174.80 118.97 o 0 10 0 817.32 521.03 148.65 o 1 10 0 5.19 57.58 80.23 o 2 10 0 694.02 622.70 231.97 o 3 10 0 43.57 78.01 82.83 o 4 10 0 142.58 125.81 137.88 o 5 10 0 570.07 474.39 161.68 o 6 10 0 18.25 26.93 115.47 o 7 10 0 22.70 116.55 133.03 o 8 10 0 41.85 4.63 141.00 o 9 10 0 73.14 0.97 139.17 o 10 10 0 59.10 0.11 166.64 o 1 11 0 1363.86 1386.16 144.50 o 2 11 0 15.76 104.21 90.60 o 3 11 0 46.22 148.00 137.88 o 4 11 0 43.29 214.36 138.74 o 5 11 0 28.73 47.72 128.94 o 6 11 0 115.43 2.91 116.01 o 7 11 0 81.42 333.82 156.73 o 8 11 0 5.82 2.69 136.80 o 9 11 0 10.73 3.45 147.14 o 0 12 0 593.68 311.19 164.16 o 1 12 0 98.67 83.85 106.16 o 2 12 0 3.85 39.46 94.75 o 3 12 0 441.36 321.64 168.04 o 4 12 0 31.59 69.37 147.25 o 5 12 0 125.47 233.96 177.84 o 6 12 0 150.66 4.20 149.19 o 7 12 0 0.11 92.42 151.02 o 8 12 0 20.54 84.13 159.74 o 1 13 0 1.05 0.16 103.25 o 2 13 0 213.60 138.63 172.89 o 3 13 0 525.96 796.24 210.59 o 4 13 0 11.84 7.22 150.70 o 5 13 0 21.84 0.22 149.51 o 6 13 0 0.55 0.65 156.94 o 7 13 0 1.08 0.00 144.66 o 0 14 0 103.98 0.43 157.59 o 1 14 0 12.17 3.73 111.55 o 2 14 0 17.96 17.45 165.56 o 3 14 0 8.20 30.59 165.67 o 4 14 0 1.21 0.75 160.93 o 5 14 0 3.39 2.26 173.75 o -13 0 1 49.15 37.05 139.49 o -11 0 1 47.77 70.34 130.23 o -9 0 1 1040.39 865.18 147.25 o -7 0 1 69.72 34.60 35.22 o -5 0 1 6546.62 7053.93 142.93 o -3 0 1 10877.94 10877.94 154.62 o -1 0 1 142.90 111.83 31.95 o 1 0 1 17968.95 20121.72 417.51 o 3 0 1 774.47 912.36 47.73 o 5 0 1 22706.09 22645.75 342.74 o 7 0 1 364.25 349.44 46.45 o 9 0 1 2045.36 2309.02 227.39 o 11 0 1 815.78 731.83 191.74 o 13 0 1 446.99 627.78 192.71 o -14 1 1 36.73 49.48 116.07 o -13 1 1 109.01 61.07 106.22 o -12 1 1 815.53 736.39 140.26 o -11 1 1 214.42 273.73 106.34 o -10 1 1 470.39 383.15 111.46 o -9 1 1 126.55 153.82 58.67 o -8 1 1 1787.61 1882.24 80.69 o -7 1 1 1048.08 1102.66 41.73 o -6 1 1 614.70 680.40 39.33 o -5 1 1 2294.39 2245.65 46.48 o -4 1 1 17281.07 15723.95 187.37 o -3 1 1 215.40 205.20 19.86 o -2 1 1 288.83 254.90 12.48 o -1 1 1 2543.25 2642.49 34.63 o 0 1 1 42704.73 45052.52 261.39 o 1 1 1 6509.45 6561.71 90.15 o 2 1 1 7813.83 7573.21 88.44 o 3 1 1 27068.70 27250.55 317.85 o 4 1 1 3142.73 3188.86 87.42 o 5 1 1 747.63 736.10 31.16 o 6 1 1 3427.83 3212.51 55.17 o 7 1 1 226.58 230.70 28.11 o 8 1 1 1161.06 1102.52 105.41 o 9 1 1 26.07 50.24 83.76 o 10 1 1 197.58 280.77 97.72 o 11 1 1 4.77 44.28 90.65 o 12 1 1 207.97 75.74 93.70 o 13 1 1 9.16 57.27 103.98 o 14 1 1 90.56 205.92 127.81 o -14 2 1 125.75 85.98 121.86 o -13 2 1 16.76 73.28 98.34 o -12 2 1 0.28 64.01 104.28 o -11 2 1 347.65 201.19 217.80 o -10 2 1 1400.14 1304.62 137.77 o -9 2 1 1674.45 1733.80 100.90 o -8 2 1 1368.65 1362.75 69.17 o -7 2 1 1421.52 1351.95 59.02 o -6 2 1 1992.92 2215.55 68.49 o -5 2 1 6102.30 5976.46 100.76 o -4 2 1 10582.49 10748.23 138.12 o -3 2 1 13331.75 14236.60 176.48 o -2 2 1 14947.96 14450.69 159.21 o -1 2 1 9978.17 10928.01 143.92 o 0 2 1 16768.96 15888.55 212.53 o 1 2 1 25440.68 25001.37 322.04 o 2 2 1 4165.87 4322.83 81.93 o 3 2 1 55.02 70.78 22.63 o 4 2 1 3201.58 3019.25 59.22 o 5 2 1 1773.09 1562.99 65.39 o 6 2 1 6.49 13.34 16.48 o 7 2 1 68.60 89.03 28.44 o 8 2 1 130.14 283.88 73.53 o 9 2 1 685.36 751.80 78.08 o 10 2 1 451.82 413.99 109.94 o 11 2 1 300.25 574.37 177.46 o 12 2 1 44.92 24.17 95.60 o 13 2 1 59.52 7.06 108.02 o 14 2 1 19.56 39.76 112.05 o -14 3 1 29.47 62.39 113.35 o -13 3 1 251.15 179.24 115.20 o -12 3 1 123.21 164.03 103.16 o -11 3 1 59.66 1.74 83.30 o -10 3 1 134.69 69.05 58.41 o -9 3 1 3.29 12.21 51.05 o -8 3 1 1454.00 1563.86 75.39 o -7 3 1 3408.39 3738.73 96.59 o -6 3 1 2100.76 2097.05 60.53 o -5 3 1 3065.41 3114.43 65.67 o -4 3 1 8033.03 7571.40 105.30 o -3 3 1 138.44 133.88 17.33 o -2 3 1 15358.82 16088.46 153.49 o -1 3 1 282.48 255.52 14.59 o 0 3 1 21091.50 22072.09 416.88 o 1 3 1 16423.51 17136.69 261.11 o 2 3 1 5704.43 5371.81 54.39 o 3 3 1 1539.16 1497.06 44.16 o 4 3 1 39.11 34.12 22.58 o 5 3 1 175.51 220.01 24.06 o 6 3 1 2526.03 2510.28 65.67 o 7 3 1 5335.70 5546.07 107.54 o 8 3 1 2172.32 2277.94 123.65 o 9 3 1 4.24 52.57 56.50 o 10 3 1 230.66 138.44 64.47 o 11 3 1 132.81 25.10 88.53 o 12 3 1 101.39 165.85 141.00 o 13 3 1 53.88 96.83 109.66 o 14 3 1 3.95 55.43 117.41 o -14 4 1 237.09 179.47 192.76 o -13 4 1 20.82 0.75 100.34 o -12 4 1 39.81 145.76 108.57 o -11 4 1 400.13 490.39 119.00 o -10 4 1 581.47 648.74 91.59 o -9 4 1 383.20 365.67 70.93 o -8 4 1 0.84 3.74 37.23 o -7 4 1 988.21 1037.48 54.78 o -6 4 1 3422.99 3454.30 80.87 o -5 4 1 147.20 181.48 31.84 o -4 4 1 334.76 331.14 22.32 o -3 4 1 2376.28 2357.10 75.19 o -2 4 1 293.08 276.52 20.04 o -1 4 1 85.31 114.51 13.99 o 0 4 1 4085.52 3870.44 56.71 o 1 4 1 6054.44 5210.81 212.36 o 2 4 1 269.75 234.73 20.62 o 3 4 1 3921.53 4308.48 57.44 o 4 4 1 8212.27 8033.85 100.71 o 5 4 1 4937.47 4670.43 89.56 o 6 4 1 16.46 26.46 25.43 o 7 4 1 415.27 452.52 44.01 o 8 4 1 10.44 42.08 40.60 o 9 4 1 610.87 737.83 85.01 o 10 4 1 54.95 51.26 54.95 o 11 4 1 1.09 66.41 97.53 o 12 4 1 0.03 31.00 94.53 o 13 4 1 8.38 4.21 102.51 o 14 4 1 1.18 57.79 122.59 o -14 5 1 59.67 54.23 114.88 o -13 5 1 18.45 1.94 100.50 o -12 5 1 39.64 7.58 98.32 o -11 5 1 37.71 173.03 78.00 o -10 5 1 30.49 24.61 66.05 o -9 5 1 279.02 393.44 89.91 o -8 5 1 732.35 769.36 54.16 o -7 5 1 2928.98 2990.37 82.22 o -6 5 1 2.78 10.51 22.44 o -5 5 1 1605.95 1779.84 50.13 o -4 5 1 182.64 234.45 20.50 o -3 5 1 11144.49 11228.48 121.34 o -2 5 1 2277.10 1925.67 47.15 o -1 5 1 954.95 1033.00 27.66 o 0 5 1 272.01 333.98 35.97 o 1 5 1 524.47 516.29 38.09 o 2 5 1 547.94 500.98 43.54 o 3 5 1 4295.18 4381.59 70.59 o 4 5 1 1994.32 1831.43 47.12 o 5 5 1 15.97 40.58 18.56 o 6 5 1 673.97 689.11 39.51 o 7 5 1 187.10 101.31 37.44 o 8 5 1 160.64 175.28 52.73 o 9 5 1 14.03 17.36 59.10 o 10 5 1 4.53 32.49 66.88 o 11 5 1 407.65 454.62 97.73 o 12 5 1 50.84 163.51 110.90 o 13 5 1 104.72 180.79 124.29 o -13 6 1 21.20 1.51 162.33 o -12 6 1 154.36 173.42 163.84 o -11 6 1 28.93 142.61 135.18 o -10 6 1 31.57 119.68 74.19 o -9 6 1 2.71 83.76 66.30 o -8 6 1 543.39 396.41 75.81 o -7 6 1 54.81 59.22 33.72 o -6 6 1 4450.20 4338.05 88.75 o -5 6 1 959.65 957.93 35.26 o -4 6 1 1227.90 1254.23 40.92 o -3 6 1 846.69 869.69 40.24 o -2 6 1 344.48 276.54 20.41 o -1 6 1 664.89 619.38 31.68 o 0 6 1 10455.88 11447.60 181.57 o 1 6 1 1321.73 1376.88 39.06 o 2 6 1 1573.40 1845.26 60.90 o 3 6 1 301.16 307.52 17.12 o 4 6 1 3081.01 3278.52 98.05 o 5 6 1 3.47 16.95 20.20 o 6 6 1 1144.55 1222.25 52.07 o 7 6 1 279.08 311.07 51.17 o 8 6 1 292.06 331.65 69.64 o 9 6 1 312.48 475.40 100.30 o 10 6 1 194.25 317.60 105.64 o 11 6 1 2.61 47.48 97.75 o 12 6 1 23.09 15.30 158.24 o 13 6 1 8.60 112.13 172.13 o -13 7 1 77.86 97.27 181.29 o -12 7 1 9.06 61.33 107.74 o -11 7 1 284.61 517.86 123.68 o -10 7 1 123.29 17.92 91.82 o -9 7 1 1082.13 1223.38 257.01 o -8 7 1 11.54 22.35 80.34 o -7 7 1 138.68 120.01 82.71 o -6 7 1 2.27 36.70 42.18 o -5 7 1 397.55 360.69 57.62 o -4 7 1 453.56 419.05 28.18 o -3 7 1 4300.56 4148.27 67.72 o -2 7 1 9.62 5.70 17.36 o -1 7 1 13.58 17.01 14.10 o 0 7 1 50.21 43.22 27.67 o 1 7 1 866.47 942.63 51.11 o 2 7 1 250.93 284.71 32.94 o 3 7 1 4097.68 3913.67 93.17 o 4 7 1 482.10 383.62 42.05 o 5 7 1 2975.39 3026.15 161.16 o 6 7 1 533.82 393.52 72.89 o 7 7 1 123.65 118.12 118.65 o 8 7 1 0.22 74.99 79.86 o 9 7 1 354.95 336.81 104.99 o 10 7 1 3.21 0.33 83.26 o 11 7 1 366.82 453.54 130.65 o 12 7 1 68.74 179.63 189.53 o -12 8 1 189.74 200.26 125.17 o -11 8 1 36.61 0.70 92.26 o -10 8 1 19.10 7.63 91.20 o -9 8 1 3.56 54.79 84.75 o -8 8 1 740.90 622.38 119.57 o -7 8 1 52.15 41.74 73.28 o -6 8 1 2361.63 2248.96 124.12 o -5 8 1 17.47 31.72 42.50 o -4 8 1 123.76 176.49 42.80 o -3 8 1 81.49 101.68 38.36 o -2 8 1 484.00 619.27 60.62 o -1 8 1 1.05 0.16 31.26 o 0 8 1 1243.53 1299.75 67.39 o 1 8 1 31.85 52.60 34.63 o 2 8 1 38.60 83.06 62.44 o 3 8 1 425.71 616.54 46.38 o 4 8 1 73.97 3.57 36.24 o 5 8 1 774.77 680.87 65.35 o 6 8 1 1547.09 920.17 109.09 o 7 8 1 0.35 3.62 72.37 o 8 8 1 314.58 98.69 84.99 o 9 8 1 27.75 18.86 91.32 o 10 8 1 195.94 206.97 109.07 o 11 8 1 8.61 1.62 98.99 o 12 8 1 3.27 93.41 116.39 o -11 9 1 57.27 17.98 97.20 o -10 9 1 0.03 1.03 93.97 o -9 9 1 393.93 537.08 119.99 o -8 9 1 53.96 116.65 85.07 o -7 9 1 31.21 58.69 69.74 o -6 9 1 14.91 57.84 116.77 o -5 9 1 16.32 11.63 108.90 o -4 9 1 88.50 34.79 115.90 o -3 9 1 943.22 906.55 152.37 o -2 9 1 243.98 319.61 90.70 o -1 9 1 4.31 17.54 71.61 o 0 9 1 15.86 23.48 75.22 o 1 9 1 1281.28 1384.64 146.12 o 2 9 1 120.23 159.65 87.95 o 3 9 1 2681.95 2615.46 152.53 o 4 9 1 28.37 85.74 124.95 o 5 9 1 871.09 695.10 159.85 o 6 9 1 206.88 261.32 91.95 o 7 9 1 46.25 152.24 126.03 o 8 9 1 1.73 3.08 84.89 o 9 9 1 87.03 13.21 91.17 o 10 9 1 0.37 69.75 101.05 o 11 9 1 50.94 54.99 112.36 o -11 10 1 9.29 171.49 179.67 o -10 10 1 277.54 278.02 185.70 o -9 10 1 36.04 60.86 143.80 o -8 10 1 9.05 320.24 166.53 o -7 10 1 13.86 0.22 121.50 o -6 10 1 154.69 429.14 166.64 o -5 10 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102.24 106.05 o -6 2 25 158.78 132.54 97.40 o -5 2 25 102.70 92.02 93.47 o -4 2 25 2.61 2.86 93.03 o -3 2 25 10.60 123.13 103.86 o -2 2 25 42.09 69.31 96.73 o -1 2 25 1.50 20.38 100.97 o 0 2 25 7.93 3.78 97.16 o 1 2 25 1.91 112.87 120.32 o 2 2 25 0.20 65.14 113.08 o -8 3 25 41.19 185.45 106.30 o -7 3 25 1.52 1.83 89.23 o -6 3 25 0.98 32.76 95.24 o -5 3 25 23.28 41.30 90.95 o -4 3 25 33.99 134.77 142.02 o -3 3 25 7.97 52.25 100.86 o -2 3 25 42.47 60.01 98.61 o -1 3 25 3.39 8.56 97.99 o 0 3 25 1.23 23.90 99.77 o 1 3 25 20.77 20.24 112.44 o 2 3 25 10.01 43.92 82.81 o -8 4 25 2.20 75.90 98.66 o -7 4 25 59.72 54.51 93.44 o -6 4 25 1.34 51.69 93.83 o -5 4 25 41.97 110.32 104.59 o -4 4 25 39.55 27.42 98.48 o -3 4 25 8.25 72.77 99.35 o -2 4 25 13.62 1.30 92.84 o -1 4 25 54.91 191.54 118.63 o 0 4 25 389.17 357.81 128.34 o 1 4 25 321.29 291.45 100.49 o -7 5 25 51.42 56.53 98.10 o -6 5 25 25.49 80.64 96.34 o -5 5 25 4.97 33.80 92.79 o -4 5 25 9.28 124.44 109.58 o -3 5 25 48.08 85.84 99.43 o -2 5 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