#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/58/2215831.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215831_Fobs loop_ _publ_author_name 'Zhang, Qiao-Chu' 'Shu, Zhan' 'Shen, Liang' 'Wang, Qi' 'Jin, Zhi-Min' _publ_section_title ; A second polymorph of 1-(carboxymethyl)-5-fluorouracil ; _journal_coeditor_code CF2143 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4214 _journal_volume 63 _journal_year 2007 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.218 _cell_angle_gamma 90.000 _cell_length_a 6.8090 _cell_length_b 4.8401 _cell_length_c 11.9461 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.8404 _[local]_cod_data_source_file cf2143Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SQ95m in Pc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 66.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1991.76 1629.86 12.16 o 2 0 0 1076.46 950.32 7.42 o 3 0 0 339.59 315.30 4.94 o 4 0 0 14.02 15.16 1.59 o 5 0 0 77.84 61.48 2.90 o 6 0 0 35.81 32.00 2.90 o 7 0 0 127.58 142.97 5.62 o 8 0 0 9.76 16.55 3.02 o 0 1 0 1500.46 1849.68 14.61 o 1 1 0 311.94 344.59 2.51 o 2 1 0 231.41 222.31 2.38 o 3 1 0 160.94 163.70 4.52 o 4 1 0 3.45 3.88 0.57 o 5 1 0 20.09 20.54 1.47 o 6 1 0 1.98 4.38 0.99 o 7 1 0 21.23 24.92 2.43 o 0 2 0 636.57 677.19 5.21 o 1 2 0 3.68 3.67 0.39 o 2 2 0 72.19 83.06 1.48 o 3 2 0 273.96 291.90 6.15 o 4 2 0 78.53 75.81 3.22 o 5 2 0 37.98 35.89 2.31 o 6 2 0 38.15 39.72 3.47 o 7 2 0 5.72 14.49 4.51 o 0 3 0 38.26 36.38 1.44 o 1 3 0 138.37 143.67 1.95 o 2 3 0 75.06 77.08 2.14 o 3 3 0 20.86 22.91 1.43 o 4 3 0 63.91 46.32 4.06 o 5 3 0 100.35 77.96 12.64 o 6 3 0 21.58 27.28 6.25 o 0 4 0 1.42 2.74 1.34 o 1 4 0 92.17 92.52 4.14 o 2 4 0 54.58 51.84 2.02 o 3 4 0 9.52 8.93 1.32 o 4 4 0 26.15 26.46 4.10 o 5 4 0 12.37 16.80 4.59 o 0 5 0 17.57 21.32 3.61 o 1 5 0 204.06 189.87 15.45 o 2 5 0 17.99 20.28 3.95 o 3 5 0 11.14 12.50 2.07 o 4 5 0 1.33 0.97 2.00 o -7 1 1 118.01 127.95 3.63 o -6 1 1 27.88 31.74 1.80 o -5 1 1 54.52 48.82 1.84 o -4 1 1 25.97 22.76 0.94 o -3 1 1 130.81 119.95 1.96 o -2 1 1 8.78 13.54 0.65 o -1 1 1 409.49 446.17 9.95 o 0 1 1 108.24 116.19 2.72 o 1 1 1 3304.66 3355.51 92.05 o 2 1 1 19.74 13.18 0.66 o 3 1 1 42.46 48.90 1.70 o 4 1 1 400.04 411.40 5.86 o 5 1 1 18.40 18.03 1.43 o 6 1 1 29.06 27.48 2.06 o 7 1 1 90.22 107.71 4.75 o -7 2 1 0.38 9.29 1.82 o -6 2 1 66.58 60.38 3.50 o -5 2 1 32.56 27.13 2.40 o -4 2 1 46.24 41.14 1.51 o -3 2 1 140.44 154.11 2.20 o -2 2 1 240.73 240.18 2.39 o -1 2 1 608.31 720.41 8.53 o 0 2 1 383.89 457.03 5.76 o 1 2 1 56.22 50.93 1.08 o 2 2 1 189.42 195.69 2.59 o 3 2 1 304.70 303.34 5.29 o 4 2 1 81.51 73.38 2.02 o 5 2 1 29.32 27.98 1.88 o 6 2 1 13.42 13.78 2.33 o 7 2 1 6.20 21.70 3.63 o -6 3 1 3.52 11.25 3.27 o -5 3 1 31.11 26.46 4.72 o -4 3 1 30.86 29.18 3.19 o -3 3 1 17.14 20.30 1.36 o -2 3 1 331.72 331.32 3.65 o -1 3 1 163.33 175.20 3.01 o 0 3 1 93.57 83.54 1.54 o 1 3 1 163.26 160.51 2.25 o 2 3 1 67.95 69.47 1.76 o 3 3 1 35.29 31.64 1.75 o 4 3 1 7.88 5.38 1.09 o 5 3 1 70.70 56.43 6.06 o 6 3 1 19.21 27.48 5.74 o -5 4 1 14.69 23.57 8.50 o -4 4 1 5.23 4.17 1.26 o -3 4 1 22.37 22.35 1.60 o -2 4 1 0.47 1.06 0.57 o -1 4 1 15.63 19.10 1.43 o 0 4 1 2.94 6.52 1.08 o 1 4 1 5.49 6.53 1.42 o 2 4 1 132.16 118.20 4.66 o 3 4 1 9.93 12.12 1.75 o 4 4 1 17.02 18.57 2.06 o 5 4 1 0.55 0.43 1.70 o -4 5 1 7.24 7.78 3.20 o -3 5 1 5.02 8.41 1.84 o -2 5 1 37.42 38.88 4.73 o -1 5 1 79.06 64.08 3.94 o 0 5 1 14.76 24.88 2.75 o 1 5 1 46.09 47.86 3.41 o 2 5 1 7.98 7.98 2.49 o 3 5 1 16.04 15.72 6.50 o -8 0 2 48.23 42.16 4.20 o -7 0 2 86.65 78.00 4.02 o -6 0 2 849.01 879.07 17.02 o -5 0 2 31.76 29.44 2.39 o -4 0 2 40.85 34.79 1.93 o -3 0 2 777.11 844.37 12.45 o -2 0 2 303.26 284.18 3.97 o -1 0 2 395.51 377.17 3.72 o 0 0 2 1125.81 1162.14 9.91 o 1 0 2 2129.12 1898.24 14.58 o 2 0 2 39.65 30.48 1.42 o 3 0 2 162.09 143.12 2.53 o 4 0 2 83.50 80.72 2.61 o 5 0 2 34.88 29.60 2.00 o 6 0 2 58.24 46.07 7.48 o 7 0 2 8.54 11.84 2.25 o -7 1 2 14.81 13.39 1.64 o -6 1 2 86.51 82.65 3.17 o -5 1 2 24.13 24.97 1.38 o -4 1 2 171.31 176.35 2.45 o -3 1 2 274.48 294.39 2.70 o -2 1 2 241.46 249.54 3.50 o -1 1 2 7.98 5.28 0.62 o 0 1 2 99.02 93.34 3.91 o 1 1 2 2383.62 2633.03 130.67 o 2 1 2 523.62 519.90 4.67 o 3 1 2 476.45 479.33 4.98 o 4 1 2 194.87 188.34 3.57 o 5 1 2 2.95 4.34 0.97 o 6 1 2 10.79 12.75 2.38 o 7 1 2 21.26 30.20 7.72 o -7 2 2 0.54 7.45 1.58 o -6 2 2 41.21 43.86 2.99 o -5 2 2 0.72 4.46 1.41 o -4 2 2 32.04 29.90 1.64 o -3 2 2 275.93 263.56 3.04 o -2 2 2 78.06 92.97 3.50 o -1 2 2 464.00 509.77 14.44 o 0 2 2 425.11 445.75 18.83 o 1 2 2 366.64 367.80 4.69 o 2 2 2 127.83 115.75 2.06 o 3 2 2 23.61 23.36 1.12 o 4 2 2 28.87 31.33 1.68 o 5 2 2 1.31 0.62 0.75 o 6 2 2 65.92 60.51 3.39 o 7 2 2 33.08 57.76 4.87 o -6 3 2 0.73 1.46 1.87 o -5 3 2 17.57 19.77 6.94 o -4 3 2 17.86 17.65 2.10 o -3 3 2 12.55 18.47 1.34 o -2 3 2 206.62 211.83 4.17 o -1 3 2 186.55 197.91 3.78 o 0 3 2 78.99 87.43 1.52 o 1 3 2 31.37 32.85 1.21 o 2 3 2 80.59 71.05 2.29 o 3 3 2 81.56 70.55 1.99 o 4 3 2 24.58 26.46 3.62 o 5 3 2 10.46 15.46 7.12 o 6 3 2 6.87 20.61 3.88 o -5 4 2 62.39 65.54 13.43 o -4 4 2 75.00 60.06 6.82 o -3 4 2 22.62 21.35 2.34 o -2 4 2 40.25 40.70 1.87 o -1 4 2 34.86 34.04 1.71 o 0 4 2 15.31 17.07 1.97 o 1 4 2 16.58 19.61 2.10 o 2 4 2 571.89 538.17 9.05 o 3 4 2 138.36 122.39 3.67 o 4 4 2 21.10 15.13 2.18 o 5 4 2 1.92 4.12 2.13 o -3 5 2 0.08 2.49 1.71 o -2 5 2 5.92 5.77 1.55 o -1 5 2 14.05 17.54 2.42 o 0 5 2 31.13 33.11 2.76 o 1 5 2 3.39 4.45 2.58 o 2 5 2 48.39 42.52 3.19 o 3 5 2 12.69 13.96 2.18 o -7 1 3 6.80 9.04 1.73 o -6 1 3 2.78 6.79 1.13 o -5 1 3 114.99 108.62 3.07 o -4 1 3 3.33 5.63 0.79 o -3 1 3 81.04 84.97 1.75 o -2 1 3 585.88 584.17 3.63 o -1 1 3 531.26 497.07 3.49 o 0 1 3 1549.19 1634.25 10.20 o 1 1 3 4409.03 4373.38 128.70 o 2 1 3 30.40 28.81 0.98 o 3 1 3 27.37 27.57 1.07 o 4 1 3 103.79 88.41 8.58 o 5 1 3 17.19 22.47 2.07 o 6 1 3 12.56 10.88 1.54 o 7 1 3 31.22 36.32 5.46 o -7 2 3 13.56 23.42 2.94 o -6 2 3 11.29 12.87 2.58 o -5 2 3 40.28 30.93 1.79 o -4 2 3 236.39 196.14 8.04 o -3 2 3 119.04 126.11 3.00 o -2 2 3 129.48 138.09 2.96 o -1 2 3 152.04 161.89 3.96 o 0 2 3 256.35 262.75 2.72 o 1 2 3 70.35 63.00 1.51 o 2 2 3 511.86 529.54 5.50 o 3 2 3 91.73 89.07 3.41 o 4 2 3 5.97 5.71 0.90 o 5 2 3 20.45 18.61 2.43 o 6 2 3 27.28 36.60 15.83 o -6 3 3 9.65 19.77 7.45 o -5 3 3 100.64 97.27 12.07 o -4 3 3 45.67 40.11 5.15 o -3 3 3 80.67 63.39 2.48 o -2 3 3 45.76 42.21 1.99 o -1 3 3 117.96 136.39 6.74 o 0 3 3 43.55 38.30 1.71 o 1 3 3 6.50 8.57 1.02 o 2 3 3 15.24 16.99 0.97 o 3 3 3 228.43 192.45 4.23 o 4 3 3 26.42 27.10 2.98 o 5 3 3 19.97 31.83 3.50 o 6 3 3 1.53 15.36 3.20 o -5 4 3 2.39 13.84 4.66 o -4 4 3 39.49 35.71 2.52 o -3 4 3 6.47 6.70 1.08 o -2 4 3 4.43 8.35 1.29 o -1 4 3 8.97 8.02 1.22 o 0 4 3 22.33 26.42 1.99 o 1 4 3 15.60 16.40 2.84 o 2 4 3 26.40 27.49 2.49 o 3 4 3 14.02 16.79 2.52 o 4 4 3 6.40 6.26 2.57 o -3 5 3 20.29 20.72 2.87 o -2 5 3 13.77 13.13 1.74 o -1 5 3 7.73 8.52 2.65 o 0 5 3 10.25 14.63 2.07 o 1 5 3 14.23 12.59 2.08 o 2 5 3 4.19 6.21 2.20 o 3 5 3 6.79 9.04 2.24 o -7 0 4 40.31 46.18 3.23 o -6 0 4 137.25 117.50 4.37 o -5 0 4 56.68 54.79 2.75 o -4 0 4 24.55 21.68 1.98 o -3 0 4 352.50 354.55 5.42 o -2 0 4 809.83 891.81 9.01 o -1 0 4 68.31 67.03 4.07 o 0 0 4 977.49 934.71 7.43 o 1 0 4 326.43 341.05 6.45 o 2 0 4 474.97 415.54 7.66 o 3 0 4 142.26 124.59 4.62 o 4 0 4 280.83 244.69 7.13 o 5 0 4 343.47 315.30 9.08 o 6 0 4 1.70 0.08 1.26 o 7 0 4 14.85 15.93 3.37 o -7 1 4 14.72 16.36 1.99 o -6 1 4 22.68 27.38 2.27 o -5 1 4 358.82 317.20 4.57 o -4 1 4 54.84 42.97 1.52 o -3 1 4 296.42 273.70 4.52 o -2 1 4 7.69 8.45 0.59 o -1 1 4 25.99 29.95 0.80 o 0 1 4 621.80 701.92 4.80 o 1 1 4 233.81 230.90 11.34 o 2 1 4 266.88 266.87 11.20 o 3 1 4 18.70 16.96 1.16 o 4 1 4 31.49 29.09 2.87 o 5 1 4 2.89 3.98 0.92 o 6 1 4 9.67 10.96 1.59 o 7 1 4 7.97 15.15 3.39 o -7 2 4 19.29 31.10 2.85 o -6 2 4 16.06 25.60 2.86 o -5 2 4 63.41 60.45 3.30 o -4 2 4 41.95 40.75 5.17 o -3 2 4 7.69 8.30 1.10 o -2 2 4 36.93 32.16 1.57 o -1 2 4 49.55 45.31 1.75 o 0 2 4 381.24 407.96 3.75 o 1 2 4 295.91 281.78 2.77 o 2 2 4 752.76 753.80 14.94 o 3 2 4 38.75 34.54 1.43 o 4 2 4 24.88 24.85 2.18 o 5 2 4 9.82 15.44 1.88 o 6 2 4 2.47 9.26 2.65 o 7 2 4 1.53 14.16 5.35 o -6 3 4 2.55 11.97 6.24 o -5 3 4 43.40 42.36 7.71 o -4 3 4 33.19 34.22 3.43 o -3 3 4 17.08 19.48 1.77 o -2 3 4 43.39 36.02 2.21 o -1 3 4 14.67 15.87 1.41 o 0 3 4 45.47 38.84 1.80 o 1 3 4 52.28 47.48 1.95 o 2 3 4 60.96 60.13 1.89 o 3 3 4 274.96 272.98 32.59 o 4 3 4 35.63 36.71 11.51 o 5 3 4 22.52 26.14 3.11 o 6 3 4 0.43 10.90 2.59 o -5 4 4 8.04 16.64 8.52 o -4 4 4 247.68 223.52 6.43 o -3 4 4 57.88 54.35 3.25 o -2 4 4 10.91 9.95 1.74 o -1 4 4 108.06 100.00 3.21 o 0 4 4 20.67 22.87 3.06 o 1 4 4 6.19 6.71 1.27 o 2 4 4 16.31 22.30 5.79 o 3 4 4 26.26 28.76 2.78 o 4 4 4 0.02 0.11 1.65 o -3 5 4 31.39 33.01 3.08 o -2 5 4 9.43 10.94 2.86 o -1 5 4 21.04 25.06 4.38 o 0 5 4 1.48 7.79 1.64 o 1 5 4 7.86 6.96 2.62 o 2 5 4 2.06 2.89 2.12 o 3 5 4 1.21 2.00 2.20 o -7 1 5 24.60 28.34 2.32 o -6 1 5 145.71 134.19 5.80 o -5 1 5 366.92 323.87 4.62 o -4 1 5 26.21 23.73 1.19 o -3 1 5 227.74 196.01 6.08 o -2 1 5 442.00 439.89 4.99 o -1 1 5 269.32 296.26 3.01 o 0 1 5 212.57 196.19 3.42 o 1 1 5 168.31 161.43 3.39 o 2 1 5 177.41 158.58 3.60 o 3 1 5 5.95 5.95 1.07 o 4 1 5 26.82 32.79 2.05 o 5 1 5 15.43 16.11 3.27 o 6 1 5 11.46 11.68 2.01 o 7 1 5 19.39 18.23 2.80 o -7 2 5 29.75 29.97 5.98 o -6 2 5 35.99 30.40 3.48 o -5 2 5 26.82 27.24 2.77 o -4 2 5 62.75 54.01 2.99 o -3 2 5 61.79 54.45 2.16 o -2 2 5 46.37 45.98 1.94 o -1 2 5 201.90 201.50 3.84 o 0 2 5 57.14 62.02 1.56 o 1 2 5 18.60 16.53 0.97 o 2 2 5 424.07 408.12 6.28 o 3 2 5 26.06 22.68 1.29 o 4 2 5 248.28 213.08 6.19 o 5 2 5 39.39 36.99 3.57 o 6 2 5 6.65 10.36 2.54 o -6 3 5 5.54 12.94 7.31 o -5 3 5 3.64 7.69 3.71 o -4 3 5 36.28 36.99 2.97 o -3 3 5 65.97 65.78 4.00 o -2 3 5 10.17 13.57 2.57 o -1 3 5 36.04 38.77 2.31 o 0 3 5 70.68 66.19 3.39 o 1 3 5 32.61 27.18 1.74 o 2 3 5 27.21 24.16 1.42 o 3 3 5 408.29 388.59 32.02 o 4 3 5 36.84 33.40 7.78 o 5 3 5 15.95 15.79 7.11 o 6 3 5 5.57 15.56 2.94 o -5 4 5 13.94 19.87 7.13 o -4 4 5 1.08 4.96 3.83 o -3 4 5 5.49 6.77 2.29 o -2 4 5 1.92 2.79 0.98 o -1 4 5 17.66 21.11 2.46 o 0 4 5 45.88 42.88 3.67 o 1 4 5 8.31 10.14 1.80 o 2 4 5 35.83 31.47 4.38 o 3 4 5 30.13 31.48 4.29 o 4 4 5 11.88 11.84 3.12 o -2 5 5 0.59 4.01 2.27 o -1 5 5 5.80 11.93 4.18 o 0 5 5 27.84 32.59 8.45 o 1 5 5 1.32 5.51 4.17 o 2 5 5 15.21 14.15 3.58 o -7 0 6 31.03 23.63 5.62 o -6 0 6 19.92 20.34 2.35 o -5 0 6 21.36 18.43 3.30 o -4 0 6 23.92 18.07 2.15 o -3 0 6 172.15 139.26 3.64 o -2 0 6 1205.78 1249.41 11.09 o -1 0 6 850.09 999.97 9.61 o 0 0 6 101.10 90.88 2.66 o 1 0 6 1179.33 1228.31 15.43 o 2 0 6 621.18 534.69 10.18 o 3 0 6 32.85 25.50 2.44 o 4 0 6 9.05 10.27 2.16 o 5 0 6 9.93 8.73 2.33 o 6 0 6 4.39 3.97 2.05 o 7 0 6 8.05 9.29 2.99 o -7 1 6 3.72 8.06 2.20 o -6 1 6 18.52 22.88 6.20 o -5 1 6 5.03 4.81 1.63 o -4 1 6 21.52 21.48 1.63 o -3 1 6 31.56 28.46 1.22 o -2 1 6 47.88 47.69 1.39 o -1 1 6 8.53 10.95 0.78 o 0 1 6 10.83 10.91 0.77 o 1 1 6 81.55 78.56 2.62 o 2 1 6 2.55 2.72 0.87 o 3 1 6 40.26 31.42 1.94 o 4 1 6 17.93 18.96 2.11 o 5 1 6 1.33 3.80 1.21 o 6 1 6 10.47 13.80 2.18 o 7 1 6 5.57 8.03 1.99 o -6 2 6 36.08 37.10 3.01 o -5 2 6 49.31 45.37 3.52 o -4 2 6 320.50 301.39 7.10 o -3 2 6 82.70 86.16 3.28 o -2 2 6 22.82 24.12 1.62 o -1 2 6 51.71 48.03 2.05 o 0 2 6 28.99 28.37 1.22 o 1 2 6 69.14 50.71 1.65 o 2 2 6 72.02 59.74 2.18 o 3 2 6 88.60 80.08 2.66 o 4 2 6 255.52 252.50 6.86 o 5 2 6 26.50 26.23 3.22 o 6 2 6 21.93 24.60 7.91 o -6 3 6 0.88 8.01 4.16 o -5 3 6 26.85 30.43 6.11 o -4 3 6 82.32 78.09 4.00 o -3 3 6 273.51 244.20 8.56 o -2 3 6 51.85 48.17 2.27 o -1 3 6 29.75 26.89 2.01 o 0 3 6 12.12 14.80 2.55 o 1 3 6 13.22 15.07 3.78 o 2 3 6 55.24 49.12 3.75 o 3 3 6 152.20 129.84 10.03 o 4 3 6 68.19 67.28 10.24 o 5 3 6 8.14 16.98 8.04 o -4 4 6 53.23 53.42 9.02 o -3 4 6 9.85 8.87 2.46 o -2 4 6 3.33 3.60 1.09 o -1 4 6 3.12 4.33 1.37 o 0 4 6 4.31 6.60 1.29 o 1 4 6 3.13 3.36 1.00 o 2 4 6 25.29 24.47 3.88 o 3 4 6 0.61 4.08 4.01 o 4 4 6 21.60 34.10 8.88 o -2 5 6 10.40 20.43 3.74 o -1 5 6 13.76 27.60 9.74 o 0 5 6 3.01 9.10 4.76 o 1 5 6 6.93 13.66 8.54 o -7 1 7 17.36 24.35 4.74 o -6 1 7 43.68 44.42 6.19 o -5 1 7 18.58 18.90 5.42 o -4 1 7 36.97 34.70 4.34 o -3 1 7 19.78 20.86 1.14 o -2 1 7 91.58 89.99 2.04 o -1 1 7 87.93 93.82 2.07 o 0 1 7 15.33 18.07 1.03 o 1 1 7 231.61 201.43 3.85 o 2 1 7 177.15 156.39 4.17 o 3 1 7 16.26 15.52 1.73 o 4 1 7 0.52 2.68 1.05 o 5 1 7 115.91 115.59 4.42 o 6 1 7 46.07 41.04 5.65 o -6 2 7 15.32 24.95 7.62 o -5 2 7 46.63 45.73 6.74 o -4 2 7 332.89 296.19 8.18 o -3 2 7 5.87 6.97 1.61 o -2 2 7 201.75 176.88 5.29 o -1 2 7 14.95 14.34 1.52 o 0 2 7 19.59 18.21 1.19 o 1 2 7 114.99 98.92 2.46 o 2 2 7 13.23 11.34 1.34 o 3 2 7 52.71 52.17 3.73 o 4 2 7 54.38 48.78 4.87 o 5 2 7 19.19 22.48 5.43 o 6 2 7 6.18 9.39 2.22 o -5 3 7 34.38 30.33 3.49 o -4 3 7 31.72 29.96 3.17 o -3 3 7 386.34 349.81 16.07 o -2 3 7 12.89 13.62 2.08 o -1 3 7 4.83 5.01 1.28 o 0 3 7 10.73 14.28 1.60 o 1 3 7 4.59 7.89 1.30 o 2 3 7 14.80 15.77 2.86 o 3 3 7 34.34 28.66 2.10 o 4 3 7 31.33 36.24 5.47 o 5 3 7 2.78 12.86 6.46 o -4 4 7 12.49 18.40 7.31 o -3 4 7 25.79 26.06 4.79 o -2 4 7 18.80 21.07 4.34 o -1 4 7 4.18 4.42 1.18 o 0 4 7 29.47 28.51 6.76 o 1 4 7 13.88 14.97 2.67 o 2 4 7 4.59 8.00 3.21 o 3 4 7 5.37 20.43 8.98 o 4 4 7 3.04 22.21 12.33 o 0 5 7 29.91 44.17 11.74 o -6 0 8 1.71 7.61 3.10 o -5 0 8 322.45 280.70 8.99 o -4 0 8 104.70 94.50 3.55 o -3 0 8 56.43 51.19 2.58 o -2 0 8 204.96 197.14 6.29 o -1 0 8 78.62 77.64 3.03 o 0 0 8 112.67 104.93 3.30 o 1 0 8 2.98 2.62 1.33 o 2 0 8 245.45 212.91 7.23 o 3 0 8 58.94 57.92 3.99 o 4 0 8 14.28 13.73 2.70 o 5 0 8 27.65 28.76 3.14 o 6 0 8 9.77 11.75 3.11 o -6 1 8 32.51 34.86 7.84 o -5 1 8 16.91 13.94 2.13 o -4 1 8 6.43 10.82 1.79 o -3 1 8 24.81 24.54 2.08 o -2 1 8 78.00 76.16 2.52 o -1 1 8 84.15 94.05 2.88 o 0 1 8 136.48 146.15 3.56 o 1 1 8 28.44 25.46 1.59 o 2 1 8 22.10 20.14 1.98 o 3 1 8 59.87 51.14 3.46 o 4 1 8 16.05 17.43 3.97 o 5 1 8 98.60 83.56 4.86 o 6 1 8 7.18 11.79 4.94 o -6 2 8 2.75 13.75 2.99 o -5 2 8 16.02 23.82 2.85 o -4 2 8 19.32 18.37 2.51 o -3 2 8 71.28 64.17 3.50 o -2 2 8 458.78 425.82 8.36 o -1 2 8 52.98 53.54 3.05 o 0 2 8 69.25 65.23 3.24 o 1 2 8 2.97 5.74 1.08 o 2 2 8 25.02 25.08 1.81 o 3 2 8 1.72 3.21 1.23 o 4 2 8 18.21 16.26 3.10 o 5 2 8 24.61 28.43 4.51 o -5 3 8 11.69 14.95 4.06 o -4 3 8 18.91 17.90 2.89 o -3 3 8 96.16 89.47 3.44 o -2 3 8 41.77 38.14 2.18 o -1 3 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