#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:41:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181079 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/59/2215967.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215967_Fobs loop_ _publ_author_name 'Han, Qiuxia' _publ_section_title ; 4,4'-Methylenedianilinium 2,2'-dithiodibenzoate ; _journal_coeditor_code HB2607 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4456 _journal_volume 63 _journal_year 2007 _space_group_IT_number 114 _symmetry_space_group_name_Hall 'P -4 2n' _symmetry_space_group_name_H-M 'P -4 21 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.4620 _cell_length_b 24.4620 _cell_length_c 8.8325 _exptl_crystal_F_000 2112.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file hb2607Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 70617cm in P-421c P-421c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'y, -x, -z' '-x, -y, z' '-y, x, -z' 'x+1/2, -y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 75867.90 45198.06 576.39 o 1 2 0 102.63 105.42 6.11 o 2 2 0 27536.13 17897.16 474.61 o 2 3 0 810.54 1135.94 19.18 o 3 3 0 8659.22 13084.11 175.06 o 1 4 0 1843.06 1936.68 24.40 o 3 4 0 2293.95 2318.55 36.12 o 4 4 0 18425.20 20981.90 175.75 o 1 5 0 2267.07 1314.75 24.35 o 2 5 0 14.14 11.80 10.91 o 4 5 0 8378.94 10277.70 75.70 o 5 5 0 1630.08 2095.15 45.52 o 0 6 0 147.62 94.47 16.95 o 1 6 0 4850.84 5286.68 62.39 o 2 6 0 69.50 136.42 14.90 o 3 6 0 8521.98 10193.50 79.15 o 4 6 0 2723.35 2885.15 46.03 o 5 6 0 2301.70 2482.36 37.99 o 6 6 0 10956.09 11846.62 115.57 o 2 7 0 996.74 1035.30 27.61 o 3 7 0 5696.39 6964.08 81.23 o 4 7 0 3490.85 4318.98 70.40 o 6 7 0 8308.28 9719.21 86.97 o 7 7 0 22.65 0.00 14.32 o 0 8 0 4381.52 6920.99 80.79 o 1 8 0 998.86 1144.05 29.66 o 2 8 0 3941.02 5243.26 67.20 o 3 8 0 2547.44 2528.88 45.29 o 4 8 0 223.68 173.83 19.72 o 5 8 0 2470.02 3090.30 53.81 o 6 8 0 862.08 969.02 33.87 o 7 8 0 44.85 41.32 10.98 o 8 8 0 2176.99 1659.50 48.57 o 1 9 0 989.89 593.47 25.46 o 2 9 0 0.01 0.00 12.68 o 3 9 0 39.59 74.84 14.41 o 4 9 0 327.14 479.73 27.35 o 5 9 0 142.20 290.51 25.40 o 6 9 0 503.97 505.43 30.28 o 7 9 0 588.68 525.05 26.85 o 8 9 0 5492.96 6499.63 65.04 o 9 9 0 1225.00 1402.89 48.26 o 0 10 0 25160.77 23373.84 210.39 o 1 10 0 133.79 142.09 17.95 o 2 10 0 41.08 0.00 12.51 o 3 10 0 6632.66 5983.32 65.15 o 4 10 0 8843.32 8434.36 88.70 o 5 10 0 2631.14 2683.19 52.66 o 6 10 0 243.55 324.76 27.92 o 7 10 0 10513.89 11021.06 146.74 o 8 10 0 735.09 1029.65 35.33 o 9 10 0 4617.78 4459.71 67.56 o 10 10 0 2627.63 2900.17 68.25 o 1 11 0 658.61 456.03 25.24 o 2 11 0 480.68 732.34 30.02 o 3 11 0 4955.30 6370.42 67.88 o 4 11 0 322.00 449.85 30.18 o 5 11 0 2272.19 2403.95 52.87 o 6 11 0 680.76 733.88 38.38 o 7 11 0 2951.06 2942.82 61.75 o 8 11 0 1424.55 1489.86 41.75 o 9 11 0 63.30 152.30 21.34 o 10 11 0 983.03 1233.37 39.94 o 11 11 0 4328.85 4693.81 142.59 o 0 12 0 630.73 626.42 36.86 o 1 12 0 11890.76 13116.67 105.27 o 2 12 0 16600.25 19146.47 197.77 o 3 12 0 1216.13 1153.73 35.25 o 4 12 0 2666.13 2572.45 55.53 o 5 12 0 1177.62 1420.90 44.92 o 6 12 0 872.48 870.76 42.01 o 7 12 0 1837.84 1722.35 51.29 o 8 12 0 355.96 476.53 30.03 o 9 12 0 571.26 574.80 32.46 o 10 12 0 407.61 386.93 33.91 o 11 12 0 5452.68 5451.13 91.86 o 12 12 0 3035.66 2809.64 94.07 o 1 13 0 1239.72 1043.02 36.41 o 2 13 0 59.64 122.66 19.86 o 3 13 0 2489.70 2121.20 44.68 o 4 13 0 1.77 6.97 16.80 o 5 13 0 700.62 798.38 40.22 o 6 13 0 1787.72 1749.75 50.48 o 7 13 0 75.98 184.73 28.31 o 8 13 0 3521.98 3470.90 63.93 o 9 13 0 929.40 1080.07 41.81 o 10 13 0 587.59 604.78 40.87 o 11 13 0 225.78 296.60 34.97 o 12 13 0 223.79 229.91 33.46 o 13 13 0 96.41 18.92 32.68 o 0 14 0 1115.21 1330.10 49.35 o 1 14 0 801.64 1011.58 36.98 o 2 14 0 22.43 78.66 18.93 o 3 14 0 1346.30 1199.07 37.76 o 4 14 0 514.14 526.10 35.22 o 5 14 0 2711.08 2537.29 60.14 o 6 14 0 7.31 30.00 21.12 o 7 14 0 494.51 520.80 39.34 o 8 14 0 142.45 125.64 22.33 o 9 14 0 726.65 824.89 39.48 o 10 14 0 2286.30 2381.06 65.53 o 11 14 0 2299.53 2069.26 63.70 o 12 14 0 616.09 774.28 49.51 o 13 14 0 714.86 666.92 45.41 o 14 14 0 1932.01 1839.60 91.13 o 1 15 0 2072.95 1985.98 47.29 o 2 15 0 0.54 37.84 18.42 o 3 15 0 0.38 29.48 19.08 o 4 15 0 176.92 186.49 26.24 o 5 15 0 1883.77 1866.80 55.07 o 6 15 0 234.42 185.57 28.97 o 7 15 0 471.51 489.82 40.85 o 8 15 0 66.76 122.05 22.31 o 9 15 0 78.29 71.37 24.25 o 10 15 0 0.51 9.90 21.65 o 11 15 0 365.22 385.12 39.82 o 12 15 0 575.44 585.86 55.00 o 13 15 0 108.15 139.72 40.34 o 14 15 0 76.03 92.60 32.76 o 15 15 0 95.74 108.74 58.24 o 0 16 0 16.14 55.85 32.62 o 1 16 0 454.81 459.30 36.77 o 2 16 0 579.82 580.76 44.51 o 3 16 0 873.09 781.77 56.72 o 4 16 0 227.84 157.89 27.48 o 5 16 0 60.81 47.62 24.01 o 6 16 0 484.29 515.84 40.04 o 7 16 0 395.49 367.93 38.98 o 8 16 0 214.47 169.63 34.03 o 9 16 0 0.33 0.00 28.67 o 10 16 0 0.95 28.00 32.64 o 11 16 0 1426.21 1301.85 70.70 o 12 16 0 0.75 0.00 33.52 o 13 16 0 227.59 200.61 42.90 o 14 16 0 146.75 121.15 37.75 o 15 16 0 1142.31 1117.56 77.95 o 16 16 0 19.69 50.16 53.09 o 1 17 0 1764.93 1624.99 62.80 o 2 17 0 405.03 399.35 42.68 o 3 17 0 1493.54 1366.96 62.87 o 4 17 0 586.58 595.71 48.28 o 5 17 0 13.38 2.38 26.64 o 6 17 0 84.22 49.10 29.70 o 7 17 0 465.59 538.16 51.65 o 8 17 0 463.02 453.40 57.52 o 9 17 0 7.23 37.20 33.43 o 10 17 0 1773.71 1784.96 77.69 o 11 17 0 293.81 286.41 48.65 o 12 17 0 7.53 41.63 36.97 o 13 17 0 1712.65 1530.50 79.87 o 14 17 0 362.02 404.87 48.20 o 15 17 0 493.64 451.13 57.07 o 16 17 0 214.04 275.31 50.07 o 17 17 0 1004.41 891.50 103.37 o 0 18 0 38.52 122.96 50.42 o 1 18 0 202.53 229.14 42.34 o 2 18 0 1509.68 1459.20 66.39 o 3 18 0 949.09 938.36 57.04 o 4 18 0 984.50 1171.34 62.60 o 5 18 0 2950.53 2823.70 89.60 o 6 18 0 998.46 929.85 58.88 o 7 18 0 873.82 897.86 62.98 o 8 18 0 279.07 260.09 53.18 o 9 18 0 1692.75 1340.48 83.99 o 10 18 0 472.94 481.91 61.47 o 11 18 0 581.45 603.38 67.45 o 12 18 0 55.07 51.02 42.66 o 13 18 0 53.14 64.95 44.17 o 14 18 0 145.14 140.08 44.83 o 15 18 0 145.20 184.77 52.10 o 16 18 0 24.56 61.08 49.08 o 17 18 0 182.77 179.53 51.12 o 18 18 0 607.44 724.38 104.06 o 1 19 0 1663.22 1510.45 77.50 o 2 19 0 586.74 564.75 56.49 o 3 19 0 478.51 574.16 55.87 o 4 19 0 5126.16 4730.31 191.49 o 5 19 0 1458.18 1367.61 69.16 o 6 19 0 21.36 14.41 31.81 o 7 19 0 198.57 229.96 52.20 o 8 19 0 333.05 343.73 55.98 o 9 19 0 224.49 173.01 49.22 o 10 19 0 709.80 725.25 70.98 o 11 19 0 565.94 533.41 66.39 o 12 19 0 33.39 24.82 41.24 o 13 19 0 254.03 247.87 50.68 o 14 19 0 0.14 51.02 40.69 o 15 19 0 308.88 312.48 60.58 o 16 19 0 75.00 72.47 42.43 o 17 19 0 248.22 213.94 53.92 o 18 19 0 211.34 248.99 55.82 o 19 19 0 107.57 157.63 179.02 o 0 20 0 184.15 168.23 62.78 o 1 20 0 673.30 794.26 63.83 o 2 20 0 172.23 177.75 42.83 o 3 20 0 1994.20 1885.54 84.63 o 4 20 0 329.94 426.55 53.46 o 5 20 0 261.71 245.38 43.17 o 6 20 0 1243.46 1048.55 64.82 o 7 20 0 129.88 163.76 49.82 o 8 20 0 104.62 111.89 47.34 o 9 20 0 549.97 519.05 65.80 o 10 20 0 50.89 66.50 42.79 o 11 20 0 233.74 278.79 54.49 o 12 20 0 29.05 69.42 43.68 o 13 20 0 132.67 54.50 43.32 o 14 20 0 1.29 1.99 43.07 o 15 20 0 8.94 54.03 43.55 o 16 20 0 325.64 216.98 54.11 o 17 20 0 4.74 12.59 41.63 o 18 20 0 0.00 49.69 43.80 o 19 20 0 75.75 188.50 58.59 o 20 20 0 17.29 127.22 79.16 o 1 21 0 489.24 437.24 54.69 o 2 21 0 779.56 665.88 62.89 o 3 21 0 956.91 971.60 71.11 o 4 21 0 53.90 100.73 38.77 o 5 21 0 259.44 346.52 51.08 o 6 21 0 393.15 473.49 62.07 o 7 21 0 68.71 72.50 42.35 o 8 21 0 506.93 494.32 63.66 o 9 21 0 31.98 72.43 43.64 o 10 21 0 44.83 17.35 43.08 o 11 21 0 409.27 387.33 61.97 o 12 21 0 516.46 580.60 70.50 o 13 21 0 193.03 264.65 57.53 o 14 21 0 1113.76 871.90 83.08 o 15 21 0 100.68 218.75 67.61 o 16 21 0 1157.15 1083.99 96.25 o 17 21 0 1.09 64.46 42.54 o 18 21 0 55.21 126.06 48.15 o 19 21 0 9.91 73.97 52.26 o 20 21 0 83.71 218.85 99.05 o 21 21 0 70.95 100.07 141.49 o 0 22 0 2272.88 2217.63 131.73 o 1 22 0 2232.41 2205.52 105.93 o 2 22 0 1864.20 1754.45 87.93 o 3 22 0 1384.24 1288.51 79.83 o 4 22 0 1.09 56.38 37.83 o 5 22 0 2119.74 1785.86 87.55 o 6 22 0 514.46 429.48 61.15 o 7 22 0 288.61 299.05 64.47 o 8 22 0 131.32 129.66 53.73 o 9 22 0 245.09 239.60 55.15 o 10 22 0 168.05 205.72 52.94 o 11 22 0 40.24 97.95 44.18 o 12 22 0 469.76 435.32 64.07 o 13 22 0 5.08 0.00 40.26 o 14 22 0 28.58 55.44 54.52 o 15 22 0 1068.31 967.51 106.49 o 16 22 0 33.81 146.13 52.48 o 17 22 0 30.98 147.01 50.48 o 18 22 0 65.85 207.20 56.48 o 19 22 0 7.49 107.61 109.06 o 20 22 0 2.07 121.96 58.06 o 1 23 0 39.92 36.14 37.61 o 2 23 0 218.38 236.69 47.44 o 3 23 0 261.96 279.85 48.30 o 4 23 0 115.82 135.96 42.02 o 5 23 0 17.42 49.64 39.86 o 6 23 0 17.87 27.14 42.04 o 7 23 0 411.00 271.35 63.89 o 8 23 0 292.06 315.94 63.47 o 9 23 0 307.81 327.79 80.03 o 10 23 0 1.80 0.00 45.21 o 11 23 0 65.66 108.37 47.67 o 12 23 0 188.67 195.19 54.12 o 13 23 0 42.00 62.78 47.77 o 14 23 0 118.49 246.03 68.08 o 15 23 0 8.18 95.58 56.78 o 16 23 0 30.75 146.06 69.47 o 17 23 0 0.02 107.83 47.81 o 18 23 0 133.79 195.10 55.25 o 19 23 0 36.06 228.13 63.77 o 0 24 0 731.77 677.74 94.96 o 1 24 0 181.89 228.41 47.73 o 2 24 0 2.84 27.91 37.34 o 3 24 0 404.68 414.57 55.18 o 4 24 0 290.03 252.61 53.60 o 5 24 0 225.94 178.37 50.34 o 6 24 0 29.15 44.90 41.64 o 7 24 0 55.90 16.88 47.33 o 8 24 0 315.07 366.50 69.54 o 9 24 0 789.02 713.25 85.46 o 10 24 0 4.33 40.40 48.59 o 11 24 0 138.15 85.09 50.51 o 12 24 0 39.57 100.11 54.40 o 13 24 0 678.21 744.93 82.11 o 14 24 0 75.27 190.28 59.74 o 15 24 0 170.22 312.30 70.88 o 16 24 0 79.66 125.42 68.55 o 17 24 0 173.08 272.11 61.47 o 18 24 0 144.97 206.54 74.96 o 1 25 0 765.85 766.21 70.53 o 2 25 0 0.03 69.42 57.35 o 3 25 0 8.68 8.99 42.05 o 4 25 0 122.76 162.96 51.11 o 5 25 0 2.50 64.94 44.23 o 6 25 0 249.28 273.79 57.19 o 7 25 0 11.83 82.78 51.99 o 8 25 0 43.97 56.04 49.05 o 9 25 0 239.37 206.93 61.91 o 10 25 0 634.78 511.30 153.56 o 11 25 0 138.87 193.68 62.88 o 12 25 0 64.07 63.11 55.12 o 13 25 0 168.05 206.69 60.09 o 14 25 0 511.04 562.42 100.71 o 15 25 0 126.04 251.93 67.01 o 16 25 0 569.81 751.98 84.75 o 0 26 0 52.45 86.35 57.70 o 1 26 0 125.30 205.43 69.70 o 2 26 0 140.18 302.88 68.50 o 3 26 0 279.14 311.31 60.65 o 4 26 0 217.15 228.66 54.81 o 5 26 0 827.56 666.97 79.09 o 6 26 0 285.11 238.24 56.96 o 7 26 0 747.93 632.56 87.12 o 8 26 0 118.35 144.56 57.18 o 9 26 0 165.52 182.10 80.03 o 10 26 0 18.83 43.38 59.72 o 11 26 0 513.17 502.67 79.61 o 12 26 0 0.03 111.27 65.24 o 13 26 0 3.66 99.64 85.80 o 14 26 0 0.35 124.04 66.81 o 15 26 0 570.79 603.63 150.28 o 1 27 0 153.65 247.08 50.58 o 2 27 0 21.20 59.08 47.47 o 3 27 0 24.64 72.99 46.16 o 4 27 0 10.67 72.53 47.99 o 5 27 0 141.94 110.93 61.43 o 6 27 0 31.80 77.03 47.18 o 7 27 0 241.63 171.65 62.02 o 8 27 0 48.32 129.99 79.75 o 9 27 0 123.79 153.39 57.16 o 10 27 0 109.60 170.78 89.77 o 11 27 0 141.91 277.61 71.37 o 12 27 0 287.49 295.28 69.94 o 13 27 0 16.68 121.74 77.81 o 0 28 0 1346.16 1147.81 214.91 o 1 28 0 91.33 207.28 50.57 o 2 28 0 189.51 233.10 58.34 o 3 28 0 435.32 358.40 64.05 o 4 28 0 124.11 163.27 53.22 o 5 28 0 0.48 28.42 66.31 o 6 28 0 7.65 57.69 52.09 o 7 28 0 15.53 66.98 54.77 o 8 28 0 69.94 71.49 60.32 o 9 28 0 178.13 176.60 85.27 o 10 28 0 101.45 146.22 77.29 o 11 28 0 0.46 47.13 52.49 o 1 29 0 142.31 197.94 83.61 o 2 29 0 17.73 39.60 87.26 o 3 29 0 44.24 142.18 60.48 o 4 29 0 2.90 1.58 65.67 o 5 29 0 13.46 60.65 50.62 o 6 29 0 122.51 113.81 65.33 o 7 29 0 0.01 31.17 85.06 o 8 29 0 3.63 36.87 59.78 o 0 30 0 316.33 226.48 109.66 o 1 30 0 76.34 129.46 127.67 o 2 30 0 16.77 69.99 61.78 o 3 30 0 3.10 0.00 55.58 o -2 3 1 27504.62 32917.45 144.95 o -1 3 1 10555.74 10122.58 72.72 o 1 3 1 10658.81 10331.08 108.95 o 2 3 1 27742.74 33055.26 177.62 o -3 4 1 43903.48 53454.46 247.09 o -2 4 1 20222.24 21828.81 108.80 o -1 4 1 25967.78 33926.16 198.76 o 1 4 1 26189.65 34309.10 141.89 o 2 4 1 20469.72 22132.19 176.14 o 3 4 1 44306.26 54215.66 201.82 o -4 5 1 2077.12 1967.02 40.23 o -3 5 1 12735.84 13049.24 84.44 o -2 5 1 20650.75 23342.33 125.38 o -1 5 1 365.58 351.65 19.15 o 0 5 1 4708.42 4162.04 47.70 o 1 5 1 361.24 352.83 15.41 o 2 5 1 20804.06 23433.89 107.59 o 3 5 1 12581.31 13081.99 79.93 o 4 5 1 2074.24 2077.61 44.98 o -5 6 1 2673.20 2859.88 50.33 o -4 6 1 5160.56 5378.65 61.75 o -3 6 1 2055.77 1979.80 33.54 o -2 6 1 22887.74 27389.62 145.61 o -1 6 1 22382.59 23433.47 148.25 o 0 6 1 32376.29 40949.27 211.25 o 1 6 1 22533.11 23477.54 108.85 o 2 6 1 23002.29 27101.46 122.68 o 3 6 1 2137.02 2115.97 32.82 o 4 6 1 5091.53 5400.06 48.58 o 5 6 1 2644.26 2879.72 38.01 o -6 7 1 5081.32 5305.23 83.53 o -5 7 1 2330.56 2454.54 48.40 o -4 7 1 894.92 1050.09 31.34 o -3 7 1 3169.34 3258.38 47.23 o -2 7 1 1283.90 1475.30 33.85 o -1 7 1 3600.59 4402.57 54.73 o 0 7 1 13663.22 17353.63 105.17 o 1 7 1 3544.51 4386.02 43.07 o 2 7 1 1345.95 1426.28 29.07 o 3 7 1 3161.44 3272.08 37.13 o 4 7 1 899.37 1077.73 24.06 o 5 7 1 2354.25 2534.20 35.25 o 6 7 1 5025.13 5267.15 54.65 o -7 8 1 51.99 84.54 17.98 o -6 8 1 6160.18 6944.20 83.48 o -5 8 1 6391.80 6958.91 76.55 o -4 8 1 2124.77 2060.29 47.73 o -3 8 1 4680.97 4375.48 56.49 o -2 8 1 5901.35 5512.79 63.83 o -1 8 1 13622.48 16113.99 105.51 o 0 8 1 208.38 328.04 20.48 o 1 8 1 13763.83 16228.66 120.04 o 2 8 1 5959.37 5727.68 56.52 o 3 8 1 4614.92 4448.48 45.14 o 4 8 1 2088.14 2066.16 34.00 o 5 8 1 6303.78 6899.89 58.79 o 6 8 1 6189.97 6948.96 62.76 o 7 8 1 44.82 66.63 15.28 o -8 9 1 2553.61 2355.16 54.89 o -7 9 1 572.05 675.78 33.04 o -6 9 1 10962.46 12487.88 115.99 o -5 9 1 945.70 1042.25 40.16 o -4 9 1 11910.20 12683.43 119.71 o -3 9 1 1409.45 1610.41 35.22 o -2 9 1 2467.04 2844.37 45.76 o -1 9 1 2151.05 2225.95 41.28 o 0 9 1 10107.68 9078.34 80.36 o 1 9 1 2158.30 2287.95 34.61 o 2 9 1 2475.63 2872.27 42.84 o 3 9 1 1432.67 1694.88 28.60 o 4 9 1 11892.29 12951.88 83.88 o 5 9 1 988.87 1125.01 28.96 o 6 9 1 10958.14 12532.73 98.56 o 7 9 1 561.32 742.87 30.45 o 8 9 1 2595.15 2440.56 42.40 o -9 10 1 691.21 740.47 35.99 o -8 10 1 2006.60 2175.21 52.45 o -7 10 1 119.12 122.50 20.64 o -6 10 1 578.46 618.48 40.27 o -5 10 1 3016.68 3369.71 61.08 o -4 10 1 3038.15 3286.66 59.50 o -3 10 1 2391.44 2273.36 42.93 o -2 10 1 4516.76 5196.61 68.39 o -1 10 1 2525.76 2475.40 45.33 o 0 10 1 1696.62 1425.28 35.62 o 1 10 1 2499.11 2521.54 37.57 o 2 10 1 4556.23 5347.32 59.81 o 3 10 1 2478.80 2329.65 41.87 o 4 10 1 3032.13 3315.98 42.29 o 5 10 1 3034.14 3384.52 46.42 o 6 10 1 561.64 567.23 25.11 o 7 10 1 105.22 137.07 19.96 o 8 10 1 2043.17 2152.28 46.29 o 9 10 1 719.94 737.90 28.54 o -10 11 1 1849.40 1740.62 50.90 o -9 11 1 512.42 568.07 33.04 o 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