#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/63/2216382.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216382_Fobs loop_ _publ_author_name 'Wu, Hua' 'Liu, Ying-Ying' 'Bai, Hong-Ye' _publ_section_title ; catena-Poly[[[bis(triphenylphosphine)silver(I)]-\m-6-aminonaphthalene-1-sulfonato-\k^2^O:N] monohydrate] ; _journal_coeditor_code CV2332 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3027 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.836 _cell_angle_beta 81.368 _cell_angle_gamma 69.089 _cell_length_a 10.0167 _cell_length_b 13.6959 _cell_length_c 16.7921 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file cv2332Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12175.36 8146.48 287.34 o 3 0 0 779.39 827.82 37.63 o 4 0 0 268.01 287.34 20.52 o 5 0 0 81.60 94.07 32.50 o 6 0 0 491.05 466.93 22.23 o 7 0 0 1104.02 1045.03 47.89 o 8 0 0 3.28 -15.39 51.31 o 9 0 0 8.61 23.95 75.26 o 10 0 0 219.35 205.24 83.81 o 11 0 0 118.05 46.18 94.07 o 12 0 0 248.77 285.63 70.13 o -11 1 0 201.35 227.48 76.97 o -10 1 0 71.96 87.23 63.28 o -9 1 0 3.44 1.71 73.55 o -8 1 0 257.31 205.24 66.70 o -7 1 0 37.10 37.63 32.50 o -6 1 0 346.32 364.31 61.57 o -5 1 0 3109.67 3182.99 53.02 o -4 1 0 59.06 129.99 42.76 o -3 1 0 3521.93 3350.61 53.02 o -2 1 0 19319.15 20129.30 407.07 o -1 1 0 1122.37 1337.51 22.23 o 0 1 0 24771.05 23.95 13.68 o 1 1 0 571.44 326.68 5.13 o 4 1 0 114.63 106.04 20.52 o 5 1 0 8.22 0.00 30.79 o 6 1 0 3556.62 3648.21 63.28 o 7 1 0 3127.51 3176.15 87.23 o 8 1 0 365.09 425.88 42.76 o 9 1 0 647.87 726.91 61.57 o 10 1 0 188.83 212.09 54.73 o 11 1 0 158.23 215.51 64.99 o 12 1 0 61.30 88.94 123.15 o -11 2 0 36.01 99.20 64.99 o -10 2 0 0.73 -3.42 61.57 o -9 2 0 1.69 -42.76 97.49 o -8 2 0 148.15 129.99 53.02 o -7 2 0 65.40 71.84 32.50 o -6 2 0 1204.00 1145.95 25.66 o -5 2 0 2946.59 2589.49 39.34 o -4 2 0 2574.01 2341.49 44.47 o -3 2 0 2489.59 2541.60 63.28 o -2 2 0 7329.17 7228.01 78.68 o -1 2 0 16408.44 15848.26 111.17 o 0 2 0 490.83 454.96 25.66 o 1 2 0 5575.53 5875.11 29.08 o 2 2 0 12989.40 13070.62 73.55 o 3 2 0 5977.22 6123.11 25.66 o 5 2 0 1440.52 1433.29 53.02 o 6 2 0 464.57 458.38 25.66 o 7 2 0 1033.34 1017.67 68.41 o 8 2 0 83.12 78.68 64.99 o 9 2 0 159.43 229.19 51.31 o 10 2 0 147.24 147.09 76.97 o 11 2 0 131.94 131.70 99.20 o 12 2 0 67.02 159.06 70.13 o -11 3 0 76.18 114.59 99.20 o -10 3 0 362.76 352.34 106.04 o -9 3 0 187.84 198.40 75.26 o -8 3 0 319.59 273.66 83.81 o -7 3 0 234.03 218.93 39.34 o -6 3 0 1374.19 1306.72 70.13 o -5 3 0 1817.50 1734.31 80.39 o -4 3 0 1870.97 1927.58 30.79 o -3 3 0 1330.21 1192.13 49.60 o -2 3 0 5312.91 5661.31 46.18 o -1 3 0 418.66 572.97 29.08 o 0 3 0 313.04 295.89 13.68 o 1 3 0 2651.99 2695.54 34.21 o 2 3 0 13902.68 14608.24 70.13 o 3 3 0 22931.09 23527.80 63.28 o 4 3 0 5237.31 5127.68 56.44 o 5 3 0 4509.73 4438.40 41.05 o 6 3 0 815.67 819.27 58.15 o 7 3 0 7.70 1.71 41.05 o 8 3 0 10.93 -25.66 35.92 o 9 3 0 0.11 -64.99 73.55 o 10 3 0 2.39 51.31 95.78 o 11 3 0 16.10 78.68 83.81 o 12 3 0 14.98 56.44 71.84 o -10 4 0 346.22 413.91 85.52 o -9 4 0 629.26 632.84 64.99 o -8 4 0 298.98 295.89 39.34 o -7 4 0 1055.98 1082.66 73.55 o -6 4 0 1439.60 1458.94 53.02 o -5 4 0 1000.21 985.17 39.34 o -4 4 0 21.04 63.28 32.50 o -3 4 0 195.66 159.06 32.50 o -2 4 0 216.35 236.03 17.10 o -1 4 0 2436.80 2647.65 35.92 o 0 4 0 2659.97 2584.36 78.68 o 1 4 0 14656.88 15025.57 129.99 o 2 4 0 6038.50 6059.83 22.23 o 3 4 0 13579.03 14794.67 116.30 o 4 4 0 899.60 908.20 11.97 o 5 4 0 4283.93 4464.06 66.70 o 6 4 0 2272.73 2216.64 80.39 o 7 4 0 10.55 23.95 51.31 o 8 4 0 50.53 126.57 68.41 o 9 4 0 284.28 225.77 58.15 o 10 4 0 0.58 49.60 75.26 o 11 4 0 42.22 94.07 58.15 o 12 4 0 481.68 487.45 61.57 o -10 5 0 136.72 112.88 53.02 o -9 5 0 302.16 311.29 46.18 o -8 5 0 126.62 97.49 39.34 o -7 5 0 119.48 106.04 41.05 o -6 5 0 1044.15 1033.06 61.57 o -5 5 0 959.03 985.17 27.37 o -4 5 0 10.39 58.15 23.95 o -3 5 0 1984.96 2090.07 47.89 o -2 5 0 138.94 34.21 32.50 o -1 5 0 7273.62 7178.41 83.81 o 0 5 0 4931.74 4927.57 56.44 o 1 5 0 11881.44 12198.33 83.81 o 2 5 0 5217.54 5531.33 116.30 o 3 5 0 3028.54 3076.95 25.66 o 4 5 0 1756.65 1866.01 18.81 o 5 5 0 80.35 76.97 29.08 o 6 5 0 53.86 73.55 29.08 o 7 5 0 279.31 237.74 44.47 o 8 5 0 566.25 627.70 71.84 o 9 5 0 650.71 595.21 92.36 o 10 5 0 27.35 51.31 46.18 o 11 5 0 66.42 42.76 63.28 o 12 5 0 647.15 614.02 94.07 o -9 6 0 7.66 20.52 73.55 o -8 6 0 0.74 49.60 54.73 o -7 6 0 195.80 174.46 44.47 o -6 6 0 287.56 270.24 58.15 o -5 6 0 232.53 232.61 34.21 o -4 6 0 845.54 850.05 39.34 o -3 6 0 2779.91 2924.73 64.99 o -2 6 0 2770.18 2851.18 51.31 o -1 6 0 1808.34 1852.33 23.95 o 0 6 0 954.92 814.13 34.21 o 1 6 0 3836.10 3583.22 78.68 o 2 6 0 50.41 58.15 32.50 o 3 6 0 56.78 51.31 18.81 o 4 6 0 2960.51 3145.36 44.47 o 5 6 0 273.76 275.37 22.23 o 6 6 0 1279.84 1272.51 37.63 o 7 6 0 2199.20 2196.11 75.26 o 8 6 0 3269.21 3157.34 140.25 o 9 6 0 666.91 726.91 58.15 o 10 6 0 86.49 169.33 73.55 o 11 6 0 7.99 -17.10 63.28 o 12 6 0 209.33 217.22 83.81 o -9 7 0 0.06 0.00 92.36 o -8 7 0 19.23 64.99 71.84 o -7 7 0 0.64 30.79 58.15 o -6 7 0 485.76 519.95 34.21 o -5 7 0 829.96 797.03 29.08 o -4 7 0 5387.25 5601.45 184.72 o -3 7 0 3067.00 3085.50 70.13 o -2 7 0 2224.34 2172.17 49.60 o -1 7 0 498.37 526.79 61.57 o 0 7 0 226.17 239.45 18.81 o 1 7 0 596.17 661.91 34.21 o 2 7 0 987.44 1060.43 47.89 o 3 7 0 1781.54 1761.68 27.37 o 4 7 0 710.90 663.62 20.52 o 5 7 0 62.52 64.99 56.44 o 6 7 0 658.23 660.20 39.34 o 7 7 0 1182.61 1173.31 29.08 o 8 7 0 2051.50 2182.43 95.78 o 9 7 0 259.85 314.71 53.02 o 10 7 0 59.56 68.41 143.67 o 11 7 0 210.18 294.18 68.41 o 12 7 0 64.49 133.41 112.88 o -8 8 0 44.55 49.60 46.18 o -7 8 0 26.99 63.28 56.44 o -6 8 0 136.37 193.27 39.34 o -5 8 0 889.62 968.07 75.26 o -4 8 0 2373.42 2524.50 53.02 o -3 8 0 2924.15 2781.06 44.47 o -2 8 0 480.66 458.38 46.18 o -1 8 0 376.78 405.36 30.79 o 0 8 0 2.23 6.84 35.92 o 1 8 0 2146.76 2233.74 46.18 o 2 8 0 4456.22 4318.68 54.73 o 3 8 0 2479.11 2500.56 42.76 o 4 8 0 457.15 442.98 47.89 o 5 8 0 399.89 448.12 66.70 o 6 8 0 333.06 302.73 39.34 o 7 8 0 775.21 802.16 35.92 o 8 8 0 122.08 119.73 54.73 o 9 8 0 44.36 53.02 42.76 o 10 8 0 150.61 114.59 71.84 o 11 8 0 255.49 307.87 94.07 o 12 8 0 41.03 1.71 102.62 o -7 9 0 233.74 188.14 53.02 o -6 9 0 433.02 331.81 39.34 o -5 9 0 375.16 357.47 54.73 o -4 9 0 55.48 102.62 46.18 o -3 9 0 81.17 92.36 35.92 o -2 9 0 1064.94 1181.86 54.73 o -1 9 0 356.19 436.14 68.41 o 0 9 0 573.19 566.13 47.89 o 1 9 0 695.45 738.88 41.05 o 2 9 0 2782.78 2827.24 51.31 o 3 9 0 2081.39 2045.60 58.15 o 4 9 0 407.99 408.78 32.50 o 5 9 0 185.42 200.11 18.81 o 6 9 0 1719.60 1730.89 39.34 o 7 9 0 671.86 610.60 42.76 o 8 9 0 0.71 -3.42 71.84 o 9 9 0 217.37 196.69 39.34 o 10 9 0 215.14 232.61 64.99 o 11 9 0 8.64 -5.13 104.33 o 12 9 0 132.44 100.91 140.25 o -7 10 0 162.01 225.77 46.18 o -6 10 0 308.21 268.53 42.76 o -5 10 0 136.80 119.73 42.76 o -4 10 0 35.28 37.63 66.70 o -3 10 0 333.59 314.71 90.65 o -2 10 0 1914.52 1836.93 25.66 o -1 10 0 1784.70 1802.73 80.39 o 0 10 0 2140.77 2302.15 85.52 o 1 10 0 1558.13 1669.32 49.60 o 2 10 0 215.40 193.27 54.73 o 3 10 0 210.73 200.11 29.08 o 4 10 0 204.70 186.43 64.99 o 5 10 0 1489.55 1505.12 44.47 o 6 10 0 1.92 41.05 34.21 o 7 10 0 56.08 75.26 41.05 o 8 10 0 19.70 41.05 44.47 o 9 10 0 86.81 112.88 32.50 o 10 10 0 285.08 232.61 76.97 o 11 10 0 81.86 109.46 63.28 o 12 10 0 516.84 494.30 87.23 o -4 11 0 91.75 66.70 29.08 o -3 11 0 812.42 750.85 97.49 o -2 11 0 1029.38 1017.67 88.94 o -1 11 0 1939.88 1893.38 90.65 o 0 11 0 1066.06 1045.03 80.39 o 1 11 0 1668.09 1739.44 46.18 o 2 11 0 1100.85 1144.24 80.39 o 3 11 0 567.81 583.23 37.63 o 4 11 0 1.76 15.39 35.92 o 5 11 0 408.40 386.54 63.28 o 6 11 0 1.90 5.13 27.37 o 7 11 0 30.88 22.23 58.15 o 8 11 0 109.57 136.83 35.92 o 9 11 0 347.65 326.68 41.05 o 10 11 0 215.33 232.61 56.44 o 11 11 0 56.23 63.28 83.81 o -2 12 0 233.77 367.73 95.78 o -1 12 0 222.87 242.87 90.65 o 0 12 0 1.21 13.68 56.44 o 1 12 0 136.71 179.59 83.81 o 3 12 0 158.34 159.06 85.52 o 4 12 0 1.95 1.71 32.50 o 5 12 0 81.56 61.57 39.34 o 6 12 0 201.85 227.48 46.18 o 7 12 0 44.42 51.31 35.92 o 8 12 0 323.00 307.87 49.60 o 9 12 0 404.85 456.67 49.60 o 10 12 0 353.49 369.44 68.41 o 11 12 0 105.86 145.38 90.65 o 1 13 0 315.78 393.38 92.36 o 3 13 0 574.97 634.55 94.07 o 4 13 0 1159.55 1015.96 41.05 o 5 13 0 32.01 46.18 37.63 o 6 13 0 28.33 29.08 46.18 o 7 13 0 10.73 34.21 30.79 o 8 13 0 45.81 73.55 54.73 o 9 13 0 366.16 389.96 58.15 o 10 13 0 126.66 172.75 68.41 o -1 14 0 156.46 237.74 119.73 o 2 14 0 91.91 162.48 97.49 o 3 14 0 689.71 720.06 97.49 o 4 14 0 1593.23 1484.60 97.49 o 5 14 0 186.92 198.40 87.23 o 6 14 0 32.93 29.08 32.50 o 7 14 0 13.20 29.08 49.60 o 8 14 0 4.21 6.84 58.15 o 9 14 0 44.01 42.76 61.57 o 10 14 0 50.78 27.37 44.47 o 0 15 0 466.37 540.48 129.99 o 2 15 0 27.88 88.94 116.30 o 3 15 0 190.18 383.12 217.22 o 4 15 0 78.22 59.86 100.91 o 5 15 0 0.93 -76.97 97.49 o 6 15 0 17.05 23.95 194.98 o 7 15 0 21.90 -17.10 97.49 o 8 15 0 23.75 -23.95 92.36 o 9 15 0 30.71 15.39 35.92 o 1 16 0 200.87 302.73 133.41 o 2 16 0 17.77 152.22 128.28 o 3 16 0 63.91 99.20 124.86 o 4 16 0 4.32 -121.44 121.44 o 5 16 0 100.79 106.04 119.73 o 6 16 0 142.99 143.67 114.59 o 7 16 0 3.09 39.34 109.46 o -6 -16 1 82.59 159.06 107.75 o -5 -16 1 236.92 391.67 111.17 o -4 -16 1 246.84 181.30 116.30 o -3 -16 1 56.16 -73.55 119.73 o -2 -16 1 31.94 145.38 131.70 o -8 -15 1 36.40 29.08 181.30 o -7 -15 1 135.54 116.30 94.07 o -6 -15 1 401.13 360.89 99.20 o -5 -15 1 504.77 540.48 102.62 o -4 -15 1 467.10 465.22 104.33 o -3 -15 1 58.17 121.44 106.04 o -2 -15 1 107.88 131.70 109.46 o 0 -15 1 93.34 147.09 133.41 o 1 -15 1 69.95 -63.28 138.54 o -9 -14 1 331.97 335.23 54.73 o -8 -14 1 325.69 261.69 64.99 o -7 -14 1 56.19 68.41 56.44 o -6 -14 1 212.49 205.24 88.94 o -5 -14 1 108.13 165.91 184.72 o -4 -14 1 15.61 -66.70 193.27 o -3 -14 1 10.79 -30.79 97.49 o -2 -14 1 215.74 141.96 99.20 o -1 -14 1 175.90 271.95 106.04 o 0 -14 1 290.97 225.77 109.46 o 1 -14 1 483.54 699.54 123.15 o 2 -14 1 504.11 766.24 131.70 o -10 -13 1 98.38 94.07 66.70 o -9 -13 1 526.57 526.79 61.57 o -8 -13 1 334.91 283.92 53.02 o -7 -13 1 199.32 129.99 29.08 o -6 -13 1 3.97 17.10 39.34 o -5 -13 1 53.17 59.86 27.37 o -4 -13 1 31.94 87.23 90.65 o -3 -13 1 1354.22 1508.54 99.20 o -2 -13 1 1284.10 1373.42 100.91 o -1 -13 1 165.62 135.12 94.07 o 0 -13 1 80.00 29.08 95.78 o 1 -13 1 3.57 -56.44 99.20 o 3 -13 1 35.96 -56.44 121.44 o -11 -12 1 0.18 -58.15 58.15 o -10 -12 1 52.62 41.05 44.47 o -9 -12 1 291.34 304.45 41.05 o -8 -12 1 0.14 0.00 61.57 o -7 -12 1 122.65 97.49 46.18 o -6 -12 1 0.56 -1.71 41.05 o -5 -12 1 155.21 140.25 37.63 o -4 -12 1 305.07 297.60 30.79 o -3 -12 1 3472.24 3521.64 97.49 o -2 -12 1 2113.68 2276.50 95.78 o -1 -12 1 1027.41 1118.58 94.07 o 0 -12 1 51.21 152.22 88.94 o 1 -12 1 1.14 27.37 90.65 o 3 -12 1 40.34 100.91 109.46 o 5 -12 1 94.44 248.00 109.46 o -11 -11 1 105.18 118.02 54.73 o -10 -11 1 105.07 116.30 35.92 o -9 -11 1 9.92 29.08 58.15 o -8 -11 1 244.14 289.05 51.31 o -7 -11 1 301.47 335.23 53.02 o -6 -11 1 418.61 454.96 39.34 o -5 -11 1 239.95 258.27 32.50 o -4 -11 1 1995.57 1932.71 51.31 o -3 -11 1 1902.39 1753.13 124.86 o -1 -11 1 121.75 164.20 85.52 o 0 -11 1 65.00 -39.34 87.23 o 2 -11 1 53.66 99.20 87.23 o 4 -11 1 306.38 176.17 102.62 o 5 -11 1 403.68 391.67 100.91 o -12 -10 1 28.64 -35.92 102.62 o -11 -10 1 33.46 -73.55 107.75 o -10 -10 1 163.57 131.70 94.07 o -9 -10 1 12.67 15.39 49.60 o -8 -10 1 373.62 359.18 46.18 o -7 -10 1 909.47 904.78 37.63 o -6 -10 1 2979.22 2900.78 102.62 o -5 -10 1 1167.18 1176.73 42.76 o -4 -10 1 4591.18 4419.59 59.86 o -3 -10 1 1498.85 1446.97 51.31 o -2 -10 1 500.51 466.93 71.84 o -1 -10 1 2046.40 1942.98 78.68 o 0 -10 1 912.82 992.01 68.41 o 1 -10 1 783.65 865.45 47.89 o 2 -10 1 30.42 54.73 82.10 o 3 -10 1 572.53 540.48 39.34 o 4 -10 1 158.88 136.83 51.31 o 5 -10 1 285.71 239.45 34.21 o -12 -9 1 66.56 87.23 87.23 o -11 -9 1 18.52 -66.70 66.70 o -10 -9 1 9.23 10.26 41.05 o -9 -9 1 276.79 268.53 61.57 o -8 -9 1 951.08 1000.56 46.18 o -7 -9 1 1223.81 1301.59 75.26 o -6 -9 1 1399.87 1335.80 32.50 o -5 -9 1 442.35 383.12 27.37 o -4 -9 1 346.01 335.23 37.63 o -3 -9 1 423.44 422.46 20.52 o -2 -9 1 343.38 141.96 131.70 o -1 -9 1 1088.71 1132.26 49.60 o 0 -9 1 1256.55 1310.14 76.97 o 1 -9 1 636.38 783.35 71.84 o 2 -9 1 702.83 682.44 46.18 o 3 -9 1 1732.58 1571.83 124.86 o 4 -9 1 285.34 256.55 30.79 o 5 -9 1 12.68 41.05 35.92 o 6 -9 1 5.14 42.76 35.92 o 7 -9 1 3.08 1.71 73.55 o -12 -8 1 136.30 179.59 76.97 o -11 -8 1 67.60 145.38 66.70 o -10 -8 1 149.68 123.15 42.76 o -9 -8 1 273.22 275.37 88.94 o -8 -8 1 621.30 668.75 56.44 o -7 -8 1 74.74 87.23 39.34 o -6 -8 1 135.08 141.96 41.05 o -5 -8 1 271.25 287.34 27.37 o -4 -8 1 537.25 509.69 35.92 o -3 -8 1 1058.27 1103.19 29.08 o -2 -8 1 3384.99 3504.54 76.97 o -1 -8 1 3498.50 3665.32 51.31 o 0 -8 1 1627.48 1655.63 39.34 o 1 -8 1 83.10 41.05 58.15 o 2 -8 1 353.55 354.05 35.92 o 3 -8 1 838.80 822.69 54.73 o 4 -8 1 80.68 80.39 58.15 o 5 -8 1 43.39 99.20 32.50 o 6 -8 1 41.38 20.52 32.50 o 7 -8 1 2.48 5.13 46.18 o 8 -8 1 0.45 80.39 39.34 o -12 -7 1 79.97 88.94 104.33 o -11 -7 1 1.01 30.79 97.49 o -10 -7 1 228.49 292.47 56.44 o -9 -7 1 67.72 97.49 61.57 o -8 -7 1 1383.81 1310.14 70.13 o -7 -7 1 958.12 932.15 54.73 o -6 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