#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:39:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181077 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/57/2215766.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215766_Fobs loop_ _publ_author_name 'Zheng, Xianfu' 'Niu, Caoyuan' 'Wan, Xinsheng' 'Kou, Chunhong' _publ_section_title ; Diaquatetrakis(1,3-di-4-pyridylpropane-\kN)manganese(II) bis(hexafluoridophosphate) monohydrate ; _journal_coeditor_code BH2123 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2682 _journal_page_last m2683 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.1098 _cell_length_b 16.1767 _cell_length_c 38.1580 _exptl_crystal_F_000 4936.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file bh2123Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I' _shelx_refln_list_code 4 _shelx_f_calc_maximum 628.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 203051.66 203654.61 2193.26 o 6 0 0 0.82 1.86 18.24 o 8 0 0 22002.97 23279.18 329.49 o 10 0 0 554.65 371.18 59.69 o 12 0 0 19654.60 18744.26 289.94 o 14 0 0 9075.12 9202.87 243.56 o 16 0 0 955.22 1066.08 98.46 o 18 0 0 3669.10 3734.40 265.65 o 20 0 0 6166.64 6821.41 379.50 o 22 0 0 758.21 950.62 192.36 o 2 1 0 45.06 -16.35 10.90 o 4 1 0 87873.88 88738.68 849.34 o 6 1 0 1392.25 1638.07 59.68 o 8 1 0 3330.64 3120.10 65.40 o 10 1 0 1848.35 1739.53 55.44 o 12 1 0 4105.81 3873.92 88.35 o 14 1 0 181.94 232.56 37.58 o 16 1 0 37.13 64.19 36.16 o 18 1 0 1824.28 1678.97 240.35 o 20 1 0 608.04 551.64 107.17 o 22 1 0 31.53 80.53 85.72 o 0 2 0 39130.70 40119.20 796.96 o 2 2 0 105342.23 103138.23 978.42 o 4 2 0 71257.28 76773.89 605.33 o 6 2 0 33004.16 31921.52 276.44 o 8 2 0 46845.53 47800.20 407.58 o 10 2 0 2082.69 2523.35 58.93 o 12 2 0 9945.35 10453.05 138.84 o 14 2 0 3.80 6.88 26.26 o 16 2 0 808.43 896.87 67.58 o 18 2 0 1127.22 1082.32 92.65 o 20 2 0 619.20 909.05 123.40 o 22 2 0 488.30 739.41 183.99 o 2 3 0 3164.82 3019.63 43.21 o 4 3 0 4267.88 4096.34 52.04 o 6 3 0 16476.53 16237.12 159.22 o 8 3 0 12734.99 12022.49 157.21 o 10 3 0 16.56 -1.58 19.07 o 12 3 0 2077.88 1738.53 55.75 o 14 3 0 61.08 85.96 29.64 o 16 3 0 13.96 -10.90 42.69 o 18 3 0 372.01 221.26 79.39 o 20 3 0 44.71 -27.48 112.74 o 22 3 0 11.86 33.31 86.27 o 0 4 0 395228.28 360765.19 5467.62 o 2 4 0 92988.48 90080.27 707.65 o 4 4 0 4514.93 3714.37 55.64 o 6 4 0 3920.83 4280.90 60.81 o 8 4 0 35432.23 37506.18 308.90 o 10 4 0 7803.74 8337.51 114.32 o 12 4 0 317.66 262.69 30.31 o 14 4 0 992.25 941.83 70.15 o 16 4 0 12.25 23.49 41.22 o 18 4 0 3533.48 3793.51 140.53 o 20 4 0 588.84 726.76 91.47 o 22 4 0 291.59 399.17 106.72 o 2 5 0 6104.75 6027.83 75.64 o 4 5 0 20484.71 19751.70 187.57 o 6 5 0 587.47 546.05 28.13 o 8 5 0 8631.81 8145.76 114.95 o 10 5 0 606.71 601.58 36.41 o 12 5 0 22.24 1.01 22.67 o 14 5 0 152.01 167.31 44.07 o 16 5 0 947.36 884.59 72.59 o 18 5 0 2151.75 2290.64 122.59 o 20 5 0 148.32 241.20 72.08 o 22 5 0 20.78 -58.24 81.90 o 0 6 0 11186.32 10005.19 189.06 o 2 6 0 26082.93 24347.00 223.88 o 4 6 0 16789.08 15781.85 188.80 o 6 6 0 38492.30 40770.87 359.23 o 8 6 0 19649.32 19267.12 201.56 o 10 6 0 34529.88 33149.42 293.89 o 12 6 0 1662.83 1958.45 66.71 o 14 6 0 763.03 751.87 49.96 o 16 6 0 23.22 28.94 45.59 o 18 6 0 192.96 179.10 93.37 o 20 6 0 452.92 332.45 112.91 o 22 6 0 146.26 89.47 71.31 o 2 7 0 34368.76 35098.88 340.66 o 4 7 0 19891.91 19335.37 194.88 o 6 7 0 58369.24 55629.89 477.13 o 8 7 0 46361.19 45767.43 409.86 o 10 7 0 2201.02 1881.96 58.48 o 12 7 0 1410.52 1431.60 69.40 o 14 7 0 557.55 700.78 136.57 o 16 7 0 9474.77 10120.69 223.25 o 18 7 0 879.20 764.66 77.40 o 20 7 0 251.43 65.91 76.40 o 0 8 0 2458.99 2239.71 75.64 o 2 8 0 499.73 490.91 30.95 o 4 8 0 5940.99 5436.40 85.91 o 6 8 0 878.07 969.41 41.35 o 8 8 0 2315.81 2542.96 65.29 o 10 8 0 8930.15 9185.67 152.04 o 12 8 0 141.30 160.47 41.04 o 14 8 0 2705.29 3259.17 133.88 o 16 8 0 404.02 419.34 64.93 o 18 8 0 690.04 702.60 91.52 o 20 8 0 16.33 51.38 83.79 o 2 9 0 19153.36 18520.76 269.58 o 4 9 0 2377.12 2551.21 61.31 o 6 9 0 1130.68 1174.67 46.13 o 8 9 0 6098.78 5921.42 116.22 o 10 9 0 1794.36 1889.23 73.44 o 12 9 0 3080.41 2836.63 91.80 o 14 9 0 2189.68 2239.14 122.87 o 16 9 0 7395.39 7491.56 362.34 o 18 9 0 1177.22 1129.07 166.68 o 20 9 0 281.71 393.16 98.46 o 0 10 0 275.85 321.44 42.96 o 2 10 0 274.74 261.78 29.31 o 4 10 0 2.43 -2.57 22.58 o 6 10 0 143.27 140.66 40.60 o 8 10 0 2691.60 2438.16 78.83 o 10 10 0 3840.59 4318.82 196.93 o 12 10 0 5.73 60.99 47.09 o 14 10 0 67.14 164.49 64.93 o 16 10 0 236.47 82.97 60.50 o 18 10 0 118.06 -69.17 59.63 o 2 11 0 14.88 3.48 23.77 o 4 11 0 4017.41 3965.05 95.17 o 6 11 0 3767.70 4102.87 98.59 o 8 11 0 8470.23 8494.13 175.71 o 10 11 0 114.91 125.81 48.45 o 12 11 0 1.01 17.19 45.33 o 14 11 0 1445.82 1156.15 104.24 o 16 11 0 2745.48 2989.86 154.14 o 18 11 0 30.11 -15.67 65.52 o 0 12 0 1421.18 1354.58 106.43 o 2 12 0 508.47 540.48 46.62 o 4 12 0 12.34 -29.95 29.28 o 6 12 0 592.15 758.58 54.04 o 8 12 0 686.89 727.15 65.82 o 10 12 0 2.73 140.04 50.59 o 12 12 0 854.50 989.05 102.81 o 14 12 0 0.43 88.65 63.02 o 16 12 0 175.41 129.26 81.59 o 18 12 0 11.72 -114.95 84.72 o 2 13 0 212.27 200.78 50.36 o 4 13 0 241.11 263.06 44.20 o 6 13 0 8692.77 8882.82 186.42 o 8 13 0 1639.06 1617.98 110.41 o 10 13 0 63.52 10.60 54.94 o 12 13 0 332.36 280.07 71.56 o 14 13 0 1620.76 1287.31 113.21 o 16 13 0 2660.74 2437.69 182.86 o 0 14 0 940.30 851.30 110.50 o 2 14 0 2414.59 2346.11 102.59 o 4 14 0 332.63 282.58 56.80 o 6 14 0 218.12 202.11 67.59 o 8 14 0 62.79 149.84 54.68 o 10 14 0 3181.69 3475.65 130.87 o 12 14 0 796.15 862.69 97.28 o 14 14 0 29.24 118.58 68.86 o 16 14 0 50.65 90.87 72.70 o 2 15 0 2935.72 3424.63 122.96 o 4 15 0 1062.51 1218.74 194.65 o 6 15 0 2872.50 2581.97 236.83 o 8 15 0 2094.98 1913.94 182.24 o 10 15 0 30.34 18.61 101.20 o 12 15 0 377.54 306.54 210.40 o 14 15 0 559.55 590.25 94.75 o 0 16 0 2478.53 2306.13 159.29 o 2 16 0 534.43 596.66 73.55 o 4 16 0 19.22 -21.50 56.88 o 6 16 0 13.77 -41.62 85.84 o 8 16 0 496.16 402.47 84.43 o 10 16 0 51.71 -15.07 77.61 o 12 16 0 307.80 177.87 115.71 o 2 17 0 212.10 189.69 111.36 o 4 17 0 423.18 310.17 79.04 o 6 17 0 1083.74 893.43 114.94 o 8 17 0 96.87 66.07 68.24 o 10 17 0 3.13 -40.74 79.25 o 0 18 0 526.26 486.79 108.03 o 2 18 0 641.64 717.71 102.99 o 4 18 0 41.53 -11.98 66.88 o 6 18 0 18.16 26.82 67.34 o 8 18 0 177.35 209.44 83.32 o 2 19 0 487.87 269.85 86.65 o 4 19 0 475.92 475.44 97.57 o 2 1 1 20484.46 20792.86 213.16 o 3 1 1 33751.55 32885.77 207.97 o 4 1 1 80579.13 78296.14 454.41 o 5 1 1 66806.80 67513.96 397.48 o 6 1 1 72382.29 69585.55 413.23 o 7 1 1 13486.30 13232.26 106.31 o 8 1 1 23558.23 25157.67 173.81 o 9 1 1 11090.21 11033.17 113.42 o 10 1 1 1484.66 1584.25 54.57 o 11 1 1 128.66 144.24 20.47 o 12 1 1 149.70 177.80 23.40 o 13 1 1 2066.81 1921.54 51.74 o 14 1 1 3436.48 3527.56 60.88 o 15 1 1 1189.76 1271.22 44.60 o 16 1 1 739.20 830.66 40.07 o 17 1 1 2072.25 2278.65 82.47 o 18 1 1 4242.41 4325.47 227.71 o 19 1 1 439.23 301.73 63.70 o 20 1 1 16.28 97.18 57.62 o 21 1 1 19.76 44.37 55.95 o 22 1 1 21.11 20.79 61.25 o 23 1 1 150.67 337.95 85.17 o 0 2 1 5114.10 6551.31 92.62 o 1 2 1 2600.95 3860.54 48.94 o 2 2 1 16685.69 15082.74 109.65 o 3 2 1 2284.53 1943.64 23.48 o 4 2 1 9504.96 9623.76 72.96 o 5 2 1 9591.24 10575.53 76.86 o 6 2 1 4026.10 4570.60 45.39 o 7 2 1 354.93 443.00 17.05 o 8 2 1 8808.28 9187.99 78.63 o 9 2 1 6596.48 6960.99 68.59 o 10 2 1 254.91 265.22 23.47 o 11 2 1 1341.53 1326.49 33.11 o 12 2 1 1838.33 2114.90 42.30 o 13 2 1 3211.90 3346.74 54.32 o 14 2 1 165.19 118.20 21.52 o 15 2 1 24.15 4.85 21.42 o 16 2 1 50.60 34.14 26.66 o 17 2 1 80.91 87.26 32.56 o 18 2 1 274.63 326.14 44.19 o 19 2 1 89.43 114.65 55.59 o 20 2 1 105.37 137.56 58.38 o 21 2 1 3.83 -36.61 51.70 o 22 2 1 74.49 72.06 60.25 o 23 2 1 85.51 235.13 72.84 o 1 3 1 56245.16 54386.19 319.15 o 2 3 1 66787.19 65520.39 382.66 o 3 3 1 103581.36 100076.59 577.63 o 4 3 1 6722.05 7566.83 55.08 o 5 3 1 4814.37 4928.39 42.80 o 6 3 1 13688.82 13866.20 99.60 o 7 3 1 12761.52 12666.71 96.12 o 8 3 1 6213.65 6527.16 69.84 o 9 3 1 4094.22 4312.94 52.12 o 10 3 1 2066.36 1999.18 41.07 o 11 3 1 1341.03 1203.48 32.01 o 12 3 1 2.92 7.36 16.17 o 13 3 1 263.79 363.45 24.75 o 14 3 1 4384.40 4226.32 67.41 o 15 3 1 477.34 546.22 37.85 o 16 3 1 353.95 367.48 38.70 o 17 3 1 874.83 849.95 50.30 o 18 3 1 586.89 523.97 49.09 o 19 3 1 579.86 510.66 56.91 o 20 3 1 211.94 204.29 54.29 o 21 3 1 1.09 57.30 56.31 o 22 3 1 169.48 135.92 66.18 o 0 4 1 220793.67 213243.50 1630.95 o 1 4 1 30974.69 31897.27 189.57 o 2 4 1 21162.97 21517.60 135.20 o 3 4 1 54133.50 55216.74 316.70 o 4 4 1 4090.57 4408.94 43.67 o 5 4 1 10467.26 11564.03 83.31 o 6 4 1 4233.91 4996.24 47.03 o 7 4 1 5215.89 5918.05 54.29 o 8 4 1 1104.43 1428.72 29.05 o 9 4 1 5687.69 5666.33 67.73 o 10 4 1 1113.99 1170.22 34.55 o 11 4 1 804.30 921.84 29.46 o 12 4 1 568.05 495.72 25.73 o 13 4 1 670.05 721.71 32.43 o 14 4 1 2341.91 2429.28 57.07 o 15 4 1 34.94 41.65 29.36 o 16 4 1 2693.77 2706.65 74.30 o 17 4 1 136.89 130.92 45.89 o 18 4 1 0.44 -14.15 33.18 o 19 4 1 6.13 15.60 39.86 o 20 4 1 522.17 564.91 60.03 o 21 4 1 0.68 48.89 58.04 o 22 4 1 8.91 -50.55 57.37 o 1 5 1 23065.47 23529.53 148.93 o 2 5 1 64.62 80.81 10.30 o 3 5 1 1038.83 1007.00 24.02 o 4 5 1 13793.38 13599.94 98.88 o 5 5 1 2252.48 2222.04 32.93 o 6 5 1 9587.99 9644.49 80.80 o 7 5 1 42.24 13.69 12.60 o 8 5 1 3706.39 3365.25 45.84 o 9 5 1 446.73 535.85 22.40 o 10 5 1 140.05 99.69 16.12 o 11 5 1 999.19 913.58 42.96 o 12 5 1 1259.68 1246.99 34.42 o 13 5 1 16.50 32.56 20.77 o 14 5 1 4.85 -20.66 20.67 o 15 5 1 3348.31 3238.36 83.04 o 16 5 1 2086.78 2070.85 83.27 o 17 5 1 420.35 331.35 42.19 o 18 5 1 1047.58 977.17 57.45 o 19 5 1 258.95 287.07 46.81 o 20 5 1 87.24 119.29 48.67 o 21 5 1 10.65 13.02 44.80 o 22 5 1 1.10 50.85 59.16 o 0 6 1 157.75 99.55 16.18 o 1 6 1 3881.81 3942.48 43.37 o 2 6 1 6679.28 6413.18 59.01 o 3 6 1 11412.58 12136.67 92.80 o 4 6 1 1272.05 1104.68 25.55 o 5 6 1 635.49 614.98 31.83 o 6 6 1 12663.80 12889.85 102.18 o 7 6 1 2698.06 3100.31 49.07 o 8 6 1 14775.54 14349.32 115.00 o 9 6 1 3173.31 2853.62 44.12 o 10 6 1 14833.41 14638.46 117.06 o 11 6 1 10536.17 10647.79 136.25 o 12 6 1 2914.28 2895.79 53.45 o 13 6 1 265.13 264.46 26.20 o 14 6 1 387.54 422.25 33.63 o 15 6 1 623.10 666.52 61.61 o 16 6 1 52.07 33.02 33.26 o 17 6 1 58.99 11.26 39.55 o 18 6 1 12.21 -22.54 33.59 o 19 6 1 250.11 315.66 50.05 o 20 6 1 4.62 -59.50 39.67 o 21 6 1 86.92 99.42 48.68 o 22 6 1 103.93 48.01 55.15 o 1 7 1 33.06 42.30 12.17 o 2 7 1 10.01 8.47 12.25 o 3 7 1 3757.82 4152.55 49.25 o 4 7 1 15212.47 13866.49 107.38 o 5 7 1 5727.15 6297.29 75.09 o 6 7 1 5449.49 5866.26 63.93 o 7 7 1 6945.15 6485.36 69.42 o 8 7 1 7875.35 8456.29 83.36 o 9 7 1 484.56 564.54 25.85 o 10 7 1 17.30 45.55 20.36 o 11 7 1 1649.82 1767.48 64.99 o 12 7 1 284.82 322.69 30.26 o 13 7 1 6356.83 6051.90 96.55 o 14 7 1 2684.74 2616.67 66.23 o 15 7 1 254.77 188.72 37.67 o 16 7 1 1400.53 1368.81 76.10 o 17 7 1 712.52 903.61 56.95 o 18 7 1 169.02 230.26 41.71 o 19 7 1 35.64 23.76 36.34 o 20 7 1 32.57 74.14 46.86 o 21 7 1 10.34 -7.56 56.54 o 0 8 1 11528.96 10833.78 128.94 o 1 8 1 33556.61 33273.14 214.95 o 2 8 1 23569.31 22781.25 164.59 o 3 8 1 3724.93 3455.24 47.13 o 4 8 1 258.21 166.44 17.34 o 5 8 1 7233.29 6613.77 69.55 o 6 8 1 7.87 -21.97 14.65 o 7 8 1 3040.13 3325.05 50.72 o 8 8 1 3818.24 3701.83 54.37 o 9 8 1 14043.94 13974.12 127.73 o 10 8 1 9275.21 9426.21 109.44 o 11 8 1 10832.04 10075.46 116.23 o 12 8 1 3142.95 2911.37 63.60 o 13 8 1 2.76 -5.51 26.07 o 14 8 1 2393.05 2494.79 77.27 o 15 8 1 280.20 275.53 48.75 o 16 8 1 1346.69 1257.13 68.30 o 17 8 1 192.99 200.22 45.38 o 18 8 1 225.85 197.03 52.94 o 19 8 1 84.45 73.91 46.44 o 20 8 1 306.87 244.69 69.55 o 21 8 1 143.85 209.58 70.62 o 1 9 1 123.73 110.94 17.01 o 2 9 1 0.24 -11.04 14.50 o 3 9 1 279.57 280.96 19.83 o 4 9 1 3.52 -4.74 14.56 o 5 9 1 7173.40 6843.54 73.66 o 6 9 1 1131.90 1059.26 31.53 o 7 9 1 121.07 131.46 19.78 o 8 9 1 1617.53 1484.17 38.15 o 9 9 1 72.98 85.49 23.37 o 10 9 1 97.26 141.01 33.65 o 11 9 1 301.69 215.90 29.64 o 12 9 1 1015.98 1212.46 62.16 o 13 9 1 264.57 234.14 36.40 o 14 9 1 1372.46 1198.50 62.19 o 15 9 1 17.53 35.07 40.73 o 16 9 1 57.28 111.61 53.27 o 17 9 1 287.67 292.95 53.12 o 18 9 1 0.03 -20.61 42.30 o 19 9 1 53.00 36.83 45.41 o 20 9 1 182.40 207.11 70.98 o 0 10 1 6678.04 7251.92 107.87 o 1 10 1 63.43 6.41 15.66 o 2 10 1 968.87 1177.09 32.13 o 3 10 1 4296.19 4466.21 58.75 o 4 10 1 2204.03 2468.27 44.81 o 5 10 1 175.47 293.62 22.02 o 6 10 1 57.57 42.79 17.55 o 7 10 1 1952.31 1924.50 45.69 o 8 10 1 5483.13 5505.17 81.05 o 9 10 1 7935.74 7472.12 105.59 o 10 10 1 10817.70 10097.97 138.51 o 11 10 1 3441.20 3707.75 85.31 o 12 10 1 1248.92 1247.83 57.42 o 13 10 1 967.92 1039.42 79.02 o 14 10 1 8.35 -24.94 37.57 o 15 10 1 75.15 11.77 40.58 o 16 10 1 46.64 44.17 42.42 o 17 10 1 170.99 146.83 48.86 o 18 10 1 1.35 79.25 55.96 o 19 10 1 86.50 16.24 45.71 o 1 11 1 1031.39 1189.43 33.89 o 2 11 1 964.58 1132.76 34.65 o 3 11 1 6045.09 6545.53 80.89 o 4 11 1 13.93 30.26 19.53 o 5 11 1 4130.31 4347.46 70.71 o 6 11 1 397.92 349.27 28.91 o 7 11 1 1015.40 1003.97 43.79 o 8 11 1 322.97 374.13 38.25 o 9 11 1 1155.15 1087.67 52.41 o 10 11 1 32.30 12.86 31.57 o 11 11 1 80.41 93.67 34.26 o 12 11 1 0.22 17.58 35.35 o 13 11 1 1312.06 1482.32 77.27 o 14 11 1 930.20 899.26 67.34 o 15 11 1 287.18 276.62 51.92 o 16 11 1 121.25 144.85 49.32 o 17 11 1 0.06 71.78 45.91 o 18 11 1 50.68 -9.62 44.33 o 19 11 1 8.15 -66.81 44.54 o 0 12 1 7508.56 7444.93 134.78 o 1 12 1 2599.88 2482.65 60.15 o 2 12 1 1835.71 1857.58 51.84 o 3 12 1 84.63 98.62 23.84 o 4 12 1 10.65 50.82 23.16 o 5 12 1 329.55 388.04 31.17 o 6 12 1 33.97 -12.01 24.95 o 7 12 1 70.93 60.39 32.05 o 8 12 1 391.58 368.83 41.46 o 9 12 1 5727.16 6336.17 115.96 o 10 12 1 2301.69 1940.74 68.36 o 11 12 1 1688.44 1735.47 66.60 o 12 12 1 663.90 608.37 53.70 o 13 12 1 28.32 37.16 40.35 o 14 12 1 446.31 477.86 58.22 o 15 12 1 8.15 -59.04 39.36 o 16 12 1 0.56 -32.33 41.82 o 17 12 1 5.67 -14.85 45.22 o 18 12 1 43.77 3.82 46.92 o 1 13 1 274.54 297.73 36.55 o 2 13 1 1500.55 1522.68 57.95 o 3 13 1 312.56 343.15 34.31 o 4 13 1 231.06 190.37 31.15 o 5 13 1 100.29 103.63 31.05 o 6 13 1 290.27 335.98 39.94 o 7 13 1 80.69 34.72 32.64 o 8 13 1 0.41 54.62 33.24 o 9 13 1 61.16 21.99 33.75 o 10 13 1 360.16 417.93 45.00 o 11 13 1 195.00 246.60 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68.33 o 6 0 28 10.87 -43.58 29.06 o 7 0 28 834.41 994.12 70.08 o 8 0 28 8.68 -11.20 42.10 o 9 0 28 1970.15 1899.66 126.31 o 10 0 28 195.21 358.25 60.78 o 11 0 28 609.78 619.66 70.05 o 12 0 28 1.88 -66.34 44.23 o 13 0 28 822.43 814.31 79.10 o 14 0 28 575.99 634.13 76.75 o 15 0 28 6.54 22.38 52.83 o 16 0 28 86.84 47.37 65.28 o 17 0 28 391.38 382.33 170.34 o 18 0 28 77.74 -17.43 69.93 o 1 1 28 443.44 559.19 27.98 o 2 1 28 4415.40 4293.52 60.57 o 3 1 28 2976.00 2802.44 52.52 o 4 1 28 1996.75 2205.49 72.65 o 5 1 28 4629.47 4915.52 78.50 o 6 1 28 554.29 503.61 40.93 o 7 1 28 6.31 2.67 25.36 o 8 1 28 1028.80 1029.11 51.90 o 9 1 28 693.56 637.40 50.50 o 10 1 28 3.97 9.19 32.88 o 11 1 28 238.28 175.58 50.89 o 12 1 28 1805.41 1861.38 70.91 o 13 1 28 278.89 224.79 47.87 o 14 1 28 9.34 35.18 52.41 o 15 1 28 21.21 73.99 42.54 o 16 1 28 1.61 -16.12 40.35 o 17 1 28 306.29 393.01 55.74 o 18 1 28 47.05 23.95 44.99 o 0 2 28 3545.23 3440.22 100.38 o 1 2 28 5282.06 5784.18 73.86 o 2 2 28 7.49 10.90 19.52 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165.56 30.34 o 1 4 28 3230.66 3132.65 63.00 o 2 4 28 286.78 286.09 28.65 o 3 4 28 825.72 825.97 39.29 o 4 4 28 60.04 59.22 25.15 o 5 4 28 123.91 135.84 29.97 o 6 4 28 390.56 327.36 37.34 o 7 4 28 342.22 303.26 38.06 o 8 4 28 1594.80 1487.28 77.49 o 9 4 28 442.00 497.10 44.67 o 10 4 28 241.32 259.50 41.25 o 11 4 28 46.52 19.63 45.51 o 12 4 28 530.52 497.31 52.84 o 13 4 28 92.26 117.13 41.68 o 14 4 28 3.00 23.84 38.82 o 15 4 28 81.84 98.96 43.52 o 16 4 28 4.90 -28.52 40.46 o 17 4 28 5.86 21.19 44.31 o 1 5 28 898.40 997.80 45.34 o 2 5 28 2863.62 2666.54 65.90 o 3 5 28 53.60 23.53 25.82 o 4 5 28 291.54 257.08 31.21 o 5 5 28 143.36 204.12 30.67 o 6 5 28 244.97 191.11 32.85 o 7 5 28 49.47 21.67 29.49 o 8 5 28 3622.10 3437.62 95.95 o 9 5 28 266.05 212.43 39.15 o 10 5 28 93.22 75.39 35.79 o 11 5 28 4.75 49.75 35.29 o 12 5 28 116.81 147.82 41.70 o 13 5 28 77.93 11.89 39.95 o 14 5 28 4.82 -55.92 37.28 o 15 5 28 223.11 197.19 47.76 o 16 5 28 29.20 -58.23 38.82 o 17 5 28 778.33 671.25 66.15 o 0 6 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41.97 o 5 10 28 33.54 55.28 35.37 o 6 10 28 16.53 16.66 34.73 o 7 10 28 132.90 144.37 40.21 o 8 10 28 79.42 95.31 54.46 o 9 10 28 42.62 -5.60 38.40 o 10 10 28 15.89 56.54 41.40 o 11 10 28 0.40 -1.07 41.05 o 12 10 28 0.22 6.18 41.39 o 13 10 28 1.48 -32.11 42.12 o 14 10 28 9.72 41.55 43.52 o 1 11 28 75.14 11.29 41.52 o 2 11 28 310.45 179.10 43.09 o 3 11 28 196.40 267.34 51.31 o 4 11 28 4.04 2.51 34.15 o 5 11 28 122.57 183.31 39.24 o 6 11 28 23.97 -0.89 35.75 o 7 11 28 851.88 838.51 59.32 o 8 11 28 1.75 -26.64 37.69 o 9 11 28 647.75 686.87 74.43 o 10 11 28 31.87 12.78 39.85 o 11 11 28 11.37 -20.17 40.65 o 12 11 28 1.97 -33.96 41.82 o 13 11 28 87.34 73.23 46.76 o 0 12 28 19.22 10.07 56.61 o 1 12 28 401.89 337.33 55.41 o 2 12 28 1.19 41.75 43.34 o 3 12 28 18.07 -27.72 40.44 o 4 12 28 566.03 577.64 57.45 o 5 12 28 127.33 71.48 37.40 o 6 12 28 26.76 51.46 37.57 o 7 12 28 80.27 45.47 38.07 o 8 12 28 143.39 97.77 41.04 o 9 12 28 8.00 -51.25 38.85 o 10 12 28 1.91 -36.40 40.62 o 11 12 28 31.44 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37.68 o 11 1 29 1268.55 1319.21 66.41 o 12 1 29 0.96 -20.65 33.60 o 13 1 29 225.20 259.67 47.93 o 14 1 29 1660.68 1392.19 73.78 o 15 1 29 619.97 614.12 59.64 o 16 1 29 569.15 704.05 68.87 o 17 1 29 649.06 738.73 67.70 o 0 2 29 3766.96 3414.41 76.21 o 1 2 29 466.64 515.21 28.08 o 2 2 29 2676.91 2690.26 52.81 o 3 2 29 37.96 48.87 22.65 o 4 2 29 1637.47 1686.18 49.37 o 5 2 29 166.75 106.51 29.20 o 6 2 29 0.88 -17.06 25.58 o 7 2 29 294.37 340.82 35.32 o 8 2 29 288.70 166.44 33.30 o 9 2 29 424.68 452.10 50.80 o 10 2 29 154.77 120.21 40.58 o 11 2 29 3.15 -3.15 36.07 o 12 2 29 3.39 -52.62 35.08 o 13 2 29 115.45 63.09 40.33 o 14 2 29 5.24 -11.84 38.98 o 15 2 29 240.00 141.88 46.27 o 16 2 29 2.11 43.15 42.41 o 17 2 29 19.36 -1.24 45.73 o 1 3 29 610.00 628.25 28.82 o 2 3 29 166.01 140.06 23.16 o 3 3 29 3846.52 3815.66 68.16 o 4 3 29 2301.48 2463.65 67.49 o 5 3 29 682.31 768.05 45.66 o 6 3 29 3045.45 2930.16 74.16 o 7 3 29 331.86 353.68 43.70 o 8 3 29 3.29 -4.90 31.02 o 9 3 29 692.98 743.83 50.22 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5 29 166.45 103.67 36.81 o 10 5 29 130.99 70.17 43.68 o 11 5 29 66.26 56.46 39.12 o 12 5 29 15.97 -41.18 35.39 o 13 5 29 3.63 -12.68 37.84 o 14 5 29 104.89 42.43 42.26 o 15 5 29 81.97 18.08 40.43 o 16 5 29 42.54 56.37 45.98 o 17 5 29 35.95 27.43 47.48 o 0 6 29 18.00 110.56 38.81 o 1 6 29 549.47 422.86 40.54 o 2 6 29 1838.29 1784.54 62.79 o 3 6 29 14.34 -11.23 26.80 o 4 6 29 284.67 345.87 37.89 o 5 6 29 1250.47 1275.07 55.51 o 6 6 29 118.53 107.07 35.70 o 7 6 29 1148.29 1198.14 60.10 o 8 6 29 8.98 2.58 34.41 o 9 6 29 1376.12 1476.48 62.50 o 10 6 29 141.39 71.05 35.05 o 11 6 29 87.43 162.10 38.44 o 12 6 29 22.89 -4.64 36.13 o 13 6 29 948.89 1137.30 67.33 o 14 6 29 219.98 127.77 42.68 o 15 6 29 189.95 181.36 49.36 o 16 6 29 342.88 333.59 67.52 o 1 7 29 20.31 17.14 31.34 o 2 7 29 17.74 10.94 30.55 o 3 7 29 751.46 735.79 48.83 o 4 7 29 953.87 988.15 54.27 o 5 7 29 1474.20 1372.07 57.38 o 6 7 29 1318.78 1417.97 64.32 o 7 7 29 618.92 694.31 59.70 o 8 7 29 139.73 111.99 37.97 o 9 7 29 1231.71 1224.10 83.58 o 10 7 29 187.12 176.55 42.59 o 11 7 29 89.51 105.77 39.92 o 12 7 29 294.30 250.41 45.48 o 13 7 29 129.91 52.80 44.20 o 14 7 29 450.01 466.77 54.75 o 15 7 29 10.31 47.04 42.62 o 16 7 29 3.80 76.51 45.26 o 0 8 29 1316.55 1422.78 102.76 o 1 8 29 1691.40 1856.19 95.08 o 2 8 29 1427.74 1290.87 65.18 o 3 8 29 6.18 -40.89 31.79 o 4 8 29 240.29 203.43 38.88 o 5 8 29 12.31 -39.49 31.47 o 6 8 29 612.72 596.72 49.91 o 7 8 29 105.68 182.26 39.99 o 8 8 29 674.59 629.40 52.60 o 9 8 29 984.08 1132.08 64.08 o 10 8 29 585.96 666.36 56.27 o 11 8 29 1472.85 1500.16 72.74 o 12 8 29 126.29 58.41 39.91 o 13 8 29 1124.85 1096.56 68.32 o 14 8 29 0.50 50.57 46.42 o 15 8 29 42.54 22.96 45.41 o 1 9 29 23.91 -16.21 38.34 o 2 9 29 588.40 668.40 50.05 o 3 9 29 0.06 -2.59 32.62 o 4 9 29 1050.14 977.85 63.31 o 5 9 29 497.29 489.46 47.72 o 6 9 29 51.18 104.23 37.48 o 7 9 29 242.07 175.64 44.04 o 8 9 29 318.29 234.96 44.96 o 9 9 29 3.02 -11.94 38.02 o 10 9 29 83.08 66.24 46.74 o 11 9 29 120.17 93.97 41.03 o 12 9 29 77.18 42.86 44.08 o 13 9 29 3.27 28.53 40.27 o 14 9 29 32.56 40.96 43.70 o 0 10 29 3568.73 3829.19 158.08 o 1 10 29 714.50 743.53 63.47 o 2 10 29 10.69 -22.67 36.00 o 3 10 29 394.29 492.81 48.11 o 4 10 29 0.58 -46.12 30.75 o 5 10 29 164.42 172.38 54.97 o 6 10 29 7.57 -22.41 36.01 o 7 10 29 439.81 431.21 53.55 o 8 10 29 589.80 615.40 57.75 o 9 10 29 93.14 159.63 45.37 o 10 10 29 32.84 45.12 41.81 o 11 10 29 192.35 188.44 49.21 o 12 10 29 153.89 187.54 48.34 o 13 10 29 167.31 201.36 67.83 o 1 11 29 138.80 58.75 44.25 o 2 11 29 5.05 -44.69 39.96 o 3 11 29 621.57 629.38 58.34 o 4 11 29 44.19 15.50 34.72 o 5 11 29 161.82 116.84 52.91 o 6 11 29 49.34 5.24 36.28 o 7 11 29 142.06 91.65 40.47 o 8 11 29 254.52 235.59 47.58 o 9 11 29 23.14 17.02 42.67 o 10 11 29 112.01 87.37 45.18 o 11 11 29 5.36 11.68 43.57 o 12 11 29 50.51 58.07 46.59 o 0 12 29 264.68 296.35 75.18 o 1 12 29 332.51 402.16 58.07 o 2 12 29 814.46 966.50 128.62 o 3 12 29 12.24 44.34 40.94 o 4 12 29 572.24 636.97 60.68 o 5 12 29 77.15 67.15 37.95 o 6 12 29 49.86 29.77 38.54 o 7 12 29 27.77 58.51 38.89 o 8 12 29 295.11 311.64 52.84 o 9 12 29 201.11 193.12 48.28 o 10 12 29 63.45 130.45 47.84 o 11 12 29 243.39 360.61 71.56 o 1 13 29 0.09 62.46 44.96 o 2 13 29 83.16 31.39 47.92 o 3 13 29 47.70 73.88 48.33 o 4 13 29 211.42 228.85 49.70 o 5 13 29 49.66 47.71 43.45 o 6 13 29 0.32 0.36 38.44 o 7 13 29 208.10 192.46 47.13 o 8 13 29 83.46 75.94 53.08 o 9 13 29 33.66 21.66 44.19 o 0 14 29 774.95 812.76 107.01 o 1 14 29 599.73 490.26 78.56 o 2 14 29 68.96 84.46 50.84 o 3 14 29 506.01 689.91 69.86 o 4 14 29 91.17 102.17 47.12 o 5 14 29 232.82 295.00 68.33 o 6 14 29 64.71 172.62 51.07 o 7 14 29 35.57 57.94 47.78 o 1 15 29 0.06 -28.95 48.52 o 2 15 29 85.19 140.50 51.48 o 3 15 29 287.22 362.79 63.65 o 0 0 30 8490.92 7927.99 182.35 o 1 0 30 1918.17 1741.29 71.30 o 2 0 30 4114.81 3807.60 98.29 o 3 0 30 840.05 943.93 57.67 o 4 0 30 953.23 1098.18 61.72 o 5 0 30 940.87 945.91 59.71 o 6 0 30 474.98 387.91 56.40 o 7 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34.35 o 6 2 30 3476.49 3470.70 74.74 o 7 2 30 176.36 189.05 33.70 o 8 2 30 4927.17 5219.59 111.31 o 9 2 30 1760.21 1955.06 80.37 o 10 2 30 2175.98 2316.62 97.24 o 11 2 30 363.79 348.08 48.80 o 12 2 30 1181.56 1386.66 72.24 o 13 2 30 219.22 305.20 48.69 o 14 2 30 762.91 814.44 75.90 o 15 2 30 119.81 110.67 45.23 o 16 2 30 34.54 57.74 44.86 o 17 2 30 6.73 -47.33 44.00 o 1 3 30 221.78 243.26 26.16 o 2 3 30 2131.60 2270.70 51.10 o 3 3 30 68.86 94.92 24.64 o 4 3 30 23.19 -6.28 26.31 o 5 3 30 85.37 -3.76 28.07 o 6 3 30 286.19 340.83 38.38 o 7 3 30 162.10 142.35 34.45 o 8 3 30 0.75 -2.34 31.71 o 9 3 30 1291.87 1401.76 84.27 o 10 3 30 116.09 172.85 45.62 o 11 3 30 537.34 557.87 54.56 o 12 3 30 50.59 62.93 49.65 o 13 3 30 102.70 35.10 40.62 o 14 3 30 66.69 68.32 43.56 o 15 3 30 0.04 16.83 41.94 o 16 3 30 1045.82 1104.79 75.86 o 17 3 30 414.65 626.08 64.00 o 0 4 30 6963.76 7322.54 130.82 o 1 4 30 11.09 -14.62 22.67 o 2 4 30 211.58 229.22 28.88 o 3 4 30 513.66 529.35 36.42 o 4 4 30 646.53 611.25 41.59 o 5 4 30 121.24 101.47 39.58 o 6 4 30 11.36 -16.92 29.72 o 7 4 30 747.91 983.25 53.79 o 8 4 30 3235.02 3400.12 94.59 o 9 4 30 381.67 368.22 43.87 o 10 4 30 2943.57 2811.49 91.09 o 11 4 30 0.78 -8.36 37.57 o 12 4 30 163.75 118.54 43.79 o 13 4 30 42.27 26.93 41.08 o 14 4 30 33.44 20.66 41.17 o 15 4 30 48.46 57.39 44.00 o 16 4 30 69.42 33.00 43.39 o 1 5 30 490.42 463.74 37.32 o 2 5 30 594.35 737.73 44.00 o 3 5 30 228.36 217.92 33.64 o 4 5 30 6.29 20.16 28.56 o 5 5 30 40.83 -13.55 30.11 o 6 5 30 2232.60 2184.90 80.75 o 7 5 30 631.41 725.10 47.72 o 8 5 30 1586.28 1568.55 61.67 o 9 5 30 495.13 461.30 46.98 o 10 5 30 7.25 -10.70 33.14 o 11 5 30 13.65 19.75 38.45 o 12 5 30 455.20 521.48 55.04 o 13 5 30 41.80 68.49 42.33 o 14 5 30 304.29 233.72 50.71 o 15 5 30 39.22 -5.83 43.55 o 16 5 30 404.14 375.94 62.22 o 0 6 30 16098.45 16737.03 270.14 o 1 6 30 22.91 57.75 32.23 o 2 6 30 2841.87 2948.41 77.04 o 3 6 30 467.57 491.18 41.45 o 4 6 30 10.08 17.19 29.65 o 5 6 30 1566.87 1691.83 74.46 o 6 6 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