#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:42:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181083 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/63/2216338.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216338_Fobs loop_ _publ_author_name 'Sivaramakrishna, Akella' 'Su, Hong' 'Moss, John R.' _publ_section_title ; cis-(Carbonato-\k^2^O,O')bis(triphenylphosphine-\kP)platinum(II)--benzene--dichloromethane mixed solvate (2/1/1) ; _journal_coeditor_code BX2113 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3097 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.576 _cell_angle_beta 71.757 _cell_angle_gamma 70.956 _cell_length_a 10.4676 _cell_length_b 12.2005 _cell_length_c 15.2380 _exptl_crystal_F_000 852.00 _reflns_d_resolution_high 0.8098 _cod_data_source_file bx2113Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rk95 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22575.41 22291.17 451.73 o 3 0 0 19653.21 19082.66 419.96 o 4 0 0 151.09 126.85 47.26 o 5 0 0 985.68 1009.00 58.08 o 6 0 0 7397.49 7417.98 151.25 o 7 0 0 20.68 200.50 67.20 o 8 0 0 1832.43 1901.11 104.38 o 9 0 0 1909.81 2111.11 181.79 o 10 0 0 1219.38 1193.13 117.08 o 11 0 0 1418.84 1612.71 228.88 o -11 1 0 2707.86 2855.11 279.06 o -10 1 0 14.63 -89.59 89.59 o -9 1 0 3846.68 3877.91 200.13 o -8 1 0 2427.00 2156.53 138.68 o -7 1 0 2835.99 2850.54 130.41 o -6 1 0 4389.63 4399.32 144.69 o -5 1 0 31.12 53.53 44.69 o -4 1 0 3021.62 2821.68 74.39 o -3 1 0 13352.19 13237.63 217.32 o -2 1 0 114.05 274.36 41.17 o 2 1 0 23030.38 22847.56 540.00 o 3 1 0 11292.80 11135.54 211.26 o 4 1 0 1130.32 1051.38 61.35 o 5 1 0 10141.12 9771.13 230.20 o 6 1 0 2344.43 2567.80 110.22 o 7 1 0 3736.10 3625.08 115.44 o 8 1 0 4356.94 4542.17 156.29 o 9 1 0 51.13 108.98 87.33 o 10 1 0 3795.44 3865.95 180.08 o 11 1 0 421.29 199.58 198.79 o -10 2 0 4294.06 4405.44 296.42 o -9 2 0 2659.78 3021.03 217.04 o -8 2 0 16.88 -42.95 92.56 o -7 2 0 4282.26 4061.74 139.59 o -6 2 0 1648.90 1759.29 79.55 o -5 2 0 200.57 176.71 43.06 o -4 2 0 10939.77 10916.85 194.23 o -3 2 0 3950.32 3897.99 73.24 o -2 2 0 4752.72 4592.66 79.86 o -1 2 0 30728.42 31119.35 438.30 o 0 2 0 2063.22 1977.97 63.64 o 1 2 0 7474.03 6982.74 205.83 o 2 2 0 10944.64 10801.22 272.00 o 3 2 0 469.00 359.35 63.94 o 4 2 0 5388.84 4959.61 114.49 o 5 2 0 6972.85 6875.65 143.43 o 6 2 0 1682.51 1756.16 94.26 o 7 2 0 17280.47 18062.17 480.46 o 8 2 0 4045.14 4038.14 147.65 o 9 2 0 4562.84 4675.99 193.40 o 10 2 0 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o 9 8 0 2992.71 3118.38 167.92 o 10 8 0 20.00 -122.98 122.98 o 11 8 0 2872.13 2879.58 279.46 o -6 9 0 1531.13 1943.19 398.97 o -5 9 0 718.76 538.65 143.91 o -4 9 0 997.81 997.44 102.21 o -3 9 0 2517.55 2524.71 131.26 o -2 9 0 79.73 -77.79 88.23 o -1 9 0 1387.29 1398.36 89.81 o 0 9 0 1611.51 1753.96 90.76 o 1 9 0 81.64 67.46 59.65 o 2 9 0 10156.54 10369.13 220.65 o 3 9 0 6147.35 5820.39 269.83 o 4 9 0 1334.24 1183.13 171.37 o 5 9 0 8732.84 8980.26 234.20 o 6 9 0 1798.43 1952.09 154.88 o 7 9 0 1580.05 1641.14 160.64 o 8 9 0 3975.30 4083.66 174.27 o 9 9 0 2347.41 2185.90 142.86 o 10 9 0 1327.56 1395.76 168.29 o 11 9 0 4150.92 4125.43 333.94 o -6 10 0 3452.41 3138.28 598.07 o -5 10 0 192.81 702.44 311.83 o -4 10 0 4276.31 4167.57 207.66 o -3 10 0 932.85 1123.83 130.96 o -2 10 0 1666.41 1656.13 134.72 o -1 10 0 3771.34 3736.04 158.89 o 0 10 0 850.85 603.89 78.46 o 1 10 0 2641.59 2593.83 98.38 o 2 10 0 4848.51 5118.21 159.82 o 3 10 0 5.78 112.01 107.14 o 4 10 0 5451.62 5420.65 224.62 o 5 10 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