#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/60/2216008.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216008_Fobs loop_ _publ_author_name 'Sheng, Xia' 'Strasser, Christoph E.' 'Raubenheimer, H. G.' 'Luckay, Robert C.' _publ_section_title ; Isopropylammonium (isopropylamino)oxoacetate monohydrate ; _journal_coeditor_code HY2088 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4361 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 104.372 _cell_angle_beta 105.944 _cell_angle_gamma 94.731 _cell_length_a 7.1719 _cell_length_b 9.1535 _cell_length_c 9.4725 _exptl_crystal_F_000 228.00 _reflns_d_resolution_high 0.7967 _[local]_cod_data_source_file hy2088Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xm in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 80.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 107.06 103.25 2.97 o 2 0 0 1980.62 2147.92 33.32 o 3 0 0 140.47 150.25 3.70 o 4 0 0 173.82 185.08 4.28 o 5 0 0 111.48 116.64 3.17 o 6 0 0 19.39 19.67 1.08 o 7 0 0 5.90 7.55 0.85 o 8 0 0 31.16 30.36 2.26 o -8 1 0 0.35 2.21 0.97 o -7 1 0 0.32 1.21 0.59 o -6 1 0 27.09 20.14 1.11 o -5 1 0 73.87 84.88 2.57 o -4 1 0 297.50 319.80 5.67 o -3 1 0 200.56 196.80 3.57 o -2 1 0 11.86 8.48 0.46 o -1 1 0 434.88 490.71 6.61 o 0 1 0 285.63 309.19 4.16 o 1 1 0 761.90 653.25 8.72 o 2 1 0 548.91 538.40 8.63 o 3 1 0 178.64 184.16 6.98 o 4 1 0 211.66 184.99 3.95 o 5 1 0 5.82 6.35 0.59 o 6 1 0 5.21 4.91 0.66 o 7 1 0 4.68 4.52 1.07 o 8 1 0 88.10 83.21 3.48 o -8 2 0 4.64 5.50 0.82 o -7 2 0 358.33 325.44 6.33 o -6 2 0 50.87 44.71 1.93 o -5 2 0 0.23 0.39 0.39 o -4 2 0 0.11 0.56 0.31 o -3 2 0 505.18 586.52 9.61 o -2 2 0 1950.73 2295.95 30.13 o -1 2 0 21.70 28.94 0.61 o 0 2 0 795.98 835.72 11.07 o 1 2 0 227.94 191.58 2.74 o 2 2 0 1247.70 1244.10 27.48 o 3 2 0 133.96 140.99 3.12 o 4 2 0 3.58 4.39 0.33 o 5 2 0 314.57 265.53 16.32 o 6 2 0 44.67 46.57 3.85 o 7 2 0 5.99 5.72 1.20 o 8 2 0 7.50 8.26 1.33 o -8 3 0 16.97 24.19 1.36 o -7 3 0 183.96 172.28 3.90 o -6 3 0 37.02 36.51 1.44 o -5 3 0 285.20 281.65 11.29 o -4 3 0 117.27 112.71 2.47 o -3 3 0 175.78 173.24 2.67 o -2 3 0 158.23 156.18 2.40 o -1 3 0 0.10 -0.02 0.29 o 0 3 0 36.29 36.10 0.77 o 1 3 0 873.60 944.96 12.62 o 2 3 0 858.56 872.33 13.47 o 3 3 0 48.47 46.91 1.05 o 4 3 0 570.85 522.33 13.66 o 5 3 0 621.73 517.11 28.83 o 6 3 0 9.26 11.31 1.42 o 7 3 0 7.26 9.58 2.11 o -8 4 0 0.02 2.09 1.11 o -7 4 0 6.42 6.07 1.31 o -6 4 0 34.82 36.89 1.47 o -5 4 0 376.49 379.98 6.87 o -4 4 0 32.25 35.23 1.18 o -3 4 0 66.11 67.94 1.33 o -2 4 0 16.29 13.05 0.47 o -1 4 0 310.18 354.08 5.00 o 0 4 0 3.25 5.18 0.33 o 1 4 0 88.69 92.05 1.73 o 2 4 0 7.01 10.39 1.15 o 3 4 0 2.39 4.66 0.53 o 4 4 0 0.11 0.80 0.41 o 5 4 0 15.64 14.54 1.48 o 6 4 0 11.97 11.78 1.41 o 7 4 0 152.83 150.73 6.63 o -8 5 0 43.84 50.03 2.43 o -7 5 0 77.47 70.90 4.60 o -6 5 0 165.33 166.65 4.68 o -5 5 0 21.39 18.92 1.80 o -4 5 0 84.16 82.22 1.82 o -3 5 0 12.66 11.08 0.49 o -2 5 0 1521.24 1626.29 21.63 o -1 5 0 49.55 52.13 1.10 o 0 5 0 1.26 0.96 0.36 o 1 5 0 30.85 31.80 0.79 o 2 5 0 437.62 416.58 7.23 o 3 5 0 82.19 84.64 2.17 o 4 5 0 0.61 1.30 0.53 o 5 5 0 6.55 7.22 1.17 o 6 5 0 34.68 42.51 2.54 o -7 6 0 5.44 4.81 0.95 o -6 6 0 12.37 12.20 1.28 o -5 6 0 24.69 23.00 1.57 o -4 6 0 11.11 7.55 0.94 o -3 6 0 33.21 30.33 1.08 o -2 6 0 38.66 33.30 1.13 o -1 6 0 4.64 5.51 0.41 o 0 6 0 90.79 86.93 1.69 o 1 6 0 0.19 1.85 0.49 o 2 6 0 64.15 61.16 1.76 o 3 6 0 26.98 23.71 1.16 o 4 6 0 4.50 3.38 1.21 o 5 6 0 1.82 2.03 0.88 o 6 6 0 0.09 2.19 1.01 o -7 7 0 6.12 6.78 1.12 o -6 7 0 67.09 64.38 2.71 o -5 7 0 45.74 41.20 2.02 o -4 7 0 22.25 23.39 1.56 o -3 7 0 0.74 0.94 0.37 o -2 7 0 70.30 69.16 1.82 o -1 7 0 1.70 1.70 0.39 o 0 7 0 599.42 523.04 15.49 o 1 7 0 197.31 177.12 3.69 o 2 7 0 20.03 27.22 1.21 o 3 7 0 28.16 21.38 1.32 o 4 7 0 9.27 8.76 0.88 o 5 7 0 30.98 36.88 2.20 o -6 8 0 12.05 13.55 1.44 o -5 8 0 33.44 36.50 2.03 o -4 8 0 61.42 58.53 2.41 o -3 8 0 84.72 76.97 2.06 o -2 8 0 59.72 56.93 1.71 o -1 8 0 23.12 24.14 1.54 o 0 8 0 135.95 132.30 5.14 o 1 8 0 0.17 0.43 0.76 o 2 8 0 3.43 8.60 1.16 o 3 8 0 29.65 29.28 1.80 o 4 8 0 88.50 96.39 4.29 o -6 9 0 1.97 2.96 1.08 o -5 9 0 34.96 30.78 2.54 o -4 9 0 37.65 33.41 2.53 o -3 9 0 0.28 1.95 0.48 o -2 9 0 33.65 32.44 1.78 o -1 9 0 1.45 1.28 0.73 o 0 9 0 22.07 24.20 1.73 o 1 9 0 26.57 29.99 4.27 o 2 9 0 45.49 46.94 2.30 o 3 9 0 6.57 7.61 1.17 o -4 10 0 69.35 69.32 2.80 o -3 10 0 52.07 49.34 2.25 o -2 10 0 14.00 16.47 1.48 o -1 10 0 3.04 3.02 0.81 o 0 10 0 0.14 1.90 2.14 o 1 10 0 0.08 0.47 0.81 o 2 10 0 189.59 198.07 5.85 o -2 11 0 0.01 0.30 0.98 o -1 11 0 3.46 6.00 1.01 o 0 -11 1 58.33 58.50 2.70 o 1 -11 1 6.27 7.02 1.10 o 2 -11 1 1.32 2.56 0.94 o 3 -11 1 16.11 14.02 2.44 o -2 -10 1 30.84 31.97 4.22 o -1 -10 1 2.19 3.99 1.00 o 0 -10 1 0.19 1.09 0.69 o 1 -10 1 19.10 21.58 1.65 o 2 -10 1 29.19 31.03 2.03 o 3 -10 1 8.17 8.52 1.20 o 4 -10 1 0.01 -0.21 0.99 o -4 -9 1 1.38 2.12 0.85 o -3 -9 1 6.40 7.06 1.15 o -2 -9 1 34.37 31.49 2.26 o -1 -9 1 5.24 5.10 1.01 o 0 -9 1 12.27 13.83 1.36 o 1 -9 1 114.69 118.14 9.58 o 2 -9 1 0.02 0.63 0.42 o 3 -9 1 2.25 0.87 0.44 o 4 -9 1 61.12 55.49 2.54 o 5 -9 1 42.82 41.98 2.18 o 6 -9 1 30.02 35.28 2.04 o -4 -8 1 13.56 11.66 2.50 o -3 -8 1 26.89 30.89 1.80 o -2 -8 1 1.51 2.15 0.81 o -1 -8 1 87.35 85.69 3.26 o 0 -8 1 806.19 767.21 15.90 o 1 -8 1 84.11 81.17 3.45 o 2 -8 1 23.59 26.03 1.14 o 3 -8 1 30.79 25.58 1.14 o 4 -8 1 202.78 190.27 5.15 o 5 -8 1 46.53 40.05 2.07 o 6 -8 1 8.92 11.89 1.42 o -6 -7 1 23.74 33.58 2.69 o -5 -7 1 37.67 46.81 2.36 o -4 -7 1 9.85 11.52 2.13 o -3 -7 1 1.89 2.56 0.57 o -2 -7 1 1.57 0.20 0.70 o -1 -7 1 211.11 192.70 6.09 o 0 -7 1 18.21 21.33 0.94 o 1 -7 1 128.97 121.90 2.63 o 2 -7 1 5.30 7.21 0.68 o 3 -7 1 3.84 4.72 0.59 o 4 -7 1 2.55 4.66 0.91 o 5 -7 1 4.11 4.31 0.95 o 6 -7 1 47.56 47.07 2.73 o 7 -7 1 0.15 1.96 0.86 o -6 -6 1 49.00 57.35 2.92 o -5 -6 1 18.08 20.62 1.78 o -4 -6 1 32.55 33.09 1.36 o -3 -6 1 189.76 189.84 4.00 o -2 -6 1 252.33 226.31 4.34 o -1 -6 1 10.99 12.83 0.53 o 0 -6 1 294.24 288.13 5.02 o 1 -6 1 373.76 369.55 6.27 o 2 -6 1 64.12 73.68 1.80 o 3 -6 1 160.63 149.33 3.03 o 4 -6 1 32.57 32.06 1.67 o 5 -6 1 38.30 33.56 1.79 o 6 -6 1 149.13 128.04 4.00 o 7 -6 1 1.65 3.47 0.82 o -7 -5 1 4.57 6.86 1.27 o -6 -5 1 2.94 3.63 0.99 o -5 -5 1 22.08 25.69 1.74 o -4 -5 1 71.42 72.84 2.02 o -3 -5 1 17.74 17.18 0.85 o -2 -5 1 79.45 84.65 1.59 o -1 -5 1 268.34 265.46 3.94 o 0 -5 1 3.44 2.96 0.37 o 1 -5 1 111.74 108.58 2.22 o 2 -5 1 203.55 203.58 4.33 o 3 -5 1 25.80 22.89 0.68 o 4 -5 1 347.15 334.39 6.04 o 5 -5 1 142.02 133.05 4.19 o 6 -5 1 27.30 24.62 2.07 o 7 -5 1 31.38 35.27 1.97 o 8 -5 1 2.65 3.12 1.03 o -7 -4 1 49.97 51.69 3.74 o -6 -4 1 60.14 55.18 2.55 o -5 -4 1 103.14 103.71 5.00 o -4 -4 1 133.50 107.63 7.06 o -3 -4 1 156.39 162.58 5.20 o -2 -4 1 2.63 2.11 0.36 o -1 -4 1 1897.07 2038.00 26.89 o 0 -4 1 63.14 66.66 1.46 o 1 -4 1 74.59 74.02 1.59 o 2 -4 1 158.51 182.80 3.28 o 3 -4 1 52.71 51.43 1.09 o 4 -4 1 77.39 77.83 1.94 o 5 -4 1 143.35 134.31 3.86 o 6 -4 1 41.39 42.54 1.56 o 7 -4 1 26.42 24.26 1.86 o 8 -4 1 1.44 4.17 1.08 o -8 -3 1 11.29 13.68 1.71 o -7 -3 1 7.08 7.87 1.29 o -6 -3 1 339.59 319.02 8.12 o -5 -3 1 47.97 47.29 2.17 o -4 -3 1 95.51 89.49 3.19 o -3 -3 1 250.41 247.03 3.69 o -2 -3 1 516.64 497.17 6.96 o -1 -3 1 71.86 77.24 1.33 o 0 -3 1 212.50 214.41 3.57 o 1 -3 1 1718.33 1907.00 28.67 o 2 -3 1 1313.64 1497.71 19.85 o 3 -3 1 185.94 201.35 3.08 o 4 -3 1 63.61 58.33 3.46 o 5 -3 1 20.09 18.92 1.32 o 6 -3 1 10.49 12.84 0.97 o 7 -3 1 49.31 49.55 1.78 o 8 -3 1 0.58 1.53 0.64 o -8 -2 1 0.09 0.62 0.95 o -7 -2 1 4.44 5.94 1.15 o -6 -2 1 11.49 12.79 1.38 o -5 -2 1 191.05 172.84 6.32 o -4 -2 1 95.38 95.03 1.71 o -3 -2 1 13.72 15.24 0.52 o -2 -2 1 1471.81 1560.60 20.57 o -1 -2 1 100.19 74.80 1.23 o 0 -2 1 526.80 521.07 7.99 o 1 -2 1 250.32 275.53 4.42 o 2 -2 1 13.44 16.19 0.90 o 3 -2 1 90.46 79.74 2.44 o 4 -2 1 157.57 173.45 3.40 o 5 -2 1 16.15 14.65 0.92 o 6 -2 1 0.06 0.68 0.52 o 7 -2 1 130.36 119.84 4.23 o 8 -2 1 3.11 2.38 1.10 o -8 -1 1 48.68 53.94 2.66 o -7 -1 1 10.07 11.83 1.45 o -6 -1 1 316.14 280.68 5.38 o -5 -1 1 41.56 38.32 1.30 o -4 -1 1 23.98 26.17 0.95 o -3 -1 1 111.13 125.29 2.00 o -2 -1 1 368.77 399.87 8.01 o -1 -1 1 147.92 161.20 2.43 o 0 -1 1 299.20 315.41 4.28 o 1 -1 1 1481.14 1532.42 20.13 o 2 -1 1 849.34 802.74 10.71 o 3 -1 1 66.52 79.82 1.76 o 4 -1 1 500.81 487.67 14.24 o 5 -1 1 0.93 2.08 0.47 o 6 -1 1 221.13 196.62 4.73 o 7 -1 1 7.93 9.67 0.93 o 8 -1 1 21.91 23.09 3.92 o -8 0 1 0.18 2.34 0.98 o -7 0 1 3.13 4.68 0.80 o -6 0 1 73.88 72.90 2.06 o -5 0 1 47.38 46.49 2.29 o -4 0 1 777.53 842.04 13.64 o -3 0 1 134.24 139.77 2.66 o -2 0 1 3297.33 3382.80 67.57 o -1 0 1 0.12 -0.13 0.13 o 0 0 1 1082.32 1159.87 15.33 o 1 0 1 111.09 112.87 1.67 o 2 0 1 96.46 89.14 1.97 o 3 0 1 62.65 63.18 1.73 o 4 0 1 67.63 67.54 1.69 o 5 0 1 15.65 14.51 0.83 o 6 0 1 107.83 94.76 2.45 o 7 0 1 8.72 10.66 1.58 o 8 0 1 5.49 8.15 1.95 o -8 1 1 44.81 45.66 2.24 o -7 1 1 1.84 1.34 0.98 o -6 1 1 0.31 1.07 0.54 o -5 1 1 18.12 17.30 0.90 o -4 1 1 655.28 718.92 20.37 o -3 1 1 319.79 312.13 9.57 o -2 1 1 10.98 11.22 0.53 o -1 1 1 172.87 143.26 2.06 o 0 1 1 367.51 377.72 5.14 o 1 1 1 1484.80 1511.99 23.46 o 2 1 1 229.16 224.50 4.96 o 3 1 1 707.56 673.85 11.13 o 4 1 1 0.00 0.60 0.40 o 5 1 1 0.14 1.55 0.45 o 6 1 1 1.23 2.01 0.89 o 7 1 1 0.02 -0.29 0.94 o 8 1 1 78.15 78.53 3.41 o -8 2 1 0.59 0.74 0.76 o -7 2 1 63.69 61.26 2.01 o -6 2 1 78.81 74.46 2.47 o -5 2 1 0.51 0.84 0.41 o -4 2 1 216.49 218.96 4.09 o -3 2 1 119.60 144.66 2.79 o -2 2 1 9.18 7.65 0.35 o -1 2 1 1660.81 1764.77 23.23 o 0 2 1 484.62 475.45 6.45 o 1 2 1 706.27 735.59 11.74 o 2 2 1 487.24 481.28 12.58 o 3 2 1 43.62 45.21 1.29 o 4 2 1 0.93 0.82 0.38 o 5 2 1 264.08 223.36 5.98 o 6 2 1 174.35 150.76 10.64 o 7 2 1 101.25 93.01 3.65 o -8 3 1 2.54 2.84 0.83 o -7 3 1 112.96 101.92 2.75 o -6 3 1 16.62 20.42 1.28 o -5 3 1 0.03 0.48 0.45 o -4 3 1 111.62 112.30 2.46 o -3 3 1 51.89 53.55 1.08 o -2 3 1 329.13 343.38 4.86 o -1 3 1 383.56 397.71 5.52 o 0 3 1 1398.03 1500.49 19.85 o 1 3 1 1682.73 1769.01 43.10 o 2 3 1 580.53 618.73 10.20 o 3 3 1 56.90 54.48 2.34 o 4 3 1 66.07 59.98 1.71 o 5 3 1 349.11 319.67 7.99 o 6 3 1 10.84 12.11 2.83 o 7 3 1 5.52 5.70 1.34 o -8 4 1 3.17 4.42 0.78 o -7 4 1 3.04 4.56 0.70 o -6 4 1 20.92 23.36 1.25 o -5 4 1 685.70 652.88 11.06 o -4 4 1 8.24 12.30 0.95 o -3 4 1 39.22 41.48 0.96 o -2 4 1 80.61 81.51 1.49 o -1 4 1 291.29 321.00 4.62 o 0 4 1 86.88 84.19 1.50 o 1 4 1 1194.07 1271.66 20.25 o 2 4 1 202.16 170.32 3.40 o 3 4 1 557.10 571.77 13.74 o 4 4 1 45.39 42.75 1.50 o 5 4 1 148.27 133.18 4.30 o 6 4 1 5.42 7.24 1.28 o 7 4 1 6.15 5.79 1.30 o -8 5 1 0.03 1.38 0.94 o -7 5 1 50.64 49.82 2.29 o -6 5 1 340.21 321.54 6.17 o -5 5 1 244.86 231.93 4.60 o -4 5 1 72.46 69.45 1.46 o -3 5 1 10.96 15.08 0.59 o -2 5 1 710.48 748.75 10.29 o -1 5 1 0.04 0.31 0.29 o 0 5 1 256.76 267.25 4.01 o 1 5 1 1.88 3.07 0.47 o 2 5 1 76.11 68.95 2.08 o 3 5 1 30.18 31.68 1.31 o 4 5 1 23.91 25.08 1.95 o 5 5 1 7.05 7.49 1.24 o 6 5 1 98.43 126.98 5.90 o -7 6 1 30.54 40.84 4.56 o -6 6 1 90.34 90.57 3.19 o -5 6 1 95.04 92.78 4.79 o -4 6 1 34.32 36.22 1.19 o -3 6 1 26.68 25.31 0.80 o -2 6 1 23.61 24.70 0.77 o -1 6 1 0.78 1.54 0.60 o 0 6 1 22.31 26.01 1.29 o 1 6 1 48.68 45.25 1.48 o 2 6 1 0.65 3.05 0.72 o 3 6 1 2.53 3.61 1.00 o 4 6 1 30.05 40.54 1.58 o 5 6 1 45.02 52.55 2.56 o 6 6 1 163.04 167.95 7.17 o -7 7 1 37.76 36.28 2.04 o -6 7 1 4.19 9.87 1.22 o -5 7 1 1.06 1.16 1.36 o -4 7 1 245.47 217.89 5.51 o -3 7 1 161.53 148.58 3.13 o -2 7 1 81.87 80.11 2.02 o -1 7 1 979.60 945.32 19.04 o 0 7 1 231.48 205.52 4.14 o 1 7 1 7.35 6.90 1.37 o 2 7 1 18.17 18.07 2.54 o 3 7 1 5.05 5.16 0.81 o 4 7 1 118.23 108.77 2.94 o 5 7 1 14.23 25.86 2.08 o -6 8 1 9.79 9.98 1.27 o -5 8 1 18.61 11.40 1.27 o -4 8 1 54.88 52.09 2.26 o -3 8 1 53.34 51.07 1.95 o -2 8 1 162.54 149.47 4.19 o -1 8 1 153.18 156.27 4.41 o 0 8 1 91.77 84.50 3.99 o 1 8 1 11.28 12.04 1.81 o 2 8 1 6.17 7.75 1.17 o 3 8 1 20.44 14.33 2.06 o 4 8 1 0.45 1.73 0.80 o -6 9 1 1.36 0.73 0.69 o -5 9 1 19.81 22.25 1.73 o -4 9 1 0.08 0.15 0.69 o -3 9 1 145.84 136.94 6.05 o -2 9 1 32.19 33.29 1.83 o -1 9 1 18.18 20.57 1.62 o 0 9 1 56.02 57.79 3.15 o 1 9 1 188.71 176.03 5.08 o 2 9 1 19.64 20.31 1.74 o 3 9 1 0.60 2.82 0.90 o -4 10 1 11.30 15.99 2.51 o -3 10 1 23.13 24.80 1.63 o -2 10 1 29.32 31.57 1.86 o -1 10 1 22.43 26.52 1.93 o 0 10 1 82.94 87.54 3.34 o 1 10 1 1.38 3.54 0.99 o -1 -11 2 1.14 1.84 1.92 o 0 -11 2 0.94 2.29 0.97 o 1 -11 2 18.83 19.80 1.74 o 2 -11 2 17.94 21.48 1.72 o 3 -11 2 1.98 4.48 0.91 o -3 -10 2 29.70 32.41 2.04 o -2 -10 2 4.30 6.60 1.35 o -1 -10 2 24.59 31.93 2.08 o 0 -10 2 44.62 46.67 2.89 o 1 -10 2 0.02 -0.46 0.57 o 2 -10 2 77.33 70.56 2.09 o 3 -10 2 7.19 7.62 0.82 o 4 -10 2 14.61 14.34 2.41 o -4 -9 2 6.71 5.72 1.09 o -3 -9 2 6.37 13.50 1.38 o -2 -9 2 97.17 101.19 3.46 o -1 -9 2 1.65 2.45 1.10 o 0 -9 2 0.00 0.55 1.27 o 1 -9 2 90.04 86.28 2.26 o 2 -9 2 9.37 10.26 0.87 o 3 -9 2 75.73 67.96 2.00 o 4 -9 2 8.30 8.71 1.17 o 5 -9 2 10.06 10.95 1.33 o -4 -8 2 80.58 71.33 2.73 o -3 -8 2 0.27 0.80 0.76 o -2 -8 2 163.74 150.46 4.41 o -1 -8 2 126.81 119.46 5.91 o 0 -8 2 176.20 159.08 4.21 o 1 -8 2 554.52 524.64 8.84 o 2 -8 2 6.59 8.29 0.77 o 3 -8 2 231.01 208.03 4.17 o 4 -8 2 166.20 160.64 4.61 o 5 -8 2 14.38 15.54 1.46 o 6 -8 2 0.01 0.31 0.76 o -6 -7 2 43.13 48.12 2.47 o -5 -7 2 18.21 18.93 1.63 o -4 -7 2 74.78 68.68 2.32 o -3 -7 2 25.70 22.80 1.49 o -2 -7 2 38.60 43.94 1.96 o -1 -7 2 11.59 13.84 0.78 o 0 -7 2 49.90 48.61 2.06 o 1 -7 2 21.42 22.86 1.28 o 2 -7 2 10.79 10.78 0.77 o 3 -7 2 47.51 37.82 1.33 o 4 -7 2 7.56 6.89 1.73 o 5 -7 2 53.00 54.94 2.40 o 6 -7 2 29.25 31.68 1.94 o 7 -7 2 58.98 70.68 3.02 o -6 -6 2 117.91 134.02 10.01 o -5 -6 2 3.80 3.94 0.96 o -4 -6 2 183.37 174.84 3.73 o -3 -6 2 311.93 291.79 6.32 o -2 -6 2 0.00 1.19 0.65 o -1 -6 2 35.71 38.72 0.95 o 0 -6 2 166.13 166.92 3.22 o 1 -6 2 4.05 6.56 0.57 o 2 -6 2 61.03 62.47 1.63 o 3 -6 2 0.03 0.17 0.31 o 4 -6 2 8.93 8.39 1.58 o 5 -6 2 75.56 71.06 5.09 o 6 -6 2 158.71 147.03 4.47 o 7 -6 2 63.16 61.91 2.73 o -7 -5 2 16.40 19.55 1.73 o -6 -5 2 87.48 90.03 6.46 o -5 -5 2 32.23 33.98 1.88 o -4 -5 2 207.01 184.77 5.10 o -3 -5 2 51.23 50.97 1.56 o -2 -5 2 179.11 175.20 2.82 o -1 -5 2 90.14 86.25 1.66 o 0 -5 2 548.26 584.16 9.30 o 1 -5 2 103.60 105.42 2.18 o 2 -5 2 268.53 275.13 5.96 o 3 -5 2 18.81 20.91 0.86 o 4 -5 2 60.85 63.87 2.35 o 5 -5 2 887.32 880.55 21.84 o 6 -5 2 29.20 36.63 2.06 o 7 -5 2 35.79 39.71 2.50 o -7 -4 2 18.98 26.18 1.85 o -6 -4 2 10.80 14.38 1.87 o -5 -4 2 507.23 410.01 38.15 o -4 -4 2 3.74 6.20 1.14 o -3 -4 2 145.03 147.59 3.14 o -2 -4 2 1.06 1.40 0.24 o -1 -4 2 716.45 746.84 10.09 o 0 -4 2 95.13 108.16 2.12 o 1 -4 2 130.14 134.59 2.93 o 2 -4 2 157.82 154.63 2.89 o 3 -4 2 112.67 110.49 1.94 o 4 -4 2 0.42 0.22 0.37 o 5 -4 2 15.04 14.17 0.92 o 6 -4 2 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