#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/57/2215751.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215751_Fobs loop_ _publ_author_name 'Dufresne, St\'ephane' 'Gaultois, Michael' 'Skene, W. G.' _publ_section_title ; Disodium 5,5'-diamino-2,2'-ethylenedibenzenesulfonate tetrahydrate ; _journal_coeditor_code AV3102 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2714 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.860 _cell_angle_gamma 90.000 _cell_length_a 8.1415 _cell_length_b 18.6885 _cell_length_c 6.3230 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.8103 _[local]_cod_data_source_file av3102Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sken23 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 124.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 249.77 273.71 100.83 o 2 0 0 1689.79 1748.84 15.92 o 3 0 0 756.01 889.38 12.63 o 4 0 0 236.29 410.90 10.65 o 5 0 0 3075.23 2784.11 31.75 o 6 0 0 320.14 304.56 11.42 o 7 0 0 316.63 337.77 12.54 o 8 0 0 492.07 477.02 16.41 o 9 0 0 3.52 4.55 2.57 o 1 1 0 1750.30 2172.19 215.80 o 2 1 0 3788.69 3947.96 102.00 o 3 1 0 56.04 46.39 4.72 o 4 1 0 1.58 2.54 1.07 o 5 1 0 195.76 205.60 9.61 o 6 1 0 527.07 440.41 33.23 o 7 1 0 24.96 27.92 3.11 o 8 1 0 11.87 8.74 2.06 o 9 1 0 19.17 19.56 2.69 o 0 2 0 571.21 615.83 209.83 o 1 2 0 3876.93 2974.70 61.75 o 2 2 0 746.04 884.25 9.51 o 3 2 0 153.61 139.62 10.07 o 4 2 0 218.87 241.33 5.72 o 5 2 0 2334.74 2172.33 100.49 o 6 2 0 30.01 30.02 3.46 o 7 2 0 247.00 274.33 16.38 o 8 2 0 14.22 14.83 2.38 o 9 2 0 3.09 3.03 1.52 o 1 3 0 962.18 818.52 60.48 o 2 3 0 1398.57 1331.65 110.71 o 3 3 0 60.27 41.24 2.65 o 4 3 0 4715.69 4716.98 43.32 o 5 3 0 554.05 495.75 10.75 o 6 3 0 23.40 19.45 2.33 o 7 3 0 2.45 4.80 2.08 o 8 3 0 3.46 2.84 1.61 o 9 3 0 321.64 282.11 6.23 o 0 4 0 10920.25 5446.33 5174.43 o 1 4 0 387.80 417.12 28.34 o 2 4 0 658.70 766.09 62.00 o 3 4 0 556.03 535.93 31.59 o 4 4 0 877.59 900.62 46.61 o 5 4 0 879.66 717.46 98.72 o 6 4 0 15.17 14.57 3.44 o 7 4 0 124.25 116.10 4.97 o 8 4 0 604.72 677.56 21.81 o 9 4 0 111.61 128.80 4.47 o 1 5 0 7509.00 6791.18 203.12 o 2 5 0 1531.58 1582.99 94.69 o 3 5 0 1334.33 1540.19 44.44 o 4 5 0 437.03 306.67 291.08 o 5 5 0 827.76 715.17 16.07 o 6 5 0 1908.24 2324.01 41.43 o 7 5 0 306.17 323.82 19.75 o 8 5 0 19.05 21.04 7.46 o 9 5 0 305.02 325.92 6.63 o 0 6 0 454.66 273.82 11.91 o 1 6 0 713.81 842.20 55.93 o 2 6 0 345.35 331.58 4.93 o 3 6 0 913.72 1028.76 55.62 o 4 6 0 15.17 21.15 2.76 o 5 6 0 1467.77 1251.15 22.60 o 6 6 0 376.97 401.57 8.52 o 7 6 0 121.59 125.14 6.63 o 8 6 0 82.00 89.21 4.55 o 9 6 0 26.49 26.71 2.82 o 1 7 0 238.37 217.47 17.68 o 2 7 0 1409.20 1454.39 131.08 o 3 7 0 70.27 57.78 3.08 o 4 7 0 486.56 481.77 12.44 o 5 7 0 1413.37 1205.17 22.17 o 6 7 0 370.37 425.34 13.32 o 7 7 0 18.65 20.28 2.75 o 8 7 0 333.32 358.05 7.85 o 9 7 0 3.72 2.94 1.37 o 0 8 0 4112.64 3444.20 54.79 o 1 8 0 1781.38 1477.73 132.53 o 2 8 0 2474.60 2474.57 262.22 o 3 8 0 1434.22 1585.57 141.51 o 4 8 0 81.22 65.54 4.60 o 5 8 0 1376.75 819.48 14.81 o 6 8 0 247.30 260.52 7.13 o 7 8 0 216.94 232.16 6.78 o 8 8 0 997.16 1008.20 12.94 o 9 8 0 276.56 283.45 16.97 o 1 9 0 1345.44 1276.22 115.37 o 2 9 0 1.59 4.55 1.58 o 3 9 0 220.61 213.89 14.91 o 4 9 0 1840.08 1270.87 180.98 o 5 9 0 418.17 432.64 14.67 o 6 9 0 249.59 276.20 8.75 o 7 9 0 958.94 1044.33 14.32 o 8 9 0 43.42 39.98 5.41 o 9 9 0 518.33 539.95 8.41 o 0 10 0 131.21 147.10 12.34 o 1 10 0 1913.03 1219.97 121.91 o 2 10 0 393.03 180.24 180.74 o 3 10 0 1510.44 762.41 19.75 o 4 10 0 240.08 146.47 9.87 o 5 10 0 16.52 17.71 2.84 o 6 10 0 63.21 76.65 4.25 o 7 10 0 125.44 133.38 5.17 o 8 10 0 138.97 124.65 6.27 o 1 11 0 0.07 0.26 1.80 o 2 11 0 636.45 632.45 24.40 o 3 11 0 258.73 99.28 6.97 o 4 11 0 143.67 67.86 6.87 o 5 11 0 1.00 1.89 2.24 o 6 11 0 249.60 254.73 7.32 o 7 11 0 240.41 234.52 16.41 o 8 11 0 171.50 165.01 6.15 o 0 12 0 467.35 183.35 8.62 o 1 12 0 70.95 27.41 3.27 o 2 12 0 6.70 3.53 2.76 o 3 12 0 268.67 196.09 12.25 o 4 12 0 29.82 40.32 6.34 o 5 12 0 1511.11 1830.95 126.38 o 6 12 0 1399.40 1536.36 50.97 o 7 12 0 109.15 112.31 5.13 o 8 12 0 83.59 68.56 4.67 o 1 13 0 182.13 102.48 19.70 o 2 13 0 323.38 230.60 14.52 o 3 13 0 12.89 4.79 4.74 o 4 13 0 8.52 14.28 4.74 o 5 13 0 57.07 74.30 7.31 o 6 13 0 281.18 310.64 8.69 o 7 13 0 411.54 389.53 19.99 o 8 13 0 339.72 320.57 16.09 o 0 14 0 1602.07 1192.77 32.24 o 1 14 0 799.72 438.11 53.32 o 3 14 0 358.56 401.03 13.21 o 4 14 0 121.17 133.06 8.47 o 5 14 0 231.19 358.77 14.23 o 6 14 0 667.17 875.39 19.89 o 7 14 0 18.69 20.71 2.51 o 3 15 0 4.46 3.49 4.07 o 4 15 0 127.87 182.82 10.65 o 5 15 0 59.18 59.83 6.00 o 6 15 0 1.89 1.45 2.37 o 7 15 0 2.88 1.21 1.84 o 2 16 0 2.32 -0.48 3.92 o 4 16 0 67.69 91.92 7.79 o 5 16 0 24.61 30.83 4.74 o 6 16 0 8.82 11.57 2.86 o 2 17 0 770.44 670.78 23.28 o 1 18 0 177.42 157.80 11.18 o 2 18 0 14.08 10.75 4.65 o 3 18 0 113.85 151.17 13.31 o 1 19 0 4.31 7.21 4.11 o 2 19 0 0.54 0.96 2.22 o 3 19 0 13.49 18.54 4.79 o 0 20 0 456.69 498.37 20.09 o 1 20 0 10.73 8.63 2.60 o 2 20 0 59.66 60.31 5.08 o 3 20 0 557.31 582.30 17.09 o 1 21 0 63.14 60.76 4.48 o 2 21 0 377.23 337.13 23.26 o 3 21 0 383.49 510.71 14.57 o 0 22 0 83.04 84.71 6.92 o 1 22 0 12.68 11.58 2.14 o 2 22 0 543.33 694.79 16.55 o -10 1 1 80.22 96.61 6.00 o -9 1 1 334.17 363.79 7.42 o -8 1 1 76.19 65.30 4.00 o -7 1 1 54.68 54.79 3.76 o -6 1 1 16.55 10.21 2.23 o -5 1 1 30.99 45.50 3.10 o -4 1 1 3374.74 4395.87 149.54 o -3 1 1 2725.26 3972.63 60.97 o -2 1 1 478.83 785.38 26.84 o -1 1 1 1014.41 1405.24 39.39 o 0 1 1 99.55 147.00 4.20 o 1 1 1 7622.44 7531.70 239.53 o 2 1 1 3872.44 3605.30 62.99 o 3 1 1 386.80 467.16 7.29 o 4 1 1 75.17 80.48 3.06 o 5 1 1 114.68 87.96 6.00 o 6 1 1 3.97 2.05 1.55 o 7 1 1 65.84 65.49 4.12 o 8 1 1 12.71 14.81 2.37 o 9 1 1 285.81 305.50 7.75 o -10 2 1 786.74 802.93 14.96 o -9 2 1 6.32 6.68 1.67 o -8 2 1 570.20 641.15 11.42 o -7 2 1 305.15 296.06 19.39 o -6 2 1 366.83 431.52 21.66 o -5 2 1 157.02 139.52 5.03 o -4 2 1 800.86 1025.12 12.49 o -3 2 1 15376.97 15723.03 362.40 o -2 2 1 9946.37 12545.46 616.17 o -1 2 1 151.37 200.78 6.92 o 0 2 1 4945.37 5842.64 636.00 o 1 2 1 405.11 401.78 21.76 o 2 2 1 1787.04 1830.60 77.82 o 3 2 1 1014.51 1132.09 43.39 o 4 2 1 358.26 305.34 6.12 o 5 2 1 20.22 17.33 2.19 o 6 2 1 978.56 1004.45 17.54 o 7 2 1 1892.03 2099.94 20.84 o 8 2 1 6.36 7.34 1.93 o 9 2 1 682.48 645.03 25.29 o -9 3 1 303.24 345.64 7.26 o -8 3 1 209.97 201.88 10.58 o -7 3 1 46.04 52.41 3.76 o -6 3 1 0.77 1.80 1.87 o -5 3 1 1515.47 1798.71 68.49 o -4 3 1 5231.26 5972.23 40.01 o -3 3 1 151.76 184.92 6.05 o -2 3 1 582.88 791.03 26.05 o -1 3 1 803.33 958.47 14.13 o 0 3 1 857.00 1051.11 10.66 o 1 3 1 8484.99 7941.19 232.78 o 2 3 1 3174.05 3227.48 84.35 o 3 3 1 59.59 68.59 3.41 o 4 3 1 95.93 85.96 3.18 o 5 3 1 2.71 0.46 1.18 o 6 3 1 942.76 994.55 16.61 o 7 3 1 65.69 56.54 3.62 o 8 3 1 60.15 62.94 3.55 o 9 3 1 409.21 399.00 6.73 o -9 4 1 48.79 38.55 2.82 o -8 4 1 251.15 292.61 7.60 o -7 4 1 10.84 13.97 2.34 o -6 4 1 365.64 348.32 13.50 o -5 4 1 967.11 1094.03 21.69 o -4 4 1 81.12 91.76 7.14 o -3 4 1 4334.41 3922.04 1207.63 o -2 4 1 2060.00 2709.18 60.22 o -1 4 1 284.60 362.29 18.26 o 0 4 1 3224.34 3489.02 180.44 o 1 4 1 5025.09 5088.14 167.31 o 2 4 1 7724.99 6637.52 348.71 o 3 4 1 159.86 134.85 9.22 o 4 4 1 6.00 3.92 1.57 o 5 4 1 244.62 289.51 11.67 o 6 4 1 313.31 348.56 8.00 o 7 4 1 11.65 15.70 3.81 o 8 4 1 872.42 873.40 12.14 o 9 4 1 159.38 149.96 5.06 o -9 5 1 17.25 18.16 2.17 o -8 5 1 49.88 55.08 6.07 o -7 5 1 1130.79 1308.12 16.90 o -6 5 1 1742.05 1730.46 87.05 o -5 5 1 871.21 818.47 17.38 o -4 5 1 216.68 135.65 58.99 o -3 5 1 259.87 298.29 42.77 o -2 5 1 678.39 773.27 27.49 o -1 5 1 165.62 134.17 5.11 o 0 5 1 3383.29 3618.55 155.44 o 1 5 1 6895.97 6021.32 187.02 o 2 5 1 3291.41 3298.85 198.03 o 3 5 1 203.63 183.88 15.55 o 4 5 1 283.59 119.56 103.39 o 5 5 1 889.05 837.88 19.12 o 6 5 1 29.34 23.86 3.25 o 7 5 1 536.38 489.36 28.95 o 8 5 1 269.36 254.59 6.54 o 9 5 1 19.58 19.12 2.28 o -9 6 1 446.98 484.18 8.26 o -8 6 1 248.07 280.28 10.62 o -7 6 1 5.86 6.34 1.97 o -6 6 1 184.63 232.49 6.99 o -5 6 1 1849.13 2013.03 31.17 o -4 6 1 478.43 457.75 85.07 o -3 6 1 89.47 144.66 50.97 o -2 6 1 637.28 909.95 52.03 o -1 6 1 1499.55 1123.51 372.67 o 0 6 1 173.05 104.55 19.36 o 1 6 1 2828.67 1871.77 556.83 o 2 6 1 829.14 812.62 32.94 o 3 6 1 442.40 529.47 51.26 o 4 6 1 238.88 169.08 7.02 o 5 6 1 2539.11 2502.06 35.43 o 6 6 1 1561.87 1806.29 117.79 o 7 6 1 104.06 108.26 5.76 o 8 6 1 67.47 60.94 4.03 o 9 6 1 13.19 9.90 2.66 o -9 7 1 261.01 284.89 9.62 o -8 7 1 104.39 127.25 5.88 o -7 7 1 2436.23 2534.71 64.08 o -6 7 1 1097.80 1234.26 15.26 o -5 7 1 24.35 37.61 5.03 o -4 7 1 2159.05 2665.21 176.24 o -3 7 1 707.55 964.84 223.84 o -2 7 1 1353.79 1433.15 210.45 o -1 7 1 5383.63 4788.79 917.89 o 0 7 1 1650.69 1598.65 248.76 o 1 7 1 877.30 889.96 70.50 o 2 7 1 639.61 625.12 163.61 o 3 7 1 168.92 119.81 9.46 o 4 7 1 2720.29 3165.24 39.30 o 5 7 1 1701.46 1520.08 26.82 o 6 7 1 1184.56 1391.31 53.27 o 7 7 1 767.64 826.27 36.81 o 8 7 1 568.91 609.21 11.57 o 9 7 1 2.45 3.67 1.35 o -9 8 1 178.28 175.37 7.26 o -8 8 1 179.19 190.01 8.13 o -7 8 1 4.56 3.67 1.93 o -6 8 1 261.43 308.89 7.79 o -5 8 1 335.43 422.57 14.38 o -4 8 1 53.03 63.54 9.00 o -3 8 1 49.29 89.46 40.71 o -2 8 1 523.66 627.15 147.28 o -1 8 1 2471.14 1265.34 534.69 o 0 8 1 484.50 335.66 57.92 o 1 8 1 871.06 617.89 102.54 o 2 8 1 3.34 3.21 1.98 o 3 8 1 354.73 341.39 49.66 o 4 8 1 2014.81 2106.35 29.87 o 5 8 1 9.24 14.54 5.48 o 6 8 1 173.76 209.95 7.82 o 7 8 1 61.40 71.27 4.77 o 8 8 1 20.16 17.41 2.51 o -9 9 1 14.62 11.98 1.57 o -8 9 1 15.79 18.23 2.25 o -7 9 1 11.58 12.95 3.79 o -6 9 1 4.02 3.22 1.93 o -5 9 1 141.71 137.08 8.37 o -4 9 1 22.93 30.78 3.73 o -3 9 1 197.13 219.38 16.22 o -2 9 1 2044.33 1254.31 128.78 o -1 9 1 1134.49 907.31 78.63 o 0 9 1 22.49 13.88 3.11 o 1 9 1 18.83 18.62 3.62 o 2 9 1 170.93 165.35 10.16 o 3 9 1 138.23 141.49 26.11 o 4 9 1 162.83 178.27 9.29 o 5 9 1 703.61 836.02 15.53 o 6 9 1 56.63 57.65 4.43 o 7 9 1 36.40 33.46 3.49 o 8 9 1 9.79 12.34 2.12 o -9 10 1 434.34 438.83 10.65 o -8 10 1 547.44 605.51 17.37 o -7 10 1 3.02 1.66 1.54 o -6 10 1 22.31 21.71 2.79 o -5 10 1 3792.61 4247.74 68.61 o -4 10 1 2.11 16.89 9.54 o -3 10 1 613.47 619.33 33.30 o -2 10 1 638.41 353.22 16.34 o -1 10 1 288.72 279.78 13.14 o 0 10 1 710.30 331.22 9.18 o 1 10 1 226.27 164.04 19.05 o 2 10 1 1056.12 815.37 21.73 o 3 10 1 3258.48 2544.70 41.39 o 5 10 1 381.14 420.27 21.35 o 6 10 1 1274.05 1380.39 19.89 o 7 10 1 27.09 28.33 3.15 o 8 10 1 373.65 358.39 7.78 o -8 11 1 0.00 -0.12 1.32 o -7 11 1 776.94 809.96 30.52 o -6 11 1 79.68 91.33 4.85 o -5 11 1 232.97 306.31 10.56 o -4 11 1 382.93 249.28 16.84 o -3 11 1 527.90 410.66 24.40 o -2 11 1 480.67 498.33 24.78 o -1 11 1 10.59 8.76 2.66 o 0 11 1 69.00 65.86 6.52 o 1 11 1 274.15 218.08 11.71 o 2 11 1 184.75 125.71 9.39 o 3 11 1 192.02 210.85 13.99 o 4 11 1 1339.09 1686.61 83.09 o 5 11 1 821.87 1025.25 30.57 o 6 11 1 92.55 101.92 5.55 o 7 11 1 532.34 554.31 37.54 o 8 11 1 9.75 9.25 1.74 o -8 12 1 171.46 139.40 5.42 o -7 12 1 467.00 462.17 32.42 o -6 12 1 363.89 335.67 30.03 o -5 12 1 1.45 2.86 3.82 o -4 12 1 202.26 201.99 12.00 o -3 12 1 269.77 304.99 23.38 o -2 12 1 2.87 2.34 2.72 o -1 12 1 122.01 114.00 8.10 o 0 12 1 1489.77 1029.41 72.75 o 1 12 1 450.55 359.46 18.47 o 2 12 1 36.84 32.96 6.53 o 3 12 1 792.26 522.96 18.39 o 4 12 1 171.40 202.76 10.31 o 5 12 1 200.92 241.77 8.63 o 6 12 1 510.50 525.39 11.47 o 7 12 1 0.11 3.05 1.71 o 8 12 1 4.39 3.59 1.35 o -8 13 1 106.01 81.15 7.58 o -7 13 1 133.18 142.43 12.75 o -6 13 1 45.78 46.01 4.63 o -5 13 1 152.18 112.35 10.46 o -4 13 1 652.51 691.79 25.70 o -3 13 1 150.12 120.09 10.94 o -2 13 1 204.76 221.59 20.38 o -1 13 1 197.70 165.29 9.63 o 0 13 1 5.26 7.00 3.84 o 1 13 1 250.74 146.64 10.58 o 2 13 1 25.72 19.07 6.10 o 3 13 1 17.97 31.08 5.61 o 4 13 1 43.25 44.39 6.20 o 5 13 1 72.86 80.15 5.07 o 6 13 1 0.06 2.62 1.77 o 7 13 1 39.82 44.07 3.16 o -7 14 1 358.74 282.05 9.10 o -6 14 1 183.04 145.07 11.08 o -5 14 1 143.93 127.79 11.42 o -4 14 1 256.94 273.92 16.80 o -3 14 1 24.99 20.71 3.54 o -2 14 1 199.01 223.96 7.45 o -1 14 1 175.42 131.79 8.04 o 0 14 1 653.24 534.42 43.71 o 1 14 1 4.69 0.82 3.05 o 2 14 1 181.38 178.08 9.15 o 3 14 1 998.86 1025.39 21.39 o 4 14 1 583.00 853.03 23.19 o 5 14 1 3.56 6.58 3.10 o 6 14 1 14.95 12.29 2.31 o 7 14 1 128.77 133.97 6.07 o -6 15 1 72.62 63.94 5.61 o -5 15 1 30.87 33.69 4.84 o -4 15 1 503.85 565.26 17.09 o -3 15 1 557.03 629.87 11.84 o -2 15 1 360.26 392.05 11.04 o -1 15 1 34.24 25.37 2.95 o 0 15 1 115.48 114.36 5.88 o 1 15 1 1374.64 1396.71 155.06 o 2 15 1 1295.55 1309.86 24.15 o 3 15 1 157.00 190.91 11.28 o 4 15 1 603.29 856.95 22.60 o 5 15 1 335.46 443.96 15.25 o 6 15 1 4.20 5.57 2.32 o 7 15 1 208.11 238.00 8.18 o -6 16 1 3.99 2.76 2.57 o -5 16 1 17.70 21.01 3.73 o -4 16 1 0.74 -0.63 2.52 o -3 16 1 537.35 577.41 19.47 o -2 16 1 1035.83 1227.07 67.20 o -1 16 1 54.78 52.76 5.91 o 0 16 1 10.13 10.21 2.65 o 1 16 1 1.23 4.35 2.23 o 2 16 1 290.23 295.61 16.19 o 3 16 1 2121.67 2241.94 37.39 o 4 16 1 263.17 313.08 11.62 o 5 16 1 7.04 15.15 3.53 o 6 16 1 198.09 221.11 8.33 o -5 17 1 2.41 1.60 2.08 o -4 17 1 0.89 2.61 2.32 o -3 17 1 217.88 202.14 7.33 o -2 17 1 297.10 285.90 8.65 o -1 17 1 440.82 423.01 11.07 o 0 17 1 98.77 71.38 6.56 o 1 17 1 63.51 69.94 5.23 o 2 17 1 217.74 211.78 7.91 o 3 17 1 105.97 93.93 5.34 o 4 17 1 17.50 24.98 4.60 o 5 17 1 78.68 90.56 6.58 o 6 17 1 1.22 0.58 1.60 o -3 18 1 155.46 116.60 5.31 o -2 18 1 1.69 1.49 1.84 o -1 18 1 279.43 257.59 8.95 o 0 18 1 823.55 850.59 50.51 o 1 18 1 388.08 374.23 12.75 o 2 18 1 217.41 193.57 19.87 o 3 18 1 9.83 10.24 2.74 o 4 18 1 346.72 373.24 11.62 o 5 18 1 11.35 6.00 2.18 o -3 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