#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/58/2215832.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215832_Fobs loop_ _publ_author_name 'Okuda, Kensuke' 'Watanabe, Hiromi' 'Hirota, Takashi' 'Gotoh, Kazuma' 'Ishida, Hiroyuki' _publ_section_title ; [(Z)-2-(3-Methyl-1,2,4-oxadiazol-5-yl)-2-(1-naphthyl)ethenylamino]formaldehyde oxime 1,4-dioxane hemisolvate ; _journal_coeditor_code CF2149 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4261 _journal_page_last o4262 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.810 _cell_angle_gamma 90.000 _cell_length_a 25.0090 _cell_length_b 21.1940 _cell_length_c 14.5843 _exptl_crystal_F_000 2848.00 _reflns_d_resolution_high 0.7112 _[local]_cod_data_source_file cf2149Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 06110711' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1127.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 108563.54 112879.34 863.82 o 6 0 0 1270750.13 1281877.00 12947.16 o 8 0 0 171119.83 177995.31 1479.47 o 10 0 0 58286.19 61878.36 828.72 o 12 0 0 92646.64 102144.57 1633.96 o 14 0 0 22520.43 24794.75 335.80 o 16 0 0 9407.93 9402.58 122.17 o 18 0 0 18891.27 19995.25 577.63 o 20 0 0 6581.14 7219.50 220.75 o 22 0 0 223.65 259.66 95.27 o 24 0 0 1111.96 1170.34 60.19 o 26 0 0 87.49 87.95 75.07 o 28 0 0 265.66 183.53 56.72 o 30 0 0 253.22 226.74 142.87 o 5 1 0 3.29 31.25 12.13 o 7 1 0 5809.74 5500.33 88.13 o 9 1 0 209.85 208.55 14.62 o 11 1 0 734.04 740.07 22.88 o 13 1 0 6457.49 6626.42 113.97 o 15 1 0 899.53 840.76 31.94 o 17 1 0 881.66 887.74 37.12 o 19 1 0 3260.38 3350.99 56.03 o 21 1 0 872.29 967.65 51.95 o 23 1 0 588.74 617.22 43.14 o 25 1 0 1246.37 1360.11 65.61 o 27 1 0 115.30 83.29 42.21 o 29 1 0 195.00 124.09 42.51 o 4 2 0 13835.43 13741.10 75.73 o 6 2 0 42454.56 45099.81 311.74 o 8 2 0 5658.74 5855.53 52.04 o 10 2 0 7893.88 8656.08 106.12 o 12 2 0 14193.50 14956.60 145.29 o 14 2 0 755.13 780.25 32.53 o 16 2 0 2088.94 2211.50 38.76 o 18 2 0 3310.48 3409.00 56.45 o 20 2 0 0.45 4.22 32.96 o 22 2 0 1118.15 1149.08 55.36 o 24 2 0 155.06 120.07 30.89 o 26 2 0 13.97 13.53 29.08 o 28 2 0 177.46 135.04 46.60 o 30 2 0 19.03 5.75 38.25 o 1 3 0 796.76 736.68 8.10 o 3 3 0 3662.28 3492.39 28.08 o 5 3 0 6971.17 6305.37 61.82 o 7 3 0 205.01 307.00 49.57 o 9 3 0 2681.77 2515.57 30.23 o 11 3 0 84.94 131.95 26.13 o 13 3 0 3552.69 3511.38 52.86 o 15 3 0 474.39 460.04 26.28 o 17 3 0 1084.38 1064.63 32.58 o 19 3 0 1089.12 1145.75 51.00 o 21 3 0 1574.29 1700.48 57.24 o 23 3 0 112.79 367.64 179.20 o 25 3 0 116.36 202.65 81.83 o 27 3 0 349.48 317.70 72.17 o 29 3 0 64.83 99.69 46.13 o 0 4 0 216415.72 209677.45 1685.96 o 2 4 0 38971.50 37714.46 206.39 o 4 4 0 39069.25 38242.13 201.11 o 6 4 0 5593.67 5533.45 40.98 o 8 4 0 155.20 169.67 14.58 o 10 4 0 35035.13 39345.75 277.95 o 12 4 0 41.33 106.76 18.35 o 14 4 0 2149.08 2382.68 41.39 o 16 4 0 1334.15 1378.19 32.58 o 18 4 0 40.33 62.78 23.07 o 20 4 0 816.47 874.71 39.94 o 22 4 0 1307.35 1415.71 43.60 o 24 4 0 13.09 0.23 27.27 o 26 4 0 1.43 3.57 29.79 o 28 4 0 100.95 62.70 37.84 o 30 4 0 95.54 114.36 43.03 o 1 5 0 861.10 826.54 11.38 o 3 5 0 2373.15 2366.37 22.39 o 5 5 0 4498.43 4201.82 36.13 o 7 5 0 3159.48 3090.06 66.88 o 9 5 0 1537.44 1621.91 25.22 o 11 5 0 37.04 41.87 15.55 o 13 5 0 93.27 83.49 18.19 o 15 5 0 13.18 6.95 16.31 o 17 5 0 819.68 826.11 49.00 o 19 5 0 174.52 167.55 32.33 o 21 5 0 79.75 83.16 28.58 o 23 5 0 16.34 26.06 24.27 o 25 5 0 1.28 -23.37 32.06 o 27 5 0 63.21 66.36 38.64 o 29 5 0 10.88 34.70 37.53 o 0 6 0 1149.30 1291.29 25.07 o 2 6 0 614.60 575.14 11.22 o 4 6 0 493.04 588.70 20.92 o 6 6 0 51.71 54.36 10.09 o 8 6 0 471.43 484.09 20.64 o 10 6 0 20.91 30.75 12.80 o 12 6 0 33.22 31.14 16.05 o 14 6 0 120.88 138.19 24.75 o 16 6 0 0.46 11.94 17.65 o 18 6 0 7.58 -3.16 18.39 o 20 6 0 12.79 16.57 23.88 o 22 6 0 26.17 52.08 35.50 o 24 6 0 72.32 27.94 27.23 o 26 6 0 9.05 -15.33 26.53 o 28 6 0 25.87 34.13 41.57 o 1 7 0 354.99 345.72 10.77 o 3 7 0 3303.68 3164.43 27.93 o 5 7 0 5614.83 5515.10 39.36 o 7 7 0 2479.64 2448.12 27.68 o 9 7 0 638.41 608.72 19.42 o 11 7 0 774.52 845.56 35.73 o 13 7 0 416.04 410.56 25.71 o 15 7 0 1136.14 1125.47 40.20 o 17 7 0 194.32 212.45 26.26 o 19 7 0 267.60 240.68 32.25 o 21 7 0 163.51 170.07 27.79 o 23 7 0 4.18 -8.36 24.11 o 25 7 0 0.02 10.24 34.17 o 27 7 0 7.13 22.31 28.55 o 29 7 0 47.07 32.03 41.16 o 0 8 0 51591.89 60419.58 462.16 o 2 8 0 4559.18 4905.44 36.38 o 4 8 0 371.31 557.67 19.45 o 6 8 0 327.35 216.29 14.65 o 8 8 0 2197.59 1887.70 29.52 o 10 8 0 5288.18 6070.92 69.80 o 12 8 0 7266.98 7458.66 135.53 o 14 8 0 0.04 1.61 17.49 o 16 8 0 1.07 2.79 17.46 o 18 8 0 84.23 125.23 29.41 o 20 8 0 1986.71 2100.72 65.55 o 22 8 0 608.50 645.91 36.47 o 24 8 0 41.78 44.95 26.55 o 26 8 0 85.25 104.27 31.13 o 28 8 0 0.56 -0.88 36.62 o 1 9 0 52.91 40.61 10.00 o 3 9 0 1.86 21.11 8.79 o 5 9 0 3304.97 3540.42 29.68 o 7 9 0 958.39 879.46 17.47 o 9 9 0 562.61 554.55 20.40 o 11 9 0 872.84 949.57 23.35 o 13 9 0 220.91 236.61 25.60 o 15 9 0 1639.08 1615.95 49.13 o 17 9 0 118.92 97.28 22.66 o 19 9 0 42.29 38.70 23.77 o 21 9 0 35.19 28.35 26.15 o 23 9 0 26.25 -0.64 30.52 o 25 9 0 158.09 225.12 34.40 o 27 9 0 32.06 16.86 29.31 o 29 9 0 4.66 -16.23 34.54 o 0 10 0 68726.38 74610.88 848.71 o 2 10 0 21029.20 22654.05 178.31 o 4 10 0 13025.75 13777.56 173.30 o 6 10 0 30954.03 32266.70 278.90 o 8 10 0 2520.16 2419.03 35.58 o 10 10 0 1711.87 1733.14 29.71 o 12 10 0 3316.86 3393.21 60.12 o 14 10 0 1504.41 1340.46 46.97 o 16 10 0 1036.08 1035.17 36.60 o 18 10 0 91.20 97.03 24.27 o 20 10 0 128.43 163.13 27.04 o 22 10 0 98.48 95.77 31.07 o 24 10 0 2.09 6.56 26.46 o 26 10 0 1.18 18.58 35.85 o 28 10 0 31.82 32.04 32.33 o 1 11 0 306.61 476.78 32.83 o 3 11 0 224.04 239.81 12.82 o 5 11 0 566.41 638.52 16.77 o 7 11 0 165.73 250.72 31.71 o 9 11 0 17.28 28.54 12.84 o 11 11 0 0.75 0.42 15.20 o 13 11 0 10.39 12.54 16.96 o 15 11 0 860.67 844.41 39.17 o 17 11 0 152.96 142.69 25.13 o 19 11 0 3.96 -20.52 24.16 o 21 11 0 657.87 737.30 38.32 o 23 11 0 2.09 1.26 24.31 o 25 11 0 79.46 89.58 31.55 o 27 11 0 24.64 3.61 25.79 o 0 12 0 22665.43 27515.51 310.72 o 2 12 0 7294.45 8202.65 67.24 o 4 12 0 3570.47 3656.11 40.08 o 6 12 0 150.67 182.75 12.66 o 8 12 0 8.93 28.20 13.04 o 10 12 0 6663.83 6570.88 95.19 o 12 12 0 352.43 423.02 24.33 o 14 12 0 675.11 640.29 30.57 o 16 12 0 8.99 5.66 18.35 o 18 12 0 133.84 114.96 22.88 o 20 12 0 2063.93 2000.93 63.46 o 22 12 0 490.49 496.91 35.40 o 24 12 0 9.97 -10.08 29.59 o 26 12 0 330.83 371.38 42.33 o 1 13 0 0.83 11.16 8.07 o 3 13 0 3.41 4.04 9.63 o 5 13 0 138.44 129.16 13.31 o 7 13 0 10.31 17.42 12.00 o 9 13 0 135.79 135.91 15.17 o 11 13 0 415.91 386.88 22.00 o 13 13 0 0.76 0.07 18.32 o 15 13 0 579.55 556.48 28.63 o 17 13 0 250.37 257.71 23.53 o 19 13 0 383.63 427.40 29.26 o 21 13 0 122.33 105.89 28.73 o 23 13 0 47.41 43.45 28.95 o 25 13 0 355.01 368.23 41.91 o 27 13 0 44.71 27.91 34.73 o 0 14 0 10553.99 11285.32 117.53 o 2 14 0 6622.77 6786.88 50.30 o 4 14 0 1064.50 1371.78 23.42 o 6 14 0 4082.49 4351.40 47.47 o 8 14 0 4647.33 4616.66 46.92 o 10 14 0 1020.39 818.64 21.53 o 12 14 0 459.16 574.61 34.59 o 14 14 0 3004.50 2843.80 70.68 o 16 14 0 10.32 3.43 23.43 o 18 14 0 9.41 12.58 22.18 o 20 14 0 264.28 270.12 33.08 o 22 14 0 50.18 42.16 26.21 o 24 14 0 93.94 75.56 29.87 o 26 14 0 77.62 63.10 32.05 o 1 15 0 4.32 0.20 8.05 o 3 15 0 359.24 354.06 14.24 o 5 15 0 474.34 457.23 15.71 o 7 15 0 4.57 8.26 12.20 o 9 15 0 705.98 696.72 23.89 o 11 15 0 667.90 696.19 32.98 o 13 15 0 167.25 185.00 20.11 o 15 15 0 325.48 338.49 26.24 o 17 15 0 3.59 -2.69 16.40 o 19 15 0 134.70 126.71 25.75 o 21 15 0 164.35 180.93 27.92 o 23 15 0 8.27 23.29 25.51 o 25 15 0 19.13 -1.49 27.16 o 0 16 0 1094.91 991.77 29.99 o 2 16 0 1415.23 1356.30 21.81 o 4 16 0 492.92 484.05 23.69 o 6 16 0 286.75 218.02 16.36 o 8 16 0 970.07 919.24 25.85 o 10 16 0 9250.92 9005.96 109.33 o 12 16 0 1089.89 1029.78 27.09 o 14 16 0 309.41 303.06 23.66 o 16 16 0 34.15 50.52 22.07 o 18 16 0 148.76 149.83 32.07 o 20 16 0 194.46 206.33 29.56 o 22 16 0 33.45 73.80 28.63 o 24 16 0 178.73 195.51 39.20 o 1 17 0 0.66 5.51 9.72 o 3 17 0 6.59 3.24 9.65 o 5 17 0 1318.73 1335.77 27.26 o 7 17 0 24.25 33.31 14.23 o 9 17 0 91.17 79.93 17.83 o 11 17 0 2985.97 2709.16 43.34 o 13 17 0 133.38 203.94 35.81 o 15 17 0 65.77 76.82 20.69 o 17 17 0 638.00 562.06 29.94 o 19 17 0 742.82 736.90 33.33 o 21 17 0 1.87 34.68 24.29 o 23 17 0 94.96 108.17 34.68 o 25 17 0 131.94 99.66 34.34 o 0 18 0 11321.19 9632.26 113.62 o 2 18 0 5027.11 4498.84 43.07 o 4 18 0 1277.03 1060.25 23.06 o 6 18 0 4765.77 4350.52 45.69 o 8 18 0 6874.54 6830.73 69.69 o 10 18 0 191.02 215.17 20.84 o 12 18 0 1704.87 1572.72 39.96 o 14 18 0 1526.90 1484.24 55.94 o 16 18 0 3.99 -4.19 21.06 o 18 18 0 139.29 123.68 28.24 o 20 18 0 0.44 -13.08 21.59 o 22 18 0 89.52 86.42 34.30 o 24 18 0 1.90 4.83 28.26 o 1 19 0 47.96 41.91 12.11 o 3 19 0 266.73 290.23 18.02 o 5 19 0 570.58 547.62 19.65 o 7 19 0 380.27 425.58 23.18 o 9 19 0 231.86 244.00 22.73 o 11 19 0 368.88 345.31 23.88 o 13 19 0 31.00 39.44 17.46 o 15 19 0 65.63 50.03 19.68 o 17 19 0 15.12 39.96 19.56 o 19 19 0 3.86 -10.28 19.63 o 21 19 0 54.52 12.79 23.93 o 23 19 0 2.26 7.55 24.20 o 0 20 0 2819.05 2226.32 43.97 o 2 20 0 444.41 425.28 18.65 o 4 20 0 127.74 93.49 15.88 o 6 20 0 0.07 -8.18 11.64 o 8 20 0 62.67 53.96 18.39 o 10 20 0 0.35 8.09 15.16 o 12 20 0 51.48 47.87 18.52 o 14 20 0 54.88 84.32 23.67 o 16 20 0 4.54 10.13 20.03 o 18 20 0 304.92 289.55 37.44 o 20 20 0 380.70 413.94 55.86 o 22 20 0 7.31 48.02 24.79 o 1 21 0 187.30 155.58 19.64 o 3 21 0 56.68 62.76 18.32 o 5 21 0 4.54 5.95 12.77 o 7 21 0 82.58 73.94 20.82 o 9 21 0 69.65 54.46 19.33 o 11 21 0 106.21 81.36 20.00 o 13 21 0 53.63 64.00 23.39 o 15 21 0 0.77 2.59 15.39 o 17 21 0 4.98 -17.08 18.87 o 19 21 0 94.91 95.13 26.85 o 21 21 0 14.67 0.16 31.83 o 0 22 0 110.48 185.10 27.12 o 2 22 0 3.33 20.98 13.34 o 4 22 0 57.79 101.12 15.81 o 6 22 0 21.78 -1.19 15.04 o 8 22 0 18.83 23.22 15.24 o 10 22 0 10.87 41.83 16.34 o 12 22 0 52.11 7.96 17.56 o 14 22 0 152.82 132.81 21.40 o 16 22 0 124.47 71.24 31.51 o 18 22 0 156.73 121.07 53.02 o 20 22 0 39.42 69.44 58.73 o 1 23 0 20.13 21.72 15.70 o 3 23 0 2.35 6.12 10.31 o 5 23 0 284.53 247.29 17.95 o 7 23 0 477.49 453.90 23.00 o 9 23 0 104.23 108.58 19.69 o 11 23 0 55.36 37.14 15.45 o 13 23 0 152.82 119.39 28.15 o 15 23 0 489.46 520.30 43.69 o 17 23 0 2.95 -7.94 32.00 o 19 23 0 57.27 44.09 33.50 o 0 24 0 305.11 339.19 33.51 o 2 24 0 3.52 21.54 15.80 o 4 24 0 23.84 30.76 15.46 o 6 24 0 65.01 104.26 20.17 o 8 24 0 421.92 454.42 27.15 o 10 24 0 201.13 192.92 36.98 o 12 24 0 187.19 110.66 37.63 o 14 24 0 2.56 -16.84 28.50 o 16 24 0 211.10 147.85 41.04 o 18 24 0 0.90 -16.87 31.45 o 1 25 0 19.72 30.44 17.34 o 3 25 0 10.96 6.28 12.98 o 5 25 0 50.94 13.90 20.09 o 7 25 0 46.48 9.03 24.59 o 9 25 0 38.28 47.03 25.94 o 11 25 0 201.04 98.74 36.53 o 13 25 0 3.75 32.70 27.54 o 15 25 0 2.10 -0.73 32.61 o 0 26 0 800.38 832.53 30.61 o 2 26 0 464.50 482.08 39.16 o 4 26 0 36.82 27.67 19.45 o 6 26 0 142.29 81.98 26.06 o 8 26 0 570.28 691.87 46.29 o 10 26 0 425.92 561.57 45.82 o 12 26 0 18.05 -25.70 25.70 o 14 26 0 288.28 202.30 49.62 o 1 27 0 6.86 0.21 32.27 o 3 27 0 0.56 11.35 29.94 o 5 27 0 12.05 -0.93 18.29 o 7 27 0 0.98 -4.15 21.83 o 9 27 0 2.18 21.92 31.09 o 11 27 0 5.85 21.25 27.53 o 0 28 0 2.86 0.90 37.07 o 2 28 0 1491.62 1957.31 65.99 o 4 28 0 55.46 40.97 42.58 o 6 28 0 1773.05 2121.43 111.43 o 8 28 0 373.89 385.67 90.05 o 10 28 0 213.99 366.33 67.72 o 1 29 0 135.66 68.97 51.66 o 3 29 0 9.90 -30.14 52.13 o 5 29 0 14.59 22.05 50.07 o -31 1 1 16.25 18.46 48.85 o -29 1 1 38.53 26.44 31.51 o -27 1 1 125.24 159.64 54.41 o -25 1 1 5.48 4.27 26.83 o -23 1 1 102.27 84.51 28.98 o -21 1 1 179.92 163.47 32.99 o -19 1 1 528.94 556.93 34.16 o -17 1 1 86.86 92.66 26.39 o -15 1 1 3268.20 3473.90 81.49 o -13 1 1 29.14 22.79 14.76 o -11 1 1 1841.90 1683.81 27.55 o -9 1 1 10734.66 10757.53 73.13 o -7 1 1 4059.46 3707.17 40.38 o -5 1 1 13140.62 12456.54 76.86 o 3 1 1 4165.84 4016.35 30.49 o 5 1 1 22690.88 21617.26 121.27 o 7 1 1 11975.71 11021.31 93.48 o 9 1 1 374.63 279.60 15.50 o 11 1 1 7622.60 7590.99 81.97 o 13 1 1 4211.25 4188.74 89.03 o 15 1 1 78.95 133.20 22.83 o 17 1 1 1758.95 1775.14 48.10 o 19 1 1 188.72 181.41 28.06 o 21 1 1 32.98 19.57 26.30 o 23 1 1 338.29 386.05 47.43 o 25 1 1 2.20 1.60 28.55 o 27 1 1 30.69 25.75 34.44 o 29 1 1 33.31 1.90 39.14 o -30 2 1 8.82 -11.84 42.33 o -28 2 1 285.49 206.39 40.10 o -26 2 1 1053.26 1084.80 59.33 o -24 2 1 2689.21 2810.40 79.16 o -22 2 1 3674.14 4103.73 71.82 o -20 2 1 24860.10 26591.65 288.14 o -18 2 1 66.37 70.59 27.75 o -16 2 1 979.46 992.37 41.13 o -14 2 1 74600.55 78021.27 884.98 o -12 2 1 9739.53 10432.03 92.79 o -10 2 1 418.24 558.03 20.76 o -8 2 1 196500.06 202576.97 1198.41 o -6 2 1 105866.55 104950.23 674.21 o -4 2 1 87375.55 87315.51 462.81 o 2 2 1 15101.71 15053.80 91.87 o 4 2 1 6624.12 6552.30 43.85 o 6 2 1 10.94 66.76 12.64 o 8 2 1 302.04 363.89 15.63 o 10 2 1 16244.99 16500.88 210.32 o 12 2 1 5372.60 5859.27 119.29 o 14 2 1 96.38 75.67 20.49 o 16 2 1 223.85 272.60 25.24 o 18 2 1 531.26 612.79 77.94 o 20 2 1 916.08 943.32 48.60 o 22 2 1 2495.49 2814.47 104.77 o 24 2 1 5.27 9.81 27.99 o 26 2 1 75.16 35.45 37.31 o 28 2 1 16.55 -0.99 35.65 o -31 3 1 139.91 139.47 49.41 o -29 3 1 110.40 99.18 40.00 o -27 3 1 91.95 62.93 38.92 o -25 3 1 58.50 59.99 31.88 o -23 3 1 0.11 -20.67 28.08 o -21 3 1 403.55 414.61 34.44 o -19 3 1 258.26 230.38 31.63 o -17 3 1 65.68 81.19 24.81 o -15 3 1 30.81 10.99 22.95 o -13 3 1 1333.60 1373.18 25.72 o -11 3 1 7559.90 7719.81 59.02 o -9 3 1 2793.63 3008.77 37.87 o -7 3 1 474.67 537.13 25.05 o -5 3 1 20533.26 21386.47 122.41 o -3 3 1 3212.11 3190.96 21.31 o -1 3 1 3595.44 3320.67 22.33 o 1 3 1 10256.52 11094.88 56.26 o 3 3 1 21613.80 21707.23 146.29 o 5 3 1 372.13 346.95 14.47 o 7 3 1 1335.29 1351.79 20.09 o 9 3 1 12071.05 12138.10 94.10 o 11 3 1 1790.60 1829.89 29.92 o 13 3 1 681.20 708.10 27.20 o 15 3 1 1175.69 1251.83 32.71 o 17 3 1 2557.29 2641.45 52.81 o 19 3 1 286.70 302.41 32.67 o 21 3 1 12.15 32.57 32.95 o 23 3 1 1187.19 1241.72 61.14 o 25 3 1 0.62 8.85 34.34 o 27 3 1 118.63 78.25 45.48 o 29 3 1 63.07 6.97 36.87 o -30 4 1 79.85 41.53 41.80 o -28 4 1 152.54 118.90 44.23 o -26 4 1 62.96 16.80 26.66 o -24 4 1 283.22 254.98 32.85 o -22 4 1 701.75 764.97 41.84 o 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