#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/62/2216224.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216224_Fobs loop_ _publ_author_name 'Tutughamiarso, Maya' 'Bolte, Michael' _publ_section_title ; Dimethyl 3,4-dihydroxy-1H-pyrrole-2,5-dicarboxylate ; _journal_coeditor_code AT2487 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4742 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.080 _cell_angle_gamma 90.000 _cell_length_a 10.1782 _cell_length_b 12.4456 _cell_length_c 7.1922 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8212 _[local]_cod_data_source_file at2487Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MT4 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 124.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1836.43 1692.88 30.22 o 3 0 0 20.65 23.78 3.65 o 4 0 0 5153.12 4802.57 187.52 o 5 0 0 3882.11 4051.79 133.83 o 6 0 0 6.90 1.12 2.44 o 7 0 0 397.47 394.29 16.98 o 8 0 0 1023.27 1140.47 32.94 o 9 0 0 138.44 128.86 7.24 o 10 0 0 1026.05 1024.03 99.12 o 11 0 0 40.19 37.33 2.65 o 12 0 0 34.27 37.16 5.15 o 2 1 0 737.69 622.69 14.42 o 3 1 0 840.47 754.68 11.65 o 4 1 0 1911.09 1646.27 61.14 o 5 1 0 717.99 658.95 21.47 o 6 1 0 75.28 64.18 2.78 o 7 1 0 0.48 2.38 1.92 o 8 1 0 344.29 355.47 12.13 o 9 1 0 497.01 506.04 25.32 o 10 1 0 179.77 177.63 6.49 o 11 1 0 8.38 7.76 1.70 o 12 1 0 19.60 18.05 2.00 o 0 2 0 4521.71 4018.35 51.66 o 1 2 0 999.55 897.10 16.81 o 2 2 0 58.97 61.50 3.00 o 3 2 0 168.19 152.32 3.69 o 4 2 0 1564.69 1427.91 73.68 o 5 2 0 741.45 693.27 25.40 o 6 2 0 373.17 368.06 13.81 o 7 2 0 2.62 2.51 2.05 o 8 2 0 120.85 132.65 6.31 o 9 2 0 2.75 5.07 1.80 o 10 2 0 95.41 92.92 2.39 o 11 2 0 24.28 18.95 1.75 o 12 2 0 1.77 0.31 1.74 o 1 3 0 1016.66 994.87 8.96 o 2 3 0 487.17 440.99 6.00 o 3 3 0 2027.17 1715.94 70.06 o 4 3 0 77.16 61.62 2.66 o 5 3 0 976.12 1077.54 12.97 o 6 3 0 81.37 81.18 2.82 o 7 3 0 66.20 59.39 2.06 o 8 3 0 3.29 3.37 1.80 o 9 3 0 30.42 34.00 1.83 o 10 3 0 69.82 67.81 2.76 o 11 3 0 27.97 28.23 1.88 o 12 3 0 0.04 3.67 1.98 o 0 4 0 1648.46 1568.65 38.01 o 1 4 0 548.21 506.98 5.88 o 2 4 0 1428.94 1350.82 44.16 o 3 4 0 17.55 15.45 2.28 o 4 4 0 1.16 3.17 2.36 o 5 4 0 111.62 112.33 3.38 o 6 4 0 168.31 148.52 4.80 o 7 4 0 82.72 93.21 4.27 o 8 4 0 207.99 227.63 7.78 o 9 4 0 151.70 146.97 5.90 o 10 4 0 2.16 2.02 1.79 o 11 4 0 3.52 5.69 1.93 o 1 5 0 4.46 3.23 2.42 o 2 5 0 331.20 374.45 4.26 o 3 5 0 3070.42 3221.61 48.44 o 4 5 0 1138.20 1256.09 44.08 o 5 5 0 369.41 429.27 9.27 o 6 5 0 158.38 152.78 5.22 o 7 5 0 939.77 911.78 26.10 o 8 5 0 449.92 451.82 14.66 o 9 5 0 419.02 397.22 13.47 o 10 5 0 13.76 12.94 1.83 o 11 5 0 67.81 71.18 2.77 o 0 6 0 98.94 92.77 4.15 o 1 6 0 1.04 5.86 2.59 o 2 6 0 201.40 217.11 5.44 o 3 6 0 5.03 4.77 2.58 o 4 6 0 481.88 536.81 9.40 o 5 6 0 3.08 3.01 2.13 o 6 6 0 9.93 8.56 1.94 o 7 6 0 110.96 101.97 3.51 o 8 6 0 0.57 2.43 1.71 o 9 6 0 132.76 123.47 3.76 o 10 6 0 21.61 19.64 1.71 o 11 6 0 25.04 28.86 1.93 o 1 7 0 968.78 1012.09 24.90 o 2 7 0 15.14 22.35 2.30 o 3 7 0 199.50 210.70 7.17 o 4 7 0 90.51 110.85 2.50 o 5 7 0 70.49 60.66 2.14 o 6 7 0 383.07 421.04 12.21 o 7 7 0 6.52 5.99 1.85 o 8 7 0 134.18 131.86 2.48 o 9 7 0 118.44 113.45 4.20 o 10 7 0 5.64 10.28 1.93 o 0 8 0 869.93 947.34 29.84 o 1 8 0 1.46 4.29 2.11 o 2 8 0 193.65 197.34 5.06 o 3 8 0 294.09 299.30 3.46 o 4 8 0 111.83 123.34 2.87 o 5 8 0 5.43 6.43 1.98 o 6 8 0 284.17 300.36 7.39 o 7 8 0 22.63 20.42 1.91 o 8 8 0 224.69 237.90 9.19 o 9 8 0 3.46 3.55 1.76 o 10 8 0 163.55 152.51 6.31 o 1 9 0 477.18 514.18 8.27 o 2 9 0 205.04 208.03 7.10 o 3 9 0 474.66 461.11 11.47 o 4 9 0 66.19 68.48 2.39 o 5 9 0 1664.54 1682.31 47.04 o 6 9 0 163.89 143.94 3.96 o 7 9 0 8.02 7.74 2.17 o 8 9 0 2.10 2.09 1.98 o 9 9 0 5.00 4.18 1.97 o 0 10 0 1.20 3.46 2.65 o 1 10 0 367.84 368.92 5.19 o 2 10 0 1006.90 1010.70 11.53 o 3 10 0 411.25 402.54 3.62 o 4 10 0 692.98 671.49 18.12 o 5 10 0 163.86 168.47 4.24 o 6 10 0 5.36 8.37 2.23 o 7 10 0 219.43 191.64 6.26 o 8 10 0 19.37 21.91 2.14 o 9 10 0 45.91 52.35 2.77 o 1 11 0 272.56 251.59 7.27 o 2 11 0 3.58 0.35 1.84 o 3 11 0 114.50 116.50 2.40 o 4 11 0 11.99 10.95 1.96 o 5 11 0 51.75 49.52 2.33 o 6 11 0 146.58 146.75 3.87 o 7 11 0 42.41 36.82 2.70 o 8 11 0 5.13 7.11 2.35 o 0 12 0 641.58 662.44 15.23 o 1 12 0 207.95 227.53 4.47 o 2 12 0 1208.92 1221.40 34.20 o 3 12 0 373.52 356.61 9.85 o 4 12 0 14.07 14.51 2.07 o 5 12 0 4.73 3.26 2.04 o 6 12 0 36.17 33.58 2.30 o 7 12 0 38.53 31.22 2.43 o 1 13 0 32.48 38.61 2.31 o 2 13 0 189.12 182.62 5.84 o 3 13 0 0.18 2.57 2.05 o 4 13 0 8.55 6.01 1.94 o 5 13 0 3.74 6.57 2.45 o 6 13 0 63.90 58.01 3.29 o 0 14 0 6.53 8.34 2.95 o 1 14 0 42.91 42.59 2.11 o 2 14 0 146.66 159.45 2.74 o 3 14 0 45.73 52.38 2.30 o 4 14 0 0.00 2.10 1.97 o 1 15 0 2.06 4.54 2.34 o -12 1 1 12.54 11.95 1.94 o -11 1 1 7.58 11.64 1.91 o -10 1 1 26.80 32.96 1.83 o -9 1 1 0.70 2.48 1.75 o -8 1 1 171.64 170.36 6.34 o -7 1 1 0.00 0.56 1.85 o -6 1 1 201.17 200.04 10.52 o -5 1 1 728.66 761.24 24.42 o -4 1 1 0.00 0.19 2.51 o -3 1 1 27.86 25.16 2.58 o -2 1 1 393.89 338.40 15.36 o -1 1 1 68.34 56.80 3.15 o 0 1 1 302.25 241.00 14.37 o 1 1 1 154.09 132.53 6.80 o 2 1 1 0.27 0.74 2.63 o 3 1 1 276.37 244.56 11.62 o 4 1 1 8.02 7.50 2.37 o 5 1 1 22.37 25.04 2.07 o 6 1 1 318.25 331.01 10.74 o 7 1 1 91.93 94.02 2.35 o 8 1 1 5.40 7.24 2.16 o 9 1 1 105.61 118.89 5.58 o 10 1 1 1.14 2.57 2.50 o 11 1 1 11.78 10.95 1.89 o 12 1 1 5.40 2.30 2.19 o -12 2 1 13.18 17.52 2.05 o -11 2 1 2.33 3.08 1.85 o -10 2 1 97.64 103.05 4.14 o -9 2 1 692.47 712.79 35.43 o -8 2 1 141.29 146.40 4.49 o -7 2 1 164.86 149.81 4.57 o -6 2 1 5.03 5.81 2.06 o -5 2 1 263.05 264.20 12.85 o -4 2 1 223.06 230.14 13.80 o -3 2 1 1053.55 1057.34 28.08 o -2 2 1 0.22 -0.57 2.47 o -1 2 1 1291.37 1116.46 36.18 o 0 2 1 1627.10 1310.63 58.29 o 1 2 1 1759.30 1621.86 44.94 o 2 2 1 1227.01 1060.62 34.99 o 3 2 1 2.52 2.12 2.23 o 4 2 1 678.19 692.57 19.95 o 5 2 1 63.71 60.58 2.87 o 6 2 1 115.31 117.93 4.69 o 7 2 1 0.48 1.70 1.82 o 8 2 1 110.25 107.98 2.97 o 9 2 1 77.91 79.42 2.51 o 10 2 1 379.66 395.40 18.12 o 11 2 1 27.79 28.94 1.89 o -12 3 1 6.88 7.08 1.69 o -11 3 1 19.08 17.01 1.65 o -10 3 1 278.42 244.62 9.26 o -9 3 1 0.26 1.99 1.89 o -8 3 1 61.77 59.39 2.13 o -7 3 1 781.12 881.17 23.54 o -6 3 1 7.76 4.41 1.82 o -5 3 1 138.47 181.88 2.92 o -4 3 1 663.64 670.94 30.03 o -3 3 1 25.59 29.01 2.60 o -2 3 1 849.71 737.37 20.35 o -1 3 1 745.82 689.29 36.31 o 0 3 1 3533.47 2944.98 69.79 o 1 3 1 3146.03 2782.69 51.73 o 2 3 1 573.39 532.88 15.32 o 3 3 1 461.37 427.53 8.35 o 4 3 1 0.69 2.62 2.31 o 5 3 1 343.18 384.50 6.61 o 6 3 1 120.78 136.03 5.01 o 7 3 1 19.31 16.91 1.96 o 8 3 1 340.71 344.19 9.45 o 9 3 1 43.17 40.39 1.98 o 10 3 1 0.01 -0.42 1.87 o 11 3 1 172.64 161.74 5.33 o -11 4 1 45.65 42.16 2.12 o -10 4 1 5.44 5.27 1.66 o -9 4 1 241.35 240.57 10.42 o -8 4 1 310.08 292.68 12.51 o -7 4 1 23.93 27.76 2.07 o -6 4 1 44.11 47.16 2.33 o -5 4 1 556.22 590.77 19.37 o -4 4 1 1545.34 1459.64 66.94 o -3 4 1 271.64 246.00 8.45 o -2 4 1 1142.44 1202.61 27.54 o -1 4 1 60.22 67.43 2.79 o 0 4 1 89.47 90.58 3.12 o 1 4 1 100.71 83.16 3.47 o 2 4 1 221.52 228.74 3.75 o 3 4 1 600.94 645.23 15.29 o 4 4 1 266.76 271.56 7.87 o 5 4 1 836.99 833.27 27.48 o 6 4 1 386.83 390.27 10.80 o 7 4 1 48.72 54.21 2.45 o 8 4 1 0.00 -0.06 1.97 o 9 4 1 195.39 203.96 4.84 o 10 4 1 98.99 94.03 2.58 o 11 4 1 0.01 1.75 1.83 o -11 5 1 2.15 1.82 1.61 o -10 5 1 7.89 4.69 1.82 o -9 5 1 84.22 86.72 3.48 o -8 5 1 36.52 45.64 2.87 o -7 5 1 1564.14 1542.95 48.21 o -6 5 1 134.40 138.00 2.48 o -5 5 1 1475.29 1487.94 55.54 o -4 5 1 312.07 320.44 12.47 o -3 5 1 273.99 306.11 11.87 o -2 5 1 2294.44 2271.41 54.25 o -1 5 1 1151.02 1242.54 19.51 o 0 5 1 2428.30 2522.00 52.23 o 1 5 1 3018.65 3192.09 90.80 o 2 5 1 434.96 441.61 19.25 o 3 5 1 1595.56 1627.33 30.30 o 4 5 1 154.04 170.84 4.21 o 5 5 1 46.01 44.99 2.32 o 6 5 1 783.02 753.22 20.51 o 7 5 1 18.47 21.56 2.11 o 8 5 1 906.94 971.34 28.39 o 9 5 1 0.60 1.90 1.88 o 10 5 1 49.42 53.56 3.26 o 11 5 1 7.44 8.83 2.06 o -11 6 1 20.10 20.95 1.81 o -10 6 1 8.70 8.80 1.99 o -9 6 1 79.12 68.22 2.84 o -8 6 1 0.00 1.53 1.64 o -7 6 1 147.27 147.27 3.54 o -6 6 1 91.71 75.06 2.88 o -5 6 1 0.22 1.91 2.12 o -4 6 1 250.21 241.03 6.98 o -3 6 1 39.31 40.86 2.33 o -2 6 1 35.81 40.33 2.60 o -1 6 1 4.60 5.02 2.51 o 0 6 1 1.38 5.93 2.41 o 1 6 1 23.43 28.36 2.54 o 2 6 1 3.81 4.61 2.83 o 3 6 1 21.20 25.65 2.25 o 4 6 1 86.37 89.75 3.58 o 5 6 1 117.48 113.33 3.06 o 6 6 1 1.99 3.81 2.10 o 7 6 1 55.20 52.65 2.26 o 8 6 1 58.96 60.62 2.79 o 9 6 1 0.35 0.85 1.82 o 10 6 1 50.03 43.28 2.22 o 11 6 1 2.06 5.98 2.10 o -10 7 1 19.46 17.89 1.83 o -9 7 1 117.22 127.65 4.53 o -8 7 1 10.41 9.35 1.91 o -7 7 1 275.69 257.22 6.80 o -6 7 1 52.49 55.29 2.23 o -5 7 1 176.09 174.83 7.41 o -4 7 1 155.48 152.97 3.20 o -3 7 1 2.29 5.04 2.06 o -2 7 1 263.15 318.40 4.90 o -1 7 1 63.13 58.79 2.42 o 0 7 1 68.85 72.63 2.53 o 1 7 1 81.29 84.51 2.62 o 2 7 1 0.66 3.15 2.56 o 3 7 1 274.40 290.44 15.15 o 4 7 1 0.89 -0.74 2.46 o 5 7 1 110.79 113.23 2.81 o 6 7 1 70.48 61.40 2.13 o 7 7 1 3.89 3.38 2.01 o 8 7 1 176.58 184.17 4.42 o 9 7 1 0.67 3.66 2.16 o 10 7 1 43.64 40.09 2.32 o -10 8 1 0.26 0.78 1.95 o -9 8 1 21.76 21.49 1.95 o -8 8 1 63.56 64.12 2.50 o -7 8 1 151.72 142.78 4.06 o -6 8 1 462.01 450.10 11.35 o -5 8 1 998.90 952.33 21.06 o -4 8 1 356.72 384.81 8.17 o -3 8 1 390.08 423.92 9.25 o -2 8 1 288.42 325.11 6.74 o -1 8 1 436.94 473.01 13.04 o 0 8 1 193.00 215.68 4.68 o 1 8 1 186.87 188.05 7.57 o 2 8 1 392.94 452.75 9.30 o 3 8 1 169.10 171.98 5.28 o 4 8 1 286.73 302.36 14.68 o 5 8 1 265.73 289.93 7.14 o 6 8 1 846.19 841.70 27.34 o 7 8 1 312.50 291.17 8.89 o 8 8 1 78.61 74.75 2.24 o 9 8 1 55.44 49.99 2.06 o 10 8 1 5.65 6.92 1.87 o -9 9 1 0.00 -0.10 1.90 o -8 9 1 17.89 20.88 2.04 o -7 9 1 10.01 6.51 2.17 o -6 9 1 99.43 99.11 2.89 o -5 9 1 98.36 101.13 3.14 o -4 9 1 139.27 144.22 5.34 o -3 9 1 66.85 65.62 2.62 o -2 9 1 31.50 33.61 2.14 o -1 9 1 67.81 74.85 2.48 o 0 9 1 2.65 0.49 2.19 o 1 9 1 0.45 1.01 1.84 o 2 9 1 49.41 55.40 2.68 o 3 9 1 8.20 12.01 2.58 o 4 9 1 56.96 60.29 2.59 o 5 9 1 59.65 62.20 2.57 o 6 9 1 37.55 37.42 2.80 o 7 9 1 58.65 58.45 2.84 o 8 9 1 6.01 6.56 1.95 o 9 9 1 9.47 14.21 1.90 o -9 10 1 11.22 15.66 2.11 o -8 10 1 4.29 7.56 2.11 o -7 10 1 11.59 13.61 2.00 o -6 10 1 137.64 128.85 3.99 o -5 10 1 69.94 60.99 2.23 o -4 10 1 173.26 160.72 4.79 o -3 10 1 37.20 41.74 2.12 o -2 10 1 239.19 220.63 9.62 o -1 10 1 19.66 29.97 2.00 o 0 10 1 815.75 841.19 15.52 o 1 10 1 811.12 819.62 23.45 o 2 10 1 0.71 6.62 2.14 o 3 10 1 209.84 207.16 4.01 o 4 10 1 15.86 20.66 2.60 o 5 10 1 146.71 151.16 3.99 o 6 10 1 40.39 33.21 2.30 o 7 10 1 89.83 75.56 4.99 o 8 10 1 8.85 8.73 2.15 o -8 11 1 49.88 47.65 2.06 o -7 11 1 1.73 -0.21 1.91 o -6 11 1 9.77 11.74 2.26 o -5 11 1 12.66 15.68 2.24 o -4 11 1 0.22 2.52 2.04 o -3 11 1 88.82 88.80 3.15 o -2 11 1 0.41 2.61 2.16 o -1 11 1 89.61 91.60 2.86 o 0 11 1 0.09 1.19 1.99 o 1 11 1 11.69 14.24 2.32 o 2 11 1 70.68 67.73 2.24 o 3 11 1 3.23 1.73 1.84 o 4 11 1 57.22 56.44 2.44 o 5 11 1 1.95 5.17 2.23 o 6 11 1 29.05 25.76 2.22 o 7 11 1 6.97 9.04 2.12 o 8 11 1 0.89 1.68 2.33 o -7 12 1 9.66 8.27 1.96 o -6 12 1 1.46 1.17 1.90 o -5 12 1 204.05 219.05 8.49 o -4 12 1 32.79 33.95 2.25 o -3 12 1 25.47 25.57 2.03 o -2 12 1 62.85 55.83 2.30 o -1 12 1 49.76 49.33 2.68 o 0 12 1 20.22 17.16 2.01 o 1 12 1 26.20 23.22 1.88 o 2 12 1 33.80 32.19 1.91 o 3 12 1 52.73 47.42 2.52 o 4 12 1 22.97 25.20 2.25 o 5 12 1 15.86 15.58 2.33 o 6 12 1 161.44 165.19 7.49 o 7 12 1 2.91 3.63 2.51 o -6 13 1 28.85 22.10 2.83 o -5 13 1 75.09 72.11 2.44 o -4 13 1 2.85 0.80 1.93 o -3 13 1 23.88 34.16 2.29 o -2 13 1 2.51 2.57 2.10 o -1 13 1 48.67 57.85 2.59 o 0 13 1 7.66 8.70 2.02 o 1 13 1 17.04 18.19 2.04 o 2 13 1 32.29 36.63 2.40 o 3 13 1 2.61 1.96 1.94 o 4 13 1 21.00 20.51 2.02 o 5 13 1 1.79 4.04 1.89 o -4 14 1 9.21 9.87 2.29 o -3 14 1 33.39 33.60 2.21 o -2 14 1 4.37 5.77 2.11 o -1 14 1 51.30 54.49 2.38 o 0 14 1 1.34 1.77 1.95 o 1 14 1 2.58 3.41 2.04 o 2 14 1 47.77 42.36 2.19 o 3 14 1 3.75 5.18 2.17 o 4 14 1 37.09 32.20 2.43 o 0 15 1 154.73 155.34 7.58 o -12 0 2 0.07 3.58 2.39 o -11 0 2 104.00 104.26 3.54 o -10 0 2 71.62 63.22 5.10 o -9 0 2 1240.62 1168.60 76.20 o -8 0 2 290.62 292.26 30.23 o -7 0 2 1070.81 1166.79 75.28 o -6 0 2 777.53 812.83 40.43 o -5 0 2 42.03 55.76 5.19 o -4 0 2 3272.63 3348.09 224.16 o -3 0 2 3482.43 3676.61 29.21 o -2 0 2 0.00 1.09 3.38 o -1 0 2 1355.62 1205.38 107.15 o 0 0 2 5691.54 5715.65 24.46 o 2 0 2 2796.19 2447.41 222.16 o 3 0 2 1309.25 1266.47 52.64 o 4 0 2 86.72 74.39 4.22 o 5 0 2 2349.61 2226.01 153.04 o 6 0 2 1646.03 1728.76 88.10 o 7 0 2 8.41 6.74 2.46 o 8 0 2 77.66 79.25 10.43 o 9 0 2 515.23 446.99 29.07 o 10 0 2 67.42 70.02 3.09 o 11 0 2 510.28 531.76 45.61 o -12 1 2 23.98 24.68 2.01 o -11 1 2 31.56 29.88 1.84 o -10 1 2 13.55 13.57 1.66 o -9 1 2 386.81 393.17 14.17 o -8 1 2 760.34 822.90 36.99 o -7 1 2 584.11 608.18 21.65 o -6 1 2 0.14 -1.79 1.79 o -5 1 2 226.58 193.64 9.17 o -4 1 2 1064.82 961.42 31.04 o -3 1 2 3551.54 3252.48 195.73 o -2 1 2 597.86 446.23 16.24 o -1 1 2 920.01 821.34 50.34 o 0 1 2 576.82 520.18 22.60 o 1 1 2 646.38 607.34 18.62 o 2 1 2 108.14 99.98 4.78 o 3 1 2 102.85 91.43 4.12 o 4 1 2 289.52 260.20 9.61 o 5 1 2 292.42 269.77 12.83 o 6 1 2 149.95 157.64 6.39 o 7 1 2 4.04 7.47 1.92 o 8 1 2 0.74 0.78 1.89 o 9 1 2 85.61 91.60 4.31 o 10 1 2 188.01 213.60 7.16 o 11 1 2 51.04 56.44 2.23 o -12 2 2 133.93 151.19 7.49 o -11 2 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546.70 494.37 19.46 o 4 3 2 987.83 915.15 22.26 o 5 3 2 18.96 20.56 2.15 o 6 3 2 390.47 393.75 12.18 o 7 3 2 3.10 -0.25 1.99 o 8 3 2 12.54 14.39 1.90 o 9 3 2 0.58 0.25 1.85 o 10 3 2 10.93 11.27 1.95 o 11 3 2 29.99 28.58 2.04 o -11 4 2 63.76 64.96 3.81 o -10 4 2 22.54 20.05 1.65 o -9 4 2 9.69 7.51 1.81 o -8 4 2 265.64 228.58 9.63 o -7 4 2 316.03 344.72 10.59 o -6 4 2 227.76 255.59 9.35 o -5 4 2 103.83 107.84 3.08 o -4 4 2 144.21 133.76 3.59 o -3 4 2 6.38 6.62 2.52 o -2 4 2 42.44 34.13 3.23 o -1 4 2 1152.22 1061.22 38.52 o 0 4 2 313.24 290.68 10.54 o 1 4 2 1103.38 1033.22 36.62 o 2 4 2 127.22 122.74 3.33 o 3 4 2 664.79 577.86 22.11 o 4 4 2 82.54 75.68 2.94 o 5 4 2 12.20 14.04 2.09 o 6 4 2 35.82 40.74 2.12 o 7 4 2 77.97 75.48 2.36 o 8 4 2 7.42 9.35 1.76 o 9 4 2 81.38 88.50 4.74 o 10 4 2 56.50 52.71 3.50 o 11 4 2 0.71 0.49 1.77 o -11 5 2 0.94 3.41 1.81 o -10 5 2 78.29 93.42 5.27 o -9 5 2 32.96 42.28 2.50 o -8 5 2 618.35 610.60 19.30 o -7 5 2 496.52 487.75 13.37 o -6 5 2 961.60 954.26 27.98 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