#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:42:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181083 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/63/2216388.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216388_Fobs loop_ _publ_author_name 'Aghabozorg, Hossein' 'Nemati, Andya' 'Derikvand, Zohreh' 'Ghadermazi, Mohammad' _publ_section_title ; Piperazinediium bis[bis(pyridine-2,6-dicarboxylato)ferrate(III)] monohydrate ; _journal_coeditor_code CV2339 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2921 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.697 _cell_angle_gamma 90.000 _cell_length_a 7.0156 _cell_length_b 24.8546 _cell_length_c 19.4220 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.7829 _cod_data_source_file cv2339Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 345.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1324.19 1196.80 69.89 o 4 0 0 245.72 283.98 71.61 o 6 0 0 0.05 28.12 64.69 o 8 0 0 578.31 545.85 322.73 o 1 1 0 10232.85 10669.82 105.35 o 2 1 0 23.81 -7.75 23.40 o 3 1 0 1249.66 1190.02 60.10 o 4 1 0 353.01 441.03 71.45 o 5 1 0 694.25 729.16 77.69 o 6 1 0 1192.44 1138.71 89.76 o 7 1 0 444.70 282.42 81.96 o 8 1 0 2670.19 2507.00 220.75 o 1 2 0 1118.67 1282.14 44.83 o 2 2 0 2024.86 2206.15 65.07 o 3 2 0 168.51 158.32 42.00 o 4 2 0 13690.20 13659.28 210.74 o 5 2 0 6915.95 6586.89 158.99 o 6 2 0 186.71 204.87 74.99 o 7 2 0 54.95 39.49 68.89 o 8 2 0 715.28 1117.71 165.94 o 1 3 0 10319.29 10243.50 145.79 o 2 3 0 513.76 588.13 34.28 o 3 3 0 116.52 118.06 29.93 o 4 3 0 1114.81 1219.08 70.88 o 5 3 0 1542.94 1731.77 118.91 o 6 3 0 3.58 3.42 44.86 o 7 3 0 4014.29 4159.62 214.17 o 8 3 0 291.40 313.47 112.62 o 0 4 0 35082.35 36024.60 404.19 o 1 4 0 3938.10 4050.95 57.13 o 2 4 0 3451.59 3303.94 102.80 o 3 4 0 1144.75 1325.75 67.92 o 4 4 0 1933.49 1842.19 79.02 o 5 4 0 483.43 526.96 58.24 o 6 4 0 14.01 -26.65 64.30 o 7 4 0 10.33 22.79 67.72 o 8 4 0 1357.36 1188.39 164.31 o 1 5 0 14841.86 15583.75 145.85 o 2 5 0 1748.90 1942.67 77.72 o 3 5 0 26044.99 26197.56 363.66 o 4 5 0 5643.92 5699.30 116.38 o 5 5 0 51.60 -76.05 62.00 o 6 5 0 265.21 284.16 110.90 o 7 5 0 36.32 63.52 74.13 o 8 5 0 472.09 462.00 128.88 o 0 6 0 1042.55 979.13 63.67 o 1 6 0 24866.26 24906.75 257.68 o 2 6 0 155.68 145.66 51.83 o 3 6 0 2960.16 2920.86 117.75 o 4 6 0 3917.23 3439.18 135.13 o 5 6 0 5869.20 5550.86 182.17 o 6 6 0 1175.41 1041.59 110.45 o 7 6 0 14.05 58.78 65.97 o 8 6 0 1127.33 992.82 157.50 o 1 7 0 277.04 251.80 32.95 o 2 7 0 1412.57 1549.47 75.62 o 3 7 0 772.62 663.78 65.32 o 4 7 0 146.53 111.13 52.45 o 5 7 0 8622.13 7974.26 218.15 o 6 7 0 51.79 85.93 72.77 o 7 7 0 2608.25 2828.14 178.37 o 8 7 0 5.26 -17.81 79.09 o 0 8 0 6120.73 6910.50 169.98 o 1 8 0 1147.21 1318.61 65.25 o 2 8 0 777.74 1000.16 49.24 o 3 8 0 512.51 438.32 120.21 o 4 8 0 10902.79 10404.36 230.05 o 5 8 0 1044.35 1053.87 101.81 o 6 8 0 63.01 100.98 67.26 o 7 8 0 98.09 -7.24 74.02 o 8 8 0 3032.88 3518.09 242.66 o 1 9 0 7624.09 8248.68 136.21 o 2 9 0 4549.66 4865.09 129.43 o 3 9 0 2016.69 1809.03 99.02 o 4 9 0 3359.09 3357.48 137.64 o 5 9 0 256.73 258.37 94.19 o 6 9 0 2648.28 2531.49 157.92 o 7 9 0 353.07 179.43 92.87 o 8 9 0 511.95 444.86 106.75 o 0 10 0 4031.73 3184.29 126.49 o 1 10 0 85.79 105.39 32.68 o 2 10 0 1860.13 1768.74 86.69 o 3 10 0 2830.29 2644.66 117.70 o 4 10 0 1334.02 1263.55 114.51 o 5 10 0 890.63 830.35 97.69 o 6 10 0 18.25 -17.01 72.50 o 7 10 0 41.12 86.27 88.75 o 8 10 0 697.63 690.78 172.54 o 1 11 0 6515.06 6709.76 134.35 o 2 11 0 1657.88 1605.47 96.81 o 3 11 0 3171.69 3122.40 127.08 o 4 11 0 2668.03 2437.73 129.77 o 5 11 0 1063.13 1100.41 105.09 o 6 11 0 936.10 799.44 123.15 o 7 11 0 931.24 585.14 151.31 o 8 11 0 2244.68 2437.89 223.45 o 0 12 0 1672.85 1767.79 114.36 o 1 12 0 1510.05 1545.14 76.29 o 2 12 0 25257.36 25923.67 303.37 o 3 12 0 97.62 53.36 48.71 o 4 12 0 10649.53 10417.65 245.77 o 5 12 0 77.29 -18.64 52.48 o 6 12 0 580.53 618.80 97.77 o 7 12 0 53.98 31.05 89.84 o 8 12 0 1653.76 1880.31 169.99 o 1 13 0 7066.90 6940.14 148.71 o 2 13 0 1479.27 1586.04 81.85 o 3 13 0 1732.45 1971.09 99.37 o 4 13 0 216.57 160.93 62.68 o 5 13 0 6.16 -96.26 47.26 o 6 13 0 1781.32 1669.83 162.10 o 7 13 0 256.45 427.76 110.14 o 8 13 0 73.36 -23.81 103.48 o 0 14 0 6407.53 5922.70 202.13 o 1 14 0 6115.52 6316.06 148.96 o 2 14 0 18.93 56.55 40.30 o 3 14 0 4035.53 4195.88 159.65 o 4 14 0 687.26 764.07 93.36 o 5 14 0 402.75 528.28 86.89 o 6 14 0 3.23 64.05 62.83 o 7 14 0 1389.72 1594.12 177.30 o 1 15 0 181.55 105.06 45.72 o 2 15 0 4348.33 4511.48 131.41 o 3 15 0 3905.22 3937.85 165.99 o 4 15 0 480.59 443.25 85.44 o 5 15 0 1569.74 1515.10 130.72 o 6 15 0 843.23 961.92 117.59 o 7 15 0 378.67 444.14 117.32 o 0 16 0 822.40 729.32 101.31 o 1 16 0 5247.09 5144.41 144.89 o 2 16 0 4211.83 4234.83 160.54 o 3 16 0 1161.67 1319.10 91.30 o 4 16 0 53.23 137.36 63.98 o 5 16 0 16.26 56.44 109.72 o 6 16 0 83.90 21.19 75.30 o 7 16 0 181.80 149.76 114.17 o 1 17 0 1651.32 1654.54 130.39 o 2 17 0 3.16 38.13 47.80 o 3 17 0 329.07 306.79 57.52 o 4 17 0 4.88 173.99 79.52 o 5 17 0 774.08 836.36 110.10 o 6 17 0 1204.04 1148.61 139.13 o 7 17 0 5731.70 5689.92 364.96 o 0 18 0 945.23 1011.44 125.57 o 1 18 0 5544.97 5525.99 158.27 o 2 18 0 25.33 71.53 60.60 o 3 18 0 1934.68 2036.19 108.29 o 4 18 0 3864.66 3854.43 185.14 o 5 18 0 1431.28 1549.93 138.47 o 6 18 0 4.51 -65.89 72.47 o 7 18 0 46.39 -23.36 156.93 o 1 19 0 3805.05 3912.21 142.02 o 2 19 0 202.76 102.70 66.88 o 3 19 0 5057.97 5386.20 200.68 o 4 19 0 741.97 851.42 109.96 o 5 19 0 9.90 15.68 68.67 o 6 19 0 529.53 198.11 110.51 o 7 19 0 0.09 51.29 119.90 o 0 20 0 1867.83 1685.80 153.13 o 1 20 0 166.75 171.95 60.26 o 2 20 0 132.61 53.96 100.01 o 3 20 0 215.48 204.75 75.31 o 4 20 0 867.34 935.25 117.66 o 5 20 0 110.56 55.55 79.69 o 6 20 0 3.05 118.28 96.26 o 1 21 0 29.93 -19.94 54.31 o 2 21 0 5142.97 4615.53 204.40 o 3 21 0 835.25 844.60 109.72 o 4 21 0 2640.79 2717.46 176.12 o 5 21 0 3529.46 3718.24 294.93 o 6 21 0 185.38 116.45 112.75 o 0 22 0 844.98 810.50 129.28 o 1 22 0 1387.65 1445.51 109.34 o 2 22 0 3511.02 3375.88 179.42 o 3 22 0 29.14 -34.10 109.29 o 4 22 0 9198.38 9660.99 292.53 o 5 22 0 95.02 65.90 93.60 o 6 22 0 157.61 413.22 201.89 o 1 23 0 656.63 565.07 83.07 o 2 23 0 1.42 -41.66 56.33 o 3 23 0 3132.60 3115.63 219.34 o 4 23 0 5.64 1.64 74.82 o 5 23 0 3.15 -35.98 122.72 o 6 23 0 928.05 1056.54 261.57 o 0 24 0 3430.62 3538.17 224.80 o 1 24 0 758.74 756.03 92.12 o 2 24 0 2070.34 2158.43 131.81 o 3 24 0 20.29 66.40 94.66 o 4 24 0 1153.54 1235.09 167.69 o 5 24 0 41.88 124.61 113.25 o 1 25 0 2689.51 2904.76 170.49 o 2 25 0 11.11 69.13 60.72 o 3 25 0 2329.65 2528.23 176.42 o 4 25 0 1079.52 886.67 209.05 o 5 25 0 87.23 67.03 133.19 o 0 26 0 74.52 79.92 98.54 o 1 26 0 718.63 825.22 109.02 o 2 26 0 1249.47 1337.68 133.76 o 3 26 0 2958.33 2998.47 192.84 o 4 26 0 1402.47 1495.38 181.14 o 5 26 0 21.64 5.36 209.70 o 1 27 0 2039.88 1997.85 155.99 o 2 27 0 357.49 439.80 101.45 o 3 27 0 122.65 75.26 102.42 o 4 27 0 531.27 469.05 162.04 o 0 28 0 4034.31 4003.62 314.57 o 1 28 0 252.57 388.04 86.60 o 2 28 0 13.22 118.97 81.92 o 3 28 0 607.49 554.56 123.65 o 4 28 0 532.44 564.89 185.07 o 1 29 0 3332.18 3619.22 194.30 o 2 29 0 1.95 -125.26 83.35 o 3 29 0 916.61 1041.60 257.99 o 0 30 0 850.66 882.48 338.86 o 1 30 0 748.25 966.74 121.90 o 2 30 0 221.75 -36.99 129.52 o 1 31 0 145.02 241.03 107.15 o -7 0 1 2.54 -28.60 99.46 o -5 0 1 8364.02 8267.19 250.97 o -3 0 1 2701.05 2283.18 199.80 o -1 0 1 172.96 228.23 23.82 o 1 0 1 28.05 23.17 22.98 o 3 0 1 1388.97 1475.00 134.41 o 5 0 1 84.16 147.54 64.68 o 7 0 1 1006.23 848.37 344.13 o -8 1 1 1836.80 1699.23 186.90 o -7 1 1 2718.39 2895.82 189.87 o -6 1 1 2010.67 2122.72 128.49 o -5 1 1 267.19 216.77 49.07 o -4 1 1 1184.25 1207.76 74.01 o -3 1 1 1452.25 1350.05 62.16 o -2 1 1 31531.25 31901.28 427.62 o -1 1 1 12462.19 12775.53 113.62 o 1 1 1 26647.27 28088.90 377.61 o 2 1 1 185.29 227.98 31.03 o 3 1 1 186.10 181.22 37.52 o 4 1 1 390.41 438.28 61.87 o 5 1 1 1812.13 1779.73 96.85 o 6 1 1 663.84 728.33 84.32 o 7 1 1 15.61 -54.61 81.11 o 8 1 1 155.91 133.24 102.88 o -8 2 1 3510.58 3655.55 254.09 o -7 2 1 10141.58 9910.54 298.60 o -6 2 1 52.31 -16.42 43.02 o -5 2 1 9.63 63.88 61.59 o -4 2 1 1699.48 1699.73 82.42 o -3 2 1 113.70 27.09 27.39 o -2 2 1 73.86 22.87 20.98 o -1 2 1 53051.25 52795.14 342.24 o 0 2 1 2145.10 2415.12 32.41 o 1 2 1 24131.79 25213.77 204.61 o 2 2 1 94.61 118.47 27.52 o 3 2 1 9333.06 9326.59 151.78 o 4 2 1 86.65 -0.47 40.13 o 5 2 1 6362.15 6130.79 174.03 o 6 2 1 5291.45 5365.89 161.76 o 7 2 1 43.11 32.52 66.96 o 8 2 1 662.84 527.18 134.59 o -8 3 1 734.50 564.61 128.38 o -7 3 1 951.81 958.21 137.22 o -6 3 1 3889.74 3817.96 175.17 o -5 3 1 1521.77 1671.47 89.90 o -4 3 1 166.22 210.71 46.56 o -3 3 1 4242.91 4491.02 98.83 o -2 3 1 355.98 512.15 68.47 o -1 3 1 1156.71 1098.37 30.76 o 0 3 1 11179.14 11372.48 102.60 o 1 3 1 980.98 984.81 27.70 o 2 3 1 254.20 168.96 22.09 o 3 3 1 13811.29 13875.64 188.32 o 4 3 1 79.46 18.72 36.42 o 5 3 1 390.98 376.36 65.28 o 6 3 1 64.55 36.44 45.05 o 7 3 1 8.87 -78.02 58.67 o 8 3 1 39.57 194.42 106.02 o -8 4 1 2081.50 1973.72 232.26 o -7 4 1 311.45 208.34 109.53 o -6 4 1 539.83 674.45 103.40 o -5 4 1 6018.31 6210.12 147.33 o -4 4 1 4201.11 3931.36 167.76 o -3 4 1 743.66 611.91 33.99 o -2 4 1 984.54 992.24 64.06 o -1 4 1 20011.07 20842.42 174.43 o 0 4 1 1185.53 1433.43 37.33 o 1 4 1 4487.53 4605.97 99.44 o 2 4 1 20.00 -25.04 33.18 o 3 4 1 5794.48 5727.97 110.28 o 4 4 1 3266.01 3321.79 120.73 o 5 4 1 50.58 96.27 48.68 o 6 4 1 144.75 229.86 69.58 o 7 4 1 2003.05 2303.04 179.79 o 8 4 1 2382.12 2587.52 228.22 o -8 5 1 45.09 10.68 94.18 o -7 5 1 248.07 156.72 173.19 o -6 5 1 1238.52 1093.41 110.80 o -5 5 1 270.08 286.75 47.17 o -4 5 1 71.22 64.95 25.53 o -3 5 1 1665.83 1595.00 85.59 o -2 5 1 3332.17 2732.37 87.25 o -1 5 1 882.90 902.83 52.21 o 0 5 1 2706.74 2851.71 61.83 o 1 5 1 78.38 58.55 21.46 o 2 5 1 85.39 91.29 34.29 o 3 5 1 47.52 -16.26 27.26 o 4 5 1 2109.55 1988.60 77.28 o 5 5 1 248.36 202.66 47.54 o 6 5 1 1026.45 1121.78 113.42 o 7 5 1 1715.31 1692.45 146.26 o 8 5 1 13.62 48.77 101.36 o -8 6 1 31.52 94.00 81.44 o -7 6 1 661.76 553.57 139.62 o -6 6 1 8.98 24.25 61.43 o -5 6 1 2591.04 2687.66 165.70 o -4 6 1 10851.05 10771.34 250.69 o -3 6 1 1648.09 1589.76 87.35 o -2 6 1 255.69 173.66 38.20 o -1 6 1 4786.06 4500.16 85.05 o 0 6 1 2334.68 2226.03 61.55 o 1 6 1 50194.42 50466.93 409.34 o 2 6 1 14.98 57.96 23.20 o 3 6 1 3530.07 3607.33 189.42 o 4 6 1 2554.72 2292.11 117.14 o 5 6 1 8058.85 7646.78 213.62 o 6 6 1 2102.12 2220.10 146.96 o 7 6 1 950.26 992.72 119.74 o 8 6 1 1151.77 1439.33 194.67 o -8 7 1 144.40 0.15 78.87 o -7 7 1 334.71 441.76 107.33 o -6 7 1 181.89 159.91 68.11 o -5 7 1 282.96 230.83 64.03 o -4 7 1 10.15 -17.58 40.97 o -3 7 1 1224.40 1336.67 90.67 o -2 7 1 2442.62 2553.71 52.88 o -1 7 1 17481.13 17582.10 223.03 o 0 7 1 6370.24 6460.74 108.60 o 1 7 1 24244.95 25419.63 251.54 o 2 7 1 1828.59 1473.21 47.89 o 3 7 1 157.45 191.84 62.97 o 4 7 1 4055.16 3774.46 139.78 o 5 7 1 1253.55 1267.86 107.77 o 6 7 1 169.81 219.43 84.16 o 7 7 1 409.54 428.78 95.96 o 8 7 1 737.24 704.83 182.22 o -8 8 1 4311.00 4047.01 227.29 o -7 8 1 617.80 520.82 148.10 o -6 8 1 50.72 20.43 58.19 o -5 8 1 1614.23 1592.66 133.17 o -4 8 1 1019.58 922.77 87.00 o -3 8 1 1002.04 1090.81 79.95 o -2 8 1 1642.81 1477.73 47.62 o -1 8 1 1103.21 1314.23 56.79 o 0 8 1 0.95 -5.06 29.58 o 1 8 1 8964.99 8969.40 137.16 o 2 8 1 1363.97 1330.11 46.33 o 3 8 1 9656.22 9342.80 327.72 o 4 8 1 3334.05 3125.23 224.33 o 5 8 1 11964.31 11976.21 272.66 o 6 8 1 326.86 273.89 86.34 o 7 8 1 846.21 981.12 123.50 o 8 8 1 886.10 986.22 136.67 o -8 9 1 348.70 253.95 91.63 o -7 9 1 422.70 478.01 97.29 o -6 9 1 461.76 252.06 139.21 o -5 9 1 1695.63 1562.25 121.22 o -4 9 1 3339.22 3152.37 175.37 o -3 9 1 1250.55 1420.95 91.37 o -2 9 1 33130.50 33733.64 333.32 o -1 9 1 9838.21 9814.07 150.82 o 0 9 1 5510.67 5067.72 107.25 o 1 9 1 7494.65 7601.77 131.83 o 2 9 1 11391.03 12050.99 170.36 o 3 9 1 2220.22 1951.28 100.93 o 4 9 1 4110.86 4052.79 149.77 o 5 9 1 634.86 681.02 89.73 o 6 9 1 2906.19 2992.27 194.45 o 7 9 1 292.24 235.14 88.46 o 8 9 1 1864.08 1855.92 170.43 o -8 10 1 11.66 109.76 106.34 o -7 10 1 53.85 -61.09 91.01 o -6 10 1 73.75 59.03 68.22 o -5 10 1 3295.01 3087.07 183.19 o -4 10 1 707.11 768.09 82.26 o -3 10 1 19402.77 18472.79 296.48 o -2 10 1 113.11 154.56 35.05 o -1 10 1 20.60 16.87 50.50 o 0 10 1 2074.81 2147.76 77.22 o 1 10 1 4402.45 4306.30 103.45 o 2 10 1 1871.00 2161.24 120.24 o 3 10 1 7.55 69.36 45.41 o 4 10 1 346.49 313.32 73.13 o 5 10 1 7.29 24.07 52.69 o 6 10 1 510.13 558.88 103.37 o 7 10 1 5865.30 5684.62 302.76 o 8 10 1 730.44 826.92 129.96 o -8 11 1 128.18 106.00 103.74 o -7 11 1 359.15 271.89 106.11 o -6 11 1 1477.30 1322.81 127.48 o -5 11 1 258.28 351.59 73.76 o -4 11 1 596.16 732.97 83.16 o -3 11 1 50.47 -29.50 39.83 o -2 11 1 1533.73 1350.93 68.55 o -1 11 1 7205.62 6542.07 132.77 o 0 11 1 14206.87 14068.72 199.89 o 1 11 1 81.06 65.86 40.83 o 2 11 1 7424.88 6842.64 135.89 o 3 11 1 4921.90 4788.01 151.61 o 4 11 1 491.67 456.10 72.79 o 5 11 1 27.78 3.47 51.42 o 6 11 1 1630.41 1837.24 201.97 o 7 11 1 98.69 -70.43 86.49 o 8 11 1 28.81 -54.05 91.13 o -8 12 1 393.22 536.63 110.61 o -7 12 1 3265.43 3224.03 218.20 o -6 12 1 3370.81 3382.71 209.02 o -5 12 1 154.59 99.83 73.86 o -4 12 1 2903.96 2944.45 140.04 o -3 12 1 250.43 389.41 40.18 o -2 12 1 6.25 27.93 38.40 o -1 12 1 2448.59 2291.00 87.89 o 0 12 1 1658.83 1805.29 81.56 o 1 12 1 4519.83 4565.13 116.35 o 2 12 1 83.88 63.32 38.11 o 3 12 1 5540.96 5522.66 159.31 o 4 12 1 15.03 80.68 50.06 o 5 12 1 200.62 238.34 70.79 o 6 12 1 7.18 137.27 69.54 o 7 12 1 0.62 32.97 71.78 o 8 12 1 0.54 -15.68 108.88 o -8 13 1 74.07 -74.17 169.82 o -7 13 1 827.27 720.09 116.73 o -6 13 1 2238.59 2074.51 198.40 o -5 13 1 3674.41 3608.37 171.95 o -4 13 1 1644.10 1733.03 132.33 o -3 13 1 1061.17 1212.90 69.58 o -2 13 1 94.53 41.67 40.90 o -1 13 1 3454.30 3422.84 107.13 o 0 13 1 1200.07 1153.66 73.42 o 1 13 1 13550.14 12970.43 208.22 o 2 13 1 8092.12 7444.19 166.31 o 3 13 1 974.51 818.46 58.79 o 4 13 1 537.92 483.72 83.55 o 5 13 1 2375.99 2036.37 138.88 o 6 13 1 3419.52 3255.38 201.76 o 7 13 1 449.13 572.60 110.36 o 8 13 1 749.38 772.35 167.29 o -7 14 1 1.51 60.19 84.05 o -6 14 1 190.30 216.60 98.63 o -5 14 1 6008.84 6016.31 209.39 o -4 14 1 2717.04 2697.83 143.69 o -3 14 1 6296.08 6111.06 158.13 o -2 14 1 961.44 1212.38 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