#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/59/2215964.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215964_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Korabik, Maria' 'Lis, Tadeusz' _publ_section_title ; Redetermination of bis(methyltriphenylphosphonium) hexachloridorhenate(IV) ; _journal_coeditor_code HB2601 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2859 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.610 _cell_angle_gamma 90.000 _cell_length_a 9.1550 _cell_length_b 16.4290 _cell_length_c 12.9640 _exptl_crystal_F_000 942.00 _reflns_d_resolution_high 0.6196 _[local]_cod_data_source_file hb2601Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kmc5 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 249.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14382.33 14087.69 194.86 o 4 0 0 18499.01 18368.76 276.93 o 6 0 0 6499.23 5801.99 614.64 o 8 0 0 7567.24 6818.78 395.91 o 10 0 0 7383.51 7087.84 650.46 o 2 1 0 8852.52 8662.81 159.20 o 3 1 0 15881.32 16061.64 205.38 o 4 1 0 308.03 585.01 137.11 o 5 1 0 3541.57 3833.58 195.86 o 6 1 0 1136.12 1058.36 172.45 o 7 1 0 1849.37 1752.96 159.75 o 8 1 0 41.78 331.11 173.10 o 9 1 0 7406.67 7284.56 336.84 o 10 1 0 75.85 555.27 296.23 o 11 1 0 1521.53 1409.04 370.55 o 1 2 0 87.07 148.13 110.97 o 2 2 0 3156.36 3032.53 115.10 o 3 2 0 5481.36 5595.98 131.67 o 4 2 0 14757.30 15044.21 287.10 o 5 2 0 1970.81 1896.32 158.37 o 6 2 0 2031.76 2250.84 187.50 o 7 2 0 0.44 262.90 123.38 o 8 2 0 3704.03 3960.99 224.67 o 9 2 0 99.72 73.95 214.08 o 10 2 0 1173.98 964.02 284.72 o 11 2 0 598.86 775.06 350.52 o 1 3 0 47561.57 49279.95 1179.62 o 2 3 0 1318.72 1469.63 100.39 o 3 3 0 35856.94 35950.28 186.92 o 4 3 0 4801.29 5144.21 101.44 o 5 3 0 21575.75 21173.74 258.34 o 6 3 0 751.84 783.99 148.80 o 7 3 0 6246.27 6097.84 189.82 o 8 3 0 11.58 288.11 189.14 o 9 3 0 2822.56 3091.31 262.77 o 10 3 0 5.61 233.57 231.82 o 11 3 0 2206.50 2111.68 375.89 o 0 4 0 8251.68 8702.32 308.68 o 1 4 0 4827.13 4944.77 112.75 o 2 4 0 47418.18 47688.16 629.31 o 3 4 0 23.62 208.05 80.65 o 4 4 0 25853.22 25279.12 460.29 o 5 4 0 1260.60 1159.20 161.59 o 6 4 0 7591.84 7660.61 174.18 o 7 4 0 10.91 161.34 121.85 o 8 4 0 3249.55 2986.32 224.61 o 9 4 0 17.32 140.66 195.56 o 10 4 0 2230.07 2395.49 287.22 o 11 4 0 0.88 0.00 373.45 o 14 4 0 2433.97 1593.70 520.85 o 1 5 0 20839.79 20492.99 212.35 o 2 5 0 3732.82 3883.41 231.76 o 3 5 0 4936.75 4714.19 119.48 o 4 5 0 720.27 758.29 105.64 o 5 5 0 11828.14 12638.29 184.64 o 6 5 0 66.01 213.53 99.21 o 7 5 0 2077.15 2082.11 143.25 o 8 5 0 1005.91 1009.16 220.13 o 9 5 0 930.79 839.33 209.49 o 10 5 0 568.73 602.40 262.96 o 11 5 0 2006.37 1755.43 282.61 o 14 5 0 20.36 410.06 544.87 o 0 6 0 12045.52 12143.33 256.63 o 1 6 0 9791.30 10108.79 270.49 o 2 6 0 33536.49 33160.97 600.85 o 3 6 0 0.72 258.03 111.01 o 4 6 0 7652.67 7875.26 233.19 o 5 6 0 223.12 262.00 118.31 o 6 6 0 3123.10 3446.69 152.96 o 7 6 0 2015.84 2143.96 151.84 o 8 6 0 3150.10 3019.13 173.23 o 9 6 0 37.33 85.14 209.43 o 10 6 0 3017.37 2856.81 313.73 o 11 6 0 131.38 588.76 355.37 o 12 6 0 1887.99 1595.04 474.38 o 13 6 0 104.12 273.73 554.88 o 14 6 0 848.42 1575.72 805.80 o 1 7 0 39630.83 39334.70 550.69 o 2 7 0 1184.72 1408.64 144.73 o 3 7 0 20240.27 20569.64 543.82 o 4 7 0 942.35 1033.58 95.67 o 5 7 0 3411.33 3470.81 131.27 o 6 7 0 63.69 253.31 109.24 o 7 7 0 8309.78 8042.24 180.30 o 8 7 0 599.67 646.26 164.24 o 9 7 0 5304.22 4808.26 337.44 o 10 7 0 40.62 239.50 285.53 o 11 7 0 5760.80 5999.91 468.80 o 12 7 0 4.03 346.75 318.59 o 13 7 0 1417.97 1317.96 632.49 o 0 8 0 26854.92 26973.44 326.60 o 1 8 0 1.62 199.66 97.15 o 2 8 0 30343.32 29531.62 234.09 o 3 8 0 406.63 551.59 103.51 o 4 8 0 991.65 875.31 94.49 o 5 8 0 755.68 959.13 127.49 o 6 8 0 10927.12 10970.87 221.91 o 7 8 0 0.03 320.83 135.94 o 8 8 0 2638.57 2873.13 178.43 o 9 8 0 201.15 283.75 173.38 o 10 8 0 4168.24 3513.60 320.74 o 11 8 0 260.86 550.81 331.61 o 12 8 0 2399.52 2883.56 396.16 o 13 8 0 4.71 0.00 398.94 o 1 9 0 10819.49 10738.09 154.77 o 2 9 0 1008.59 1108.18 134.73 o 3 9 0 10193.25 10701.64 132.30 o 4 9 0 234.27 319.72 94.46 o 5 9 0 863.01 963.85 133.26 o 6 9 0 858.57 953.34 131.66 o 7 9 0 3201.72 2974.94 163.57 o 8 9 0 275.58 540.46 169.45 o 9 9 0 985.55 1368.75 217.15 o 10 9 0 444.72 718.28 286.45 o 11 9 0 2535.83 2831.61 402.28 o 12 9 0 420.43 490.28 374.49 o 13 9 0 126.99 323.70 396.33 o 0 10 0 11446.12 11578.79 283.76 o 1 10 0 2567.45 2251.99 156.76 o 2 10 0 19213.04 19680.24 317.76 o 3 10 0 191.54 256.64 102.79 o 4 10 0 4543.39 4577.48 130.05 o 5 10 0 85.45 230.76 133.20 o 6 10 0 10439.05 10800.42 455.75 o 7 10 0 1585.30 1715.53 174.62 o 8 10 0 3633.27 3512.98 240.98 o 9 10 0 262.40 426.16 214.02 o 10 10 0 2726.62 2371.00 306.56 o 11 10 0 146.22 789.17 346.26 o 12 10 0 1939.63 1349.36 382.65 o 13 10 0 123.19 277.82 430.57 o 1 11 0 13450.92 13683.16 189.24 o 2 11 0 329.13 499.13 103.92 o 3 11 0 19908.65 20180.24 449.61 o 4 11 0 2.21 279.13 137.97 o 5 11 0 11155.51 11137.09 409.06 o 6 11 0 14.32 250.38 223.94 o 7 11 0 9219.38 9565.40 270.81 o 8 11 0 552.59 660.91 226.85 o 9 11 0 1812.32 2425.80 304.49 o 10 11 0 246.28 309.23 266.98 o 11 11 0 3409.82 2693.18 439.44 o 12 11 0 53.05 0.00 417.37 o 13 11 0 2646.17 2791.94 443.05 o 0 12 0 4857.39 5049.57 174.00 o 1 12 0 41.24 360.14 126.30 o 2 12 0 6899.64 7105.27 149.19 o 3 12 0 2708.06 2655.26 126.46 o 4 12 0 10539.70 10682.37 294.61 o 5 12 0 276.32 484.20 190.44 o 6 12 0 2079.61 2531.18 250.74 o 7 12 0 284.83 282.75 175.78 o 8 12 0 260.58 531.23 232.69 o 9 12 0 215.11 160.90 219.41 o 10 12 0 895.02 958.81 272.08 o 11 12 0 3.06 641.81 422.67 o 12 12 0 1302.53 1012.81 585.90 o 1 13 0 7208.65 7107.36 137.25 o 2 13 0 931.17 1129.94 121.35 o 3 13 0 4956.40 5358.47 197.59 o 4 13 0 5101.57 4856.87 198.58 o 5 13 0 5456.49 5661.17 246.24 o 6 13 0 376.18 676.32 236.68 o 7 13 0 2107.51 2201.32 255.84 o 8 13 0 26.20 369.71 218.36 o 9 13 0 804.62 1272.34 285.99 o 10 13 0 222.26 405.82 259.23 o 11 13 0 1709.63 1546.18 456.33 o 12 13 0 17.62 680.67 508.75 o 0 14 0 16712.64 16835.62 815.02 o 1 14 0 2.12 313.96 118.43 o 2 14 0 8047.79 8121.66 171.79 o 3 14 0 3587.36 3425.28 172.10 o 4 14 0 10161.09 10548.78 362.98 o 5 14 0 0.09 323.63 220.12 o 6 14 0 5258.83 5361.99 301.31 o 7 14 0 96.75 313.52 238.07 o 8 14 0 6383.79 6006.35 337.14 o 9 14 0 98.36 290.10 258.59 o 10 14 0 5191.00 5209.09 380.34 o 11 14 0 12.54 222.38 472.37 o 12 14 0 1147.83 1589.18 589.12 o 1 15 0 11922.82 12111.28 185.39 o 2 15 0 200.31 316.07 127.03 o 3 15 0 4873.76 5004.65 167.81 o 4 15 0 97.15 370.04 190.15 o 5 15 0 2027.30 2722.25 250.37 o 6 15 0 0.04 394.71 218.58 o 7 15 0 2609.31 2294.00 258.30 o 8 15 0 69.22 207.04 270.80 o 9 15 0 5841.64 5926.24 376.54 o 10 15 0 36.48 204.48 291.27 o 11 15 0 954.36 1093.22 362.98 o 0 16 0 12325.64 12215.08 341.73 o 1 16 0 32.51 197.98 165.82 o 2 16 0 3247.35 3074.67 190.20 o 3 16 0 508.35 658.23 160.42 o 4 16 0 2235.88 2229.83 220.81 o 5 16 0 119.69 404.23 204.85 o 6 16 0 375.49 344.00 209.86 o 7 16 0 296.30 420.98 228.40 o 8 16 0 2948.35 2807.27 332.32 o 9 16 0 20.21 400.83 285.51 o 10 16 0 1293.09 1235.60 334.65 o 11 16 0 20.44 502.96 361.42 o 1 17 0 6057.18 5986.10 278.74 o 2 17 0 3.02 360.91 178.05 o 3 17 0 3557.64 3775.70 197.23 o 4 17 0 107.61 251.51 200.53 o 5 17 0 6288.79 5942.77 278.80 o 6 17 0 641.53 999.73 273.52 o 7 17 0 1506.18 1456.01 276.00 o 8 17 0 1.54 273.03 299.18 o 9 17 0 4083.77 4059.15 394.30 o 10 17 0 411.66 657.94 350.11 o 11 17 0 789.76 644.40 368.62 o 0 18 0 7882.76 6936.15 535.81 o 1 18 0 1.38 197.71 206.38 o 2 18 0 2960.79 3124.78 220.62 o 3 18 0 247.21 177.08 174.04 o 4 18 0 9177.64 9535.95 310.74 o 5 18 0 879.01 610.43 215.74 o 6 18 0 4661.65 4610.78 263.12 o 7 18 0 55.37 377.72 299.55 o 8 18 0 3383.43 3333.29 377.67 o 9 18 0 20.58 348.26 307.77 o 10 18 0 855.73 1326.93 371.23 o 1 19 0 2781.78 2234.96 338.83 o 2 19 0 189.97 281.71 241.59 o 3 19 0 3210.85 2827.41 312.02 o 4 19 0 61.27 443.20 270.03 o 5 19 0 6049.03 6124.10 384.91 o 6 19 0 448.99 445.28 282.40 o 7 19 0 677.33 742.45 346.19 o 8 19 0 1.24 466.74 343.48 o 9 19 0 1542.86 1549.27 328.17 o 10 19 0 2.80 429.32 365.97 o 0 20 0 1255.19 1069.34 493.58 o 1 20 0 1997.76 2108.69 444.99 o 2 20 0 1997.18 1478.24 362.27 o 3 20 0 95.60 244.72 277.03 o 4 20 0 3061.24 3117.16 471.73 o 5 20 0 484.61 530.68 340.61 o 6 20 0 1989.71 1674.40 357.09 o 7 20 0 162.07 420.63 300.73 o 8 20 0 1195.00 1400.09 370.43 o 9 20 0 190.64 1106.11 408.15 o 1 21 0 3450.22 3473.00 888.37 o 2 21 0 1024.79 856.50 762.39 o 3 21 0 3742.69 3751.02 437.58 o 4 21 0 333.87 751.45 556.07 o 5 21 0 3516.21 3825.69 678.92 o 6 21 0 34.68 179.92 299.05 o 7 21 0 3894.26 3892.98 410.57 o 8 21 0 457.57 897.93 340.18 o 4 22 0 2274.81 2687.71 570.60 o 5 22 0 105.01 380.98 375.69 o 6 22 0 2042.62 2192.86 360.61 o 7 22 0 52.99 477.17 419.71 o 8 22 0 2283.20 2151.94 402.76 o 5 23 0 209.25 658.80 423.55 o 6 23 0 211.93 197.26 455.08 o 7 23 0 1531.23 1397.38 367.25 o 4 24 0 856.75 1085.18 555.17 o 5 24 0 186.18 663.48 745.01 o 6 24 0 1874.47 2380.33 814.11 o 4 25 0 1.58 0.00 557.69 o -11 0 1 1784.53 1423.83 571.25 o -9 0 1 11008.78 10949.53 478.85 o -7 0 1 860.89 443.39 233.74 o -5 0 1 7001.37 7271.79 229.15 o -3 0 1 532.21 905.61 165.49 o 3 0 1 4220.13 4248.13 122.37 o 5 0 1 7653.89 7947.28 199.67 o 7 0 1 5291.81 5037.05 370.13 o 9 0 1 4641.64 4083.89 472.38 o 11 0 1 493.66 878.42 447.98 o -11 1 1 778.88 706.02 356.97 o -10 1 1 7352.39 6812.93 371.62 o -9 1 1 1312.77 977.28 304.22 o -8 1 1 9385.89 9350.80 392.55 o -7 1 1 164.19 289.16 133.67 o -6 1 1 2598.62 2726.28 215.07 o -5 1 1 120.91 202.99 130.32 o -4 1 1 11135.98 11292.95 207.18 o -3 1 1 1836.77 1962.21 123.72 o -2 1 1 15907.07 15433.64 155.41 o 1 1 1 1301.98 1260.74 143.43 o 2 1 1 59825.69 61907.20 846.27 o 3 1 1 4145.79 4374.98 99.34 o 4 1 1 21999.89 22279.96 179.67 o 5 1 1 1241.22 1156.42 102.52 o 6 1 1 4915.11 4995.73 186.09 o 7 1 1 1313.31 1210.85 202.92 o 8 1 1 10581.94 10592.38 234.69 o 9 1 1 533.12 513.77 271.55 o 10 1 1 2185.75 1897.34 288.00 o 11 1 1 32.46 171.21 343.09 o -11 2 1 3669.44 3276.62 366.78 o -10 2 1 103.93 306.38 376.40 o -9 2 1 8869.10 8534.40 361.59 o -8 2 1 191.22 472.47 161.88 o -7 2 1 7404.50 7235.39 180.50 o -6 2 1 2615.21 2800.88 236.20 o -5 2 1 14455.32 14058.75 375.97 o -4 2 1 2767.51 2852.56 251.59 o -3 2 1 4403.47 4232.09 146.60 o -2 2 1 1281.65 1270.06 114.21 o -1 2 1 52316.32 53598.49 442.52 o 0 2 1 1330.34 1498.93 159.95 o 1 2 1 34744.08 34596.26 472.23 o 2 2 1 9732.58 10140.30 154.66 o 3 2 1 48708.69 49169.46 227.69 o 4 2 1 442.88 540.11 91.24 o 5 2 1 23342.65 23429.24 251.72 o 6 2 1 1322.80 1292.59 167.34 o 7 2 1 3925.85 3890.60 200.29 o 8 2 1 26.53 284.28 174.66 o 9 2 1 7916.86 7734.17 298.94 o 10 2 1 230.71 470.71 325.77 o 11 2 1 1979.42 1636.26 355.87 o -11 3 1 781.75 824.60 342.12 o -10 3 1 1618.89 1717.87 366.90 o -9 3 1 66.12 459.92 223.69 o -8 3 1 1588.26 1705.02 188.36 o -7 3 1 705.03 850.36 168.54 o -6 3 1 5018.26 5041.30 163.70 o -5 3 1 1355.94 1392.24 147.10 o -4 3 1 4669.52 4389.56 140.02 o -3 3 1 1541.00 1700.52 84.76 o -2 3 1 5740.83 5719.83 117.43 o -1 3 1 327.54 294.00 81.09 o 0 3 1 38262.99 38301.56 356.56 o 1 3 1 4646.93 4693.77 105.47 o 2 3 1 3840.31 3550.97 168.30 o 3 3 1 6292.65 6162.34 124.29 o 4 3 1 31503.25 31483.14 252.90 o 5 3 1 3991.34 4342.47 176.19 o 6 3 1 4790.60 4904.62 293.52 o 7 3 1 1193.41 1105.22 134.54 o 8 3 1 4015.81 3723.89 256.92 o 9 3 1 324.09 401.80 195.44 o 10 3 1 972.96 938.38 217.12 o 11 3 1 818.70 1157.59 371.60 o 14 3 1 1390.06 987.19 632.31 o -11 4 1 2238.31 2226.97 391.08 o -10 4 1 12.62 449.52 232.92 o -9 4 1 1956.81 2051.66 233.71 o -8 4 1 2430.29 2549.39 195.05 o -7 4 1 4050.25 3914.51 145.43 o -6 4 1 87.57 358.75 117.06 o -5 4 1 6600.27 6235.99 162.66 o -4 4 1 595.23 708.41 89.15 o -3 4 1 17379.90 17304.14 191.69 o -2 4 1 2086.38 2172.72 188.16 o -1 4 1 10176.52 9801.62 143.72 o 0 4 1 1.03 151.24 105.32 o 1 4 1 24951.77 25264.15 501.08 o 2 4 1 5041.79 5384.92 119.97 o 3 4 1 28392.37 28540.37 203.39 o 4 4 1 222.18 348.67 110.92 o 5 4 1 14742.63 14668.53 266.71 o 6 4 1 106.86 325.18 102.47 o 7 4 1 5581.05 5628.01 173.28 o 8 4 1 129.11 377.31 189.66 o 9 4 1 575.77 601.89 207.60 o 10 4 1 941.44 870.61 231.12 o 11 4 1 1068.86 1319.98 297.76 o 13 4 1 1864.37 2059.42 577.44 o 14 4 1 270.70 394.57 679.29 o -11 5 1 63.49 367.01 318.79 o -10 5 1 5601.68 5064.89 337.16 o -9 5 1 256.49 443.77 209.21 o -8 5 1 3731.72 3833.41 211.90 o -7 5 1 2772.49 2838.28 147.95 o -6 5 1 10270.46 10326.30 182.97 o -5 5 1 3.63 407.30 141.71 o -4 5 1 14298.96 14695.31 180.07 o -3 5 1 1062.08 1137.15 95.14 o -2 5 1 9104.08 8769.99 117.86 o -1 5 1 5298.43 5249.19 118.93 o 0 5 1 17663.97 17714.22 180.04 o 1 5 1 10779.55 11038.63 129.02 o 2 5 1 27080.46 26386.78 506.42 o 3 5 1 147.23 453.74 156.16 o 4 5 1 29822.87 30053.48 234.58 o 5 5 1 1382.39 1470.48 175.74 o 6 5 1 20652.23 20785.99 272.60 o 7 5 1 545.29 826.45 155.72 o 8 5 1 1530.27 1627.34 180.75 o 9 5 1 299.68 253.53 245.02 o 10 5 1 2208.10 2290.45 281.61 o 11 5 1 6.24 284.19 281.55 o 12 5 1 2954.44 3392.95 781.48 o 13 5 1 228.17 438.02 489.35 o 14 5 1 2433.72 2336.72 818.87 o -14 6 1 194.40 939.87 720.56 o -11 6 1 4158.21 4257.04 437.64 o -10 6 1 1096.26 1149.25 318.48 o -9 6 1 3116.70 3281.08 296.51 o -8 6 1 1640.35 1654.51 198.47 o -7 6 1 8982.77 8775.14 185.96 o -6 6 1 1028.72 1186.40 147.62 o -5 6 1 3456.00 3600.44 146.28 o -4 6 1 115.06 257.81 135.44 o -3 6 1 13390.68 13467.21 149.31 o -2 6 1 9334.39 9392.81 230.24 o -1 6 1 8867.59 8669.11 135.63 o 0 6 1 1594.09 1930.32 140.09 o 1 6 1 23444.95 23019.97 491.70 o 2 6 1 8.48 198.62 125.83 o 3 6 1 22876.68 22383.02 353.22 o 4 6 1 16.00 304.11 119.96 o 5 6 1 10082.54 10054.47 140.03 o 6 6 1 0.12 176.11 113.98 o 7 6 1 11553.78 11376.98 226.19 o 8 6 1 341.24 547.84 174.26 o 9 6 1 2766.41 3022.80 300.82 o 10 6 1 108.80 301.67 256.17 o 11 6 1 4337.51 3914.50 304.40 o 12 6 1 87.80 212.76 319.22 o 13 6 1 722.29 521.35 681.28 o -14 7 1 708.95 909.93 575.59 o -13 7 1 3.96 295.99 636.24 o -12 7 1 2571.61 2854.69 512.55 o -11 7 1 22.75 337.74 305.29 o -10 7 1 3472.33 3110.26 330.83 o -9 7 1 13.42 381.79 294.71 o -8 7 1 7052.88 6843.06 190.09 o -7 7 1 3.74 169.28 123.86 o -6 7 1 3088.28 3005.17 148.91 o -5 7 1 15.12 291.27 121.32 o -4 7 1 223.65 501.74 121.92 o -3 7 1 474.36 505.74 101.51 o -2 7 1 22426.36 22591.60 193.92 o -1 7 1 2947.41 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