#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:42:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181082 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/62/2216201.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216201_Fobs loop_ _publ_author_name 'Liu, T.' 'Zhu, J. Y.' _publ_section_title ; Tetrakis(pyridine-\kN)bis(thiocyanato-\kN)vanadium(II) ; _journal_coeditor_code AT2459 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2912 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.981 _cell_angle_gamma 90.000 _cell_length_a 12.5011 _cell_length_b 13.0026 _cell_length_c 14.9986 _exptl_crystal_F_000 996.00 _reflns_d_resolution_high 0.7941 _cod_data_source_file at2459Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aa in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 328.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3456.57 4371.51 78.69 o 6 0 0 4308.20 4193.53 56.81 o 8 0 0 1674.78 1834.44 28.85 o 10 0 0 2350.96 2529.11 39.37 o 12 0 0 391.17 395.73 13.28 o 14 0 0 173.72 147.98 24.57 o 3 1 0 7516.59 5714.20 52.34 o 5 1 0 1200.53 871.55 10.24 o 7 1 0 1155.96 1005.69 12.49 o 9 1 0 66.09 73.16 4.32 o 11 1 0 0.09 -2.90 3.75 o 13 1 0 51.66 67.12 6.28 o 15 1 0 5.34 5.98 6.62 o 2 2 0 26705.17 30613.85 294.41 o 4 2 0 19241.66 20316.23 163.38 o 6 2 0 14563.89 14759.62 137.28 o 8 2 0 1876.32 2054.69 38.13 o 10 2 0 633.27 688.51 11.15 o 12 2 0 264.98 281.32 8.31 o 14 2 0 172.27 165.21 8.17 o 1 3 0 28671.81 27136.76 364.08 o 3 3 0 499.27 359.50 4.38 o 5 3 0 40.12 40.06 2.61 o 7 3 0 3607.81 2939.35 26.30 o 9 3 0 0.70 -1.20 2.97 o 11 3 0 74.97 51.75 5.06 o 13 3 0 7.64 4.55 5.14 o 2 4 0 26786.19 28026.49 310.91 o 4 4 0 18505.45 18959.73 152.58 o 6 4 0 2026.96 2406.95 21.69 o 8 4 0 3652.51 3908.95 39.21 o 10 4 0 162.31 199.35 6.50 o 12 4 0 465.97 455.02 10.56 o 14 4 0 335.71 388.06 13.32 o 1 5 0 341.84 265.25 3.35 o 3 5 0 1.46 1.28 1.73 o 5 5 0 66.74 63.03 2.60 o 7 5 0 240.14 269.75 17.03 o 9 5 0 845.71 812.07 12.35 o 11 5 0 186.66 206.08 8.42 o 13 5 0 24.18 27.09 6.22 o 0 6 0 204.15 408.04 6.61 o 2 6 0 9125.18 8816.13 72.17 o 4 6 0 1677.06 1761.05 18.69 o 6 6 0 264.80 429.38 6.51 o 8 6 0 2173.20 2342.25 29.82 o 10 6 0 1138.96 1204.62 16.78 o 12 6 0 460.36 479.43 11.38 o 14 6 0 146.95 122.20 8.33 o 1 7 0 2330.20 1720.06 16.00 o 3 7 0 2131.61 1921.08 18.10 o 5 7 0 1552.66 1258.52 14.87 o 7 7 0 856.29 838.41 12.08 o 9 7 0 77.80 84.29 5.13 o 11 7 0 49.82 68.45 6.18 o 13 7 0 3.67 5.60 6.42 o 0 8 0 1917.67 1925.24 23.19 o 2 8 0 1312.79 1542.01 13.75 o 4 8 0 1075.28 1222.83 14.70 o 6 8 0 983.33 1087.24 15.28 o 8 8 0 165.81 189.67 19.19 o 10 8 0 1182.29 1285.72 17.95 o 12 8 0 468.91 551.89 12.64 o 1 9 0 189.51 183.88 5.27 o 3 9 0 77.63 79.38 4.47 o 5 9 0 180.67 167.81 6.54 o 7 9 0 0.33 -0.84 4.49 o 9 9 0 10.69 17.13 9.62 o 11 9 0 32.22 36.41 8.62 o 0 10 0 4722.27 4764.27 66.38 o 2 10 0 156.60 116.13 9.73 o 4 10 0 796.08 932.02 13.52 o 6 10 0 1644.53 1714.25 32.83 o 8 10 0 309.40 280.10 16.61 o 10 10 0 294.44 258.56 17.87 o 1 11 0 64.35 94.24 5.27 o 3 11 0 69.08 59.90 6.88 o 5 11 0 207.80 221.87 11.17 o 7 11 0 150.20 160.25 11.99 o 9 11 0 92.35 91.08 13.47 o 11 11 0 2.95 6.94 9.55 o 0 12 0 208.70 252.68 10.30 o 2 12 0 558.57 578.30 13.79 o 4 12 0 391.69 431.48 18.35 o 6 12 0 555.14 594.78 13.62 o 8 12 0 216.61 192.67 15.94 o 10 12 0 103.78 69.68 14.73 o 1 13 0 198.76 219.70 12.59 o 3 13 0 35.21 43.08 5.13 o 5 13 0 26.98 44.28 6.52 o 7 13 0 7.47 2.47 7.96 o 9 13 0 11.70 9.38 11.30 o 0 14 0 188.91 167.75 13.53 o 2 14 0 692.54 773.23 16.63 o 4 14 0 219.17 226.94 31.43 o 6 14 0 15.56 3.80 7.18 o 1 15 0 14.29 21.45 6.04 o 3 15 0 0.00 -1.42 5.83 o 5 15 0 7.19 9.44 7.83 o 0 16 0 152.54 142.64 20.90 o 2 16 0 199.22 225.97 9.57 o -15 1 1 304.93 311.59 12.68 o -13 1 1 323.37 353.53 9.84 o -11 1 1 227.88 280.19 7.63 o -9 1 1 6323.80 6343.83 60.94 o -7 1 1 826.56 1213.55 14.18 o -5 1 1 8478.14 9011.03 82.14 o -3 1 1 35095.63 39802.50 363.37 o -1 1 1 28386.69 34897.69 925.28 o 1 1 1 13088.17 15975.00 144.15 o 5 1 1 641.87 194.39 5.59 o 9 1 1 3240.81 3107.12 32.50 o 11 1 1 41.69 53.61 5.33 o 13 1 1 263.18 247.17 8.47 o -14 2 1 4.41 8.71 5.55 o -12 2 1 285.86 300.39 8.59 o -10 2 1 1040.97 1028.63 14.33 o -8 2 1 199.23 161.91 4.86 o -6 2 1 555.03 402.66 6.87 o -4 2 1 1873.19 1432.22 11.80 o -2 2 1 28122.96 26295.39 405.01 o 0 2 1 1974.31 1444.32 13.77 o 2 2 1 8669.40 7115.55 57.67 o 4 2 1 196.31 139.26 2.56 o 6 2 1 2072.81 1723.72 14.49 o 8 2 1 369.81 321.57 12.13 o 10 2 1 292.39 274.72 7.31 o 12 2 1 78.97 74.19 5.67 o 14 2 1 10.77 8.22 6.32 o -15 3 1 125.80 111.02 8.20 o -13 3 1 378.46 405.67 13.62 o -11 3 1 420.71 459.01 9.57 o -9 3 1 1259.65 1547.42 20.73 o -7 3 1 9726.42 9713.16 79.91 o -5 3 1 9706.63 10290.83 83.79 o -1 3 1 2573.06 3531.49 37.54 o 1 3 1 15253.72 16732.64 165.53 o 3 3 1 9105.85 9802.45 79.48 o 5 3 1 8738.75 8585.16 70.32 o 7 3 1 421.06 483.23 7.91 o 9 3 1 23.25 10.13 3.40 o 11 3 1 743.79 777.61 12.85 o 13 3 1 171.78 115.81 10.69 o -14 4 1 9.02 9.70 6.24 o -12 4 1 0.38 0.95 4.67 o -10 4 1 215.83 177.74 6.11 o -8 4 1 2.08 5.49 2.98 o -6 4 1 484.73 453.84 6.03 o -4 4 1 144.82 121.66 2.90 o -2 4 1 4067.51 3249.33 24.96 o 0 4 1 1512.94 1158.34 10.74 o 2 4 1 3433.97 2768.94 23.68 o 4 4 1 9132.79 7854.03 64.55 o 6 4 1 417.20 346.98 5.25 o 8 4 1 75.41 82.99 5.58 o 10 4 1 92.02 76.38 4.95 o 12 4 1 115.01 121.71 6.48 o 14 4 1 4.01 5.60 6.56 o -13 5 1 356.46 365.80 10.46 o -11 5 1 2464.42 2734.82 30.75 o -9 5 1 307.53 208.12 6.13 o -7 5 1 3031.19 3296.96 29.33 o -5 5 1 1400.53 1797.98 16.89 o -3 5 1 6693.34 7446.99 61.24 o -1 5 1 7014.53 7153.67 53.36 o 3 5 1 3649.33 4433.84 41.79 o 5 5 1 6529.46 6369.06 53.27 o 7 5 1 621.74 737.25 14.22 o 9 5 1 88.11 106.04 5.03 o 11 5 1 1426.46 1447.31 23.35 o 13 5 1 179.82 156.56 8.20 o -14 6 1 13.96 19.32 6.76 o -12 6 1 66.18 70.08 6.47 o -10 6 1 0.10 0.38 3.99 o -8 6 1 0.14 -0.19 3.10 o -6 6 1 339.41 300.36 5.39 o -4 6 1 3424.42 2867.20 25.45 o -2 6 1 4521.54 3551.46 30.55 o 0 6 1 5073.86 4002.67 30.84 o 2 6 1 3447.20 2931.96 25.60 o 4 6 1 586.45 515.20 7.52 o 6 6 1 611.98 616.60 8.06 o 8 6 1 220.57 233.38 12.15 o 10 6 1 0.34 2.44 4.28 o 12 6 1 3.81 10.82 5.77 o -13 7 1 187.92 177.50 8.60 o -11 7 1 446.76 488.84 10.90 o -9 7 1 593.02 660.09 11.21 o -7 7 1 555.15 686.27 9.10 o -5 7 1 852.21 1054.87 14.90 o -3 7 1 1815.89 1935.12 20.34 o -1 7 1 2658.54 3067.91 24.37 o 1 7 1 246.66 406.68 6.06 o 3 7 1 1596.28 1605.79 15.60 o 5 7 1 1339.30 1580.80 20.45 o 7 7 1 2493.72 2657.65 32.24 o 9 7 1 1033.83 1041.78 18.39 o 11 7 1 799.19 817.91 17.19 o 13 7 1 97.03 60.37 8.64 o -12 8 1 0.02 1.33 5.63 o -10 8 1 495.35 590.17 21.10 o -8 8 1 159.66 148.65 9.75 o -6 8 1 0.61 -0.01 3.00 o -4 8 1 22.78 12.24 2.82 o -2 8 1 67.00 45.58 2.67 o 0 8 1 1998.93 1744.09 16.84 o 2 8 1 605.26 463.55 7.47 o 4 8 1 28.54 25.98 3.01 o 6 8 1 198.93 184.01 5.50 o 8 8 1 13.01 9.89 5.64 o 10 8 1 81.31 87.51 8.18 o 12 8 1 23.22 17.16 8.33 o -11 9 1 90.49 69.83 15.00 o -9 9 1 1396.43 1529.89 27.98 o -7 9 1 1.11 8.17 3.74 o -5 9 1 176.58 272.24 6.64 o -3 9 1 2079.90 2249.85 24.39 o -1 9 1 274.81 383.43 7.21 o 1 9 1 2655.84 2798.93 29.71 o 3 9 1 2351.71 2613.64 24.49 o 5 9 1 301.82 367.24 10.07 o 7 9 1 706.83 675.03 15.70 o 9 9 1 1169.42 1278.80 36.07 o 11 9 1 93.51 59.72 8.95 o -12 10 1 3.51 3.80 9.60 o -10 10 1 26.28 23.14 11.30 o -8 10 1 3.23 -0.12 7.87 o -6 10 1 34.86 31.62 4.99 o -4 10 1 2.94 5.17 3.32 o -2 10 1 1655.32 1391.22 17.09 o 0 10 1 72.05 54.15 4.64 o 2 10 1 1472.00 1296.64 16.27 o 4 10 1 203.45 211.78 6.41 o 6 10 1 7.57 7.11 4.73 o 8 10 1 57.30 36.73 10.28 o 10 10 1 13.85 18.03 11.66 o -11 11 1 77.62 64.05 22.27 o -9 11 1 404.86 464.89 21.55 o -7 11 1 231.96 234.13 26.75 o -5 11 1 765.05 812.65 21.80 o -3 11 1 574.08 673.57 16.03 o -1 11 1 12.99 20.80 3.68 o 1 11 1 380.89 449.88 8.93 o 3 11 1 1727.61 1804.24 21.54 o 5 11 1 813.74 786.25 14.84 o 7 11 1 412.21 409.98 13.88 o 9 11 1 336.11 313.19 18.78 o -10 12 1 11.70 11.54 11.66 o -8 12 1 285.42 323.72 18.29 o -6 12 1 4.54 1.48 5.51 o -4 12 1 135.08 153.56 11.41 o -2 12 1 116.21 133.27 5.82 o 0 12 1 158.83 181.88 6.33 o 2 12 1 2.01 2.32 3.99 o 4 12 1 17.20 21.39 4.79 o 6 12 1 12.42 19.82 6.21 o 8 12 1 0.53 0.66 10.58 o -9 13 1 47.08 13.52 11.60 o -7 13 1 276.00 277.02 10.85 o -5 13 1 381.94 398.50 11.94 o -3 13 1 98.66 111.96 6.17 o -1 13 1 1046.39 1129.56 22.56 o 1 13 1 881.65 934.38 19.30 o 3 13 1 12.50 5.43 4.58 o 5 13 1 451.02 435.79 12.38 o 7 13 1 104.51 85.88 14.73 o -8 14 1 35.23 25.12 12.44 o -6 14 1 0.73 -0.82 7.10 o -4 14 1 17.18 14.65 6.34 o -2 14 1 2.74 -0.54 4.95 o 0 14 1 5.97 13.49 5.15 o 2 14 1 0.77 3.26 4.99 o 4 14 1 4.00 6.07 6.64 o 6 14 1 3.19 7.26 6.80 o -5 15 1 104.80 96.10 9.24 o -3 15 1 141.36 124.02 8.85 o -1 15 1 396.37 405.71 11.68 o 1 15 1 176.31 177.40 7.94 o 3 15 1 70.92 42.65 6.50 o 5 15 1 125.49 140.67 9.73 o -2 16 1 54.64 89.04 9.51 o 0 16 1 23.91 34.49 8.16 o 2 16 1 20.26 27.43 8.30 o -14 0 2 403.16 383.86 15.15 o -12 0 2 1083.48 1214.72 33.29 o -10 0 2 33.11 63.95 6.16 o -8 0 2 2302.48 2486.49 36.82 o -6 0 2 5346.69 5462.74 72.55 o -2 0 2 5885.10 7512.69 78.03 o 0 0 2 21716.06 27040.00 491.71 o 2 0 2 33148.11 25783.09 267.65 o 6 0 2 3760.72 3719.70 71.11 o 8 0 2 89.69 129.03 6.61 o 10 0 2 855.35 944.15 51.34 o 12 0 2 30.85 18.62 6.61 o 14 0 2 161.75 126.41 13.35 o -15 1 2 6.42 9.73 6.76 o -13 1 2 9.75 13.23 5.12 o -11 1 2 228.06 206.36 9.40 o -9 1 2 383.58 281.82 6.63 o -7 1 2 1886.67 1643.69 15.55 o -5 1 2 7193.74 6061.28 58.58 o -3 1 2 10509.50 8441.00 76.03 o 1 1 2 1616.65 1203.08 13.46 o 3 1 2 16608.62 14091.13 138.44 o 5 1 2 584.70 519.71 5.44 o 7 1 2 748.52 609.71 9.17 o 9 1 2 62.52 48.79 4.00 o 11 1 2 28.78 23.95 4.43 o 13 1 2 45.65 44.35 6.25 o -14 2 2 185.62 176.76 8.16 o -12 2 2 337.05 312.71 10.30 o -10 2 2 1011.04 1131.65 15.37 o -8 2 2 2003.88 2042.01 22.16 o -6 2 2 5726.26 6341.43 53.10 o 0 2 2 4084.74 5312.81 48.55 o 6 2 2 65.80 141.43 2.92 o 8 2 2 1041.98 1137.01 14.54 o 10 2 2 426.86 407.28 14.38 o 12 2 2 106.74 81.32 5.83 o 14 2 2 150.99 125.66 10.29 o -15 3 2 20.86 28.19 7.26 o -13 3 2 1.77 5.98 5.04 o -11 3 2 712.13 672.88 18.94 o -9 3 2 1475.56 1231.93 15.59 o -7 3 2 72.22 73.39 4.20 o -5 3 2 4649.50 3717.51 28.86 o -3 3 2 0.37 -1.39 1.06 o -1 3 2 2950.67 2279.47 21.69 o 1 3 2 14625.08 12387.25 99.45 o 3 3 2 111.56 93.82 2.62 o 5 3 2 763.26 665.21 7.46 o 7 3 2 660.04 544.42 20.63 o 9 3 2 1372.53 1340.84 30.80 o 11 3 2 46.07 59.26 4.99 o 13 3 2 60.07 69.25 6.53 o -14 4 2 266.20 238.62 9.12 o -12 4 2 177.52 161.44 6.77 o -10 4 2 514.38 585.24 11.73 o -8 4 2 789.47 998.06 18.99 o -6 4 2 47.20 9.21 1.81 o -4 4 2 13138.72 13401.57 108.54 o 2 4 2 22576.52 23609.29 209.79 o 4 4 2 6.38 76.32 2.77 o 6 4 2 238.79 374.70 8.43 o 8 4 2 283.54 378.54 11.18 o 10 4 2 226.47 213.62 9.69 o 12 4 2 700.34 716.59 13.46 o 14 4 2 221.25 212.68 9.76 o -13 5 2 4.09 10.67 5.30 o -11 5 2 134.65 150.36 7.46 o -9 5 2 18.63 16.05 3.58 o -7 5 2 1097.96 979.81 10.47 o -5 5 2 325.58 302.78 6.79 o -3 5 2 1.17 0.61 1.37 o -1 5 2 241.78 200.76 4.50 o 1 5 2 1640.61 1302.07 13.16 o 3 5 2 1168.15 1043.47 14.50 o 5 5 2 474.38 408.90 6.50 o 7 5 2 496.86 460.96 9.63 o 9 5 2 10.78 7.72 3.77 o 11 5 2 44.24 61.30 5.69 o 13 5 2 16.80 13.00 6.46 o -14 6 2 86.59 62.31 7.33 o -12 6 2 115.65 100.44 6.52 o -10 6 2 859.43 880.83 13.48 o -8 6 2 327.08 451.40 8.87 o -6 6 2 59.81 172.76 7.54 o -4 6 2 5677.00 6045.14 50.71 o -2 6 2 1741.57 2040.98 18.62 o 2 6 2 5469.49 5708.54 47.61 o 4 6 2 1648.10 1989.92 20.73 o 6 6 2 2350.27 2558.88 26.29 o 8 6 2 1311.99 1265.12 25.44 o 10 6 2 57.82 44.08 4.92 o 12 6 2 305.73 284.68 9.60 o -13 7 2 11.66 10.12 6.31 o -11 7 2 71.91 82.12 10.52 o -9 7 2 617.35 639.64 10.97 o -7 7 2 0.99 3.02 2.81 o -5 7 2 792.36 629.47 18.59 o -3 7 2 709.16 518.80 7.36 o -1 7 2 1519.74 1333.88 11.76 o 1 7 2 889.15 593.62 6.40 o 3 7 2 690.02 532.27 8.45 o 5 7 2 0.93 0.01 2.74 o 7 7 2 856.79 791.56 13.17 o 9 7 2 206.26 263.34 10.53 o 11 7 2 86.76 119.72 12.68 o 13 7 2 1.63 -1.96 7.54 o -12 8 2 360.99 390.62 11.73 o -10 8 2 560.20 557.89 12.56 o -8 8 2 16.35 36.05 4.26 o -6 8 2 938.94 1039.31 13.61 o -4 8 2 21.37 94.68 4.72 o -2 8 2 3704.68 3971.95 34.71 o 0 8 2 3460.99 3652.95 32.13 o 2 8 2 324.62 481.63 7.00 o 4 8 2 3037.33 3092.65 42.55 o 6 8 2 397.28 475.61 11.82 o 8 8 2 857.09 848.51 26.62 o 10 8 2 569.07 655.89 20.58 o 12 8 2 51.64 16.90 9.51 o -11 9 2 0.11 1.15 6.13 o -9 9 2 13.12 6.25 6.29 o -7 9 2 4.70 6.62 3.66 o -5 9 2 0.65 -0.64 3.07 o -3 9 2 54.11 71.13 3.45 o -1 9 2 320.90 292.07 5.54 o 1 9 2 695.15 638.53 8.52 o 3 9 2 30.08 23.61 2.94 o 5 9 2 1.98 1.27 3.91 o 7 9 2 14.46 13.51 5.84 o 9 9 2 10.02 6.73 8.71 o 11 9 2 11.89 14.65 8.98 o -12 10 2 169.77 172.01 12.27 o -10 10 2 36.79 13.09 7.07 o -8 10 2 403.34 422.27 13.19 o -6 10 2 900.66 996.55 16.58 o -4 10 2 12.93 24.37 4.18 o -2 10 2 950.73 1101.74 26.87 o 0 10 2 2935.84 3064.59 35.73 o 2 10 2 45.08 66.27 4.11 o 4 10 2 1944.96 2072.75 23.64 o 6 10 2 802.25 804.03 14.80 o 8 10 2 15.24 14.30 9.68 o 10 10 2 348.28 347.51 20.28 o -11 11 2 63.25 81.71 15.12 o -9 11 2 3.67 8.95 10.76 o -7 11 2 32.13 25.67 5.57 o -5 11 2 92.48 88.75 6.28 o -3 11 2 22.71 13.99 3.85 o -1 11 2 13.12 12.89 3.46 o 1 11 2 23.13 32.42 3.93 o 3 11 2 241.58 232.79 9.55 o 5 11 2 136.21 130.96 6.94 o 7 11 2 100.58 99.30 8.71 o 9 11 2 66.75 77.07 13.47 o -10 12 2 58.35 38.89 13.83 o -8 12 2 394.61 343.14 19.02 o -6 12 2 310.76 352.82 11.21 o -4 12 2 714.66 707.08 14.45 o -2 12 2 89.46 97.96 6.25 o 0 12 2 584.03 616.43 11.03 o 2 12 2 676.42 670.36 11.64 o 4 12 2 248.81 246.74 8.51 o 6 12 2 325.04 330.62 10.70 o 8 12 2 151.14 162.12 15.21 o -9 13 2 0.01 3.43 12.38 o -7 13 2 12.13 16.56 6.75 o -5 13 2 0.09 3.31 5.85 o -3 13 2 78.39 95.84 6.00 o -1 13 2 56.19 63.40 5.25 o 1 13 2 168.65 195.33 7.15 o 3 13 2 12.21 21.06 4.97 o 5 13 2 1.56 8.22 6.34 o 7 13 2 6.58 14.42 11.42 o -8 14 2 156.36 126.58 15.64 o -6 14 2 65.45 36.51 9.13 o -4 14 2 566.70 617.30 14.94 o -2 14 2 198.44 161.98 8.04 o 0 14 2 158.08 131.21 6.84 o 2 14 2 464.22 533.39 11.69 o 4 14 2 6.66 0.54 8.92 o 6 14 2 120.26 106.31 11.89 o -5 15 2 2.26 0.49 7.68 o -3 15 2 3.38 -1.53 6.77 o -1 15 2 7.72 7.73 6.55 o 1 15 2 9.62 8.87 6.95 o 3 15 2 0.00 1.52 6.57 o 5 15 2 23.93 34.11 11.24 o -2 16 2 181.46 171.37 14.09 o 0 16 2 81.02 67.69 9.07 o 2 16 2 103.41 72.21 8.96 o -15 1 3 415.76 428.24 11.89 o -13 1 3 148.88 133.57 6.78 o -11 1 3 880.98 860.46 13.12 o -9 1 3 2654.34 2632.59 27.96 o -7 1 3 40.75 138.18 3.66 o -5 1 3 8877.01 8816.02 71.82 o 5 1 3 9.56 59.74 3.15 o 7 1 3 4129.11 4135.60 40.81 o 9 1 3 822.53 882.32 12.97 o 11 1 3 126.59 149.01 13.04 o 13 1 3 329.03 329.13 10.63 o -14 2 3 55.09 65.86 6.69 o -12 2 3 73.41 79.76 7.68 o -10 2 3 965.60 875.93 12.80 o -8 2 3 720.50 620.49 9.32 o -6 2 3 670.46 477.47 5.41 o -4 2 3 3671.02 2902.46 22.58 o -2 2 3 5837.58 4395.88 48.21 o 0 2 3 38854.09 37650.26 390.27 o 2 2 3 4497.06 3472.62 37.33 o 4 2 3 15.51 20.45 2.52 o 6 2 3 257.32 175.45 3.46 o 8 2 3 167.26 175.99 8.09 o 10 2 3 169.87 176.06 8.51 o 12 2 3 49.46 54.78 5.80 o 14 2 3 0.36 -0.91 6.81 o -15 3 3 51.26 14.65 6.69 o -13 3 3 568.70 557.34 11.97 o -11 3 3 280.33 283.02 7.81 o -9 3 3 1086.70 1142.86 14.72 o -7 3 3 4814.25 4697.85 36.52 o -3 3 3 2090.54 2594.66 22.41 o -1 3 3 5884.95 6785.71 55.21 o 1 3 3 82.51 21.38 1.40 o 3 3 3 2666.62 3385.45 32.05 o 5 3 3 3245.54 3458.29 29.95 o 7 3 3 963.03 1173.37 14.60 o 9 3 3 431.81 493.78 9.44 o 11 3 3 538.33 589.68 11.52 o 13 3 3 147.21 128.25 7.68 o -14 4 3 0.31 0.05 5.60 o -12 4 3 3.59 8.17 4.80 o -10 4 3 4.98 6.66 3.60 o -8 4 3 264.32 262.06 12.22 o -6 4 3 816.37 611.30 6.77 o -4 4 3 480.77 438.34 5.65 o -2 4 3 224.63 215.26 3.45 o 0 4 3 3890.82 3295.87 30.33 o 2 4 3 8450.93 7417.86 60.64 o 4 4 3 1115.25 1034.71 11.73 o 6 4 3 1024.27 796.84 9.20 o 8 4 3 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