#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/58/2215812.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215812_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Hrib, Cristian G.' 'Petrovic, Dejan' 'Tamm, Matthias' _publ_section_title ; A solvent-free modification of {2,6-bis[(1,3-di-tert-butylimidazolin-2-ylideneamino)methyl]pyridine}(hydrogen carbonato)copper(II) hexafluoridophosphate ; _journal_coeditor_code BT2543 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2768 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 109.619 _cell_angle_beta 101.729 _cell_angle_gamma 94.164 _cell_length_a 9.0309 _cell_length_b 13.8239 _cell_length_c 15.6540 _exptl_crystal_F_000 798.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file bt2543Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dean72 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 241.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ 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691.77 722.65 20.32 o 7 1 0 107.73 114.61 14.09 o 8 1 0 421.52 487.05 32.33 o 9 1 0 716.89 663.69 51.52 o 10 1 0 270.61 260.61 28.35 o 11 1 0 12.29 -33.71 38.01 o -11 2 0 287.48 338.15 38.49 o -10 2 0 9.24 16.24 17.68 o -9 2 0 352.51 413.86 21.46 o -8 2 0 35.73 34.54 13.96 o -7 2 0 496.68 490.01 15.01 o -6 2 0 2324.33 2439.54 41.20 o -5 2 0 987.04 955.81 20.15 o -4 2 0 5632.38 5977.29 83.03 o -3 2 0 4.53 2.53 4.08 o -2 2 0 3308.98 3404.79 65.19 o -1 2 0 122.23 107.86 26.33 o 0 2 0 17450.16 18029.46 268.61 o 1 2 0 16066.79 17371.01 187.19 o 2 2 0 7441.60 7761.75 100.88 o 3 2 0 299.28 293.32 8.71 o 4 2 0 2709.20 2631.86 34.56 o 5 2 0 856.97 852.07 19.49 o 6 2 0 134.40 149.76 12.88 o 7 2 0 45.93 27.14 11.97 o 8 2 0 511.66 497.01 23.27 o 9 2 0 68.31 56.28 17.88 o 10 2 0 55.43 107.35 27.00 o 11 2 0 56.20 38.62 29.29 o -11 3 0 146.17 148.92 32.62 o -10 3 0 393.15 391.23 24.22 o -9 3 0 78.97 68.18 27.44 o -8 3 0 470.71 433.99 20.18 o -7 3 0 871.23 820.92 20.72 o -6 3 0 2891.58 2955.71 46.68 o 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163.23 14.61 o 7 4 0 471.48 508.23 25.69 o 8 4 0 13.08 9.20 20.88 o 9 4 0 262.68 257.07 32.08 o 10 4 0 262.40 240.60 29.43 o -11 5 0 47.68 28.72 57.38 o -10 5 0 363.75 418.87 68.01 o -9 5 0 0.96 -17.21 26.80 o -8 5 0 1359.14 1368.50 57.69 o -7 5 0 1286.28 1270.57 41.35 o -6 5 0 736.87 669.84 29.50 o -5 5 0 1712.68 1713.85 44.11 o -4 5 0 24.20 4.49 10.30 o -3 5 0 1462.79 1432.14 37.61 o -2 5 0 685.81 644.87 40.22 o -1 5 0 152.27 124.87 7.02 o 0 5 0 2.86 -3.91 4.11 o 1 5 0 1363.66 1258.33 18.48 o 2 5 0 265.91 322.02 13.97 o 3 5 0 528.02 476.05 12.79 o 4 5 0 191.47 179.99 11.83 o 5 5 0 8.91 -4.56 8.24 o 6 5 0 1111.79 1067.93 28.71 o 7 5 0 113.25 112.93 16.55 o 8 5 0 74.79 55.48 17.86 o 9 5 0 593.05 589.35 53.79 o 10 5 0 110.99 99.64 30.26 o -11 6 0 522.63 557.16 83.42 o -10 6 0 0.08 -7.01 33.58 o -9 6 0 333.45 405.73 42.06 o -8 6 0 693.74 639.14 42.56 o -7 6 0 3155.47 3015.18 72.66 o -6 6 0 8.19 -1.98 14.92 o -5 6 0 97.98 82.64 15.26 o -4 6 0 672.86 693.96 25.70 o -3 6 0 2175.40 2277.14 65.23 o -2 6 0 460.82 360.44 37.92 o -1 6 0 586.22 603.19 14.30 o 0 6 0 534.68 465.63 11.35 o 1 6 0 570.58 559.05 13.73 o 2 6 0 809.17 750.83 15.26 o 3 6 0 368.08 357.82 12.66 o 4 6 0 568.58 549.26 15.70 o 5 6 0 39.69 22.68 9.79 o 6 6 0 151.32 167.99 16.86 o 7 6 0 103.93 46.34 16.65 o 8 6 0 261.08 281.48 25.54 o 9 6 0 65.98 36.84 25.47 o 10 6 0 4.77 -23.07 28.32 o -11 7 0 3.63 27.88 56.55 o -10 7 0 97.91 147.26 39.69 o -9 7 0 32.08 40.01 33.89 o -8 7 0 1615.39 1577.78 64.64 o -7 7 0 271.00 268.22 32.72 o -6 7 0 4.67 -11.77 15.89 o -5 7 0 106.88 114.23 22.75 o -4 7 0 4.66 -11.55 11.55 o -3 7 0 830.69 719.55 46.53 o -2 7 0 646.48 560.76 15.91 o -1 7 0 2530.81 2464.01 74.64 o 0 7 0 43.16 35.34 9.39 o 1 7 0 892.55 911.26 18.56 o 2 7 0 282.71 287.40 10.93 o 3 7 0 2226.89 2227.91 33.09 o 4 7 0 1.11 -8.87 8.87 o 5 7 0 11.24 -9.80 9.80 o 6 7 0 483.59 506.17 20.63 o 7 7 0 653.49 786.76 34.05 o 8 7 0 29.09 16.99 23.53 o 9 7 0 45.42 79.04 30.04 o -11 8 0 229.27 295.51 72.91 o -10 8 0 28.58 21.32 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19.01 o 7 9 0 584.13 666.15 80.37 o 8 9 0 218.62 308.94 77.86 o 9 9 0 17.76 -27.01 46.99 o -10 10 0 0.35 -1.14 51.77 o -9 10 0 39.80 1.34 82.46 o -8 10 0 239.30 217.82 38.73 o -7 10 0 293.30 373.43 61.80 o -6 10 0 96.66 119.87 61.71 o -5 10 0 1170.67 939.06 37.08 o -4 10 0 2.18 -6.11 16.84 o -3 10 0 5.64 -14.25 14.48 o -2 10 0 442.83 431.00 23.51 o -1 10 0 649.90 640.22 16.63 o 0 10 0 220.35 234.52 17.28 o 1 10 0 1179.83 1223.33 32.29 o 2 10 0 4740.38 4662.52 83.55 o 3 10 0 438.18 435.02 24.22 o 4 10 0 335.28 388.61 25.07 o 5 10 0 14.56 12.39 17.70 o 6 10 0 303.46 320.69 30.28 o 7 10 0 202.23 193.57 46.75 o 8 10 0 96.58 199.43 78.58 o -10 11 0 337.01 382.88 58.04 o -9 11 0 141.56 100.14 40.80 o -8 11 0 87.66 122.75 38.19 o -7 11 0 5.11 -16.37 30.34 o -6 11 0 217.22 25.97 33.80 o -5 11 0 9.60 -9.45 20.13 o -4 11 0 388.00 403.29 29.40 o -3 11 0 298.78 291.47 24.95 o -2 11 0 85.61 84.73 11.35 o -1 11 0 516.45 516.43 32.65 o 0 11 0 1.20 -11.22 11.22 o 1 11 0 2081.90 1989.39 44.93 o 2 11 0 157.23 139.94 17.83 o 3 11 0 369.19 428.42 26.05 o 4 11 0 224.21 254.94 23.49 o 5 11 0 430.28 468.97 46.63 o 6 11 0 169.97 124.61 25.28 o 7 11 0 406.57 397.19 84.25 o -9 12 0 40.21 80.63 56.49 o -8 12 0 45.28 118.22 42.72 o -7 12 0 375.69 398.96 90.64 o -6 12 0 0.55 3.28 27.25 o -5 12 0 117.06 128.92 32.99 o -4 12 0 912.10 902.21 38.85 o -3 12 0 379.10 461.33 74.91 o -2 12 0 1.53 -7.02 10.69 o -1 12 0 734.69 726.88 24.72 o 0 12 0 765.91 762.93 27.24 o 1 12 0 718.37 668.91 27.89 o 2 12 0 859.66 759.44 29.39 o 3 12 0 11.83 24.01 18.10 o 4 12 0 341.84 365.81 27.35 o 5 12 0 170.07 167.77 32.78 o 6 12 0 913.90 989.97 130.42 o 7 12 0 28.22 72.49 75.59 o -9 13 0 10.21 21.54 49.23 o -8 13 0 153.32 262.77 125.54 o -7 13 0 39.53 45.51 59.11 o -6 13 0 177.86 98.52 52.25 o -5 13 0 14.27 -36.12 44.13 o -4 13 0 579.93 639.99 86.25 o -3 13 0 280.11 315.12 72.25 o -2 13 0 1140.84 1046.50 82.24 o -1 13 0 220.34 214.66 17.99 o 0 13 0 1016.38 962.79 31.85 o 1 13 0 535.76 574.13 30.49 o 2 13 0 17.48 20.04 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