#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215738.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215738_Fobs loop_ _publ_author_name 'Liu, T.' 'Zhu, J. Y.' _publ_section_title ; Tetrakis(pyridine-\kN)bis(thiocyanato-\kN)chromium(II) ; _journal_coeditor_code AT2432 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2809 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.313 _cell_angle_gamma 90.000 _cell_length_a 12.4232 _cell_length_b 12.9354 _cell_length_c 15.1331 _exptl_crystal_F_000 1000.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file at2432Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aa in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 335.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4082.87 4703.30 84.66 o 4 0 0 1809.33 2391.51 33.02 o 6 0 0 4787.83 4523.86 61.29 o 8 0 0 1850.99 1986.82 31.25 o 10 0 0 2597.93 2738.49 42.63 o 12 0 0 428.28 429.27 14.41 o 14 0 0 183.34 160.55 26.65 o 1 1 0 120.05 42.79 1.97 o 3 1 0 7623.41 6050.46 55.42 o 5 1 0 1169.46 942.59 11.08 o 7 1 0 1159.20 1088.93 13.52 o 9 1 0 81.92 79.39 4.69 o 11 1 0 0.11 -3.14 4.07 o 13 1 0 63.25 72.83 6.82 o 2 2 0 28326.27 31487.13 302.81 o 4 2 0 20552.79 21353.60 171.72 o 6 2 0 15337.71 15682.57 145.86 o 8 2 0 2061.29 2224.86 41.29 o 10 2 0 736.82 746.78 12.09 o 12 2 0 304.50 305.21 9.01 o 14 2 0 187.71 179.25 8.86 o 1 3 0 28705.84 27562.84 369.80 o 3 3 0 530.06 389.59 4.75 o 5 3 0 57.88 43.47 2.83 o 7 3 0 3773.49 3172.74 28.39 o 9 3 0 0.67 -1.30 3.22 o 11 3 0 77.29 56.15 5.49 o 13 3 0 8.74 4.94 5.58 o 2 4 0 28157.59 29116.53 323.00 o 4 4 0 19619.25 20016.55 161.08 o 6 4 0 2319.05 2606.36 23.49 o 8 4 0 4061.70 4226.68 42.39 o 10 4 0 184.41 216.29 7.05 o 12 4 0 504.57 493.54 11.46 o 14 4 0 371.97 420.99 14.46 o 1 5 0 335.39 287.53 3.63 o 3 5 0 0.92 1.39 1.88 o 5 5 0 64.74 68.38 2.83 o 7 5 0 250.65 292.61 18.47 o 9 5 0 904.61 880.38 13.38 o 11 5 0 216.31 223.59 9.14 o 13 5 0 27.82 29.39 6.75 o 2 6 0 9688.31 9430.01 77.19 o 4 6 0 1870.22 1906.99 20.24 o 6 6 0 333.31 465.88 7.06 o 8 6 0 2439.48 2536.86 32.30 o 10 6 0 1270.51 1305.97 18.19 o 12 6 0 519.32 520.07 12.34 o 1 7 0 2404.46 1858.76 17.29 o 3 7 0 2164.23 2076.87 19.57 o 5 7 0 1571.09 1362.32 16.09 o 7 7 0 921.53 908.90 13.09 o 9 7 0 86.41 91.46 5.57 o 11 7 0 57.12 74.27 6.70 o 13 7 0 3.38 6.07 6.97 o 0 8 0 2153.66 2084.72 25.11 o 2 8 0 1463.98 1670.80 14.89 o 4 8 0 1187.75 1325.36 15.93 o 6 8 0 1102.15 1178.72 16.56 o 8 8 0 180.51 205.77 20.82 o 10 8 0 1293.95 1393.81 19.46 o 12 8 0 539.72 598.69 13.71 o 1 9 0 205.26 199.48 5.72 o 3 9 0 87.07 86.13 4.85 o 5 9 0 193.39 182.06 7.10 o 7 9 0 0.01 -0.91 4.88 o 9 9 0 13.84 18.59 10.43 o 11 9 0 39.13 39.50 9.35 o 0 10 0 5201.27 5146.51 71.71 o 2 10 0 165.09 125.98 10.56 o 4 10 0 892.51 1010.65 14.66 o 6 10 0 1805.97 1857.50 35.58 o 8 10 0 341.38 303.86 18.02 o 10 10 0 327.72 280.51 19.39 o 1 11 0 74.64 102.25 5.71 o 3 11 0 76.21 65.00 7.46 o 5 11 0 235.61 240.71 12.12 o 7 11 0 164.49 173.86 13.01 o 9 11 0 108.33 98.83 14.61 o 0 12 0 237.12 274.14 11.18 o 2 12 0 616.14 627.22 14.95 o 4 12 0 434.81 468.05 19.90 o 6 12 0 613.70 645.12 14.77 o 8 12 0 239.39 209.03 17.29 o 1 13 0 225.46 238.37 13.66 o 3 13 0 45.44 46.75 5.57 o 5 13 0 38.72 48.05 7.07 o 7 13 0 8.23 2.68 8.64 o 0 14 0 210.69 182.00 14.68 o 2 14 0 777.22 838.64 18.03 o 4 14 0 241.54 246.21 34.10 o 6 14 0 17.23 4.12 7.79 o 1 15 0 16.91 23.28 6.55 o 3 15 0 0.00 -1.54 6.33 o -13 1 1 363.06 383.53 10.67 o -11 1 1 276.18 304.00 8.28 o -9 1 1 6830.15 6837.07 65.67 o -7 1 1 1061.44 1316.54 15.38 o -5 1 1 9419.39 9653.86 88.00 o -3 1 1 37520.00 40830.52 372.76 o -1 1 1 30203.27 35322.61 936.55 o 1 1 1 14169.87 16627.37 150.03 o 7 1 1 2511.85 2567.65 26.80 o 9 1 1 3477.15 3359.61 35.14 o 11 1 1 39.67 58.17 5.78 o 13 1 1 281.40 268.14 9.18 o -14 2 1 4.15 9.45 6.02 o -12 2 1 319.46 325.88 9.32 o -10 2 1 1098.43 1114.85 15.53 o -8 2 1 213.28 175.64 5.27 o -6 2 1 594.78 436.51 7.45 o -4 2 1 1919.83 1546.16 12.73 o -2 2 1 28479.22 26711.67 411.42 o 0 2 1 2019.61 1550.54 14.78 o 2 2 1 8822.08 7508.63 60.86 o 4 2 1 224.27 151.07 2.78 o 6 2 1 2184.90 1864.04 15.67 o 8 2 1 359.88 348.71 13.15 o 10 2 1 297.13 297.99 7.93 o 12 2 1 79.05 80.49 6.15 o 14 2 1 11.38 8.92 6.86 o -13 3 1 428.07 440.08 14.78 o -11 3 1 481.30 497.92 10.38 o -9 3 1 1488.02 1677.74 22.48 o -7 3 1 10325.21 10407.07 85.62 o -5 3 1 10592.77 11010.15 89.65 o -1 3 1 3181.91 3821.74 40.63 o 1 3 1 16523.99 17588.61 174.00 o 3 3 1 10119.38 10478.89 84.96 o 5 3 1 9277.70 9188.91 75.26 o 7 3 1 480.46 524.13 8.58 o 9 3 1 17.79 11.00 3.69 o 11 3 1 825.88 843.28 13.94 o 13 3 1 186.36 125.65 11.59 o -14 4 1 11.80 10.52 6.77 o -12 4 1 1.24 1.03 5.07 o -10 4 1 238.33 192.83 6.63 o -8 4 1 4.42 5.96 3.24 o -6 4 1 514.05 492.08 6.54 o -4 4 1 144.38 131.96 3.14 o -2 4 1 4230.79 3489.98 26.81 o 0 4 1 1495.66 1250.37 11.60 o 2 4 1 3547.55 2978.97 25.47 o 4 4 1 9304.42 8375.92 68.83 o 6 4 1 420.31 376.22 5.70 o 8 4 1 83.26 90.05 6.05 o 10 4 1 93.12 82.87 5.37 o 12 4 1 135.39 132.06 7.03 o -13 5 1 388.39 396.82 11.34 o -11 5 1 2742.96 2962.01 33.30 o -9 5 1 284.92 225.71 6.65 o -7 5 1 3351.81 3566.03 31.72 o -5 5 1 1628.43 1948.33 18.30 o -3 5 1 7330.33 7998.89 65.78 o -1 5 1 7655.34 7669.10 57.21 o 1 5 1 921.92 1163.23 10.14 o 3 5 1 4230.12 4791.85 45.17 o 5 5 1 7270.46 6860.53 57.38 o 7 5 1 729.15 799.62 15.42 o 9 5 1 111.79 115.06 5.45 o 11 5 1 1509.89 1568.38 25.30 o 13 5 1 195.31 169.85 8.90 o -12 6 1 76.64 76.04 7.02 o -10 6 1 0.06 0.41 4.33 o -8 6 1 1.21 -0.21 3.37 o -6 6 1 366.90 325.78 5.84 o -4 6 1 3447.94 3091.66 27.44 o -2 6 1 4684.88 3821.44 32.87 o 0 6 1 5184.87 4299.08 33.12 o 2 6 1 3452.14 3158.83 27.58 o 4 6 1 593.59 558.44 8.15 o 6 6 1 636.21 668.49 8.74 o 8 6 1 229.86 253.17 13.18 o 10 6 1 0.13 2.65 4.65 o 12 6 1 4.09 11.74 6.27 o -13 7 1 223.21 192.59 9.33 o -11 7 1 488.36 530.24 11.83 o -9 7 1 635.00 715.84 12.16 o -7 7 1 649.68 744.38 9.88 o -5 7 1 994.05 1143.86 16.15 o -3 7 1 2029.74 2095.36 22.02 o -1 7 1 3029.45 3319.27 26.37 o 1 7 1 331.01 441.30 6.58 o 3 7 1 1819.76 1739.62 16.90 o 5 7 1 1548.58 1713.44 22.17 o 7 7 1 2789.36 2877.60 34.91 o 9 7 1 1139.94 1129.45 19.93 o 11 7 1 899.33 887.04 18.64 o -12 8 1 0.06 1.44 6.10 o -10 8 1 547.34 640.14 22.89 o -8 8 1 161.90 161.27 10.57 o -6 8 1 1.77 -0.01 3.26 o -4 8 1 22.44 13.28 3.06 o -2 8 1 68.04 49.46 2.90 o 0 8 1 2025.09 1886.16 18.21 o 2 8 1 579.49 502.40 8.10 o 4 8 1 31.03 28.19 3.26 o 6 8 1 215.01 199.62 5.97 o 8 8 1 17.44 10.73 6.12 o 10 8 1 80.49 94.95 8.88 o 12 8 1 28.24 18.62 9.04 o -11 9 1 98.22 75.77 16.28 o -9 9 1 1529.10 1658.20 30.33 o -7 9 1 1.74 8.87 4.05 o -5 9 1 220.49 295.39 7.21 o -3 9 1 2308.12 2436.29 26.41 o -1 9 1 337.74 416.00 7.82 o 1 9 1 2952.78 3029.01 32.15 o 3 9 1 2575.28 2829.15 26.51 o 5 9 1 348.78 398.40 10.92 o 7 9 1 789.98 732.06 17.03 o 9 9 1 1285.63 1386.36 39.11 o 11 9 1 103.07 64.80 9.71 o -10 10 1 33.61 25.11 12.26 o -8 10 1 4.36 -0.13 8.54 o -6 10 1 34.24 34.31 5.41 o -4 10 1 3.11 5.61 3.60 o -2 10 1 1707.63 1506.43 18.51 o 0 10 1 76.77 58.75 5.03 o 2 10 1 1566.05 1404.65 17.63 o 4 10 1 203.40 229.73 6.96 o 6 10 1 9.44 7.72 5.13 o 8 10 1 59.41 39.85 11.15 o 10 10 1 16.96 19.56 12.65 o -9 11 1 455.90 504.31 23.38 o -7 11 1 251.79 254.00 29.02 o -5 11 1 848.11 881.25 23.64 o -3 11 1 615.46 730.46 17.38 o -1 11 1 21.59 22.57 3.99 o 1 11 1 446.33 488.05 9.69 o 3 11 1 1864.06 1954.54 23.34 o 5 11 1 903.53 852.60 16.09 o 7 11 1 453.93 444.73 15.06 o 9 11 1 370.04 339.76 20.37 o -8 12 1 312.87 351.19 19.84 o -6 12 1 6.60 1.61 5.98 o -4 12 1 150.29 166.61 12.37 o -2 12 1 124.01 144.59 6.31 o 0 12 1 188.05 197.34 6.87 o 2 12 1 1.20 2.52 4.33 o 4 12 1 16.34 23.21 5.20 o 6 12 1 15.42 21.51 6.73 o 8 12 1 0.05 0.72 11.48 o -7 13 1 317.57 300.55 11.77 o -5 13 1 429.62 432.30 12.96 o -3 13 1 111.49 121.47 6.69 o -1 13 1 1149.52 1224.65 24.46 o 1 13 1 961.39 1013.15 20.93 o 3 13 1 14.79 5.89 4.96 o 5 13 1 495.73 472.71 13.42 o 7 13 1 114.45 93.18 15.98 o -6 14 1 1.01 -0.89 7.71 o -4 14 1 18.75 15.89 6.88 o -2 14 1 3.47 -0.58 5.37 o 0 14 1 9.36 14.63 5.59 o 2 14 1 1.05 3.53 5.42 o 4 14 1 6.70 6.59 7.21 o 6 14 1 3.61 7.87 7.38 o -5 15 1 114.37 104.27 10.02 o -3 15 1 165.05 134.56 9.61 o -1 15 1 434.09 440.10 12.67 o 1 15 1 195.60 192.47 8.62 o 3 15 1 73.95 46.27 7.05 o -14 0 2 429.31 416.38 16.44 o -12 0 2 1188.79 1316.90 36.09 o -10 0 2 47.99 69.40 6.69 o -8 0 2 2657.26 2692.57 39.87 o -6 0 2 6047.67 5888.19 78.20 o -2 0 2 6829.27 8046.40 83.57 o 0 0 2 22898.77 27656.08 502.92 o 2 0 2 31366.64 25730.90 267.11 o 4 0 2 194.09 350.00 10.32 o 6 0 2 4133.41 4016.42 76.79 o 8 0 2 115.05 140.01 7.17 o 10 0 2 947.38 1023.73 55.67 o 12 0 2 32.71 20.21 7.17 o 14 0 2 174.97 137.15 14.48 o -15 1 2 7.36 10.56 7.34 o -13 1 2 10.36 14.36 5.55 o -11 1 2 247.63 223.87 10.19 o -9 1 2 362.87 305.59 7.19 o -7 1 2 1984.97 1778.17 16.82 o -5 1 2 7237.37 6468.43 62.52 o -3 1 2 10618.20 8871.15 79.91 o -1 1 2 92.50 47.13 1.75 o 1 1 2 1642.70 1295.32 14.49 o 3 1 2 16701.83 14710.54 144.52 o 5 1 2 575.32 563.15 5.90 o 7 1 2 713.58 660.62 9.93 o 9 1 2 67.03 52.93 4.34 o 11 1 2 33.16 25.99 4.81 o 13 1 2 49.88 48.12 6.78 o -14 2 2 206.04 191.77 8.85 o -12 2 2 387.01 339.25 11.18 o -10 2 2 1173.60 1227.08 16.67 o -8 2 2 2219.97 2210.88 23.99 o -6 2 2 6331.18 6828.21 57.17 o 0 2 2 4838.81 5722.38 52.29 o 4 2 2 982.23 1268.15 16.31 o 6 2 2 95.38 153.47 3.16 o 8 2 2 1190.95 1232.67 15.76 o 10 2 2 508.12 441.83 15.60 o 12 2 2 124.19 88.24 6.33 o -13 3 2 2.08 6.49 5.47 o -11 3 2 744.03 729.57 20.54 o -9 3 2 1550.95 1334.32 16.88 o -7 3 2 69.86 79.62 4.56 o -5 3 2 4843.38 3998.08 31.04 o -3 3 2 0.36 -1.51 1.15 o -1 3 2 2999.12 2448.16 23.30 o 1 3 2 14478.44 12915.24 103.69 o 3 3 2 135.50 101.79 2.84 o 5 3 2 784.58 720.77 8.09 o 7 3 2 636.90 590.03 22.36 o 9 3 2 1480.14 1452.90 33.38 o 11 3 2 49.66 64.30 5.42 o 13 3 2 68.83 75.14 7.08 o -14 4 2 297.83 258.88 9.90 o -12 4 2 197.95 175.15 7.34 o -10 4 2 588.99 634.80 12.72 o -8 4 2 929.30 1082.37 20.59 o -6 4 2 16.77 9.99 1.96 o -4 4 2 14323.87 14272.99 115.60 o -2 4 2 1490.75 1956.90 15.73 o 2 4 2 24095.51 24770.51 220.11 o 4 4 2 34.83 82.83 3.01 o 6 4 2 297.66 406.54 9.14 o 8 4 2 321.70 410.65 12.13 o 10 4 2 250.14 231.75 10.51 o 12 4 2 775.18 777.17 14.60 o -13 5 2 4.13 11.58 5.75 o -11 5 2 145.68 163.13 8.09 o -9 5 2 22.12 17.41 3.88 o -7 5 2 1194.60 1061.80 11.35 o -5 5 2 301.17 328.28 7.36 o -3 5 2 1.90 0.66 1.49 o -1 5 2 234.45 217.69 4.88 o 1 5 2 1589.81 1406.53 14.21 o 3 5 2 1175.59 1129.45 15.69 o 5 5 2 514.47 443.41 7.05 o 7 5 2 547.00 499.92 10.44 o 9 5 2 6.48 8.38 4.09 o 11 5 2 52.00 66.51 6.17 o 13 5 2 18.36 14.11 7.01 o -12 6 2 127.62 108.98 7.07 o -10 6 2 941.47 955.07 14.61 o -8 6 2 419.36 489.78 9.62 o -6 6 2 91.83 187.47 8.18 o -4 6 2 6354.89 6517.42 54.67 o -2 6 2 2086.41 2211.49 20.18 o 0 6 2 1166.40 812.37 8.97 o 2 6 2 6224.52 6157.14 51.35 o 4 6 2 1875.06 2155.61 22.46 o 6 6 2 2650.34 2770.67 28.46 o 8 6 2 1429.76 1371.05 27.57 o 10 6 2 57.10 47.83 5.34 o 12 6 2 331.01 308.83 10.41 o -13 7 2 13.56 10.98 6.85 o -11 7 2 80.16 89.10 11.41 o -9 7 2 669.27 693.67 11.90 o -7 7 2 1.13 3.28 3.05 o -5 7 2 844.82 682.33 20.15 o -3 7 2 685.73 562.13 7.97 o -1 7 2 1555.87 1443.43 12.72 o 1 7 2 904.99 643.09 6.93 o 3 7 2 706.73 576.91 9.16 o 5 7 2 1.62 0.01 2.97 o 7 7 2 909.99 858.11 14.28 o 9 7 2 214.06 285.68 11.42 o 11 7 2 98.63 129.90 13.75 o -12 8 2 398.19 423.75 12.72 o -10 8 2 613.93 605.08 13.62 o -8 8 2 23.50 39.11 4.62 o -6 8 2 1113.24 1127.11 14.76 o -4 8 2 45.59 102.74 5.12 o -2 8 2 4096.03 4292.32 37.51 o 0 8 2 3881.37 3949.51 34.74 o 2 8 2 407.38 522.55 7.60 o 4 8 2 3319.26 3345.09 46.02 o 6 8 2 469.06 515.96 12.82 o 8 8 2 938.96 920.04 28.86 o 10 8 2 614.93 711.37 22.32 o 12 8 2 51.41 18.34 10.32 o -11 9 2 0.10 1.25 6.65 o -9 9 2 12.68 6.78 6.82 o -7 9 2 4.66 7.18 3.98 o -5 9 2 0.59 -0.70 3.33 o -3 9 2 54.92 77.17 3.74 o -1 9 2 335.76 316.78 6.01 o 1 9 2 738.79 692.26 9.24 o 3 9 2 32.23 25.62 3.19 o 5 9 2 1.59 1.38 4.25 o 7 9 2 14.63 14.66 6.33 o 9 9 2 12.62 7.30 9.46 o 11 9 2 13.16 15.90 9.75 o -10 10 2 40.72 14.21 7.67 o -8 10 2 430.24 458.03 14.31 o -6 10 2 1016.75 1080.61 17.98 o -4 10 2 19.32 26.45 4.54 o -2 10 2 1081.75 1194.57 29.14 o 0 10 2 3267.54 3316.55 38.67 o 2 10 2 51.89 71.91 4.46 o 4 10 2 2142.31 2245.26 25.61 o 6 10 2 875.65 871.84 16.05 o 8 10 2 17.95 15.52 10.50 o 10 10 2 385.64 376.99 22.00 o -9 11 2 3.89 9.72 11.67 o -7 11 2 39.32 27.85 6.04 o -5 11 2 93.13 96.30 6.81 o -3 11 2 22.80 15.18 4.17 o -1 11 2 13.69 13.99 3.76 o 1 11 2 24.53 35.18 4.26 o 3 11 2 250.31 252.53 10.36 o 5 11 2 142.63 142.08 7.53 o 7 11 2 112.89 107.74 9.45 o 9 11 2 70.89 83.62 14.61 o -10 12 2 64.41 42.20 15.00 o -8 12 2 428.53 372.22 20.64 o -6 12 2 342.80 382.75 12.16 o -4 12 2 795.44 766.82 15.67 o -2 12 2 98.46 106.29 6.78 o 0 12 2 652.84 668.58 11.96 o 2 12 2 751.50 727.01 12.62 o 4 12 2 273.85 267.68 9.23 o 6 12 2 350.76 358.65 11.61 o 8 12 2 163.06 175.90 16.51 o -7 13 2 13.81 17.97 7.32 o -5 13 2 0.06 3.59 6.35 o -3 13 2 88.11 103.99 6.51 o -1 13 2 67.46 68.80 5.70 o 1 13 2 189.47 211.92 7.76 o 3 13 2 14.98 22.85 5.40 o 5 13 2 2.00 8.92 6.88 o 7 13 2 11.75 15.65 12.39 o -6 14 2 71.53 39.61 9.91 o -4 14 2 619.77 669.54 16.21 o -2 14 2 208.76 175.73 8.72 o 0 14 2 166.50 142.36 7.42 o 2 14 2 513.32 578.59 12.68 o 4 14 2 5.73 0.59 9.68 o 6 14 2 131.81 115.34 12.90 o -5 15 2 2.77 0.53 8.34 o -3 15 2 3.83 -1.66 7.35 o -1 15 2 9.95 8.39 7.11 o 1 15 2 11.87 9.62 7.54 o 3 15 2 0.02 1.65 7.13 o -15 1 3 457.55 464.55 12.89 o -13 1 3 155.29 144.91 7.36 o -11 1 3 958.32 932.91 14.23 o -9 1 3 2925.85 2848.81 30.25 o -7 1 3 72.30 149.95 3.97 o -5 1 3 9561.65 9423.88 76.78 o 1 1 3 24372.03 26933.68 505.64 o 7 1 3 4509.42 4466.81 44.08 o 9 1 3 933.49 956.78 14.07 o 11 1 3 156.88 161.68 14.15 o 13 1 3 372.92 357.07 11.53 o -14 2 3 63.19 71.46 7.26 o -12 2 3 81.47 86.54 8.33 o -10 2 3 1015.07 949.39 13.87 o -8 2 3 738.91 672.53 10.10 o -6 2 3 670.07 517.35 5.86 o -4 2 3 3692.18 3118.94 24.27 o -2 2 3 5786.82 4675.66 51.28 o 0 2 3 39146.60 38054.57 394.46 o 2 2 3 4501.51 3719.85 39.99 o 4 2 3 11.92 22.19 2.73 o 6 2 3 284.51 190.31 3.75 o 8 2 3 183.01 190.93 8.78 o 10 2 3 187.69 191.01 9.23 o 12 2 3 51.27 59.44 6.29 o -13 3 3 626.19 604.51 12.98 o -11 3 3 315.65 307.03 8.47 o -9 3 3 1190.58 1238.70 15.96 o -7 3 3 5160.77 5065.02 39.37 o -5 3 3 338.56 610.15 6.51 o -3 3 3 2530.70 2809.83 24.26 o -1 3 3 6803.59 7298.14 59.37 o 1 3 3 38.24 23.18 1.52 o 3 3 3 3187.99 3664.49 34.69 o 5 3 3 3529.14 3736.08 32.36 o 7 3 3 1144.69 1272.42 15.83 o 9 3 3 520.89 535.69 10.24 o 11 3 3 622.48 639.66 12.50 o 13 3 3 163.37 139.15 8.33 o -14 4 3 0.10 0.05 6.08 o -12 4 3 6.10 8.87 5.21 o -10 4 3 3.59 7.22 3.90 o -8 4 3 288.67 284.28 13.25 o -6 4 3 818.04 662.28 7.34 o -4 4 3 494.32 475.15 6.12 o -2 4 3 246.28 233.47 3.74 o 0 4 3 4176.77 3547.88 32.65 o 2 4 3 8685.39 7914.91 64.71 o 4 4 3 1168.00 1120.61 12.70 o 6 4 3 1020.43 863.16 9.97 o 8 4 3 270.48 299.46 7.48 o 10 4 3 62.28 73.41 5.79 o 12 4 3 46.84 50.83 6.60 o -13 5 3 462.89 443.49 15.89 o -11 5 3 251.13 242.42 11.51 o -9 5 3 20.79 12.72 3.68 o -7 5 3 5753.76 5610.61 43.78 o -5 5 3 1374.29 1724.37 16.61 o -3 5 3 1932.00 2129.04 19.32 o -1 5 3 5510.68 5464.57 45.59 o 3 5 3 6080.02 6195.69 57.71 o 5 5 3 4353.14 4394.72 42.35 o 7 5 3 241.04 167.33 7.71 o 9 5 3 1262.79 1389.71 18.49 o 11 5 3 600.65 632.10 13.94 o -14 6 3 62.76 85.53 11.27 o -12 6 3 3.86 0.54 5.14 o -10 6 3 0.23 -2.70 4.39 o -8 6 3 282.60 257.30 8.26 o -6 6 3 2432.92 2230.88 21.25 o -4 6 3 37.20 26.72 2.95 o -2 6 3 2401.32 1992.06 21.38 o 0 6 3 4370.28 3712.79 32.12 o 2 6 3 2787.24 2463.53 22.15 o 4 6 3 131.99 138.75 4.27 o 6 6 3 108.91 95.61 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