#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:41:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181079 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/59/2215963.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215963_Fobs loop_ _publ_author_name 'Yin, Yan-Bing' 'Yu, Hai-Xia' _publ_section_title ; catena-Poly[[(4,7-diphenyl-1,10-phenanthroline)lead(II)]-\m-benzene-1,4-dicarboxylato] ; _journal_coeditor_code HB2600 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2803 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.355 _cell_angle_beta 101.142 _cell_angle_gamma 92.036 _cell_length_a 9.8547 _cell_length_b 10.0457 _cell_length_c 13.5394 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file hb2600Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Yin in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 248.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18386.42 18600.90 280.69 o 3 0 0 22909.85 23608.01 364.47 o 4 0 0 19474.84 19877.80 335.38 o 5 0 0 13735.27 14003.83 215.30 o 6 0 0 7627.91 7135.47 115.58 o 7 0 0 7552.22 7659.66 272.72 o 8 0 0 6264.48 6206.93 120.41 o 9 0 0 1687.28 1677.68 170.98 o 10 0 0 1424.60 1446.88 60.45 o 11 0 0 854.47 934.41 93.64 o 12 0 0 454.32 525.49 114.22 o -12 1 0 1621.38 1587.21 129.48 o -11 1 0 2010.18 1919.47 89.36 o -10 1 0 1817.29 1910.04 66.70 o -9 1 0 3867.62 3582.66 119.77 o -8 1 0 6377.22 6197.07 118.20 o -7 1 0 3501.40 3378.06 68.34 o -6 1 0 6046.78 6146.62 108.15 o -5 1 0 9869.92 9816.42 145.42 o -4 1 0 3644.08 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