#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2215973.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2215973_Fobs loop_ _publ_author_name 'McKay, Michael G.' 'Friedrich, Holger B.' 'Maguire, Glenn E. M.' _publ_section_title ; 7,11,15,28-Tetrakis(bromomethyl)-1,21,23,25-tetrapentylresorcin[4]arene cavitand 0.415-hydrate ; _journal_coeditor_code HG2300 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4345 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.655 _cell_angle_beta 92.921 _cell_angle_gamma 118.676 _cell_length_a 11.5151 _cell_length_b 11.9323 _cell_length_c 22.7986 _exptl_crystal_F_000 1226.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file hg2300Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 7m_kznd12_0a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 319.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1167.54 800.79 5.46 o 2 0 0 22190.86 24010.12 135.57 o 3 0 0 220.91 186.79 7.27 o 4 0 0 722.46 388.81 13.31 o 5 0 0 491.70 438.60 16.27 o 6 0 0 2532.61 2486.99 28.51 o 7 0 0 1073.41 941.15 25.39 o 8 0 0 492.03 464.52 21.41 o 9 0 0 32.87 17.58 18.71 o 10 0 0 93.86 74.96 23.74 o 11 0 0 633.58 793.44 39.64 o 12 0 0 9.48 -3.45 30.96 o -12 1 0 1.37 -7.66 30.04 o -11 1 0 1434.81 1590.37 42.90 o -10 1 0 19.20 8.59 21.76 o -9 1 0 56.69 42.70 18.57 o -8 1 0 370.43 308.40 19.08 o -7 1 0 1556.55 1582.42 26.80 o -6 1 0 6094.49 6350.06 41.68 o -5 1 0 21004.28 21401.68 98.15 o -4 1 0 20904.91 21816.71 210.22 o -3 1 0 27791.06 30148.80 230.13 o -2 1 0 7451.09 7960.84 41.56 o -1 1 0 532.04 516.23 10.19 o 0 1 0 235.16 20.87 10.44 o 1 1 0 5694.88 4715.49 28.51 o 2 1 0 15641.00 14657.83 127.13 o 3 1 0 1948.15 2042.37 21.41 o 4 1 0 166.13 286.37 13.47 o 5 1 0 724.21 738.28 19.74 o 6 1 0 8095.62 8412.54 90.67 o 7 1 0 4.24 4.74 15.26 o 8 1 0 1103.67 1010.40 30.61 o 9 1 0 576.58 545.13 27.32 o 10 1 0 16.11 23.05 23.97 o 11 1 0 276.14 237.85 31.75 o -13 2 0 6.36 21.04 32.03 o -12 2 0 241.93 314.45 29.67 o -11 2 0 6.03 10.72 24.18 o -10 2 0 170.37 100.79 22.58 o -9 2 0 3643.57 3831.13 58.85 o -8 2 0 890.32 934.66 26.33 o -7 2 0 217.26 214.51 14.08 o -6 2 0 4893.99 5331.96 50.95 o -5 2 0 9173.05 9511.81 75.69 o -4 2 0 497.24 558.84 11.84 o -3 2 0 36.78 31.99 5.52 o -2 2 0 419.16 229.05 9.50 o -1 2 0 1046.02 1064.81 16.33 o 0 2 0 216.53 195.92 40.85 o 1 2 0 4158.73 3351.60 443.37 o 2 2 0 19783.99 18047.11 996.99 o 3 2 0 8930.40 9752.42 99.37 o 4 2 0 1977.52 1854.50 21.82 o 5 2 0 17.67 -3.62 10.53 o 6 2 0 584.33 712.65 24.23 o 7 2 0 154.76 153.77 18.50 o 8 2 0 5290.60 5762.99 131.46 o 9 2 0 1098.94 1070.93 36.75 o 10 2 0 1410.09 1386.27 41.93 o 11 2 0 18.65 13.25 30.69 o -13 3 0 2.49 -1.24 28.58 o -12 3 0 1.55 -20.09 25.14 o -11 3 0 166.94 188.87 24.60 o -10 3 0 19.89 13.83 20.80 o -9 3 0 2977.90 2894.01 39.27 o -8 3 0 160.13 149.98 17.74 o -7 3 0 1043.89 1179.81 25.74 o -6 3 0 1026.31 987.86 20.26 o -5 3 0 2529.61 2798.81 26.32 o -4 3 0 22.72 53.90 9.10 o -3 3 0 102050.87 107345.08 5690.84 o -2 3 0 21339.67 24973.02 168.56 o -1 3 0 135.10 226.10 12.76 o 0 3 0 3090.13 3579.08 20.47 o 1 3 0 0.31 29.42 9.04 o 2 3 0 7.63 26.76 12.47 o 3 3 0 8085.95 8659.68 471.65 o 4 3 0 2566.40 1959.13 21.21 o 5 3 0 894.59 865.58 21.11 o 6 3 0 26.64 9.07 15.40 o 7 3 0 29.70 6.20 18.95 o 8 3 0 1858.33 1905.85 39.54 o 9 3 0 19.90 11.31 23.93 o 10 3 0 204.70 180.25 29.30 o -13 4 0 41.33 51.51 26.57 o -12 4 0 4.27 9.98 23.50 o -11 4 0 312.27 366.63 24.37 o -10 4 0 819.56 873.86 32.15 o -9 4 0 22.15 33.84 16.83 o -8 4 0 6567.46 6266.35 84.91 o -7 4 0 6314.54 5794.56 50.01 o -6 4 0 2284.61 2472.74 34.26 o -5 4 0 81.77 136.21 12.10 o -4 4 0 2494.55 2082.17 27.13 o -3 4 0 10.65 46.27 21.48 o -2 4 0 820.47 682.62 22.44 o -1 4 0 2691.54 2211.78 22.55 o 0 4 0 24.27 24.88 7.98 o 1 4 0 239.37 248.70 27.23 o 2 4 0 0.83 5.29 4.48 o 3 4 0 6191.24 3712.95 1275.04 o 4 4 0 2718.16 3084.10 78.79 o 5 4 0 1632.65 1380.07 20.44 o 6 4 0 80.27 50.39 13.77 o 7 4 0 32.95 12.96 19.49 o 8 4 0 2.89 3.57 21.62 o 9 4 0 52.56 31.28 24.45 o 10 4 0 67.32 155.10 30.49 o -14 5 0 17.17 16.18 36.78 o -13 5 0 105.69 133.31 34.91 o -12 5 0 174.09 212.68 32.36 o -11 5 0 185.33 210.18 32.28 o -10 5 0 120.00 136.26 27.55 o -9 5 0 360.39 287.11 25.12 o -8 5 0 176.74 126.49 19.59 o -7 5 0 63.03 59.31 13.90 o -6 5 0 464.36 374.53 19.44 o -5 5 0 787.49 600.35 23.76 o -4 5 0 107.17 57.14 9.28 o -3 5 0 1035.21 1091.50 44.62 o -2 5 0 6291.32 6528.13 115.26 o -1 5 0 15734.32 15326.96 214.67 o 0 5 0 107.78 40.35 10.82 o 1 5 0 870.67 744.42 17.11 o 2 5 0 1196.55 1143.50 67.94 o 3 5 0 127.57 115.46 14.84 o 4 5 0 51.92 27.06 10.64 o 5 5 0 2692.76 1725.61 686.26 o 6 5 0 98.21 36.55 27.74 o 7 5 0 586.08 430.44 124.28 o 8 5 0 2.80 29.62 23.05 o 9 5 0 1.50 -42.75 42.75 o -14 6 0 3.31 20.07 36.43 o -13 6 0 67.06 55.90 33.99 o -12 6 0 49.08 30.18 33.26 o -11 6 0 1014.52 998.05 45.58 o -10 6 0 99.21 166.52 26.85 o -9 6 0 373.31 359.16 25.83 o -8 6 0 4372.46 4772.91 65.48 o -7 6 0 48.65 54.27 16.19 o -6 6 0 6235.24 5430.28 109.84 o -5 6 0 269.41 315.72 19.34 o -4 6 0 3184.00 2944.25 49.37 o -3 6 0 3401.66 3373.64 71.06 o -2 6 0 4.17 7.44 27.27 o -1 6 0 171.01 154.75 12.94 o 0 6 0 5508.95 5474.23 41.61 o 1 6 0 5384.79 4561.51 284.94 o 2 6 0 617.55 536.15 19.66 o 3 6 0 81.88 80.87 16.70 o 4 6 0 81.69 85.14 19.91 o 5 6 0 866.85 712.04 34.14 o 6 6 0 38.31 55.53 25.56 o 7 6 0 39.53 0.48 28.98 o 8 6 0 0.15 -2.64 42.75 o -14 7 0 17.41 48.64 42.93 o -13 7 0 194.95 239.33 50.98 o -12 7 0 126.42 127.51 41.50 o -11 7 0 368.14 369.35 41.23 o -10 7 0 1173.11 1022.14 52.15 o -9 7 0 14.14 13.55 26.84 o -8 7 0 448.67 416.77 20.24 o -7 7 0 60.12 24.10 16.43 o -6 7 0 158.98 140.82 18.74 o -5 7 0 1516.12 1583.55 50.83 o -4 7 0 3493.53 2792.77 74.36 o -3 7 0 31.44 23.96 32.22 o -2 7 0 1090.24 1375.73 64.45 o -1 7 0 2.84 9.09 10.21 o 0 7 0 4647.24 3977.14 900.44 o 1 7 0 767.01 567.75 20.21 o 2 7 0 1156.66 1250.81 34.23 o 3 7 0 92.62 93.81 22.63 o 4 7 0 275.87 222.66 26.55 o 5 7 0 2.47 3.60 28.43 o 6 7 0 162.84 170.80 30.53 o 7 7 0 315.83 400.22 66.91 o -14 8 0 106.24 -2.85 51.92 o -13 8 0 387.62 346.90 49.84 o -12 8 0 15.53 41.50 42.52 o -11 8 0 0.57 -21.06 33.76 o -10 8 0 22.44 3.38 31.45 o -9 8 0 46.82 36.38 30.97 o -8 8 0 56.82 7.02 19.78 o -7 8 0 47.93 43.78 16.31 o -6 8 0 286.14 297.11 22.83 o -5 8 0 2234.33 2270.12 57.01 o -4 8 0 3939.37 4004.90 92.54 o -3 8 0 580.16 559.38 58.66 o -2 8 0 4.77 -33.05 39.66 o -1 8 0 1975.71 1848.11 32.15 o 0 8 0 1076.44 1021.45 32.78 o 1 8 0 237.89 293.41 22.62 o 2 8 0 1081.87 1157.34 44.26 o 3 8 0 233.22 255.10 26.80 o 4 8 0 663.81 689.24 39.36 o 5 8 0 3.62 -15.29 53.12 o 6 8 0 6.76 2.84 54.79 o -14 9 0 208.94 158.32 51.18 o -13 9 0 143.50 167.09 48.18 o -12 9 0 234.78 216.95 42.96 o -11 9 0 796.87 689.39 45.21 o -10 9 0 0.83 -11.58 32.64 o -9 9 0 2505.70 2467.99 56.85 o -8 9 0 475.58 453.13 28.39 o -7 9 0 3771.76 3987.90 105.64 o -6 9 0 788.88 756.30 52.33 o -5 9 0 1405.44 1453.07 55.15 o -4 9 0 713.77 889.89 69.41 o -3 9 0 1555.68 1555.86 78.50 o -2 9 0 2380.77 2470.62 33.91 o -1 9 0 624.17 568.68 27.98 o 0 9 0 133.85 121.95 20.04 o 1 9 0 992.42 957.77 43.26 o 2 9 0 815.41 932.83 48.57 o 3 9 0 32.99 49.83 31.49 o 4 9 0 41.15 -16.05 52.25 o 5 9 0 12.20 -18.25 55.94 o -13 10 0 83.28 73.36 45.53 o -12 10 0 615.12 667.05 48.87 o -11 10 0 181.01 109.56 37.45 o -10 10 0 147.41 184.72 35.30 o -9 10 0 868.28 885.75 47.62 o -8 10 0 22.97 11.71 19.70 o -7 10 0 4283.41 4277.96 98.05 o -6 10 0 866.17 910.50 61.21 o -5 10 0 406.58 366.04 57.84 o -4 10 0 205.01 166.91 53.71 o -3 10 0 1094.49 1095.63 81.80 o -2 10 0 37.54 32.91 17.19 o -1 10 0 1402.01 1501.41 38.38 o 0 10 0 1195.06 1149.75 44.74 o 1 10 0 406.89 302.88 34.23 o 2 10 0 117.64 112.84 48.01 o 3 10 0 58.93 48.81 51.38 o 4 10 0 343.35 363.75 63.63 o -13 11 0 9.80 -26.62 45.30 o -12 11 0 14.50 -1.81 40.95 o -11 11 0 25.98 57.04 38.65 o -10 11 0 2.35 -4.96 33.01 o -9 11 0 31.41 12.74 30.90 o -8 11 0 388.44 325.91 22.07 o -7 11 0 280.72 322.02 45.84 o -6 11 0 1172.05 1128.59 52.69 o -5 11 0 2.55 -36.36 57.84 o -4 11 0 1738.20 1860.75 104.11 o -3 11 0 242.15 165.41 16.96 o -2 11 0 275.95 284.28 23.49 o -1 11 0 310.00 377.73 47.92 o 0 11 0 65.58 90.78 41.39 o 1 11 0 2172.63 2362.57 80.79 o 2 11 0 185.40 184.76 51.66 o 3 11 0 74.84 33.61 56.22 o -12 12 0 33.26 10.71 42.33 o -11 12 0 19.36 1.62 38.94 o -10 12 0 235.09 256.21 38.38 o -9 12 0 48.50 26.22 30.52 o -8 12 0 294.92 274.08 34.92 o -7 12 0 109.94 151.92 48.23 o -6 12 0 411.34 420.94 41.46 o -5 12 0 1358.13 1341.85 97.50 o -4 12 0 765.82 680.84 78.50 o -3 12 0 1112.28 1074.86 72.47 o -2 12 0 12.20 -6.43 35.12 o -1 12 0 189.08 237.69 43.03 o 0 12 0 80.06 59.00 46.75 o 1 12 0 5.32 30.37 51.20 o -11 13 0 9.05 58.01 40.97 o -10 13 0 9.72 23.12 36.66 o -9 13 0 11.59 36.20 30.53 o -8 13 0 33.42 22.77 24.70 o -7 13 0 0.14 14.91 48.45 o -6 13 0 110.10 147.54 41.30 o -5 13 0 71.27 20.66 70.23 o -4 13 0 471.83 447.34 37.69 o -3 13 0 25.64 29.35 34.58 o -2 13 0 302.43 335.56 44.44 o -1 13 0 121.19 95.56 68.58 o -10 14 0 31.60 4.05 37.04 o -9 14 0 285.53 250.78 33.90 o -8 14 0 265.99 212.77 54.69 o -7 14 0 365.74 444.36 60.69 o -6 14 0 46.72 20.07 44.83 o -5 14 0 76.16 145.42 87.58 o -4 14 0 661.35 601.22 51.64 o -3 14 0 0.55 8.58 40.72 o 3 -14 1 6.96 13.39 40.93 o 4 -14 1 116.26 120.87 68.17 o 5 -14 1 64.73 46.59 55.35 o 6 -14 1 80.66 36.02 44.78 o 7 -14 1 375.70 436.02 61.70 o 8 -14 1 38.06 73.38 56.27 o 9 -14 1 562.77 439.90 36.65 o 10 -14 1 12.94 -21.45 36.09 o 1 -13 1 43.70 19.36 45.15 o 2 -13 1 124.43 121.24 41.11 o 3 -13 1 19.10 2.76 34.07 o 4 -13 1 386.27 365.99 52.88 o 5 -13 1 130.13 157.72 49.24 o 6 -13 1 114.28 107.25 40.45 o 7 -13 1 29.54 9.21 50.56 o 8 -13 1 56.66 34.90 18.48 o 9 -13 1 8.94 -7.21 31.57 o 10 -13 1 46.46 46.37 36.75 o 11 -13 1 20.50 -5.97 39.90 o -1 -12 1 46.34 86.34 51.15 o 0 -12 1 138.78 122.01 48.42 o 1 -12 1 189.34 197.47 43.54 o 2 -12 1 32.76 14.78 34.08 o 3 -12 1 189.98 208.98 36.40 o 4 -12 1 38.11 72.71 67.75 o 5 -12 1 648.08 590.91 51.29 o 6 -12 1 374.40 400.90 41.39 o 7 -12 1 91.97 94.80 47.88 o 8 -12 1 1033.25 1032.89 38.16 o 9 -12 1 7.44 32.84 34.23 o 10 -12 1 18.66 14.23 35.52 o 11 -12 1 44.72 43.85 38.62 o 12 -12 1 169.04 167.83 43.97 o -3 -11 1 47.83 66.22 55.94 o -2 -11 1 58.05 43.39 51.20 o -1 -11 1 838.19 1001.33 69.70 o 0 -11 1 12.61 -4.59 39.04 o 1 -11 1 651.46 655.64 51.03 o 2 -11 1 485.62 491.02 30.60 o 3 -11 1 697.52 571.88 43.79 o 4 -11 1 862.07 824.61 87.58 o 5 -11 1 382.78 411.48 66.93 o 6 -11 1 281.14 270.20 35.59 o 7 -11 1 519.60 568.64 50.47 o 8 -11 1 35.30 28.72 19.42 o 9 -11 1 0.12 -2.67 30.00 o 10 -11 1 356.89 352.44 37.64 o 11 -11 1 153.89 173.06 38.49 o 12 -11 1 27.28 5.25 40.75 o 13 -11 1 6.57 12.24 45.36 o -4 -10 1 186.06 212.13 57.78 o -3 -10 1 236.42 269.83 52.01 o -2 -10 1 336.83 342.04 49.21 o -1 -10 1 1768.59 1694.01 52.15 o 0 -10 1 84.83 108.09 36.68 o 1 -10 1 1980.78 1929.36 40.66 o 2 -10 1 80.41 95.82 17.99 o 3 -10 1 172.30 200.78 56.19 o 4 -10 1 29.94 25.61 50.40 o 5 -10 1 564.24 560.80 43.13 o 6 -10 1 58.59 48.19 37.34 o 7 -10 1 1787.27 1680.10 73.10 o 8 -10 1 74.69 72.65 20.19 o 9 -10 1 42.71 15.51 29.91 o 10 -10 1 586.59 570.05 41.49 o 11 -10 1 321.04 318.61 42.98 o 12 -10 1 124.91 175.87 44.28 o 13 -10 1 296.26 278.88 51.51 o -5 -9 1 4.59 -3.26 55.57 o -4 -9 1 115.15 89.63 53.34 o -3 -9 1 95.36 70.66 46.73 o -2 -9 1 586.77 654.37 42.82 o -1 -9 1 1353.22 1192.10 44.48 o 0 -9 1 1084.82 1020.81 32.09 o 1 -9 1 64.82 42.48 18.82 o 2 -9 1 4511.93 4403.44 36.23 o 3 -9 1 2506.23 2487.88 90.06 o 4 -9 1 425.01 549.47 67.75 o 5 -9 1 2244.58 2270.73 61.89 o 6 -9 1 9.75 -5.93 32.98 o 7 -9 1 5575.63 5797.31 53.79 o 8 -9 1 48.85 27.36 19.79 o 9 -9 1 3017.89 2867.94 69.13 o 10 -9 1 91.96 107.65 33.41 o 11 -9 1 231.59 227.01 39.36 o 12 -9 1 211.55 232.30 43.92 o 13 -9 1 28.40 26.20 45.51 o -6 -8 1 13.84 -12.65 56.40 o -5 -8 1 13.34 -6.08 49.82 o -4 -8 1 578.74 642.63 34.85 o -3 -8 1 72.45 59.38 23.43 o -2 -8 1 1492.88 1479.04 45.15 o -1 -8 1 771.54 724.89 31.35 o 0 -8 1 439.37 360.70 19.75 o 1 -8 1 1473.37 1488.14 28.92 o 2 -8 1 3341.35 3716.54 96.67 o 3 -8 1 804.09 891.54 69.41 o 4 -8 1 11150.92 11071.12 141.29 o 5 -8 1 1114.94 1000.84 39.46 o 6 -8 1 63.51 70.37 17.23 o 7 -8 1 1037.43 1297.16 30.59 o 8 -8 1 9150.38 9788.44 160.05 o 9 -8 1 0.35 -6.34 27.70 o 10 -8 1 93.00 100.03 32.40 o 11 -8 1 80.90 79.35 36.98 o 12 -8 1 6.23 -9.68 40.11 o 13 -8 1 117.13 100.44 47.02 o 14 -8 1 151.43 148.14 44.16 o -7 -7 1 404.09 517.75 67.24 o -6 -7 1 21.94 20.75 52.12 o -5 -7 1 2.51 -12.66 26.92 o -4 -7 1 153.90 133.39 24.99 o -3 -7 1 101.05 92.41 21.49 o -2 -7 1 781.42 729.20 24.68 o -1 -7 1 557.54 423.82 19.38 o 0 -7 1 3019.58 2730.96 34.54 o 1 -7 1 105.50 205.24 13.98 o 2 -7 1 3398.03 3540.54 85.11 o 3 -7 1 100.95 133.85 36.36 o 4 -7 1 1322.93 1202.21 61.14 o 5 -7 1 50.87 39.74 25.41 o 6 -7 1 4.53 1.53 13.01 o 7 -7 1 2192.09 2314.49 36.42 o 8 -7 1 862.82 787.95 26.54 o 9 -7 1 420.97 456.86 36.79 o 10 -7 1 3607.50 3692.63 83.34 o 11 -7 1 93.25 115.54 38.03 o 12 -7 1 115.66 101.55 40.58 o 13 -7 1 50.29 36.39 40.36 o 14 -7 1 2.60 5.59 43.26 o -8 -6 1 0.57 14.00 44.57 o -7 -6 1 145.74 77.29 38.48 o -6 -6 1 37.94 36.36 25.31 o -5 -6 1 653.11 776.81 34.55 o -4 -6 1 0.92 -1.74 18.24 o -3 -6 1 821.22 668.65 26.46 o -2 -6 1 2242.45 2216.67 37.81 o -1 -6 1 7007.47 7272.96 65.32 o 0 -6 1 1214.92 1209.97 22.21 o 1 -6 1 2594.75 1272.27 1394.73 o 2 -6 1 14.97 12.39 28.09 o 3 -6 1 1172.90 1127.85 53.71 o 4 -6 1 10258.66 10559.41 283.42 o 5 -6 1 1594.92 1423.54 32.75 o 6 -6 1 4051.50 3048.95 55.10 o 7 -6 1 8.24 -6.03 12.02 o 8 -6 1 1225.85 1226.15 28.88 o 9 -6 1 1192.29 1176.22 37.58 o 10 -6 1 560.31 507.40 32.96 o 11 -6 1 33.14 24.45 29.44 o 12 -6 1 317.90 324.48 32.92 o 13 -6 1 28.94 17.37 33.61 o 14 -6 1 2.20 8.44 37.19 o -9 -5 1 6.86 8.03 44.21 o -8 -5 1 0.92 -27.98 28.57 o -7 -5 1 609.14 691.31 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