#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:41:39 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181081 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/61/2216146.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216146_Fobs loop_ _publ_author_name 'Hu, Miao-Miao' 'Lv, Lu-Ping' 'Chen, Zhen-Hua' 'Zhou, Lin' 'Hu, Xian-Chao' _publ_section_title ; 3-Amino-6-chloropyridazinium chloride ; _journal_coeditor_code TK2198 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4292 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.763 _cell_angle_beta 75.980 _cell_angle_gamma 84.015 _cell_length_a 6.1543 _cell_length_b 6.4278 _cell_length_c 9.0298 _exptl_crystal_F_000 168.00 _reflns_d_resolution_high 0.8352 _cod_data_source_file tk2198Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p in C -1 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 47.23 40.17 0.66 o 2 0 0 0.66 0.42 0.10 o 3 0 0 395.27 400.21 4.14 o 4 0 0 490.62 477.41 3.98 o 5 0 0 111.63 109.56 2.06 o 6 0 0 9.74 10.17 0.32 o 7 0 0 57.21 59.97 1.37 o -7 1 0 2.13 0.79 0.13 o -6 1 0 235.64 235.74 5.10 o -5 1 0 131.82 125.06 1.60 o -4 1 0 10.12 9.14 0.19 o -3 1 0 145.45 130.80 1.26 o -2 1 0 2687.53 2159.65 37.20 o -1 1 0 1628.48 1508.58 54.59 o 1 1 0 401.28 437.45 7.70 o 2 1 0 1084.34 1086.35 18.69 o 3 1 0 753.32 706.61 14.21 o 4 1 0 297.92 301.96 4.37 o 5 1 0 208.87 215.78 2.31 o 6 1 0 92.76 97.33 1.59 o 7 1 0 21.53 22.23 0.79 o -6 2 0 2.67 2.19 0.53 o -5 2 0 20.54 19.80 0.44 o -4 2 0 243.57 234.21 2.91 o -3 2 0 387.13 355.93 3.69 o -2 2 0 665.09 704.08 8.32 o -1 2 0 137.24 140.91 2.14 o 0 2 0 1576.55 831.59 17.71 o 1 2 0 3444.37 2770.33 42.69 o 2 2 0 61.50 57.37 0.69 o 3 2 0 16.56 14.57 0.32 o 4 2 0 410.59 420.64 4.33 o 5 2 0 112.68 108.84 1.29 o 6 2 0 24.97 25.66 0.84 o 7 2 0 0.00 0.11 0.07 o -6 3 0 18.38 19.57 0.57 o -5 3 0 185.51 178.22 2.75 o -4 3 0 78.73 73.59 1.37 o -3 3 0 20.37 24.42 0.58 o -2 3 0 819.40 826.63 12.24 o -1 3 0 643.56 621.65 10.35 o 0 3 0 741.06 642.15 13.41 o 1 3 0 32.82 36.90 0.71 o 2 3 0 189.77 195.29 3.62 o 3 3 0 445.34 452.18 6.66 o 4 3 0 209.77 201.20 3.18 o 5 3 0 3.36 3.61 0.16 o 6 3 0 64.72 67.11 0.95 o -5 4 0 3.29 3.58 0.38 o -4 4 0 53.49 56.79 1.16 o -3 4 0 128.07 123.71 2.06 o -2 4 0 292.45 270.84 4.05 o -1 4 0 97.74 104.49 1.37 o 0 4 0 141.95 136.55 3.10 o 1 4 0 908.77 965.59 21.27 o 2 4 0 136.94 128.12 2.12 o 3 4 0 22.49 21.30 0.58 o 4 4 0 7.23 6.53 0.33 o 5 4 0 193.95 191.17 2.56 o 6 4 0 1.59 1.70 0.19 o -5 5 0 41.43 43.15 1.51 o -4 5 0 70.47 71.16 2.04 o -3 5 0 11.59 12.51 0.43 o -2 5 0 24.49 23.13 0.55 o -1 5 0 902.89 882.16 12.62 o 0 5 0 22.58 23.23 1.19 o 1 5 0 80.16 83.38 1.49 o 2 5 0 0.39 0.46 0.11 o 3 5 0 115.25 109.20 1.95 o 4 5 0 83.92 84.24 1.64 o 5 5 0 43.94 43.57 0.86 o -3 6 0 48.96 52.78 1.67 o -2 6 0 93.84 92.74 2.42 o -1 6 0 47.41 50.29 0.94 o 0 6 0 1.91 0.70 0.12 o 1 6 0 85.50 86.03 1.59 o 2 6 0 78.87 79.58 1.54 o 3 6 0 87.71 85.06 1.67 o 4 6 0 9.00 9.20 0.37 o -2 7 0 0.62 0.76 0.22 o -1 7 0 26.57 26.14 1.05 o 1 7 0 17.81 17.28 0.57 o 2 7 0 11.19 11.50 0.40 o 3 7 0 14.40 13.83 0.46 o -2 -7 1 9.84 9.37 0.44 o -1 -7 1 4.56 5.03 0.40 o 2 -7 1 35.56 39.35 1.39 o -4 -6 1 4.88 3.94 0.31 o -3 -6 1 1.76 1.75 0.20 o -2 -6 1 12.44 11.98 0.48 o -1 -6 1 13.55 13.29 0.33 o 0 -6 1 142.21 143.15 2.38 o 1 -6 1 7.97 7.76 0.28 o 2 -6 1 21.03 19.50 0.86 o 3 -6 1 4.18 4.43 0.43 o -5 -5 1 0.10 0.00 0.10 o -4 -5 1 0.73 0.67 0.15 o -3 -5 1 0.96 0.99 0.16 o -2 -5 1 15.98 18.08 0.56 o -1 -5 1 18.22 18.55 0.38 o 0 -5 1 4.40 3.68 0.13 o 1 -5 1 4.78 4.29 0.18 o 2 -5 1 1.83 1.31 0.21 o 3 -5 1 33.85 35.47 0.81 o 4 -5 1 28.05 24.38 1.02 o 5 -5 1 2.92 1.70 0.27 o -6 -4 1 12.70 12.86 0.42 o -5 -4 1 0.57 0.71 0.15 o -4 -4 1 1.51 1.06 0.15 o -3 -4 1 2.09 1.66 0.16 o -2 -4 1 61.91 65.52 1.24 o -1 -4 1 3.24 2.49 0.29 o 0 -4 1 110.49 123.30 1.37 o 1 -4 1 2.68 2.17 0.10 o 2 -4 1 40.66 38.29 0.75 o 3 -4 1 2.85 1.94 0.16 o 4 -4 1 3.62 3.11 0.23 o 5 -4 1 0.47 0.27 0.17 o -6 -3 1 7.12 6.15 0.23 o -5 -3 1 3.20 2.78 0.19 o -4 -3 1 4.86 4.75 0.27 o -3 -3 1 19.52 21.78 0.57 o -2 -3 1 343.81 369.40 5.47 o -1 -3 1 44.30 47.29 0.69 o 0 -3 1 33.19 33.46 0.59 o 1 -3 1 4.06 3.41 0.14 o 2 -3 1 8.89 9.95 0.25 o 3 -3 1 25.58 24.86 0.58 o 4 -3 1 24.26 24.29 0.63 o 5 -3 1 1.35 0.89 0.19 o 6 -3 1 0.93 0.89 0.10 o -6 -2 1 11.38 10.59 0.50 o -5 -2 1 39.72 39.56 0.68 o -4 -2 1 0.20 0.24 0.05 o -3 -2 1 3.24 4.42 0.15 o -2 -2 1 62.35 63.07 1.30 o -1 -2 1 10.43 13.75 0.27 o 0 -2 1 30.42 31.84 0.56 o 1 -2 1 923.14 998.88 21.12 o 2 -2 1 159.36 192.56 2.37 o 3 -2 1 50.30 57.00 0.82 o 4 -2 1 3.85 3.40 0.16 o 5 -2 1 5.02 4.96 0.21 o 6 -2 1 6.68 7.18 0.42 o -6 -1 1 0.79 0.34 0.08 o -5 -1 1 36.03 34.78 0.67 o -4 -1 1 1.23 0.59 0.12 o -3 -1 1 10.57 11.84 0.19 o -2 -1 1 13.56 18.76 0.82 o -1 -1 1 2797.33 2423.84 29.66 o 0 -1 1 1187.17 1036.11 23.54 o 1 -1 1 2.53 5.96 0.23 o 2 -1 1 98.45 105.14 1.65 o 3 -1 1 22.74 22.76 0.29 o 4 -1 1 13.21 12.21 0.20 o 5 -1 1 19.20 19.14 0.38 o 6 -1 1 56.26 57.95 1.09 o 7 -1 1 17.86 19.02 0.75 o -6 0 1 0.39 0.14 0.04 o -5 0 1 4.81 5.37 0.22 o -4 0 1 0.07 0.05 0.04 o -3 0 1 20.09 20.76 0.31 o -2 0 1 114.18 130.54 2.03 o -1 0 1 23.83 29.32 1.02 o 0 0 1 4.69 3.61 0.06 o 1 0 1 18.99 15.39 0.25 o 2 0 1 196.56 186.86 13.03 o 3 0 1 52.03 53.93 0.74 o 4 0 1 80.98 89.26 0.83 o 5 0 1 11.80 11.55 0.27 o 6 0 1 35.42 39.91 0.78 o 7 0 1 11.03 11.40 0.37 o -6 1 1 1.48 0.80 0.12 o -5 1 1 6.52 6.86 0.20 o -4 1 1 18.35 20.00 0.32 o -3 1 1 167.34 176.00 1.67 o -2 1 1 6.24 5.04 0.24 o -1 1 1 1614.46 1486.45 57.67 o 0 1 1 566.06 535.72 8.43 o 1 1 1 157.70 169.16 2.95 o 2 1 1 12.73 15.56 0.28 o 3 1 1 68.79 75.18 0.76 o 4 1 1 2.49 3.99 0.11 o 5 1 1 11.14 11.05 0.23 o 6 1 1 0.60 0.23 0.05 o 7 1 1 2.30 2.02 0.24 o -6 2 1 6.67 7.55 0.44 o -5 2 1 3.40 3.97 0.20 o -4 2 1 30.61 32.58 0.57 o -3 2 1 258.07 270.25 4.22 o -2 2 1 83.03 101.46 1.13 o -1 2 1 362.64 391.75 12.69 o 0 2 1 9.41 15.33 0.46 o 1 2 1 0.75 1.35 0.10 o 2 2 1 177.39 175.25 1.67 o 3 2 1 120.48 125.74 1.40 o 4 2 1 79.70 88.46 1.04 o 5 2 1 2.04 2.21 0.12 o 6 2 1 6.05 6.16 0.23 o 7 2 1 5.13 5.43 0.38 o -6 3 1 0.57 0.42 0.11 o -5 3 1 0.50 0.20 0.06 o -4 3 1 4.52 4.74 0.42 o -3 3 1 84.10 86.24 1.50 o -2 3 1 33.79 33.86 0.68 o -1 3 1 0.31 0.28 0.05 o 0 3 1 512.63 563.48 11.77 o 1 3 1 171.83 217.28 3.26 o 2 3 1 102.08 109.47 1.24 o 3 3 1 4.61 4.87 0.20 o 4 3 1 28.83 27.52 0.54 o 5 3 1 0.96 0.70 0.07 o 6 3 1 8.55 7.94 0.25 o -5 4 1 3.13 4.30 0.43 o -4 4 1 11.61 12.24 0.45 o -3 4 1 26.19 25.02 0.63 o -2 4 1 146.37 147.63 2.35 o -1 4 1 15.56 18.44 0.43 o 0 4 1 83.25 81.06 0.95 o 1 4 1 69.62 81.97 1.12 o 2 4 1 30.02 30.63 0.56 o 3 4 1 32.29 30.32 0.58 o 4 4 1 29.47 29.23 0.60 o 5 4 1 55.22 55.47 0.96 o 6 4 1 19.91 18.33 0.50 o -4 5 1 1.31 0.57 0.20 o -3 5 1 34.62 35.98 0.83 o -2 5 1 39.85 39.48 0.83 o -1 5 1 6.10 5.64 0.34 o 0 5 1 0.08 0.15 0.16 o 1 5 1 9.20 8.05 0.22 o 2 5 1 37.35 36.64 0.93 o 3 5 1 1.32 0.93 0.15 o 4 5 1 2.91 2.45 0.18 o 5 5 1 13.36 12.56 0.41 o -3 6 1 16.38 15.49 0.80 o -2 6 1 17.63 17.35 0.82 o -1 6 1 34.66 31.77 0.76 o 0 6 1 57.09 56.89 1.60 o 1 6 1 42.65 39.43 0.72 o 2 6 1 0.04 0.00 0.07 o 3 6 1 0.20 0.43 0.11 o 4 6 1 13.72 14.59 0.45 o 5 6 1 0.05 0.00 0.11 o -2 7 1 27.38 28.90 1.16 o -1 7 1 21.43 19.61 0.89 o 1 7 1 0.40 0.31 0.17 o 2 7 1 19.81 18.56 0.59 o 3 7 1 0.26 0.04 0.09 o -2 -7 2 13.11 13.00 0.76 o -1 -7 2 18.83 23.02 0.73 o 0 -7 2 12.05 11.78 0.71 o -4 -6 2 30.37 31.60 1.28 o -3 -6 2 21.68 23.43 0.75 o -2 -6 2 20.91 22.39 0.70 o -1 -6 2 9.34 9.21 0.29 o 0 -6 2 51.26 53.45 0.87 o 1 -6 2 96.25 99.81 1.80 o 2 -6 2 22.95 22.40 0.91 o 3 -6 2 7.78 7.13 0.52 o -5 -5 2 17.61 19.99 0.96 o -4 -5 2 23.11 21.98 0.71 o -3 -5 2 2.90 1.82 0.20 o -2 -5 2 55.12 54.43 0.89 o -1 -5 2 12.69 11.36 0.30 o 0 -5 2 534.03 540.93 6.51 o 1 -5 2 51.78 53.13 0.83 o 2 -5 2 36.46 39.27 0.82 o 3 -5 2 124.42 120.73 2.06 o 4 -5 2 61.32 64.26 1.88 o 5 -5 2 0.08 0.31 0.17 o -5 -4 2 0.04 0.11 0.11 o -4 -4 2 16.98 16.04 0.56 o -3 -4 2 32.71 30.97 0.78 o -2 -4 2 355.31 358.74 5.41 o -1 -4 2 30.23 32.15 0.56 o 0 -4 2 125.24 135.53 1.50 o 1 -4 2 333.10 337.56 3.52 o 2 -4 2 137.24 136.04 1.80 o 3 -4 2 39.08 41.35 0.87 o 4 -4 2 0.01 0.19 0.14 o 5 -4 2 160.14 152.28 3.61 o -6 -3 2 0.50 0.73 0.19 o -5 -3 2 52.74 53.22 0.90 o -4 -3 2 100.28 104.94 1.87 o -3 -3 2 33.75 33.17 0.76 o -2 -3 2 0.30 0.18 0.08 o -1 -3 2 488.27 493.26 5.12 o 0 -3 2 287.42 272.30 2.88 o 1 -3 2 839.87 875.06 8.86 o 2 -3 2 102.93 118.97 1.90 o 3 -3 2 188.09 184.85 3.35 o 4 -3 2 342.43 318.80 7.62 o 5 -3 2 40.94 43.81 0.95 o 6 -3 2 5.61 5.11 0.36 o -6 -2 2 14.03 14.65 0.61 o -5 -2 2 88.83 87.25 1.27 o -4 -2 2 0.53 0.62 0.06 o -3 -2 2 38.17 35.38 0.58 o -2 -2 2 778.25 765.04 9.04 o -1 -2 2 842.34 816.81 7.59 o 0 -2 2 22.30 23.11 0.32 o 1 -2 2 993.30 1049.84 15.81 o 2 -2 2 575.67 535.09 7.69 o 3 -2 2 350.07 336.64 3.51 o 4 -2 2 13.74 14.22 0.28 o 5 -2 2 6.78 6.21 0.28 o 6 -2 2 226.15 228.46 4.99 o -6 -1 2 33.02 34.77 1.05 o -5 -1 2 68.61 67.68 1.19 o -4 -1 2 170.41 180.30 6.36 o -3 -1 2 236.49 239.80 2.27 o -2 -1 2 61.29 66.97 0.69 o -1 -1 2 21.62 21.53 0.36 o 0 -1 2 1452.05 1457.79 15.44 o 1 -1 2 2396.80 2142.51 31.86 o 2 -1 2 206.37 202.77 3.44 o 3 -1 2 52.83 53.55 0.73 o 4 -1 2 354.24 344.95 3.62 o 5 -1 2 611.18 622.04 7.41 o 6 -1 2 6.14 6.42 0.24 o 7 -1 2 0.08 0.01 0.06 o -6 0 2 22.66 24.21 0.56 o -5 0 2 98.38 97.75 1.60 o -4 0 2 49.78 50.13 0.73 o -3 0 2 2.63 2.52 0.13 o -2 0 2 9.29 13.22 0.19 o -1 0 2 11350.33 6346.75 81.41 o 0 0 2 90.81 98.25 1.08 o 1 0 2 28.57 35.68 0.51 o 2 0 2 885.44 852.20 24.49 o 3 0 2 1004.64 958.77 9.90 o 4 0 2 197.93 185.29 1.61 o 5 0 2 13.54 16.64 2.09 o 6 0 2 164.15 173.15 2.67 o 7 0 2 38.50 41.04 0.83 o -6 1 2 18.24 21.58 0.79 o -5 1 2 0.03 0.00 0.03 o -4 1 2 21.40 19.26 0.39 o -3 1 2 807.82 794.05 8.47 o -2 1 2 330.71 339.66 3.16 o -1 1 2 0.16 0.80 0.04 o 0 1 2 476.30 494.03 10.09 o 1 1 2 1302.54 1225.31 17.24 o 2 1 2 1095.96 1055.58 17.09 o 3 1 2 692.71 730.76 6.03 o 4 1 2 658.51 685.94 6.95 o 5 1 2 249.73 250.31 2.36 o 6 1 2 110.11 110.53 1.49 o 7 1 2 0.16 0.08 0.06 o -6 2 2 6.85 7.32 0.45 o -5 2 2 59.72 59.54 0.96 o -4 2 2 82.95 75.60 1.21 o -3 2 2 139.11 145.59 2.13 o -2 2 2 98.44 99.73 1.32 o -1 2 2 608.53 609.67 11.84 o 0 2 2 3413.88 2663.11 63.45 o 1 2 2 4.28 3.13 0.10 o 2 2 2 106.79 114.92 1.13 o 3 2 2 840.40 840.38 9.90 o 4 2 2 292.05 285.53 2.99 o 5 2 2 49.57 51.80 0.70 o 6 2 2 0.19 0.26 0.06 o 7 2 2 75.57 73.89 1.88 o -5 3 2 8.14 7.75 0.28 o -4 3 2 0.52 0.44 0.11 o -3 3 2 251.58 245.73 3.77 o -2 3 2 352.80 343.44 5.08 o -1 3 2 284.18 286.24 3.00 o 0 3 2 89.37 102.01 1.12 o 1 3 2 278.40 282.13 3.77 o 2 3 2 679.31 685.62 12.86 o 3 3 2 336.63 328.69 3.96 o 4 3 2 13.51 13.75 0.35 o 5 3 2 262.43 264.37 3.31 o 6 3 2 88.37 90.37 1.15 o 7 3 2 5.68 5.62 0.28 o -5 4 2 20.10 18.52 0.88 o -4 4 2 34.30 31.53 0.80 o -3 4 2 81.34 78.53 1.45 o -2 4 2 31.65 32.72 0.71 o -1 4 2 159.38 158.83 2.47 o 0 4 2 761.52 793.70 6.91 o 1 4 2 149.27 137.84 1.36 o 2 4 2 7.50 9.09 0.22 o 3 4 2 33.04 32.22 0.60 o 4 4 2 486.56 470.65 5.66 o 5 4 2 3.81 3.71 0.28 o 6 4 2 21.94 22.92 0.56 o -4 5 2 0.28 0.64 0.19 o -3 5 2 10.10 9.94 0.40 o -2 5 2 617.21 594.91 8.68 o -1 5 2 3.00 3.12 0.18 o 0 5 2 33.90 36.50 0.56 o 1 5 2 10.66 9.36 0.30 o 2 5 2 194.94 194.80 2.50 o 3 5 2 142.56 144.39 1.96 o 4 5 2 79.79 80.40 1.25 o 5 5 2 60.54 59.36 1.50 o 6 5 2 12.21 12.75 0.51 o -3 6 2 29.60 27.60 1.13 o -2 6 2 11.79 12.11 0.70 o -1 6 2 0.43 0.24 0.13 o 0 6 2 108.81 109.33 1.78 o 1 6 2 83.20 84.05 1.48 o 2 6 2 113.86 108.83 2.31 o 3 6 2 46.81 42.17 0.80 o 4 6 2 21.93 20.87 0.54 o 5 6 2 27.60 28.75 0.82 o -2 7 2 18.82 16.95 0.88 o -1 7 2 72.35 72.09 2.08 o 0 7 2 4.15 4.27 0.42 o 1 7 2 2.16 2.32 0.28 o 2 7 2 31.96 29.71 0.84 o 3 7 2 23.67 25.57 1.57 o 0 -7 3 2.57 2.25 0.33 o -3 -6 3 0.43 0.28 0.20 o -2 -6 3 0.36 0.41 0.14 o -1 -6 3 149.75 148.06 3.64 o 0 -6 3 5.04 4.48 0.31 o 1 -6 3 6.89 5.27 0.46 o 2 -6 3 3.71 4.24 0.40 o 3 -6 3 19.08 22.26 0.96 o -4 -5 3 0.80 0.57 0.14 o -3 -5 3 29.24 29.21 0.83 o -2 -5 3 20.12 19.23 0.46 o -1 -5 3 0.07 0.12 0.08 o 0 -5 3 7.66 8.52 0.28 o 1 -5 3 13.69 15.34 0.45 o 2 -5 3 73.70 84.38 1.25 o 3 -5 3 26.31 22.24 0.91 o 4 -5 3 31.22 28.54 1.10 o -5 -4 3 5.68 4.87 0.49 o -4 -4 3 6.06 5.65 0.42 o -3 -4 3 17.99 17.83 0.45 o -2 -4 3 12.47 11.52 0.33 o -1 -4 3 124.86 126.94 1.72 o 0 -4 3 42.07 44.37 0.72 o 1 -4 3 15.15 13.38 0.62 o 2 -4 3 6.85 8.03 0.25 o 3 -4 3 68.29 68.10 1.05 o 4 -4 3 10.22 13.40 0.47 o -5 -3 3 0.18 0.19 0.06 o -4 -3 3 1.21 1.45 0.14 o -3 -3 3 197.73 189.54 2.49 o -2 -3 3 8.54 7.77 0.25 o -1 -3 3 32.31 31.65 0.55 o 0 -3 3 15.51 17.15 0.35 o 1 -3 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0.52 o 3 4 9 75.73 75.81 1.82 o 4 4 9 14.90 18.15 1.26 o 1 5 9 19.36 21.25 1.08 o 2 5 9 24.16 25.79 1.20 o 0 -1 10 3.16 2.43 0.21 o 1 -1 10 2.23 2.01 0.15 o 2 -1 10 24.24 24.13 0.48 o 3 -1 10 2.12 1.28 0.23 o 0 0 10 1.89 0.98 0.32 o 1 0 10 0.05 0.00 0.03 o 2 0 10 15.21 16.04 0.31 o 3 0 10 2.62 2.90 0.13 o 4 0 10 1.73 1.05 0.15 o -1 1 10 4.91 5.23 0.29 o 0 1 10 0.27 0.29 0.11 o 1 1 10 11.34 11.48 0.32 o 2 1 10 0.14 0.14 0.05 o 3 1 10 9.24 8.76 0.27 o 4 1 10 20.10 19.61 0.43 o 0 2 10 1.68 2.00 0.27 o 1 2 10 1.40 0.97 0.20 o 2 2 10 12.63 12.94 0.33 o 3 2 10 7.75 8.54 0.27 o 4 2 10 6.06 6.36 0.24 o 0 3 10 34.56 35.40 0.70 o 1 3 10 11.58 10.11 0.34 o 2 3 10 25.61 27.30 0.59 o 3 3 10 3.86 4.01 0.20 o