#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/61/2216114.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216114_Fobs loop_ _publ_author_name 'Dahlenburg, Lutz' 'Menzel, Ralf' 'Heinemann, Frank W.' _publ_section_title ; (OC-6-13)-Bis(acetone)dihydridobis(tricyclohexylphosphine)iridium(III) tetrafluoridoborate acetone solvate ; _journal_coeditor_code SI2038 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2769 _journal_page_last m2770 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.060 _cell_angle_gamma 90.000 _cell_length_a 10.2180 _cell_length_b 25.1990 _cell_length_c 19.6210 _exptl_crystal_F_000 2112.00 _reflns_d_resolution_high 0.7401 _[local]_cod_data_source_file si2038Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ir(H)2(PCy3)2(Me2CO)2]BF4 * Me2CO in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 461.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 97506.39 98404.07 1311.53 o 3 0 0 71722.87 72783.88 861.84 o 4 0 0 29741.44 29027.96 308.88 o 5 0 0 105783.80 105938.20 1061.59 o 6 0 0 11999.11 12091.43 190.10 o 7 0 0 86103.51 84145.20 979.35 o 8 0 0 3532.12 3523.96 136.30 o 9 0 0 30611.77 30638.86 524.55 o 10 0 0 15864.79 15258.61 441.70 o 11 0 0 15645.57 14873.41 596.21 o 12 0 0 17034.36 17635.23 488.19 o 13 0 0 1751.67 1056.20 577.99 o 2 1 0 248.53 335.41 22.10 o 3 1 0 806.15 762.81 38.73 o 4 1 0 3501.53 3558.37 54.57 o 5 1 0 1880.20 1966.01 49.75 o 6 1 0 2974.75 3252.58 83.94 o 7 1 0 35.66 138.38 53.09 o 8 1 0 1539.16 1656.50 93.88 o 9 1 0 41.56 195.08 81.31 o 10 1 0 2329.05 2385.01 109.71 o 11 1 0 420.59 514.75 185.12 o 12 1 0 90.97 155.40 203.49 o 13 1 0 1201.64 1108.98 343.44 o 2 2 0 69261.92 70857.88 474.54 o 3 2 0 13644.28 13033.40 105.17 o 4 2 0 9338.22 9225.43 94.37 o 5 2 0 34556.78 34483.70 269.82 o 6 2 0 8729.21 8658.45 103.57 o 7 2 0 42544.64 41562.38 351.74 o 8 2 0 1519.24 1575.47 76.88 o 9 2 0 12065.84 11751.69 272.95 o 10 2 0 12855.22 12934.78 275.11 o 11 2 0 9098.88 9572.05 266.06 o 12 2 0 7710.49 8040.91 272.32 o 13 2 0 1678.14 1669.72 289.51 o 2 3 0 70231.47 71589.71 479.84 o 3 3 0 44536.61 45413.59 323.00 o 4 3 0 9246.61 9274.14 88.90 o 5 3 0 9460.51 9036.49 101.18 o 6 3 0 22626.43 22298.69 204.30 o 7 3 0 3786.26 3922.12 80.63 o 8 3 0 22505.54 22085.10 252.69 o 9 3 0 921.48 763.31 86.05 o 10 3 0 6379.19 6816.29 232.77 o 11 3 0 4030.49 4264.85 279.25 o 12 3 0 3062.29 3329.00 235.84 o 13 3 0 4811.39 4525.33 352.04 o 0 4 0 2569.26 1832.61 46.56 o 1 4 0 49.45 125.57 18.77 o 2 4 0 282.26 302.48 21.28 o 3 4 0 9002.79 9212.47 79.03 o 4 4 0 269.73 279.63 35.89 o 5 4 0 2648.47 2286.17 53.89 o 6 4 0 1525.76 1528.65 51.51 o 7 4 0 11827.28 11196.35 156.36 o 8 4 0 517.92 535.69 106.11 o 9 4 0 3032.84 3031.29 113.14 o 10 4 0 2298.85 2515.41 149.09 o 11 4 0 808.02 835.23 229.16 o 12 4 0 2223.69 2617.12 230.22 o 13 4 0 300.06 344.07 343.03 o 1 5 0 915.80 1096.33 23.37 o 2 5 0 6066.19 6007.02 63.39 o 3 5 0 41777.70 42856.64 307.67 o 4 5 0 12732.52 13217.05 125.07 o 5 5 0 18144.48 17552.94 160.74 o 6 5 0 31677.42 31618.07 298.06 o 7 5 0 606.09 623.13 68.07 o 8 5 0 38198.02 37629.66 450.76 o 9 5 0 761.06 764.83 112.87 o 10 5 0 5522.35 5672.31 189.72 o 11 5 0 4479.99 4599.03 212.37 o 12 5 0 3380.38 3224.92 278.91 o 13 5 0 6765.66 6928.33 581.06 o 0 6 0 29742.74 29224.78 297.66 o 1 6 0 3912.36 3978.42 46.66 o 2 6 0 1682.00 1782.99 32.85 o 3 6 0 12590.12 13088.83 111.11 o 4 6 0 1370.70 1630.15 50.56 o 5 6 0 913.81 1005.65 48.31 o 6 6 0 352.52 355.51 69.88 o 7 6 0 960.15 1050.59 73.17 o 8 6 0 91.19 383.53 89.37 o 9 6 0 314.80 479.93 119.96 o 10 6 0 115.71 211.02 147.59 o 11 6 0 27.27 151.44 158.27 o 12 6 0 69.09 333.52 387.95 o 13 6 0 1.79 -158.77 343.11 o 1 7 0 46532.14 48677.78 350.88 o 2 7 0 8733.22 9336.61 84.03 o 3 7 0 13088.23 12345.58 107.93 o 4 7 0 5052.70 4320.36 57.87 o 5 7 0 6708.58 6224.54 85.06 o 6 7 0 31018.92 30475.96 316.52 o 7 7 0 1052.61 1023.93 101.47 o 8 7 0 26240.14 25407.77 325.75 o 9 7 0 6021.47 5861.53 188.27 o 10 7 0 9926.59 9553.66 276.28 o 11 7 0 4403.98 4567.28 208.10 o 12 7 0 3622.50 3905.75 332.84 o 13 7 0 8345.71 8191.34 587.61 o 0 8 0 24602.56 24668.49 262.84 o 1 8 0 11.61 -18.19 36.62 o 2 8 0 17077.80 17664.09 141.74 o 3 8 0 10224.83 10870.46 100.82 o 4 8 0 6225.79 6213.65 71.65 o 5 8 0 10112.61 10221.20 113.33 o 6 8 0 10.47 -24.73 62.90 o 7 8 0 6926.48 6734.98 155.28 o 8 8 0 326.20 186.14 102.98 o 9 8 0 1476.38 1773.69 195.32 o 10 8 0 511.92 605.97 143.40 o 11 8 0 2304.51 2370.13 179.77 o 12 8 0 2813.10 3158.71 331.90 o 13 8 0 202.03 596.35 407.93 o 1 9 0 92691.14 94693.95 691.05 o 2 9 0 9680.08 9824.61 93.59 o 3 9 0 17664.56 17979.73 154.41 o 4 9 0 15951.91 15333.72 133.19 o 5 9 0 2696.37 2547.36 61.61 o 6 9 0 26112.73 26333.88 283.79 o 7 9 0 73.00 41.23 86.30 o 8 9 0 18269.24 18527.28 262.12 o 9 9 0 3452.91 3462.00 163.51 o 10 9 0 7416.69 7318.37 280.14 o 11 9 0 6211.21 6153.75 243.47 o 12 9 0 5359.62 5197.16 574.19 o 13 9 0 7122.35 7610.36 585.97 o 0 10 0 212619.59 223136.52 2125.77 o 1 10 0 426.49 420.41 42.72 o 2 10 0 48043.49 47178.98 341.57 o 3 10 0 29484.16 29912.06 238.38 o 4 10 0 4903.96 4493.58 68.81 o 5 10 0 29575.55 29219.03 245.75 o 6 10 0 4080.21 4040.01 88.42 o 7 10 0 41734.36 40884.37 436.19 o 8 10 0 908.60 801.52 107.05 o 9 10 0 12921.56 13069.14 249.59 o 10 10 0 11989.77 12062.84 273.87 o 11 10 0 3575.03 3965.23 282.59 o 12 10 0 11406.37 11888.25 553.82 o 1 11 0 9720.31 9091.49 95.32 o 2 11 0 8633.00 8709.81 95.40 o 3 11 0 5177.28 4823.07 68.91 o 4 11 0 1998.79 1974.16 58.34 o 5 11 0 1766.04 1827.16 68.61 o 6 11 0 12880.85 12754.56 166.66 o 7 11 0 181.03 110.96 92.31 o 8 11 0 10106.37 9896.86 200.38 o 9 11 0 348.98 322.13 153.28 o 10 11 0 990.76 664.32 221.96 o 11 11 0 4107.63 4141.94 585.75 o 12 11 0 466.14 784.09 635.34 o 0 12 0 82040.71 80681.20 803.15 o 1 12 0 11421.27 11393.10 114.39 o 2 12 0 39764.22 38696.75 300.06 o 3 12 0 20242.70 20122.36 176.31 o 4 12 0 12378.94 12351.70 140.98 o 5 12 0 44003.79 43992.68 413.58 o 6 12 0 8898.92 8908.84 135.64 o 7 12 0 45091.08 45008.08 480.97 o 8 12 0 1744.82 1774.18 117.50 o 9 12 0 21494.54 22310.51 361.42 o 10 12 0 14576.67 13432.33 735.34 o 11 12 0 7382.96 7800.79 386.30 o 12 12 0 10821.44 10062.05 432.11 o 1 13 0 1189.94 1505.29 49.91 o 2 13 0 1042.29 1087.75 59.16 o 3 13 0 861.95 802.75 48.48 o 4 13 0 88.40 3.71 51.54 o 5 13 0 26.19 0.71 70.23 o 6 13 0 980.25 920.81 71.31 o 7 13 0 5.42 -58.56 80.19 o 8 13 0 572.82 545.15 103.91 o 9 13 0 234.19 144.65 136.50 o 10 13 0 1268.41 1168.91 242.36 o 11 13 0 160.68 226.85 280.30 o 12 13 0 39.95 -27.54 406.08 o 0 14 0 53438.61 51393.55 725.02 o 1 14 0 1825.93 1665.65 54.69 o 2 14 0 12134.18 11279.14 121.61 o 3 14 0 23684.93 23106.75 214.66 o 4 14 0 6633.40 6278.08 132.87 o 5 14 0 6265.16 6133.32 122.86 o 6 14 0 5448.32 4967.30 103.58 o 7 14 0 24288.19 24820.60 301.71 o 8 14 0 1227.58 1120.98 118.43 o 9 14 0 12316.68 12345.23 430.42 o 10 14 0 6274.81 6108.80 345.29 o 11 14 0 4560.17 4265.17 308.49 o 12 14 0 6519.00 6710.94 396.39 o 1 15 0 1291.56 1140.67 58.58 o 2 15 0 2044.40 2181.87 71.63 o 3 15 0 12201.10 12122.30 199.49 o 4 15 0 2111.86 1922.12 78.78 o 5 15 0 4363.28 4624.23 110.02 o 6 15 0 5365.66 5162.27 128.36 o 7 15 0 283.82 209.88 93.83 o 8 15 0 11211.00 11089.50 244.44 o 9 15 0 87.54 169.39 174.39 o 10 15 0 5433.38 5009.46 295.84 o 11 15 0 1564.04 1246.46 270.25 o 12 15 0 2507.73 2736.14 349.22 o 0 16 0 67706.52 69839.14 967.20 o 1 16 0 84.42 74.74 65.70 o 2 16 0 4933.27 5063.07 132.66 o 3 16 0 314.35 339.67 80.47 o 4 16 0 4362.51 4282.91 101.39 o 5 16 0 6942.03 6596.57 146.69 o 6 16 0 991.03 1126.24 100.56 o 7 16 0 12582.75 12566.85 255.06 o 8 16 0 217.52 120.31 148.37 o 9 16 0 3835.68 4217.47 251.10 o 10 16 0 1948.22 2090.94 321.85 o 11 16 0 4593.29 5483.27 586.41 o 1 17 0 21022.07 21004.98 254.61 o 2 17 0 3111.96 3212.76 106.77 o 3 17 0 1111.46 1180.25 112.77 o 4 17 0 2250.57 2304.27 85.17 o 5 17 0 3960.79 4071.15 122.04 o 6 17 0 13913.78 14059.51 238.97 o 7 17 0 765.58 952.82 130.82 o 8 17 0 6454.10 6764.23 196.34 o 9 17 0 115.09 -128.02 202.51 o 10 17 0 7013.72 7164.75 374.18 o 11 17 0 1226.39 1086.48 348.29 o 0 18 0 484.26 481.47 164.81 o 1 18 0 978.01 1244.98 90.73 o 2 18 0 1181.93 1483.44 108.90 o 3 18 0 28.03 -71.49 70.94 o 4 18 0 849.16 857.75 81.44 o 5 18 0 962.75 979.41 108.67 o 6 18 0 960.84 1049.56 129.92 o 7 18 0 2221.46 2250.66 144.39 o 8 18 0 11.61 -141.67 217.36 o 9 18 0 718.16 931.01 207.27 o 10 18 0 1531.17 1542.22 306.79 o 11 18 0 509.78 129.64 336.97 o 1 19 0 18780.59 18991.12 247.65 o 2 19 0 4087.67 4205.41 123.67 o 3 19 0 15519.59 15822.39 216.14 o 4 19 0 15773.23 15745.24 227.44 o 5 19 0 9444.37 9121.07 187.78 o 6 19 0 19079.86 19015.48 280.69 o 7 19 0 818.07 827.45 162.51 o 8 19 0 15721.83 15523.48 320.86 o 9 19 0 2933.56 3108.39 265.21 o 10 19 0 5960.31 6350.94 360.82 o 11 19 0 5125.49 5691.58 418.95 o 0 20 0 899.42 1360.96 202.91 o 1 20 0 362.16 467.41 101.75 o 2 20 0 8061.71 8133.98 197.90 o 3 20 0 185.96 189.81 101.78 o 4 20 0 153.79 91.53 141.47 o 5 20 0 805.74 845.87 127.70 o 6 20 0 295.44 229.69 120.63 o 7 20 0 468.88 549.87 160.08 o 8 20 0 260.33 584.71 240.52 o 9 20 0 328.22 226.50 280.09 o 10 20 0 1054.22 1260.84 327.24 o 1 21 0 40298.77 40664.45 473.01 o 2 21 0 7275.71 6979.34 163.46 o 3 21 0 24851.64 25522.06 315.48 o 4 21 0 23774.61 24359.14 417.32 o 5 21 0 8061.81 7668.43 219.39 o 6 21 0 31066.30 31034.01 435.39 o 7 21 0 562.25 454.64 181.08 o 8 21 0 28854.04 29470.57 484.25 o 9 21 0 3237.89 3236.31 313.66 o 10 21 0 8594.58 8416.82 409.65 o 0 22 0 13105.63 13997.78 348.92 o 1 22 0 2234.26 2585.83 145.49 o 2 22 0 13483.78 13184.46 227.73 o 3 22 0 2849.88 3166.86 170.41 o 4 22 0 7840.60 7540.22 178.92 o 5 22 0 9269.89 9864.58 232.84 o 6 22 0 95.59 175.15 156.94 o 7 22 0 9967.79 10124.04 259.65 o 8 22 0 1639.27 1589.98 233.92 o 9 22 0 8019.89 7775.55 347.74 o 10 22 0 3810.86 3618.01 428.33 o 1 23 0 21823.36 21755.12 356.25 o 2 23 0 3058.44 3309.26 168.17 o 3 23 0 7398.54 7337.14 224.92 o 4 23 0 2917.74 3062.53 181.25 o 5 23 0 274.14 162.17 164.57 o 6 23 0 10336.33 10026.17 257.56 o 7 23 0 284.84 286.41 221.44 o 8 23 0 7479.14 7681.70 343.09 o 9 23 0 551.59 326.84 314.07 o 0 24 0 46151.53 43749.86 784.37 o 1 24 0 4198.62 4394.66 216.77 o 2 24 0 17397.01 17332.25 303.76 o 3 24 0 9135.92 8664.34 197.39 o 4 24 0 14131.64 13900.40 283.86 o 5 24 0 10641.56 10672.47 266.00 o 6 24 0 2903.57 2749.87 241.90 o 7 24 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3871.09 240.23 o 4 28 0 2874.40 2845.77 308.97 o 5 28 0 7351.34 6794.16 269.12 o 6 28 0 2657.94 1963.85 292.89 o 7 28 0 6734.78 6227.35 363.26 o 1 29 0 5874.13 5581.11 251.10 o 2 29 0 761.85 388.69 207.47 o 3 29 0 4758.53 4864.01 240.68 o 4 29 0 3815.32 3378.95 258.76 o 5 29 0 1530.97 1457.52 260.49 o 6 29 0 2696.93 2902.50 326.89 o 7 29 0 13.40 -250.67 318.80 o 0 30 0 5646.07 5034.71 387.96 o 1 30 0 49.16 -128.70 224.53 o 2 30 0 1175.53 1011.93 227.34 o 3 30 0 2140.50 2461.94 274.29 o 4 30 0 3402.08 3313.94 304.98 o 5 30 0 1017.69 734.17 303.95 o 6 30 0 598.77 656.89 303.28 o 1 31 0 19941.18 20483.28 402.12 o 2 31 0 5117.18 4851.48 265.13 o 3 31 0 14297.62 14521.27 365.52 o 4 31 0 10773.40 10060.25 381.85 o 5 31 0 2951.41 2463.85 313.63 o 0 32 0 611.37 302.06 372.58 o 1 32 0 1.58 737.67 252.46 o 2 32 0 91.35 469.68 266.04 o 3 32 0 672.15 681.70 317.03 o 4 32 0 537.36 223.17 318.33 o 1 33 0 20302.26 20019.60 442.12 o 2 33 0 2167.35 1763.54 314.11 o 3 33 0 8123.30 7496.85 348.60 o 0 34 0 5412.48 5973.10 527.25 o -13 1 1 13753.65 14193.95 450.48 o -12 1 1 8196.21 8435.97 292.43 o -11 1 1 16915.63 17282.56 410.95 o -10 1 1 17615.90 17920.38 264.36 o -9 1 1 1993.35 2003.52 93.85 o -8 1 1 33703.46 33310.56 345.48 o -7 1 1 23.88 13.96 50.05 o -6 1 1 68855.39 68929.43 592.97 o -5 1 1 16697.40 17203.34 160.78 o -4 1 1 35329.04 34945.98 320.86 o -3 1 1 46262.21 46215.84 394.69 o -2 1 1 5891.56 5986.31 64.31 o 2 1 1 16859.19 16960.94 122.47 o 3 1 1 34347.64 35032.18 261.25 o 4 1 1 41566.71 41309.49 320.85 o 5 1 1 2570.80 2281.76 49.12 o 6 1 1 58117.32 58508.50 471.67 o 7 1 1 1558.69 1517.19 67.60 o 8 1 1 39268.10 39062.61 397.50 o 9 1 1 12486.67 12226.80 221.40 o 10 1 1 11337.77 11235.47 237.50 o 11 1 1 19888.41 19968.34 434.92 o 12 1 1 631.13 634.91 221.49 o 13 1 1 15924.04 15781.26 532.60 o -13 2 1 792.00 786.02 316.25 o -12 2 1 3615.83 3395.89 281.42 o -11 2 1 2231.82 2061.55 232.85 o -10 2 1 2119.85 2447.67 184.42 o -9 2 1 4882.42 4651.67 128.64 o -8 2 1 611.81 550.70 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