#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/59/2215938.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215938_Fobs loop_ _publ_author_name 'Han, Jia-Jun' 'Li, Ning' _publ_section_title ; (2-Amino-3,5-dimethylbenzenesulfonato-\kN)bis(triphenylphosphine-\kP)silver(I) acetonitrile solvate ; _journal_coeditor_code HB2567 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2650 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.325 _cell_angle_gamma 90.000 _cell_length_a 13.7825 _cell_length_b 12.2524 _cell_length_c 25.2425 _exptl_crystal_F_000 1800.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file hb2567Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21N in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 317.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 24558.93 25741.17 694.72 o 6 0 0 19593.07 19528.25 522.20 o 8 0 0 11130.93 10882.15 323.50 o 10 0 0 5911.70 6195.42 176.11 o 12 0 0 115.23 115.74 39.67 o 14 0 0 1407.53 1449.19 126.07 o 16 0 0 2046.69 2075.87 193.47 o 2 1 0 5550.82 5105.66 74.56 o 3 1 0 8484.00 8565.83 110.09 o 4 1 0 93.79 115.13 8.19 o 5 1 0 3884.68 3778.67 51.36 o 6 1 0 3136.40 3136.54 50.58 o 7 1 0 5092.27 5317.66 97.37 o 8 1 0 1113.65 1175.33 32.40 o 9 1 0 408.28 466.28 39.87 o 10 1 0 1340.12 1378.90 47.02 o 11 1 0 3490.70 3343.95 99.81 o 12 1 0 1027.67 1162.21 110.49 o 13 1 0 16.04 33.19 19.78 o 14 1 0 66.75 95.83 31.36 o 15 1 0 13.93 8.81 33.37 o 16 1 0 135.10 150.20 49.24 o 17 1 0 146.36 188.61 42.02 o 0 2 0 129.94 168.81 72.81 o 1 2 0 6305.46 6380.39 112.52 o 2 2 0 6521.05 6496.05 77.54 o 3 2 0 1595.29 1498.08 23.05 o 4 2 0 1731.17 1802.46 31.25 o 5 2 0 10960.24 10446.39 189.68 o 6 2 0 4531.46 5073.85 78.82 o 7 2 0 51395.04 51950.13 1503.73 o 8 2 0 1.98 -7.66 17.89 o 9 2 0 13646.07 13145.49 283.00 o 10 2 0 20.78 27.33 20.48 o 11 2 0 188.51 189.89 23.94 o 12 2 0 255.26 251.89 26.04 o 13 2 0 1241.43 1276.31 50.19 o 14 2 0 95.96 119.78 28.90 o 15 2 0 2996.98 3104.13 121.13 o 16 2 0 46.81 50.68 41.81 o 17 2 0 1195.01 1158.94 68.35 o 1 3 0 26649.72 27065.67 478.69 o 2 3 0 6803.06 6954.23 104.65 o 3 3 0 11526.20 10784.06 190.88 o 4 3 0 7468.64 7651.48 121.49 o 5 3 0 7740.30 7336.36 119.05 o 6 3 0 4886.95 4836.94 92.77 o 7 3 0 1545.34 1656.80 48.82 o 8 3 0 2038.74 2009.24 42.50 o 9 3 0 2783.00 2842.97 60.56 o 10 3 0 256.36 228.12 22.55 o 11 3 0 109.32 97.56 17.63 o 12 3 0 1.72 -5.92 16.13 o 13 3 0 332.81 311.24 30.97 o 14 3 0 108.93 98.15 25.47 o 15 3 0 10.00 30.65 31.16 o 16 3 0 68.43 74.61 39.98 o 17 3 0 198.44 203.19 59.43 o 0 4 0 78901.17 78344.61 3394.58 o 1 4 0 700.36 587.65 9.46 o 2 4 0 7091.41 7428.56 98.68 o 3 4 0 3213.83 3499.10 41.19 o 4 4 0 362.92 404.71 21.69 o 5 4 0 31.41 43.22 10.33 o 6 4 0 11257.17 10500.16 187.94 o 7 4 0 361.06 340.82 24.87 o 8 4 0 5578.61 5586.30 108.20 o 9 4 0 35.33 48.09 14.38 o 10 4 0 2755.35 2602.27 81.82 o 11 4 0 80.93 55.04 18.11 o 12 4 0 652.23 657.87 35.71 o 13 4 0 84.30 75.05 24.56 o 14 4 0 897.87 891.03 66.71 o 15 4 0 1.55 10.23 39.18 o 16 4 0 1760.25 1940.45 92.23 o 17 4 0 176.96 147.61 54.73 o 1 5 0 4354.18 4718.78 123.92 o 2 5 0 6613.44 6637.00 121.02 o 3 5 0 400.07 496.93 21.51 o 4 5 0 11174.52 10627.87 169.90 o 5 5 0 618.07 590.51 30.62 o 6 5 0 1746.56 1765.24 46.04 o 7 5 0 5218.67 5427.13 104.83 o 8 5 0 95.53 84.36 13.46 o 9 5 0 151.80 163.22 19.24 o 10 5 0 3450.65 3565.35 97.70 o 11 5 0 1329.22 1384.46 63.72 o 12 5 0 2540.49 2532.35 76.34 o 13 5 0 3.37 36.31 23.55 o 14 5 0 675.30 818.56 54.84 o 15 5 0 55.31 97.90 27.42 o 16 5 0 143.41 197.87 48.30 o 0 6 0 2423.05 2866.22 81.51 o 1 6 0 7687.17 7874.03 116.22 o 2 6 0 518.28 440.26 45.23 o 3 6 0 1157.75 1319.75 39.74 o 4 6 0 4235.64 4124.57 166.32 o 5 6 0 397.42 336.21 23.79 o 6 6 0 3.99 1.87 8.80 o 7 6 0 7325.46 7069.39 165.28 o 8 6 0 221.76 206.38 26.02 o 9 6 0 3543.89 3452.45 91.22 o 10 6 0 147.99 166.46 23.05 o 11 6 0 0.29 21.53 17.89 o 12 6 0 0.98 12.27 24.22 o 13 6 0 121.15 198.43 27.72 o 14 6 0 58.27 76.53 26.95 o 15 6 0 479.77 559.73 53.40 o 16 6 0 97.34 92.65 30.68 o 1 7 0 3082.49 3242.46 45.63 o 2 7 0 3678.55 3465.36 64.02 o 3 7 0 9656.73 9610.66 193.94 o 4 7 0 321.72 319.41 18.05 o 5 7 0 8906.15 8801.58 153.12 o 6 7 0 22.73 12.71 10.44 o 7 7 0 3115.30 3156.28 65.95 o 8 7 0 258.65 233.55 19.72 o 9 7 0 1365.02 1415.16 80.99 o 10 7 0 467.14 394.87 39.75 o 11 7 0 480.20 437.73 41.15 o 12 7 0 795.00 714.83 54.08 o 13 7 0 739.20 776.47 65.36 o 14 7 0 26.69 33.08 28.82 o 15 7 0 152.01 166.35 37.38 o 16 7 0 38.41 43.38 92.78 o 0 8 0 7328.20 7857.41 141.84 o 1 8 0 233.89 223.36 39.63 o 2 8 0 50.48 80.68 12.01 o 3 8 0 320.98 377.64 26.05 o 4 8 0 817.35 808.21 30.29 o 5 8 0 0.32 -3.05 12.92 o 6 8 0 5539.46 5420.42 93.46 o 7 8 0 1018.06 1020.16 57.08 o 8 8 0 123.53 163.57 18.69 o 9 8 0 20.83 31.02 14.81 o 10 8 0 56.20 55.57 17.46 o 11 8 0 9.74 4.40 25.09 o 12 8 0 387.93 330.66 107.55 o 13 8 0 4.40 -11.54 17.88 o 14 8 0 519.15 534.55 52.04 o 15 8 0 30.08 -8.75 24.65 o 1 9 0 860.78 845.50 63.43 o 2 9 0 2303.91 2447.76 71.22 o 3 9 0 1181.48 1125.49 46.03 o 4 9 0 947.77 986.12 43.64 o 5 9 0 8263.37 8166.97 183.98 o 6 9 0 729.76 696.60 32.09 o 7 9 0 0.44 -1.66 12.47 o 8 9 0 438.78 413.58 25.49 o 9 9 0 162.20 189.05 30.56 o 10 9 0 1824.28 1885.18 76.49 o 11 9 0 669.54 742.47 47.00 o 12 9 0 1676.23 1611.08 66.75 o 13 9 0 21.73 46.48 32.48 o 14 9 0 305.03 239.25 64.89 o 0 10 0 523.29 489.41 20.09 o 1 10 0 3746.86 3680.06 86.17 o 2 10 0 2122.30 2102.66 62.48 o 3 10 0 1295.53 1369.31 101.44 o 4 10 0 2.26 -4.59 14.68 o 5 10 0 91.55 56.08 21.48 o 6 10 0 333.65 401.95 60.77 o 7 10 0 329.02 304.79 29.23 o 8 10 0 1002.22 1045.13 54.30 o 9 10 0 544.29 533.99 28.36 o 10 10 0 120.94 105.93 38.25 o 11 10 0 44.13 61.46 31.12 o 12 10 0 208.43 116.38 91.14 o 13 10 0 41.58 35.11 43.38 o 1 11 0 6.84 -0.76 13.03 o 2 11 0 331.67 306.95 51.05 o 3 11 0 2771.87 2930.39 98.35 o 4 11 0 537.10 528.90 51.86 o 5 11 0 280.81 293.75 29.30 o 6 11 0 1.16 -1.68 16.91 o 7 11 0 458.44 484.29 45.51 o 8 11 0 170.36 155.05 48.75 o 9 11 0 1072.01 1084.92 52.41 o 10 11 0 907.15 939.93 59.56 o 11 11 0 149.18 111.80 48.42 o 12 11 0 734.50 718.75 80.01 o 0 12 0 17.04 36.32 48.71 o 1 12 0 56.76 70.97 16.38 o 2 12 0 0.97 13.17 13.48 o 3 12 0 37.84 32.80 37.30 o 4 12 0 273.14 294.47 36.52 o 5 12 0 218.94 309.44 33.98 o 6 12 0 552.51 667.66 45.49 o 7 12 0 418.60 557.90 57.92 o 8 12 0 312.21 366.95 38.21 o 9 12 0 301.38 373.48 42.51 o 10 12 0 82.52 21.77 31.15 o 11 12 0 5.92 14.60 29.79 o 1 13 0 655.80 589.00 26.61 o 2 13 0 543.02 550.74 44.25 o 3 13 0 560.06 597.11 44.66 o 4 13 0 656.78 679.61 45.51 o 5 13 0 957.91 962.93 64.83 o 6 13 0 302.65 355.00 32.15 o 7 13 0 33.43 58.10 30.50 o 8 13 0 0.11 17.69 21.59 o 9 13 0 3.20 20.18 30.53 o 10 13 0 232.49 230.44 42.12 o 1 14 0 188.55 326.35 62.83 o 2 14 0 698.06 839.32 63.65 o 3 14 0 91.76 104.06 28.61 o 4 14 0 1.03 30.30 25.49 o 5 14 0 103.71 114.62 27.41 o 6 14 0 89.05 87.04 31.96 o 7 14 0 460.95 633.82 48.46 o 8 14 0 553.04 648.11 65.80 o 1 15 0 3.76 65.24 46.65 o 2 15 0 19.70 -11.88 64.20 o 3 15 0 184.08 261.43 39.74 o 4 15 0 29.61 22.56 24.18 o 5 15 0 2.26 31.91 29.21 o -17 0 1 47.62 75.90 50.58 o -15 0 1 586.41 731.42 100.27 o -13 0 1 216.95 154.09 32.25 o -11 0 1 640.33 676.87 135.46 o -9 0 1 2306.47 2264.37 80.42 o -7 0 1 12644.58 12379.86 310.46 o -5 0 1 250.14 346.99 15.09 o -3 0 1 76506.27 78488.15 3403.05 o 3 0 1 3238.40 3371.72 115.50 o 5 0 1 314.36 323.34 60.59 o 7 0 1 30409.49 29727.10 981.00 o 9 0 1 4972.30 4960.30 222.64 o 11 0 1 45.30 9.82 63.43 o 13 0 1 1401.19 1465.44 75.94 o 15 0 1 1523.12 1539.83 112.53 o 17 0 1 668.79 587.13 84.40 o -17 1 1 581.01 626.07 63.54 o -16 1 1 1420.36 1487.64 78.55 o -15 1 1 180.76 240.56 37.78 o -14 1 1 477.65 473.52 47.59 o -13 1 1 2.20 -3.52 15.23 o -12 1 1 2144.86 2087.83 91.33 o -11 1 1 2111.21 2010.04 72.71 o -10 1 1 7089.02 7162.21 160.71 o -9 1 1 2307.77 2194.56 55.67 o -8 1 1 10574.29 10170.53 190.72 o -7 1 1 3228.41 3382.28 64.76 o -6 1 1 5504.08 5398.35 91.75 o -5 1 1 18302.07 18144.04 337.84 o -4 1 1 2348.88 2369.84 34.68 o -3 1 1 100936.05 98468.12 3386.86 o -2 1 1 3975.57 3852.99 40.92 o 2 1 1 720.46 613.08 9.73 o 3 1 1 7023.76 6557.07 90.23 o 4 1 1 1557.75 1539.83 31.78 o 5 1 1 11201.47 10429.79 165.96 o 6 1 1 5851.08 5636.08 92.32 o 7 1 1 16755.92 16957.76 332.38 o 8 1 1 50.37 51.67 13.01 o 9 1 1 2783.24 2927.47 68.19 o 10 1 1 237.65 277.67 22.84 o 11 1 1 797.25 872.65 42.82 o 12 1 1 3247.86 3162.18 95.73 o 13 1 1 87.47 76.63 21.73 o 14 1 1 1394.99 1283.65 73.24 o 15 1 1 20.92 38.40 29.55 o 16 1 1 525.73 569.96 55.34 o 17 1 1 60.76 92.74 35.92 o -17 2 1 23.66 30.13 39.53 o -16 2 1 1224.70 1261.83 102.55 o -15 2 1 19.50 14.21 28.70 o -14 2 1 341.24 488.77 42.56 o -13 2 1 45.04 45.03 18.76 o -12 2 1 3314.68 3341.09 132.67 o -11 2 1 295.59 294.74 25.23 o -10 2 1 1568.62 1520.69 54.57 o -9 2 1 985.36 1139.90 38.63 o -8 2 1 3532.76 3671.47 80.09 o -7 2 1 76.50 51.28 12.20 o -6 2 1 23722.70 22499.00 467.97 o -5 2 1 476.41 612.46 17.99 o -4 2 1 1491.06 1552.41 28.28 o -3 2 1 4.67 20.13 5.91 o -2 2 1 132.63 203.77 7.49 o -1 2 1 15785.37 16042.79 216.25 o 0 2 1 54343.57 54163.67 1297.24 o 1 2 1 6590.59 6910.49 108.92 o 2 2 1 140.32 192.22 8.75 o 3 2 1 893.06 741.10 39.04 o 4 2 1 6192.22 6472.91 91.65 o 5 2 1 65.41 120.61 11.44 o 6 2 1 30547.42 30619.71 691.09 o 7 2 1 303.40 236.86 17.02 o 8 2 1 7432.10 7258.44 139.50 o 9 2 1 817.73 799.50 32.60 o 10 2 1 4177.81 4109.20 97.29 o 11 2 1 95.51 71.30 20.16 o 12 2 1 0.68 21.63 17.07 o 13 2 1 260.88 256.31 28.79 o 14 2 1 767.61 784.48 51.23 o 15 2 1 62.84 26.88 29.29 o 16 2 1 2396.13 2440.06 124.16 o 17 2 1 66.49 18.19 25.13 o -17 3 1 649.35 726.03 67.09 o -16 3 1 359.40 467.64 60.04 o -15 3 1 337.67 341.94 42.71 o -14 3 1 53.50 13.62 20.14 o -13 3 1 1593.77 1469.88 59.95 o -12 3 1 1037.82 984.78 49.24 o -11 3 1 987.97 1063.67 49.07 o -10 3 1 1727.86 1701.71 59.28 o -9 3 1 295.37 345.46 19.85 o -8 3 1 1813.41 1722.05 63.69 o -7 3 1 4940.00 4896.85 94.18 o -6 3 1 1017.13 957.48 25.94 o -5 3 1 15825.75 15810.61 284.00 o -4 3 1 6021.88 5721.27 81.95 o -3 3 1 6078.03 6163.13 186.50 o -2 3 1 954.76 768.38 11.77 o -1 3 1 9125.71 8796.49 124.60 o 0 3 1 65336.30 65511.87 1793.22 o 1 3 1 4548.12 4571.63 63.46 o 2 3 1 29461.76 30420.93 856.62 o 3 3 1 4935.35 5059.43 76.44 o 4 3 1 23097.73 22394.64 445.16 o 5 3 1 20820.46 20173.35 400.24 o 6 3 1 8680.37 8610.58 240.84 o 7 3 1 1682.53 1438.93 48.21 o 8 3 1 245.76 316.57 20.23 o 9 3 1 3098.07 2784.82 63.97 o 10 3 1 591.17 668.12 47.33 o 11 3 1 758.80 818.68 37.48 o 12 3 1 1657.98 1663.38 59.21 o 13 3 1 5.74 24.75 20.45 o 14 3 1 934.92 1026.83 76.37 o 15 3 1 449.54 350.42 49.07 o 16 3 1 26.39 -27.40 33.08 o 17 3 1 4.40 -13.72 28.59 o -17 4 1 145.97 172.12 57.50 o -16 4 1 507.30 681.66 71.90 o -15 4 1 703.84 834.85 74.01 o -14 4 1 0.95 -19.70 19.70 o -13 4 1 1354.52 1402.86 64.15 o -12 4 1 1.45 -5.55 15.01 o -11 4 1 57.83 36.41 16.95 o -10 4 1 1.20 15.27 20.52 o -9 4 1 2533.86 2458.35 97.36 o -8 4 1 5.88 19.45 11.50 o -7 4 1 6948.78 7001.66 133.68 o -6 4 1 120.54 177.41 13.14 o -5 4 1 4057.90 4150.22 70.65 o -4 4 1 0.36 -3.44 6.67 o -3 4 1 3445.03 3856.32 71.53 o -2 4 1 1725.25 1641.81 20.85 o -1 4 1 10435.73 11137.45 153.38 o 0 4 1 577.59 559.19 38.28 o 1 4 1 20907.72 20643.61 427.86 o 2 4 1 7551.19 6733.43 355.62 o 3 4 1 11696.24 11220.06 216.29 o 4 4 1 1934.62 1816.91 34.89 o 5 4 1 4815.93 4995.90 101.58 o 6 4 1 5062.30 5219.18 88.63 o 7 4 1 3586.76 3348.11 59.98 o 8 4 1 55.76 83.47 15.22 o 9 4 1 4794.69 4635.11 111.78 o 10 4 1 515.25 475.29 34.18 o 11 4 1 540.81 566.04 33.03 o 12 4 1 86.63 160.27 22.98 o 13 4 1 267.11 243.88 31.91 o 14 4 1 94.97 72.09 24.40 o 15 4 1 1197.53 1268.29 71.89 o 16 4 1 86.87 84.16 39.44 o 17 4 1 786.15 865.35 147.99 o -16 5 1 254.28 375.77 64.04 o -15 5 1 109.07 121.01 28.84 o -14 5 1 25.51 47.09 26.73 o -13 5 1 514.38 535.99 40.38 o -12 5 1 277.05 316.76 27.96 o -11 5 1 1650.88 1676.61 71.29 o -10 5 1 2253.30 2382.17 74.68 o -9 5 1 4802.37 4626.98 98.23 o -8 5 1 3447.16 3456.92 80.33 o -7 5 1 365.11 460.02 33.31 o -6 5 1 4775.29 5236.70 129.98 o -5 5 1 3191.74 2976.07 68.08 o -4 5 1 2006.31 2125.76 36.05 o -3 5 1 11551.03 11568.11 176.83 o -2 5 1 2967.72 3030.45 54.15 o -1 5 1 12756.18 14228.04 220.85 o 0 5 1 29912.40 32498.83 705.98 o 1 5 1 14628.37 15715.04 317.99 o 2 5 1 24.61 65.70 13.17 o 3 5 1 3502.33 3273.36 52.79 o 4 5 1 308.63 290.67 20.64 o 5 5 1 8996.14 8798.85 185.27 o 6 5 1 2265.70 2221.46 53.97 o 7 5 1 2371.24 2553.30 124.31 o 8 5 1 19.03 22.03 11.23 o 9 5 1 1543.38 1573.87 61.94 o 10 5 1 41.89 65.82 21.06 o 11 5 1 4465.81 4342.79 131.92 o 12 5 1 1108.23 1070.83 74.02 o 13 5 1 1289.95 1245.37 57.06 o 14 5 1 407.23 394.01 38.54 o 15 5 1 353.85 373.60 38.26 o 16 5 1 517.63 472.54 53.54 o -16 6 1 119.39 100.66 34.34 o -15 6 1 66.93 81.22 35.33 o -14 6 1 555.70 583.57 51.58 o -13 6 1 210.54 230.95 31.46 o -12 6 1 1553.54 1591.63 77.69 o -11 6 1 356.81 367.39 39.20 o -10 6 1 146.06 140.43 22.10 o -9 6 1 551.31 471.66 33.14 o -8 6 1 479.30 460.12 39.14 o -7 6 1 1291.85 1145.41 40.95 o -6 6 1 8274.40 8241.80 204.10 o -5 6 1 1321.71 1237.18 128.14 o -4 6 1 302.66 278.82 25.48 o -3 6 1 5784.30 6125.23 111.95 o -2 6 1 430.51 458.92 17.11 o -1 6 1 4141.50 4251.04 55.93 o 0 6 1 30749.30 33098.81 771.99 o 1 6 1 328.19 342.25 16.90 o 2 6 1 3856.87 3264.61 63.99 o 3 6 1 1581.38 1638.53 32.02 o 4 6 1 1835.11 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