#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/58/2215894.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215894_Fobs loop_ _publ_author_name 'Varga, Richard A.' 'Rus, Adina' 'Venter, Monica M.' 'Negreanu-Pirjol, Ticuta' 'Guran, Cornelia' _publ_section_title ; 3,6-Diaminoacridinium perchlorate ; _journal_coeditor_code EZ2099 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4317 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.212 _cell_angle_gamma 90.000 _cell_length_a 15.1217 _cell_length_b 13.4772 _cell_length_c 6.6922 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file ez2099Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 133rich in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 227.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6118.90 6795.16 309.70 o 4 0 0 10284.75 10291.00 327.09 o 6 0 0 3840.76 4031.34 79.37 o 8 0 0 810.00 744.98 17.60 o 10 0 0 394.37 389.18 13.97 o 12 0 0 9241.07 9144.58 209.31 o 14 0 0 52.85 57.92 8.81 o 16 0 0 251.52 247.77 16.41 o 18 0 0 12.00 18.03 5.09 o 1 1 0 1326.67 1343.19 20.61 o 3 1 0 1656.41 1910.46 26.72 o 5 1 0 3599.76 3891.99 62.83 o 7 1 0 1202.59 1291.03 25.53 o 9 1 0 68.18 53.57 2.52 o 11 1 0 17.70 24.91 2.61 o 13 1 0 825.71 794.17 18.54 o 15 1 0 57.00 59.91 5.93 o 17 1 0 28.05 29.68 4.49 o 0 2 0 7978.72 7785.11 170.25 o 2 2 0 9186.19 9639.22 130.32 o 4 2 0 0.62 4.10 0.56 o 6 2 0 26.34 22.93 1.62 o 8 2 0 3.41 16.44 1.37 o 10 2 0 347.59 286.60 7.19 o 12 2 0 364.97 376.20 10.37 o 14 2 0 289.42 260.02 9.60 o 16 2 0 1.26 2.70 2.05 o 18 2 0 51.90 70.84 6.88 o 1 3 0 7566.35 8297.08 119.54 o 3 3 0 10844.50 11039.56 149.18 o 5 3 0 304.11 260.84 5.18 o 7 3 0 286.70 217.82 6.33 o 9 3 0 1976.53 2025.23 30.43 o 11 3 0 280.79 294.96 8.56 o 13 3 0 580.20 566.20 15.60 o 15 3 0 166.21 155.84 8.33 o 17 3 0 1.48 5.36 2.42 o 0 4 0 197.85 174.17 5.61 o 2 4 0 1095.41 1045.83 15.57 o 4 4 0 3047.03 3098.02 43.53 o 6 4 0 2759.44 3012.83 42.96 o 8 4 0 918.04 922.36 15.32 o 10 4 0 184.52 203.23 5.98 o 12 4 0 0.80 0.82 1.42 o 14 4 0 2.86 3.99 2.37 o 16 4 0 0.02 6.17 3.34 o 18 4 0 5.25 14.78 4.08 o 1 5 0 0.66 10.06 1.90 o 3 5 0 6.47 18.99 1.28 o 5 5 0 519.68 636.82 10.80 o 7 5 0 71.73 105.57 3.45 o 9 5 0 88.77 84.93 3.59 o 11 5 0 116.45 105.06 4.91 o 13 5 0 26.36 30.13 3.56 o 15 5 0 67.95 72.16 6.62 o 17 5 0 18.33 17.97 4.32 o 0 6 0 1974.11 1900.81 39.18 o 2 6 0 159.36 109.05 2.95 o 4 6 0 1002.81 953.52 15.46 o 6 6 0 1041.61 1026.62 19.25 o 8 6 0 1075.32 1029.69 17.16 o 10 6 0 364.70 373.50 9.12 o 12 6 0 492.70 453.81 15.48 o 14 6 0 104.01 128.58 9.04 o 16 6 0 66.78 93.03 9.32 o 1 7 0 709.28 845.80 18.07 o 3 7 0 479.13 521.33 9.44 o 5 7 0 597.42 590.68 10.74 o 7 7 0 1023.64 1007.42 18.37 o 9 7 0 43.11 45.21 3.22 o 11 7 0 101.69 104.88 6.63 o 13 7 0 111.51 83.06 7.24 o 15 7 0 32.51 50.31 5.45 o 0 8 0 713.06 1000.55 33.90 o 2 8 0 36.46 28.82 1.85 o 4 8 0 3.54 6.61 1.29 o 6 8 0 5299.55 5176.17 78.65 o 8 8 0 146.96 139.74 5.31 o 10 8 0 298.19 310.04 10.40 o 12 8 0 2.20 11.77 2.96 o 14 8 0 26.21 45.58 5.26 o 16 8 0 5.56 6.49 2.93 o 1 9 0 61.07 73.57 3.60 o 3 9 0 172.22 167.92 5.22 o 5 9 0 0.91 1.40 1.20 o 7 9 0 165.10 185.06 6.10 o 9 9 0 322.07 301.95 9.24 o 11 9 0 111.16 113.15 7.17 o 13 9 0 102.82 100.36 8.14 o 15 9 0 40.10 67.76 6.71 o 0 10 0 49.64 55.71 5.49 o 2 10 0 34.97 37.29 2.80 o 4 10 0 34.92 45.20 3.26 o 6 10 0 2893.62 2801.55 45.45 o 8 10 0 159.11 158.04 6.21 o 10 10 0 9.51 9.64 2.19 o 12 10 0 0.54 2.44 2.09 o 14 10 0 9.49 24.77 4.01 o 1 11 0 59.22 67.98 4.58 o 3 11 0 392.11 362.14 10.03 o 5 11 0 869.82 876.49 17.43 o 7 11 0 1070.46 978.83 19.33 o 9 11 0 193.23 192.74 8.71 o 11 11 0 15.83 16.46 3.30 o 13 11 0 35.18 34.67 5.55 o 0 12 0 204.50 208.81 10.32 o 2 12 0 264.69 282.98 10.31 o 4 12 0 404.00 400.55 13.81 o 6 12 0 6.97 17.58 3.20 o 8 12 0 211.07 198.12 8.37 o 10 12 0 34.27 48.27 6.02 o 12 12 0 68.66 95.71 10.29 o 1 13 0 26.84 29.58 3.95 o 3 13 0 30.61 36.42 4.52 o 5 13 0 29.67 28.03 3.99 o 7 13 0 2.92 2.06 2.43 o 9 13 0 9.88 23.76 4.68 o 11 13 0 0.01 7.08 3.37 o 0 14 0 515.73 472.21 23.40 o 2 14 0 238.63 239.80 10.72 o 4 14 0 211.13 225.01 10.43 o 6 14 0 368.56 370.16 18.46 o 8 14 0 94.56 109.63 13.88 o 10 14 0 30.29 38.24 17.08 o 1 15 0 67.10 92.30 7.79 o 3 15 0 118.66 119.56 8.81 o 5 15 0 5.32 7.97 2.76 o 7 15 0 5.02 3.48 4.34 o 0 16 0 2.96 0.00 3.78 o 2 16 0 4.26 8.88 2.71 o 4 16 0 1.45 1.60 4.08 o -17 1 1 9.51 11.71 3.01 o -15 1 1 204.61 188.92 7.66 o -13 1 1 22.67 36.60 3.61 o -11 1 1 35.93 38.58 3.30 o -9 1 1 33.68 28.28 1.93 o -7 1 1 229.47 212.30 5.01 o -5 1 1 12.23 7.02 0.71 o -3 1 1 12419.72 12728.28 171.75 o -1 1 1 2785.86 2976.93 40.82 o 1 1 1 4704.16 5216.55 71.20 o 3 1 1 3840.48 4017.60 55.57 o 5 1 1 1208.79 1131.33 17.12 o 7 1 1 602.76 512.86 9.30 o 9 1 1 1833.19 1756.97 29.66 o 11 1 1 236.97 214.96 9.10 o 13 1 1 190.05 169.72 9.67 o 15 1 1 206.59 194.39 11.02 o 17 1 1 37.55 49.45 5.60 o -18 2 1 2.02 5.92 2.58 o -16 2 1 9.08 15.65 2.42 o -14 2 1 148.88 146.14 7.28 o -12 2 1 675.12 695.42 15.95 o -10 2 1 0.36 1.76 1.13 o -8 2 1 331.15 294.46 11.41 o -6 2 1 367.27 499.71 9.99 o -4 2 1 2012.05 2133.20 32.08 o -2 2 1 9349.37 9598.75 129.93 o 0 2 1 23753.91 23947.18 345.08 o 2 2 1 2103.98 2319.99 32.48 o 4 2 1 8306.84 8769.11 119.30 o 6 2 1 12.40 1.93 0.81 o 8 2 1 2336.07 2315.16 34.15 o 10 2 1 1554.84 1512.63 25.73 o 12 2 1 1076.44 973.21 23.04 o 14 2 1 134.74 132.06 8.85 o 16 2 1 183.99 187.42 11.40 o -17 3 1 58.95 59.16 6.19 o -15 3 1 42.39 48.25 4.58 o -13 3 1 44.16 41.29 3.69 o -11 3 1 170.30 159.27 5.97 o -9 3 1 1.57 1.76 0.85 o -7 3 1 6995.99 7943.37 125.30 o -5 3 1 51.11 45.64 1.84 o -3 3 1 0.03 2.39 0.36 o -1 3 1 455.35 548.92 10.84 o 1 3 1 485.41 505.21 8.08 o 3 3 1 1465.05 1444.14 22.53 o 5 3 1 11131.69 12326.47 167.34 o 7 3 1 1266.87 1554.36 32.19 o 9 3 1 449.47 473.22 10.55 o 11 3 1 4.62 4.64 1.37 o 13 3 1 1.93 4.69 1.89 o 15 3 1 13.99 19.57 3.04 o 17 3 1 23.49 45.73 5.15 o -18 4 1 207.77 251.35 12.83 o -16 4 1 135.32 127.96 9.55 o -14 4 1 311.92 325.55 11.82 o -12 4 1 1045.33 986.14 20.84 o -10 4 1 826.10 856.15 16.21 o -8 4 1 312.99 317.60 6.69 o -6 4 1 7964.41 8639.06 118.40 o -4 4 1 1026.97 943.61 14.59 o -2 4 1 1804.27 1678.84 26.09 o 0 4 1 16199.36 17306.87 233.42 o 2 4 1 951.79 842.79 14.96 o 4 4 1 3.56 2.24 0.55 o 6 4 1 8549.91 9472.80 129.83 o 8 4 1 103.12 89.61 3.50 o 10 4 1 293.98 289.50 8.71 o 12 4 1 1150.37 1060.72 24.44 o 14 4 1 34.79 21.87 3.57 o 16 4 1 18.40 15.02 3.11 o -17 5 1 20.84 30.82 4.40 o -15 5 1 82.62 92.62 7.58 o -13 5 1 419.52 337.30 11.36 o -11 5 1 195.37 199.38 6.83 o -9 5 1 679.35 700.41 13.72 o -7 5 1 249.87 304.93 6.43 o -5 5 1 831.85 807.58 13.11 o -3 5 1 108.11 86.34 2.82 o -1 5 1 5820.79 6789.39 92.95 o 1 5 1 428.76 351.59 6.41 o 3 5 1 981.43 914.23 14.46 o 5 5 1 94.63 72.14 2.91 o 7 5 1 1194.89 1146.70 18.50 o 9 5 1 276.15 263.82 7.06 o 11 5 1 6.80 8.82 1.77 o 13 5 1 2.96 5.02 2.04 o 15 5 1 29.98 30.22 6.62 o 17 5 1 1.76 3.62 4.81 o -16 6 1 1.03 5.72 2.53 o -14 6 1 49.79 61.09 6.10 o -12 6 1 13.78 10.97 2.35 o -10 6 1 35.31 32.72 3.03 o -8 6 1 48.11 48.58 3.07 o -6 6 1 189.70 226.81 7.91 o -4 6 1 41.85 42.22 2.53 o -2 6 1 973.06 971.11 17.50 o 0 6 1 3590.65 4290.97 59.88 o 2 6 1 34.25 34.33 2.02 o 4 6 1 345.85 351.09 7.02 o 6 6 1 1306.87 1368.07 21.50 o 8 6 1 35.50 42.93 3.04 o 10 6 1 28.48 30.26 2.96 o 12 6 1 624.67 563.70 15.69 o 14 6 1 22.52 15.41 6.55 o 16 6 1 2.40 13.35 4.78 o -17 7 1 53.70 55.67 7.71 o -15 7 1 61.04 85.40 7.72 o -13 7 1 976.43 855.88 31.90 o -11 7 1 294.66 310.95 10.66 o -9 7 1 1459.89 1396.36 57.42 o -7 7 1 1064.41 1058.83 22.31 o -5 7 1 353.45 335.69 7.81 o -3 7 1 419.46 357.59 7.92 o -1 7 1 1579.80 1731.30 25.90 o 1 7 1 4.67 12.71 2.25 o 3 7 1 1017.27 947.28 16.38 o 5 7 1 180.50 164.56 4.75 o 7 7 1 184.09 188.46 5.17 o 9 7 1 344.42 334.45 8.53 o 11 7 1 178.17 180.80 7.99 o 13 7 1 43.69 41.01 4.91 o 15 7 1 80.55 83.99 8.72 o -16 8 1 7.87 20.88 3.88 o -14 8 1 63.61 90.33 7.65 o -12 8 1 18.79 28.89 3.44 o -10 8 1 121.07 136.44 6.59 o -8 8 1 459.28 438.46 15.17 o -6 8 1 948.67 934.20 17.41 o -4 8 1 19.33 23.14 2.11 o -2 8 1 146.06 148.22 4.59 o 0 8 1 163.10 191.73 4.73 o 2 8 1 133.34 140.14 4.01 o 4 8 1 725.40 707.36 15.03 o 6 8 1 366.94 368.26 8.07 o 8 8 1 6.46 5.08 1.70 o 10 8 1 73.05 64.36 5.26 o 12 8 1 29.50 31.94 3.77 o 14 8 1 44.56 51.63 5.66 o -15 9 1 0.53 3.88 2.58 o -13 9 1 2.22 0.95 2.20 o -11 9 1 125.37 107.49 6.31 o -9 9 1 74.07 67.12 4.92 o -7 9 1 2.98 4.15 1.37 o -5 9 1 95.05 98.92 4.55 o -3 9 1 0.05 2.04 0.96 o -1 9 1 0.68 -0.32 1.26 o 1 9 1 60.74 61.70 3.19 o 3 9 1 1.05 3.30 1.01 o 5 9 1 3.48 4.98 1.41 o 7 9 1 11.79 15.02 2.43 o 9 9 1 33.81 48.01 3.91 o 11 9 1 7.17 19.15 3.54 o 13 9 1 3.68 2.63 3.05 o 15 9 1 4.49 14.89 4.60 o -14 10 1 50.00 63.32 6.28 o -12 10 1 134.82 141.26 9.60 o -10 10 1 336.77 325.16 10.11 o -8 10 1 1293.24 1220.28 27.53 o -6 10 1 2698.93 2629.79 46.50 o -4 10 1 506.39 502.64 11.29 o -2 10 1 199.95 210.43 6.11 o 0 10 1 157.50 164.87 5.98 o 2 10 1 492.89 473.84 12.97 o 4 10 1 768.09 748.95 16.53 o 6 10 1 2287.99 2201.46 43.85 o 8 10 1 163.04 161.83 7.74 o 10 10 1 71.63 85.91 7.17 o 12 10 1 20.91 22.08 3.94 o 14 10 1 41.71 76.43 8.48 o -13 11 1 142.02 195.65 11.21 o -11 11 1 7.82 12.66 3.43 o -9 11 1 129.81 147.99 7.43 o -7 11 1 184.40 170.31 7.60 o -5 11 1 30.04 35.80 3.54 o -3 11 1 157.12 176.02 6.57 o -1 11 1 264.22 239.78 8.71 o 1 11 1 121.11 125.93 6.59 o 3 11 1 159.42 171.73 7.35 o 5 11 1 298.53 271.77 9.63 o 7 11 1 78.59 87.38 6.05 o 9 11 1 5.93 3.95 2.21 o 11 11 1 20.40 36.20 4.71 o 13 11 1 54.76 85.32 8.93 o -12 12 1 38.81 47.48 6.20 o -10 12 1 6.33 2.93 2.21 o -8 12 1 27.79 33.67 3.79 o -6 12 1 21.12 21.04 4.29 o -4 12 1 49.51 44.59 4.44 o -2 12 1 3.32 2.26 1.66 o 0 12 1 242.76 195.47 8.04 o 2 12 1 27.10 27.06 3.43 o 4 12 1 67.29 69.74 5.60 o 6 12 1 2.57 5.07 2.14 o 8 12 1 80.62 76.94 6.76 o 10 12 1 1.19 6.47 2.80 o 12 12 1 96.75 158.40 10.60 o -11 13 1 61.60 55.77 8.24 o -9 13 1 120.18 132.87 8.19 o -7 13 1 129.82 112.54 7.25 o -5 13 1 343.54 332.90 11.48 o -3 13 1 415.49 387.10 12.49 o -1 13 1 0.24 9.38 2.22 o 1 13 1 210.63 219.93 8.78 o 3 13 1 346.56 372.10 12.20 o 5 13 1 188.22 184.87 10.17 o 7 13 1 85.45 86.35 7.71 o 9 13 1 91.20 110.28 10.15 o 11 13 1 0.07 13.18 6.76 o -10 14 1 12.50 22.96 6.04 o -8 14 1 42.67 57.89 6.88 o -6 14 1 286.26 304.80 12.59 o -4 14 1 63.43 59.49 6.05 o -2 14 1 172.65 184.07 9.03 o 0 14 1 776.36 616.44 18.18 o 2 14 1 31.90 39.41 4.06 o 4 14 1 26.40 39.66 4.74 o 6 14 1 239.14 294.03 12.39 o 8 14 1 2.82 4.81 2.57 o -7 15 1 242.36 235.16 13.52 o -5 15 1 44.55 37.36 4.67 o -3 15 1 16.08 18.59 4.19 o -1 15 1 157.24 118.34 9.63 o 1 15 1 46.34 45.29 5.29 o 3 15 1 40.79 38.36 5.65 o 5 15 1 240.72 237.18 13.62 o 7 15 1 33.47 36.19 5.68 o -4 16 1 112.97 116.51 9.16 o -2 16 1 165.05 164.26 10.92 o 0 16 1 112.66 144.25 11.56 o 2 16 1 111.44 108.98 10.36 o 4 16 1 99.17 95.82 9.57 o -18 0 2 32.77 30.00 5.81 o -16 0 2 91.23 98.47 9.41 o -14 0 2 2074.61 2076.46 55.55 o -12 0 2 1120.42 1151.97 33.47 o -10 0 2 36.89 38.89 4.68 o -8 0 2 62.25 79.26 5.71 o -6 0 2 2.20 3.01 0.65 o -4 0 2 3785.81 3550.53 72.13 o -2 0 2 19828.59 21046.96 401.34 o 0 0 2 42496.50 42484.03 806.97 o 2 0 2 572.96 493.12 11.59 o 4 0 2 86.40 76.97 3.17 o 6 0 2 720.19 672.11 16.22 o 8 0 2 1800.73 1675.94 71.85 o 10 0 2 1407.70 1268.78 34.68 o 12 0 2 4983.43 4603.37 134.40 o 14 0 2 62.64 63.34 9.20 o 16 0 2 91.75 90.25 11.21 o -17 1 2 3.52 5.91 2.62 o -15 1 2 166.68 177.88 8.14 o -13 1 2 2495.43 2503.61 45.54 o -11 1 2 140.57 143.38 5.93 o -9 1 2 11.66 16.14 1.96 o -7 1 2 67.41 62.68 2.65 o -5 1 2 54.08 67.57 2.12 o -3 1 2 2588.36 2685.01 37.74 o -1 1 2 51834.11 51452.31 690.82 o 1 1 2 3005.29 3178.18 44.21 o 3 1 2 8.84 10.17 1.99 o 5 1 2 187.82 208.52 4.59 o 7 1 2 494.97 491.54 9.22 o 9 1 2 601.48 570.55 21.36 o 11 1 2 1354.09 1272.00 24.96 o 13 1 2 186.34 177.61 9.74 o 15 1 2 1.13 4.69 3.78 o 17 1 2 57.07 54.16 6.38 o -18 2 2 108.58 127.47 10.33 o -16 2 2 54.49 51.82 4.73 o -14 2 2 6.18 9.64 2.23 o -12 2 2 68.50 73.57 4.94 o -10 2 2 42.71 62.13 4.10 o -8 2 2 162.63 174.78 5.52 o -6 2 2 1537.10 1616.59 23.92 o -4 2 2 249.44 228.89 4.91 o -2 2 2 2482.36 2346.97 33.12 o 0 2 2 1.13 7.69 1.08 o 2 2 2 160.88 163.43 3.98 o 4 2 2 219.91 193.29 8.06 o 6 2 2 250.40 269.03 6.47 o 8 2 2 10.57 17.89 1.86 o 10 2 2 273.06 225.72 7.68 o 12 2 2 213.99 253.01 10.52 o 14 2 2 42.07 30.30 4.23 o 16 2 2 38.34 42.89 4.94 o -17 3 2 107.83 112.33 9.06 o -15 3 2 100.59 111.99 7.58 o -13 3 2 780.04 753.57 17.50 o -11 3 2 110.36 115.96 5.59 o -9 3 2 315.87 306.10 11.53 o -7 3 2 3.63 21.17 1.49 o -5 3 2 317.97 280.07 5.95 o -3 3 2 1070.91 868.42 14.38 o -1 3 2 4895.86 4777.07 76.57 o 1 3 2 103.87 81.07 2.93 o 3 3 2 825.41 810.13 13.98 o 5 3 2 69.79 44.84 2.86 o 7 3 2 663.05 664.63 12.88 o 9 3 2 614.57 616.43 17.78 o 11 3 2 817.73 748.47 18.59 o 13 3 2 88.36 84.81 6.98 o 15 3 2 167.34 140.32 9.80 o -18 4 2 19.65 25.22 3.99 o -16 4 2 2.47 5.41 1.98 o -14 4 2 15.36 21.29 3.07 o -12 4 2 26.85 30.64 3.18 o -10 4 2 1.79 2.85 1.31 o -8 4 2 167.42 174.49 6.19 o -6 4 2 1.82 2.27 0.63 o -4 4 2 1080.46 1216.41 18.57 o -2 4 2 707.61 866.76 13.52 o 0 4 2 73.22 114.90 3.64 o 2 4 2 3.45 3.58 0.68 o 4 4 2 1260.54 1250.92 19.24 o 6 4 2 728.40 753.41 14.08 o 8 4 2 70.86 86.98 4.20 o 10 4 2 143.23 157.56 5.59 o 12 4 2 10.92 19.20 2.66 o 14 4 2 28.40 32.73 4.58 o 16 4 2 63.17 55.09 5.53 o -17 5 2 40.45 41.86 5.56 o -15 5 2 123.69 116.12 7.91 o -13 5 2 112.78 134.81 7.91 o -11 5 2 333.84 324.20 11.25 o -9 5 2 246.65 219.72 6.84 o -7 5 2 180.45 174.95 4.47 o -5 5 2 1051.04 979.05 15.60 o -3 5 2 2031.01 1946.00 28.40 o -1 5 2 581.41 505.52 9.67 o 1 5 2 369.02 337.36 7.24 o 3 5 2 30.82 22.70 1.47 o 5 5 2 15.25 26.18 2.18 o 7 5 2 25.15 25.75 2.37 o 9 5 2 82.51 91.21 4.69 o 11 5 2 0.12 3.30 1.47 o 13 5 2 0.72 6.50 2.26 o 15 5 2 0.49 1.11 2.21 o -16 6 2 38.72 40.16 4.20 o -14 6 2 470.00 417.35 13.69 o -12 6 2 834.27 803.44 20.46 o -10 6 2 747.05 705.95 28.66 o -8 6 2 1241.98 1215.58 23.55 o -6 6 2 1683.45 1685.93 27.84 o -4 6 2 267.93 210.51 5.51 o -2 6 2 1147.31 1107.72 17.18 o 0 6 2 1892.24 1858.19 29.68 o 2 6 2 458.16 381.85 7.37 o 4 6 2 1598.86 1625.08 24.90 o 6 6 2 686.30 680.76 16.40 o 8 6 2 201.68 205.33 6.29 o 10 6 2 252.93 268.27 7.66 o 12 6 2 253.57 239.97 9.09 o 14 6 2 7.85 10.91 4.81 o -17 7 2 0.03 5.75 3.07 o -15 7 2 3.12 9.34 4.03 o -13 7 2 90.01 87.51 6.57 o -11 7 2 19.54 28.48 3.49 o -9 7 2 44.48 41.76 3.55 o -7 7 2 1416.63 1378.50 23.97 o -5 7 2 66.92 77.84 3.64 o -3 7 2 31.94 38.72 2.49 o -1 7 2 1839.15 2130.09 35.05 o 1 7 2 10.62 6.62 1.08 o 3 7 2 63.49 62.93 2.67 o 5 7 2 1273.24 1215.96 26.92 o 7 7 2 0.01 3.19 1.25 o 9 7 2 4.17 6.77 1.67 o 11 7 2 93.69 68.02 5.48 o 13 7 2 0.09 6.94 3.57 o 15 7 2 7.18 15.07 5.00 o -16 8 2 44.43 35.46 4.55 o -14 8 2 6.71 19.94 2.99 o -12 8 2 70.70 83.90 6.27 o -10 8 2 403.70 384.24 11.98 o -8 8 2 2022.76 1990.53 36.52 o -6 8 2 1962.91 2059.68 33.99 o -4 8 2 471.22 451.34 15.53 o -2 8 2 56.03 47.44 3.49 o 0 8 2 4.98 3.76 1.09 o 2 8 2 643.45 658.49 12.99 o 4 8 2 867.44 836.46 17.35 o 6 8 2 2707.03 2700.20 47.15 o 8 8 2 65.48 82.94 5.16 o 10 8 2 2.03 11.02 2.25 o 12 8 2 19.56 12.41 2.60 o 14 8 2 25.70 15.48 6.94 o -15 9 2 57.57 67.36 6.64 o -13 9 2 192.01 172.73 8.88 o -11 9 2 207.59 198.54 8.57 o -9 9 2 1292.47 1231.61 36.05 o -7 9 2 797.31 815.68 19.55 o -5 9 2 1159.85 1140.28 22.74 o -3 9 2 202.82 198.39 6.59 o -1 9 2 558.75 574.11 13.25 o 1 9 2 485.67 488.59 12.76 o 3 9 2 1394.20 1396.39 24.36 o 5 9 2 1218.02 1215.40 24.07 o 7 9 2 269.38 264.37 9.40 o 9 9 2 3.85 3.27 2.50 o 11 9 2 55.98 57.44 5.86 o 13 9 2 37.78 50.61 6.65 o -14 10 2 13.06 21.12 4.49 o -12 10 2 2.10 4.69 2.29 o -10 10 2 10.88 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