#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216407.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216407_Fobs loop_ _publ_author_name 'Zhu, Licai' 'Sun, Feng' _publ_section_title ; Poly[[diaqua-\m~3~-malonato-iron(II)] monohydrate] ; _journal_coeditor_code DN2256 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2966 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.2225 _cell_length_b 8.2788 _cell_length_c 14.7043 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.8257 _[local]_cod_data_source_file dn2256Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xb1328m in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 228.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 52258.13 48686.62 364.05 o 4 0 0 14675.89 14854.53 138.87 o 6 0 0 204.89 229.57 16.85 o 8 0 0 2623.35 2919.62 65.08 o 10 0 0 1455.39 1416.85 32.30 o 12 0 0 8497.95 8289.90 91.68 o 14 0 0 1620.16 1588.84 63.81 o 16 0 0 648.53 649.73 45.45 o 2 1 0 26666.93 28619.79 110.86 o 4 1 0 13567.73 13653.04 71.18 o 6 1 0 24332.97 24074.86 126.43 o 8 1 0 30874.80 31346.17 312.86 o 10 1 0 2316.01 2121.14 34.18 o 12 1 0 1979.13 1954.23 36.17 o 14 1 0 17.30 40.75 11.07 o 16 1 0 0.16 9.06 9.70 o 0 2 0 21530.54 22706.47 173.16 o 2 2 0 5574.03 4907.93 27.78 o 4 2 0 4192.10 3834.55 24.79 o 6 2 0 10809.95 11768.59 121.30 o 8 2 0 2031.81 2240.40 28.07 o 10 2 0 1355.87 1305.27 27.61 o 12 2 0 2422.08 2431.74 41.42 o 14 2 0 1641.96 1641.85 36.55 o 16 2 0 1429.74 1396.57 46.08 o 2 3 0 30157.50 31347.73 134.29 o 4 3 0 1593.39 1493.26 15.08 o 6 3 0 10772.28 11109.81 56.87 o 8 3 0 3201.88 3425.70 36.02 o 10 3 0 1309.70 1291.05 23.96 o 12 3 0 557.60 581.95 21.01 o 14 3 0 67.25 35.05 8.85 o 16 3 0 10.11 28.98 14.61 o 0 4 0 547.89 540.41 12.00 o 2 4 0 565.62 586.69 11.79 o 4 4 0 12.25 19.49 3.43 o 6 4 0 974.02 1047.79 23.90 o 8 4 0 264.34 241.48 12.70 o 10 4 0 427.53 342.61 33.40 o 12 4 0 6.73 2.15 6.91 o 14 4 0 124.07 96.12 15.94 o 2 5 0 403.34 454.43 12.65 o 4 5 0 3399.84 3453.87 34.40 o 6 5 0 1415.36 1276.07 21.77 o 8 5 0 306.02 325.96 15.38 o 10 5 0 82.40 52.90 8.59 o 12 5 0 59.29 52.45 16.24 o 14 5 0 365.52 363.37 25.91 o 0 6 0 765.25 630.50 22.46 o 2 6 0 589.44 611.25 18.37 o 4 6 0 2504.89 2474.88 37.29 o 6 6 0 1.76 6.49 5.21 o 8 6 0 23.17 25.30 6.99 o 10 6 0 78.01 73.29 10.23 o 12 6 0 766.68 786.10 27.72 o 2 7 0 3017.55 3094.26 44.45 o 4 7 0 6163.22 6529.56 151.58 o 6 7 0 2080.88 2181.13 49.93 o 8 7 0 1888.80 1818.72 48.05 o 10 7 0 2034.84 1885.93 51.46 o 12 7 0 599.24 606.97 31.95 o 0 8 0 7869.06 8509.19 112.81 o 2 8 0 5500.73 5682.25 121.96 o 4 8 0 1768.63 1831.45 111.74 o 6 8 0 126.40 145.68 16.74 o 8 8 0 29.12 17.07 10.02 o 10 8 0 99.01 81.21 19.19 o 2 9 0 48.93 23.87 7.52 o 4 9 0 107.53 121.29 46.42 o 6 9 0 963.48 1076.48 64.95 o 0 10 0 484.84 533.52 28.38 o 1 1 1 1234.00 1093.59 7.81 o 2 1 1 4249.88 4469.35 29.04 o 3 1 1 1060.38 956.94 13.05 o 4 1 1 24751.04 26085.87 186.10 o 5 1 1 66.51 79.01 4.38 o 6 1 1 6031.00 6213.25 58.59 o 7 1 1 725.78 917.71 13.36 o 8 1 1 4447.83 4410.64 45.52 o 9 1 1 0.85 4.01 2.78 o 10 1 1 10.03 3.47 3.04 o 11 1 1 268.75 296.57 10.51 o 12 1 1 3.85 6.19 4.28 o 13 1 1 24.70 21.81 5.54 o 14 1 1 9.04 3.19 4.76 o 15 1 1 257.48 231.46 16.55 o 16 1 1 138.83 148.92 16.35 o 17 1 1 106.20 119.85 12.83 o 0 2 1 19307.00 18986.73 156.77 o 1 2 1 13555.06 15156.82 49.26 o 2 2 1 4431.46 4493.67 24.60 o 3 2 1 11.26 17.15 2.04 o 4 2 1 39.48 7.74 1.37 o 5 2 1 2687.74 2562.27 17.62 o 6 2 1 79.34 127.65 4.73 o 7 2 1 6670.63 6643.22 53.40 o 8 2 1 40.81 45.52 10.51 o 9 2 1 3845.80 3774.89 32.06 o 10 2 1 327.29 313.99 15.56 o 11 2 1 162.88 141.18 7.93 o 12 2 1 1337.51 1376.72 21.91 o 13 2 1 1761.24 1680.35 27.12 o 14 2 1 1239.89 1217.75 25.32 o 15 2 1 27.19 16.00 6.18 o 16 2 1 350.74 372.23 18.37 o 1 3 1 14536.07 14013.49 44.10 o 2 3 1 1468.21 1390.12 9.92 o 3 3 1 5407.91 5415.50 23.43 o 4 3 1 6639.84 6885.96 33.79 o 5 3 1 1773.78 1644.47 12.19 o 6 3 1 13100.98 12902.13 80.53 o 7 3 1 15.52 46.75 3.79 o 8 3 1 4086.19 3962.64 27.63 o 9 3 1 138.70 137.86 6.16 o 10 3 1 4059.45 4084.26 33.08 o 11 3 1 996.17 1011.35 18.38 o 12 3 1 451.37 432.93 12.90 o 13 3 1 808.90 824.11 18.10 o 14 3 1 614.07 613.81 21.34 o 15 3 1 1039.61 1021.55 41.21 o 16 3 1 42.96 31.06 9.25 o 0 4 1 14828.69 15133.42 84.39 o 1 4 1 65.82 97.00 3.31 o 2 4 1 28980.10 29220.77 89.11 o 3 4 1 12481.27 12798.57 65.37 o 4 4 1 7897.02 8066.24 41.72 o 5 4 1 7180.50 7672.22 34.90 o 6 4 1 1086.60 1114.46 12.31 o 7 4 1 2184.28 2050.92 17.29 o 8 4 1 6.55 4.15 2.76 o 9 4 1 2758.12 2701.76 34.00 o 10 4 1 871.90 841.73 17.25 o 11 4 1 239.56 257.63 12.88 o 12 4 1 389.97 395.06 14.94 o 13 4 1 548.52 568.36 20.18 o 14 4 1 544.23 555.68 26.48 o 15 4 1 130.14 104.00 11.33 o 1 5 1 1358.34 1329.14 14.74 o 2 5 1 1330.77 1305.74 13.53 o 3 5 1 9522.77 9469.05 42.70 o 4 5 1 3389.68 3301.87 24.74 o 5 5 1 2412.15 2348.15 20.28 o 6 5 1 1223.82 1225.12 16.46 o 7 5 1 170.29 158.77 8.27 o 8 5 1 2538.27 2468.67 28.45 o 9 5 1 309.65 315.65 11.18 o 10 5 1 2000.68 2096.67 28.23 o 11 5 1 286.01 300.86 12.12 o 12 5 1 1083.66 1150.90 22.57 o 13 5 1 356.66 381.75 16.54 o 14 5 1 35.36 38.47 13.03 o 0 6 1 3245.45 3213.46 35.49 o 1 6 1 159.54 185.90 7.97 o 2 6 1 2442.12 2418.01 25.47 o 3 6 1 244.45 217.44 8.63 o 4 6 1 1535.24 1488.00 20.25 o 5 6 1 2351.94 2404.86 24.01 o 6 6 1 9.56 9.58 3.76 o 7 6 1 966.96 948.05 18.63 o 8 6 1 0.09 -1.11 3.50 o 9 6 1 850.66 897.52 20.62 o 10 6 1 423.59 424.53 13.70 o 11 6 1 210.89 237.68 12.31 o 12 6 1 720.73 680.07 18.40 o 13 6 1 367.38 360.57 14.80 o 1 7 1 358.50 337.26 9.92 o 2 7 1 166.81 159.49 13.08 o 3 7 1 1769.00 1781.45 34.58 o 4 7 1 1142.10 1150.11 19.54 o 5 7 1 54.29 51.23 6.73 o 6 7 1 401.03 391.50 15.58 o 7 7 1 122.09 99.63 12.20 o 8 7 1 442.91 421.83 16.94 o 9 7 1 544.64 463.72 18.40 o 10 7 1 440.38 405.91 22.29 o 11 7 1 18.25 16.58 7.06 o 12 7 1 27.35 8.71 6.79 o 0 8 1 904.12 926.81 30.09 o 1 8 1 10.09 3.74 3.88 o 2 8 1 153.25 148.24 8.62 o 3 8 1 52.53 34.40 6.55 o 4 8 1 22.08 21.73 6.26 o 5 8 1 375.21 333.90 18.10 o 6 8 1 61.17 65.67 9.58 o 7 8 1 29.25 20.70 7.45 o 8 8 1 190.86 192.97 14.06 o 9 8 1 19.04 8.36 6.52 o 10 8 1 56.82 51.09 9.26 o 1 9 1 0.49 0.23 4.49 o 2 9 1 517.78 509.83 14.27 o 3 9 1 19.30 11.07 5.57 o 4 9 1 439.02 475.21 19.46 o 5 9 1 166.39 147.44 19.78 o 6 9 1 284.18 273.23 16.57 o 7 9 1 17.37 22.32 8.15 o 0 10 1 214.20 211.34 17.68 o 0 0 2 8.84 -3.09 2.06 o 1 0 2 2548.10 2671.10 25.84 o 2 0 2 11160.02 11959.66 57.10 o 3 0 2 1804.51 2389.75 19.89 o 4 0 2 7949.32 8409.84 112.31 o 5 0 2 17452.31 16946.52 359.61 o 6 0 2 22.66 30.58 4.06 o 7 0 2 35098.55 35912.95 412.67 o 8 0 2 0.78 -0.98 4.18 o 9 0 2 2688.64 2542.21 47.73 o 10 0 2 345.66 291.28 13.37 o 11 0 2 1605.41 1624.92 40.17 o 12 0 2 1183.71 1154.89 51.92 o 13 0 2 1914.50 1993.22 37.85 o 14 0 2 345.50 300.79 19.92 o 15 0 2 815.60 874.12 35.68 o 16 0 2 34.89 30.52 11.42 o 17 0 2 1.77 12.96 10.18 o 1 1 2 24878.03 24257.46 173.16 o 2 1 2 1186.47 1191.57 8.92 o 3 1 2 5219.62 4737.52 47.69 o 4 1 2 649.76 597.92 8.44 o 5 1 2 15061.81 15290.15 160.69 o 6 1 2 1060.65 1161.40 12.01 o 7 1 2 4495.52 4596.56 27.65 o 8 1 2 156.33 248.19 9.88 o 9 1 2 3.58 14.32 7.29 o 10 1 2 19.76 24.72 4.52 o 11 1 2 16.48 12.35 4.20 o 12 1 2 26.20 16.74 4.70 o 13 1 2 3799.90 3780.82 41.93 o 14 1 2 543.78 514.65 16.60 o 15 1 2 3975.03 3797.87 90.13 o 16 1 2 3.79 7.64 6.39 o 17 1 2 1064.11 1146.34 38.41 o 0 2 2 14085.17 15233.25 98.40 o 1 2 2 7123.67 7820.09 32.88 o 2 2 2 3411.21 3521.71 14.70 o 3 2 2 2592.09 2341.04 16.70 o 4 2 2 1897.95 2153.47 14.39 o 5 2 2 1843.95 1572.68 12.66 o 6 2 2 2.68 1.33 1.91 o 7 2 2 10268.87 10193.27 122.06 o 8 2 2 81.61 113.19 5.69 o 9 2 2 3456.41 3250.33 27.44 o 10 2 2 23.39 23.23 4.72 o 11 2 2 4161.53 4198.40 58.23 o 12 2 2 278.25 258.56 10.85 o 13 2 2 2017.62 2000.66 45.48 o 14 2 2 397.59 391.55 16.83 o 15 2 2 0.86 2.61 5.04 o 16 2 2 50.78 45.07 8.19 o 1 3 2 6560.11 6569.65 33.89 o 2 3 2 448.91 496.22 6.18 o 3 3 2 111.58 44.26 2.70 o 4 3 2 31.69 30.04 2.06 o 5 3 2 1503.80 1421.12 14.03 o 6 3 2 16.61 34.28 2.94 o 7 3 2 1960.77 2078.81 17.33 o 8 3 2 4.85 4.94 2.64 o 9 3 2 3042.42 3050.82 35.61 o 10 3 2 110.90 103.99 7.63 o 11 3 2 116.28 105.11 6.80 o 12 3 2 475.70 458.28 25.93 o 13 3 2 84.20 90.61 7.78 o 14 3 2 314.02 308.67 14.01 o 15 3 2 60.05 68.16 9.80 o 16 3 2 3.14 8.17 7.36 o 0 4 2 1412.37 1556.55 16.52 o 1 4 2 550.67 555.10 6.96 o 2 4 2 3443.54 3710.36 20.16 o 3 4 2 10.80 27.18 2.35 o 4 4 2 508.08 499.37 7.47 o 5 4 2 509.76 458.76 7.50 o 6 4 2 114.34 139.88 5.47 o 7 4 2 167.01 174.70 6.35 o 8 4 2 221.44 241.19 7.50 o 9 4 2 0.77 2.39 3.21 o 10 4 2 173.15 157.46 8.60 o 11 4 2 90.09 114.51 8.92 o 12 4 2 98.78 86.39 8.41 o 13 4 2 436.07 362.63 16.91 o 14 4 2 73.41 52.91 9.14 o 15 4 2 40.34 40.22 13.91 o 1 5 2 2392.97 2347.20 20.10 o 2 5 2 2038.16 2117.30 17.44 o 3 5 2 1327.82 1313.38 14.25 o 4 5 2 118.51 146.77 5.77 o 5 5 2 651.53 718.49 11.37 o 6 5 2 1343.76 1327.48 17.55 o 7 5 2 48.19 55.56 5.07 o 8 5 2 0.52 2.71 3.08 o 9 5 2 10.13 15.92 4.33 o 10 5 2 668.56 632.78 15.75 o 11 5 2 801.66 768.67 18.01 o 12 5 2 10.60 4.09 5.06 o 13 5 2 294.16 297.72 14.55 o 14 5 2 2.65 17.28 7.11 o 0 6 2 417.99 389.88 12.73 o 1 6 2 5.66 2.69 3.16 o 2 6 2 906.79 949.53 15.96 o 3 6 2 280.13 295.49 9.71 o 4 6 2 9.34 6.61 3.92 o 5 6 2 1328.95 1295.06 19.58 o 6 6 2 149.51 144.55 7.97 o 7 6 2 858.85 848.30 15.32 o 8 6 2 55.36 36.96 5.25 o 9 6 2 2980.36 3028.63 39.97 o 10 6 2 567.64 521.10 15.10 o 11 6 2 2872.20 2882.48 36.10 o 12 6 2 15.92 18.47 5.66 o 13 6 2 393.54 419.55 22.98 o 1 7 2 1016.43 1022.99 16.36 o 2 7 2 188.64 168.97 8.62 o 3 7 2 3735.86 3800.15 35.45 o 4 7 2 1282.00 1303.18 33.53 o 5 7 2 1919.84 1983.75 37.47 o 6 7 2 1073.46 1089.82 22.09 o 7 7 2 202.22 199.11 12.62 o 8 7 2 669.36 657.85 20.77 o 9 7 2 1.89 6.33 5.42 o 10 7 2 4.20 9.84 6.29 o 11 7 2 265.42 262.79 15.74 o 12 7 2 12.74 16.69 6.64 o 0 8 2 415.68 414.67 15.62 o 1 8 2 42.47 37.08 4.96 o 2 8 2 1031.51 1010.85 19.54 o 3 8 2 708.13 719.13 18.81 o 4 8 2 402.42 400.31 16.22 o 5 8 2 2034.63 2144.59 44.53 o 6 8 2 30.22 26.33 7.31 o 7 8 2 1464.69 1591.64 33.09 o 8 8 2 24.36 17.09 7.96 o 9 8 2 1123.24 1206.35 34.54 o 10 8 2 72.01 58.64 9.76 o 1 9 2 1693.97 1878.45 31.60 o 2 9 2 5.78 -2.49 5.56 o 3 9 2 1421.92 1419.90 33.56 o 4 9 2 128.39 100.81 11.59 o 5 9 2 653.67 603.18 41.20 o 6 9 2 13.27 19.70 9.28 o 7 9 2 120.38 116.09 20.61 o 1 1 3 703.97 500.80 8.14 o 2 1 3 2370.90 2501.21 20.40 o 3 1 3 11.97 38.93 2.30 o 4 1 3 89.29 128.09 4.34 o 5 1 3 2672.82 3078.01 35.06 o 6 1 3 1400.08 1458.44 16.68 o 7 1 3 607.19 660.72 9.82 o 8 1 3 118.12 154.35 7.27 o 9 1 3 1.13 4.25 3.73 o 10 1 3 497.00 505.72 13.69 o 11 1 3 34.99 47.76 6.21 o 12 1 3 169.14 160.15 9.72 o 13 1 3 766.42 791.30 24.47 o 14 1 3 1.07 -6.38 4.25 o 15 1 3 338.45 314.51 14.53 o 16 1 3 0.41 3.28 5.60 o 0 2 3 98.17 163.75 4.87 o 1 2 3 700.18 780.87 6.60 o 2 2 3 4311.12 4145.67 22.92 o 3 2 3 5131.27 5849.98 43.39 o 4 2 3 832.97 942.02 9.26 o 5 2 3 2040.74 1740.02 16.58 o 6 2 3 1237.72 1134.43 13.46 o 7 2 3 6443.04 6295.92 93.15 o 8 2 3 3949.31 4213.80 64.37 o 9 2 3 6033.33 6014.59 81.75 o 10 2 3 6.07 7.66 3.17 o 11 2 3 6691.81 6505.68 85.21 o 12 2 3 266.96 270.75 10.75 o 13 2 3 825.33 791.63 33.40 o 14 2 3 1170.07 1105.03 39.46 o 15 2 3 1076.33 1034.34 37.21 o 16 2 3 85.69 98.95 14.48 o 1 3 3 11059.58 10198.16 64.41 o 2 3 3 2079.57 2250.68 12.65 o 3 3 3 7274.87 7102.10 30.65 o 4 3 3 142.09 95.77 3.20 o 5 3 3 2562.16 2372.56 16.70 o 6 3 3 276.50 237.93 5.93 o 7 3 3 3454.75 3632.96 23.66 o 8 3 3 1937.31 1957.24 32.08 o 9 3 3 51.61 52.62 4.97 o 10 3 3 897.26 850.96 15.01 o 11 3 3 514.40 477.18 12.11 o 12 3 3 284.65 260.03 10.92 o 13 3 3 1968.76 1950.27 31.05 o 14 3 3 174.03 156.75 12.51 o 15 3 3 924.28 862.44 25.36 o 16 3 3 81.95 57.98 11.31 o 0 4 3 19.51 9.78 6.11 o 1 4 3 2647.01 2724.09 16.45 o 2 4 3 1115.75 1066.58 11.99 o 3 4 3 3352.90 3220.59 28.61 o 4 4 3 1231.40 1215.67 12.93 o 5 4 3 5185.72 5013.46 29.10 o 6 4 3 75.84 73.87 4.41 o 7 4 3 4048.21 4020.15 28.11 o 8 4 3 4.54 11.97 3.12 o 9 4 3 3042.26 2987.10 28.18 o 10 4 3 649.52 696.49 17.80 o 11 4 3 3184.47 3228.53 39.26 o 12 4 3 34.72 36.55 6.78 o 13 4 3 104.62 102.37 9.43 o 14 4 3 46.96 53.76 9.42 o 15 4 3 328.48 318.76 20.72 o 1 5 3 4006.14 3958.03 24.25 o 2 5 3 142.27 119.85 4.91 o 3 5 3 4602.67 4350.14 27.04 o 4 5 3 444.33 470.75 10.68 o 5 5 3 5477.99 5517.82 36.22 o 6 5 3 11.89 23.87 4.01 o 7 5 3 2039.52 2062.22 22.97 o 8 5 3 549.48 545.13 12.46 o 9 5 3 306.35 275.09 9.84 o 10 5 3 2121.10 2177.79 28.98 o 11 5 3 449.14 458.05 15.87 o 12 5 3 366.21 377.21 15.62 o 13 5 3 966.58 1022.19 24.81 o 14 5 3 121.84 117.08 10.93 o 0 6 3 109.64 120.05 9.88 o 1 6 3 120.12 102.09 5.81 o 2 6 3 962.20 1022.52 18.08 o 3 6 3 156.86 132.32 7.20 o 4 6 3 2.26 1.05 3.45 o 5 6 3 40.37 29.68 4.79 o 6 6 3 67.17 54.65 5.84 o 7 6 3 390.56 395.23 11.56 o 8 6 3 493.56 476.65 12.33 o 9 6 3 1908.93 1901.92 27.24 o 10 6 3 55.98 51.27 6.54 o 11 6 3 2713.22 2772.30 35.73 o 12 6 3 138.27 113.29 10.51 o 13 6 3 443.39 457.27 18.20 o 1 7 3 324.08 324.33 9.83 o 2 7 3 169.24 160.55 11.05 o 3 7 3 2.41 1.56 4.32 o 4 7 3 794.59 754.52 25.02 o 5 7 3 8.46 3.07 4.94 o 6 7 3 9.52 4.99 4.37 o 7 7 3 31.66 16.53 5.42 o 8 7 3 101.65 101.83 10.16 o 9 7 3 49.59 34.55 7.64 o 10 7 3 14.99 20.58 6.60 o 11 7 3 156.64 126.85 10.91 o 0 8 3 7.12 16.81 7.78 o 1 8 3 1.23 7.34 4.95 o 2 8 3 23.08 18.99 6.42 o 3 8 3 26.45 13.66 6.99 o 4 8 3 47.12 27.81 7.52 o 5 8 3 1.82 6.75 6.18 o 6 8 3 19.02 17.16 8.23 o 7 8 3 7.19 5.05 7.20 o 8 8 3 22.13 16.25 8.66 o 9 8 3 29.63 26.17 9.73 o 1 9 3 49.74 48.49 7.71 o 2 9 3 69.02 50.72 8.15 o 3 9 3 160.17 145.57 13.32 o 4 9 3 3.62 -1.50 8.36 o 5 9 3 84.65 72.93 12.52 o 6 9 3 6.58 -5.28 8.19 o 7 9 3 11.01 19.99 9.81 o 0 0 4 20533.51 19353.12 184.61 o 1 0 4 1.98 3.85 2.66 o 2 0 4 36471.18 35727.18 645.95 o 3 0 4 2537.64 2470.70 34.75 o 4 0 4 833.40 1173.03 13.72 o 5 0 4 1051.56 1448.28 19.38 o 6 0 4 5020.80 5121.38 61.37 o 7 0 4 135.01 59.91 7.66 o 8 0 4 19.22 12.42 4.13 o 9 0 4 5989.34 6035.88 249.27 o 10 0 4 73.07 77.81 11.12 o 11 0 4 1394.07 1407.91 38.21 o 12 0 4 6.07 9.74 8.48 o 13 0 4 1151.19 1089.10 36.75 o 14 0 4 4451.50 4589.02 79.44 o 15 0 4 13.65 7.28 15.10 o 16 0 4 393.05 409.68 27.73 o 1 1 4 7218.71 7083.55 77.42 o 2 1 4 67.57 86.49 3.17 o 3 1 4 3290.85 2994.50 27.88 o 4 1 4 2547.87 3482.71 37.08 o 5 1 4 2196.95 2148.74 24.04 o 6 1 4 10090.97 9807.97 102.93 o 7 1 4 3923.43 4083.70 29.88 o 8 1 4 6352.86 6007.57 71.02 o 9 1 4 624.56 636.62 16.14 o 10 1 4 2671.60 2701.70 30.70 o 11 1 4 951.04 969.92 30.44 o 12 1 4 3178.70 3223.52 84.91 o 13 1 4 447.03 417.83 16.29 o 14 1 4 2194.90 2122.85 73.94 o 15 1 4 758.89 748.92 21.01 o 16 1 4 4.50 11.47 7.41 o 0 2 4 365.73 258.12 6.58 o 1 2 4 1037.54 1105.82 12.39 o 2 2 4 445.19 760.28 7.79 o 3 2 4 2763.52 2463.64 23.84 o 4 2 4 5542.58 5319.63 35.92 o 5 2 4 1261.80 1194.31 16.94 o 6 2 4 5993.46 6050.00 82.84 o 7 2 4 2427.82 2410.85 36.51 o 8 2 4 527.44 582.44 12.06 o 9 2 4 3993.07 3999.82 61.45 o 10 2 4 0.84 5.30 3.21 o 11 2 4 85.80 78.84 6.75 o 12 2 4 75.55 54.27 8.23 o 13 2 4 300.53 302.19 15.26 o 14 2 4 2103.33 2027.65 34.58 o 15 2 4 75.13 63.36 8.65 o 16 2 4 1242.08 1276.37 33.94 o 1 3 4 40.60 20.69 1.81 o 2 3 4 2821.43 2770.15 24.92 o 3 3 4 24.38 10.47 1.59 o 4 3 4 523.22 489.68 7.32 o 5 3 4 209.03 234.98 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13.34 o 2 2 8 3572.81 3593.78 26.88 o 3 2 8 620.08 521.62 13.44 o 4 2 8 474.08 409.87 9.07 o 5 2 8 8356.51 8541.51 52.82 o 6 2 8 2757.74 2782.10 30.05 o 7 2 8 5140.24 4996.68 77.02 o 8 2 8 53.53 49.44 5.25 o 9 2 8 581.49 560.19 14.92 o 10 2 8 177.60 177.46 11.07 o 11 2 8 961.67 1008.94 25.69 o 12 2 8 140.25 119.97 13.98 o 13 2 8 139.18 146.57 12.71 o 14 2 8 1014.40 1029.09 46.47 o 15 2 8 209.49 224.11 27.11 o 1 3 8 1064.25 1004.53 13.78 o 2 3 8 5320.83 5401.55 51.01 o 3 3 8 1970.97 1979.93 19.87 o 4 3 8 1325.44 1330.55 16.44 o 5 3 8 525.09 558.41 12.11 o 6 3 8 415.61 428.69 10.17 o 7 3 8 328.16 333.95 12.36 o 8 3 8 71.25 68.18 7.40 o 9 3 8 166.62 168.16 8.48 o 10 3 8 22.60 22.94 4.95 o 11 3 8 80.48 101.23 9.01 o 12 3 8 2.40 3.02 4.73 o 13 3 8 63.35 77.24 9.03 o 14 3 8 61.00 53.97 10.22 o 0 4 8 602.93 652.86 14.85 o 1 4 8 329.71 339.17 8.20 o 2 4 8 0.07 2.50 2.42 o 3 4 8 39.66 36.48 5.00 o 4 4 8 916.85 925.26 17.96 o 5 4 8 269.71 269.68 8.74 o 6 4 8 391.15 402.56 10.60 o 7 4 8 2.72 4.50 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8.36 o 8 5 9 3091.59 3293.35 37.35 o 9 5 9 0.56 7.58 5.21 o 10 5 9 3005.10 3214.04 42.46 o 11 5 9 3.45 5.51 6.14 o 12 5 9 1216.57 1374.10 33.34 o 0 6 9 1096.85 1096.83 90.60 o 1 6 9 195.24 182.47 10.10 o 2 6 9 1049.50 1057.85 27.18 o 3 6 9 19.26 10.05 5.10 o 4 6 9 1457.08 1444.62 61.68 o 5 6 9 4.55 0.94 4.38 o 6 6 9 377.69 375.18 15.04 o 7 6 9 236.73 242.84 17.00 o 8 6 9 96.87 106.44 9.83 o 9 6 9 160.17 160.07 11.81 o 10 6 9 238.68 263.55 16.47 o 1 7 9 355.14 276.90 15.24 o 2 7 9 150.29 154.69 14.81 o 3 7 9 12.16 11.16 8.23 o 4 7 9 651.89 648.22 31.51 o 5 7 9 66.05 59.88 11.52 o 6 7 9 36.95 26.29 11.87 o 7 7 9 193.48 162.93 13.98 o 8 7 9 266.83 254.49 20.91 o 0 8 9 152.78 109.37 17.05 o 1 8 9 0.44 2.82 7.00 o 2 8 9 58.94 52.77 9.89 o 3 8 9 0.10 10.02 8.89 o 4 8 9 35.44 61.52 13.44 o 5 8 9 15.27 24.84 8.19 o 0 0 10 8638.37 8851.15 127.18 o 1 0 10 3690.73 3774.06 54.56 o 2 0 10 1562.88 1581.46 27.16 o 3 0 10 359.01 359.78 13.50 o 4 0 10 3988.10 3886.50 57.27 o 5 0 10 981.41 994.50 38.97 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9 5 10 14.58 20.51 6.34 o 10 5 10 375.14 388.47 18.26 o 11 5 10 1.89 3.95 6.26 o 0 6 10 2467.23 2379.32 53.37 o 1 6 10 54.90 27.89 6.00 o 2 6 10 1080.25 1067.27 38.23 o 3 6 10 236.50 208.31 11.83 o 4 6 10 1435.22 1409.00 28.59 o 5 6 10 17.77 7.65 8.64 o 6 6 10 539.09 522.92 23.29 o 7 6 10 138.09 118.00 10.44 o 8 6 10 57.75 44.72 7.89 o 9 6 10 76.60 82.96 9.74 o 1 7 10 41.44 30.91 7.93 o 2 7 10 309.48 250.89 17.78 o 3 7 10 186.57 165.99 17.29 o 4 7 10 587.55 650.32 37.09 o 5 7 10 8.70 7.26 7.28 o 6 7 10 1355.37 1501.83 34.18 o 7 7 10 8.41 13.17 7.60 o 0 8 10 2053.22 2135.65 57.65 o 1 8 10 18.65 8.74 7.46 o 2 8 10 1097.79 1210.26 31.10 o 3 8 10 169.10 125.76 15.47 o 1 1 11 2971.98 3066.36 33.96 o 2 1 11 214.77 231.66 9.79 o 3 1 11 1332.89 1334.82 23.74 o 4 1 11 417.38 383.48 10.91 o 5 1 11 5.48 1.71 4.19 o 6 1 11 104.40 88.64 8.24 o 7 1 11 114.39 109.44 9.19 o 8 1 11 414.16 405.78 26.30 o 9 1 11 29.79 12.15 5.46 o 10 1 11 127.00 123.33 11.32 o 11 1 11 8.12 2.38 5.43 o 12 1 11 621.46 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37.43 o 7 4 11 1401.86 1507.76 22.45 o 8 4 11 95.07 81.48 8.27 o 9 4 11 1531.17 1680.62 30.50 o 10 4 11 86.52 70.33 8.62 o 11 4 11 504.92 543.77 18.64 o 1 5 11 67.32 58.00 6.03 o 2 5 11 50.51 42.50 7.19 o 3 5 11 1504.68 1500.75 31.50 o 4 5 11 723.19 766.91 28.59 o 5 5 11 388.49 408.76 12.22 o 6 5 11 1424.78 1506.94 24.99 o 7 5 11 303.90 321.23 12.03 o 8 5 11 1363.87 1444.74 35.08 o 9 5 11 5.29 15.18 6.56 o 10 5 11 280.91 331.66 17.78 o 0 6 11 1915.03 1947.99 38.76 o 1 6 11 5.77 0.78 4.59 o 2 6 11 826.75 851.77 23.19 o 3 6 11 143.99 124.50 10.70 o 4 6 11 165.01 182.85 11.63 o 5 6 11 441.80 472.04 16.61 o 6 6 11 5.87 7.02 5.69 o 7 6 11 68.62 79.55 9.22 o 8 6 11 35.35 32.16 7.45 o 1 7 11 253.93 230.69 14.84 o 2 7 11 66.83 42.64 8.63 o 3 7 11 912.01 801.53 58.09 o 4 7 11 13.79 -4.32 7.41 o 5 7 11 2.08 -10.04 8.75 o 6 7 11 258.52 276.25 23.60 o 0 0 12 1774.66 1821.33 58.60 o 1 0 12 68.74 84.16 11.43 o 2 0 12 790.25 856.70 28.74 o 3 0 12 2432.76 2499.74 49.87 o 4 0 12 1085.40 1008.65 38.67 o 5 0 12 4001.63 4234.76 120.77 o 6 0 12 0.35 10.18 7.61 o 7 0 12 5175.24 5209.57 109.94 o 8 0 12 422.92 367.51 22.00 o 9 0 12 4675.98 4576.07 189.45 o 10 0 12 282.46 267.42 21.78 o 11 0 12 1769.23 1941.97 53.30 o 12 0 12 14.48 -1.68 8.74 o 1 1 12 5096.21 5102.62 50.21 o 2 1 12 40.49 32.61 5.37 o 3 1 12 2398.65 2425.41 33.50 o 4 1 12 1576.69 1560.64 34.01 o 5 1 12 1910.91 1918.44 31.36 o 6 1 12 63.90 60.16 7.65 o 7 1 12 89.15 79.90 8.61 o 8 1 12 2.84 7.69 5.48 o 9 1 12 0.92 0.81 5.31 o 10 1 12 275.57 231.19 17.35 o 11 1 12 1100.47 1183.54 29.52 o 12 1 12 2.15 -1.78 6.34 o 0 2 12 1401.72 1385.75 29.54 o 1 2 12 23.94 26.91 4.52 o 2 2 12 1148.86 1135.68 20.90 o 3 2 12 1754.17 1820.43 24.26 o 4 2 12 155.56 144.23 8.87 o 5 2 12 1073.61 1100.03 23.75 o 6 2 12 123.99 126.69 10.08 o 7 2 12 1433.14 1377.50 27.95 o 8 2 12 4.37 5.49 5.39 o 9 2 12 2032.56 2053.72 42.51 o 10 2 12 51.58 37.22 15.53 o 11 2 12 742.62 875.39 42.93 o 12 2 12 1.42 -5.10 6.13 o 1 3 12 2724.77 2793.45 26.94 o 2 3 12 2219.05 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612.03 671.03 29.94 o 1 7 12 1200.43 1311.18 36.71 o 2 7 12 0.10 -0.22 6.96 o 3 7 12 940.53 940.09 66.84 o 4 7 12 12.31 6.70 14.37 o 1 1 13 73.78 86.12 7.48 o 2 1 13 8.38 3.85 3.90 o 3 1 13 1069.23 1016.55 23.29 o 4 1 13 504.41 498.13 14.93 o 5 1 13 973.88 924.10 22.79 o 6 1 13 235.56 185.14 12.03 o 7 1 13 502.23 452.95 17.22 o 8 1 13 120.26 138.99 11.67 o 9 1 13 94.69 80.82 10.09 o 10 1 13 0.45 -1.57 5.71 o 11 1 13 0.71 0.92 7.06 o 0 2 13 2089.78 2005.78 36.92 o 1 2 13 1017.61 1039.98 19.59 o 2 2 13 654.63 653.66 15.33 o 3 2 13 346.22 294.43 12.21 o 4 2 13 410.69 361.82 14.62 o 5 2 13 1096.32 1122.15 25.07 o 6 2 13 40.64 25.19 6.28 o 7 2 13 938.35 925.94 26.02 o 8 2 13 67.90 78.07 12.02 o 9 2 13 480.92 453.61 28.75 o 10 2 13 12.67 -3.18 6.11 o 11 2 13 686.82 705.34 24.10 o 1 3 13 5200.01 5286.13 44.65 o 2 3 13 81.71 66.84 6.60 o 3 3 13 1174.18 1216.73 21.23 o 4 3 13 2280.59 2294.96 29.28 o 5 3 13 603.41 605.39 21.86 o 6 3 13 695.52 729.96 20.99 o 7 3 13 75.20 69.40 11.65 o 8 3 13 1263.13 1290.38 34.70 o 9 3 13 141.63 156.62 15.27 o 10 3 13 16.63 6.20 8.85 o 0 4 13 2284.36 2407.00 47.22 o 1 4 13 862.18 865.28 16.70 o 2 4 13 1647.26 1669.40 37.58 o 3 4 13 1380.43 1467.42 23.69 o 4 4 13 550.95 578.61 15.43 o 5 4 13 1294.70 1349.62 23.33 o 6 4 13 182.73 139.17 10.43 o 7 4 13 2543.16 2803.52 92.68 o 8 4 13 438.62 467.31 20.30 o 9 4 13 1923.78 2233.17 53.61 o 1 5 13 3242.44 3266.23 36.53 o 2 5 13 86.20 74.32 8.38 o 3 5 13 380.50 401.98 15.06 o 4 5 13 654.64 635.29 29.19 o 5 5 13 365.61 363.51 16.25 o 6 5 13 385.08 369.43 14.65 o 7 5 13 5.35 5.24 4.89 o 8 5 13 377.87 420.26 19.36 o 0 6 13 5.90 0.34 6.28 o 1 6 13 216.33 213.99 11.27 o 2 6 13 470.69 432.83 16.59 o 3 6 13 83.83 64.63 9.34 o 4 6 13 261.66 220.34 14.64 o 5 6 13 426.76 410.34 19.36 o 0 0 14 3295.88 3241.34 85.19 o 1 0 14 28.81 25.52 8.83 o 2 0 14 8151.03 8207.95 144.28 o 3 0 14 6.32 1.13 8.96 o 4 0 14 757.98 776.90 30.34 o 5 0 14 338.88 327.53 21.58 o 6 0 14 21.39 33.11 10.01 o 7 0 14 21.55 17.16 9.44 o 8 0 14 234.53 204.79 25.16 o 9 0 14 1002.19 1041.89 39.58 o 10 0 14 825.76 790.13 35.78 o 1 1 14 46.38 40.25 7.02 o 2 1 14 655.77 677.55 24.55 o 3 1 14 1912.19 1860.81 58.45 o 4 1 14 4199.00 4231.26 45.09 o 5 1 14 18.64 18.27 7.02 o 6 1 14 4564.35 4654.72 82.68 o 7 1 14 89.43 56.83 8.78 o 8 1 14 2029.62 2094.06 48.26 o 9 1 14 45.21 42.61 9.19 o 10 1 14 1274.61 1308.50 32.53 o 0 2 14 2093.29 2142.70 39.99 o 1 2 14 65.74 71.67 6.97 o 2 2 14 3961.17 4155.65 48.87 o 3 2 14 666.56 689.00 16.47 o 4 2 14 2697.90 2651.29 49.68 o 5 2 14 792.44 759.94 21.85 o 6 2 14 38.71 39.10 7.72 o 7 2 14 20.64 19.19 6.87 o 8 2 14 73.24 89.04 10.48 o 9 2 14 152.73 126.09 12.30 o 10 2 14 532.85 575.60 24.98 o 1 3 14 80.35 70.54 7.08 o 2 3 14 3.42 8.30 4.53 o 3 3 14 266.15 240.98 13.65 o 4 3 14 910.26 888.30 18.93 o 5 3 14 33.45 10.24 11.01 o 6 3 14 894.79 983.37 25.23 o 7 3 14 44.27 32.82 8.99 o 8 3 14 531.31 505.65 38.31 o 9 3 14 353.95 307.34 20.28 o 0 4 14 0.39 -8.24 6.03 o 1 4 14 353.21 301.44 13.73 o 2 4 14 92.00 71.86 8.02 o 3 4 14 55.41 33.93 6.84 o 4 4 14 55.24 52.95 9.82 o 5 4 14 11.48 6.56 5.35 o 6 4 14 0.31 -2.20 7.52 o 7 4 14 42.98 41.94 9.99 o 8 4 14 0.27 -1.51 7.19 o 1 5 14 287.61 308.78 12.82 o 2 5 14 52.13 33.73 6.46 o 3 5 14 3.95 3.25 5.11 o 4 5 14 50.59 60.63 8.14 o 5 5 14 72.16 73.99 10.72 o 6 5 14 434.81 426.11 15.62 o 0 6 14 863.54 895.11 29.45 o 1 6 14 120.78 109.01 9.22 o 2 6 14 1264.71 1283.42 29.19 o 1 1 15 401.69 335.35 15.91 o 2 1 15 498.30 427.09 34.89 o 3 1 15 85.79 73.03 9.08 o 4 1 15 135.08 91.67 10.03 o 5 1 15 23.31 13.93 6.69 o 6 1 15 155.62 145.41 12.40 o 7 1 15 94.14 77.46 10.17 o 8 1 15 11.75 23.40 7.82 o 9 1 15 82.78 75.43 11.15 o 0 2 15 3454.10 3608.70 134.88 o 1 2 15 26.41 13.66 5.94 o 2 2 15 2524.73 2725.54 36.75 o 3 2 15 63.84 49.32 8.48 o 4 2 15 1036.48 1047.87 26.06 o 5 2 15 113.63 94.55 14.92 o 6 2 15 251.27 264.94 15.36 o 7 2 15 299.24 292.51 16.37 o 8 2 15 103.18 85.00 11.00 o 1 3 15 130.55 121.22 10.69 o 2 3 15 558.45 561.26 15.80 o 3 3 15 17.83 16.35 5.48 o 4 3 15 805.85 838.58 35.24 o 5 3 15 19.06 1.91 6.04 o 6 3 15 2534.64 2761.42 55.83 o 7 3 15 340.77 318.39 20.28 o 0 4 15 1751.38 1938.19 51.85 o 1 4 15 372.12 359.01 15.35 o 2 4 15 1109.13 1259.37 26.30 o 3 4 15 75.91 72.51 8.57 o 4 4 15 895.59 988.67 25.38 o 5 4 15 50.67 65.26 10.79 o 6 4 15 231.51 243.87 22.57 o 1 5 15 175.96 167.83 13.67 o 2 5 15 542.14 493.94 20.15 o 3 5 15 50.28 51.21 9.29 o 0 0 16 253.81 203.26 27.37 o 1 0 16 32.07 34.00 11.03 o 2 0 16 201.22 199.16 20.11 o 3 0 16 443.31 432.65 56.11 o 4 0 16 504.73 545.03 28.25 o 5 0 16 872.71 866.88 35.58 o 6 0 16 52.16 47.42 18.46 o 7 0 16 1028.70 1090.20 57.14 o 1 1 16 746.55 798.37 29.66 o 2 1 16 256.00 226.12 14.85 o 3 1 16 1292.17 1282.87 43.76 o 4 1 16 1331.62 1308.17 36.65 o 5 1 16 129.65 122.12 11.81 o 6 1 16 39.02 68.27 10.31 o 7 1 16 484.44 508.61 24.79 o 0 2 16 687.98 730.46 63.66 o 1 2 16 13.89 7.62 6.45 o 2 2 16 298.02 292.19 23.29 o 3 2 16 132.23 123.45 11.68 o 4 2 16 164.21 175.90 13.41 o 5 2 16 106.56 75.36 9.86 o 6 2 16 1.37 15.17 6.72 o 1 3 16 242.01 196.84 11.52 o 2 3 16 251.15 219.07 12.00 o 3 3 16 176.81 141.75 12.40 o 4 3 16 168.65 136.33 14.11 o 5 3 16 3.98 -5.07 5.77 o 0 4 16 85.08 24.28 17.92 o 1 4 16 38.13 17.79 7.97 o 2 4 16 83.07 64.75 8.97 o 3 4 16 34.44 8.18 6.50 o 1 1 17 75.29 95.61 11.22 o 2 1 17 2.18 6.45 7.30 o 3 1 17 212.11 180.08 14.12 o 4 1 17 9.60 10.32 7.05 o 0 2 17 139.03 143.33 17.70 o 1 2 17 4.91 8.06 6.63 o 2 2 17 188.87 179.28 14.19 o 3 2 17 406.27 435.06 19.21 o