#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216409.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216409_Fobs loop_ _publ_author_name 'Li, Shun-Li' 'Liu, Jie' 'Liu, Ying-Ying' _publ_section_title ; Diaquabis{4-[(6-chloropyridin-3-yl)methoxy]benzoato}cadmium(II) ; _journal_coeditor_code DN2258 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2956 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.688 _cell_angle_gamma 90.000 _cell_length_a 42.1790 _cell_length_b 5.3550 _cell_length_c 12.0680 _exptl_crystal_F_000 1352.00 _reflns_d_resolution_high 0.7446 _[local]_cod_data_source_file dn2258Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mm in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 565.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 30011.86 -2.77 2.77 o 4 0 0 31163.65 29086.75 772.79 o 6 0 0 32674.53 32686.90 1479.38 o 8 0 0 4019.04 3475.26 149.81 o 10 0 0 41794.25 38155.92 1499.99 o 12 0 0 1834.00 1516.60 80.91 o 14 0 0 16438.57 14107.78 573.11 o 16 0 0 113.47 105.82 15.30 o 18 0 0 20675.72 19865.48 566.98 o 20 0 0 376.63 356.51 26.90 o 22 0 0 13684.27 12108.18 356.46 o 24 0 0 8699.22 9324.31 281.15 o 26 0 0 9017.75 8709.16 265.76 o 28 0 0 7184.85 7429.50 232.08 o 30 0 0 5840.41 6059.64 287.02 o 32 0 0 3220.84 2743.42 158.43 o 34 0 0 1374.48 1404.63 105.82 o 36 0 0 3296.14 3483.88 195.96 o 38 0 0 180.01 183.96 53.83 o 40 0 0 1790.57 1834.07 134.43 o 42 0 0 706.87 761.68 91.98 o 44 0 0 3473.51 3783.20 222.72 o 46 0 0 2483.41 2358.27 168.27 o 48 0 0 347.96 398.99 83.98 o 50 0 0 32.45 30.76 62.45 o 52 0 0 203.34 169.50 78.44 o 1 1 0 5535.42 5534.39 171.18 o 3 1 0 5992.96 5761.98 137.18 o 5 1 0 4679.27 4570.96 93.27 o 7 1 0 16053.28 14548.00 366.14 o 9 1 0 222550.58 202899.39 3869.37 o 11 1 0 488.18 482.95 18.99 o 13 1 0 24737.02 23233.30 453.68 o 15 1 0 6705.86 6701.09 139.58 o 17 1 0 12886.66 11548.49 233.28 o 19 1 0 7842.40 7768.45 162.34 o 21 1 0 3563.97 3469.94 81.68 o 23 1 0 5601.41 5250.59 134.12 o 25 1 0 66.77 53.96 16.79 o 27 1 0 7186.91 6944.47 175.57 o 29 1 0 151.05 180.60 19.18 o 31 1 0 3846.10 3683.98 92.51 o 33 1 0 1779.19 1866.49 70.27 o 35 1 0 4615.44 4765.30 173.91 o 37 1 0 3466.97 3707.88 153.97 o 39 1 0 1581.61 1683.08 89.08 o 41 1 0 90.87 115.41 35.83 o 43 1 0 231.41 245.82 45.23 o 45 1 0 1026.27 965.81 75.13 o 47 1 0 31.52 96.00 41.03 o 49 1 0 326.13 379.03 55.85 o 51 1 0 111.80 20.22 38.43 o 0 2 0 874.94 752.63 74.75 o 2 2 0 5648.41 5870.08 124.22 o 4 2 0 550.73 473.04 18.71 o 6 2 0 150.78 191.21 11.33 o 8 2 0 2390.37 2283.27 49.48 o 10 2 0 68.89 51.12 8.49 o 12 2 0 231.29 221.17 17.01 o 14 2 0 861.02 938.89 33.25 o 16 2 0 3336.18 3326.90 78.61 o 18 2 0 24618.06 23464.97 464.14 o 20 2 0 16.09 7.62 11.63 o 22 2 0 3809.12 3752.62 89.87 o 24 2 0 173.80 156.12 16.74 o 26 2 0 4136.99 3903.04 95.22 o 28 2 0 853.93 866.44 36.14 o 30 2 0 1187.29 1238.12 44.91 o 32 2 0 173.19 178.07 21.82 o 34 2 0 618.72 649.55 40.32 o 36 2 0 2192.16 2178.80 69.08 o 38 2 0 152.90 124.62 22.84 o 40 2 0 271.75 307.87 38.85 o 42 2 0 34.46 17.10 32.18 o 44 2 0 129.84 100.63 41.10 o 46 2 0 32.20 50.61 40.54 o 48 2 0 86.93 109.79 43.35 o 50 2 0 64.37 64.35 45.45 o 1 3 0 1025.03 1008.75 32.68 o 3 3 0 1266.09 1221.53 36.99 o 5 3 0 1057.26 1001.66 32.62 o 7 3 0 11081.43 11189.12 206.04 o 9 3 0 762.19 835.23 33.19 o 11 3 0 7172.51 6749.65 130.30 o 13 3 0 250.00 213.43 15.56 o 15 3 0 3258.07 3322.87 81.45 o 17 3 0 7.05 12.52 11.59 o 19 3 0 1462.24 1443.53 53.66 o 21 3 0 67.72 53.41 21.98 o 23 3 0 934.26 842.44 36.58 o 25 3 0 1855.20 2085.74 62.44 o 27 3 0 3090.91 2887.32 79.23 o 29 3 0 1567.28 1528.63 52.94 o 31 3 0 40.93 37.63 18.08 o 33 3 0 370.82 432.62 41.60 o 35 3 0 190.40 210.73 27.71 o 37 3 0 323.52 312.72 30.12 o 39 3 0 161.28 169.49 26.05 o 41 3 0 52.73 46.66 25.82 o 43 3 0 112.08 100.16 35.70 o 45 3 0 7.24 19.46 33.11 o 47 3 0 96.14 149.06 85.83 o 0 4 0 3694.31 3478.34 186.42 o 2 4 0 14390.00 14565.42 442.01 o 4 4 0 1909.76 1830.63 84.69 o 6 4 0 3839.01 3725.07 139.39 o 8 4 0 1986.87 1943.34 69.80 o 10 4 0 2312.88 2174.38 74.95 o 12 4 0 1504.91 1495.73 74.00 o 14 4 0 2693.54 2523.73 103.68 o 16 4 0 14711.22 14527.21 426.50 o 18 4 0 577.82 597.11 48.51 o 20 4 0 5319.98 5028.71 172.84 o 22 4 0 3262.36 3266.73 125.13 o 24 4 0 3426.36 3378.46 315.78 o 26 4 0 2752.35 2750.73 112.05 o 28 4 0 2629.20 2728.99 125.95 o 30 4 0 1710.55 1688.92 77.01 o 32 4 0 455.48 473.17 50.96 o 34 4 0 140.15 177.08 29.51 o 36 4 0 100.65 117.98 28.69 o 38 4 0 602.91 672.15 49.64 o 40 4 0 226.53 252.58 37.23 o 42 4 0 721.18 706.54 54.54 o 44 4 0 561.42 424.53 89.21 o 1 5 0 1665.06 1818.14 91.89 o 3 5 0 1897.58 1897.25 93.64 o 5 5 0 1306.53 1322.63 77.01 o 7 5 0 11331.95 11642.05 359.27 o 9 5 0 2740.86 2855.43 122.00 o 11 5 0 6600.32 6754.01 228.38 o 13 5 0 4286.58 4174.62 158.34 o 15 5 0 2862.19 2684.76 116.82 o 17 5 0 3277.63 3036.45 127.05 o 19 5 0 2184.72 2045.83 97.63 o 21 5 0 1622.75 1529.47 159.50 o 23 5 0 1791.69 1759.87 89.24 o 25 5 0 1050.84 1069.65 69.66 o 27 5 0 1040.70 940.97 66.01 o 29 5 0 1530.09 1370.22 198.73 o 31 5 0 861.57 760.35 61.92 o 33 5 0 2148.80 2198.11 105.71 o 35 5 0 1484.97 1679.91 93.89 o 0 6 0 2518.33 2578.53 177.19 o 2 6 0 2935.84 2891.08 191.04 o 4 6 0 1137.94 1414.38 90.39 o 6 6 0 1158.25 1199.74 83.53 o 8 6 0 781.82 804.32 71.13 o 10 6 0 764.54 852.33 102.90 o 12 6 0 434.87 434.84 55.43 o 14 6 0 774.60 731.77 71.22 o 16 6 0 773.36 878.38 74.29 o 18 6 0 720.36 730.84 65.78 o 20 6 0 1649.24 1559.92 94.32 o 22 6 0 539.60 420.35 57.37 o 24 6 0 1173.29 1187.34 85.21 o 7 7 0 82.59 79.68 70.75 o 9 7 0 161.99 57.22 74.45 o -51 1 1 272.50 341.55 59.58 o -49 1 1 284.69 188.85 79.06 o -47 1 1 37.22 73.95 36.69 o -45 1 1 174.55 177.39 41.70 o -43 1 1 1015.60 1075.28 239.49 o -41 1 1 1701.46 1626.31 89.51 o -39 1 1 775.68 773.82 80.44 o -37 1 1 6.16 -14.87 23.78 o -35 1 1 789.74 858.58 47.26 o -33 1 1 1090.83 1077.45 41.26 o -31 1 1 1061.60 884.70 42.33 o -29 1 1 4053.21 4036.60 112.93 o -27 1 1 3705.48 3495.50 99.15 o -25 1 1 6745.41 6927.22 172.27 o -23 1 1 4847.78 4593.22 119.05 o -21 1 1 4746.33 4389.77 113.08 o -19 1 1 6980.14 6839.40 164.52 o -17 1 1 4694.74 4114.87 103.60 o -15 1 1 5006.23 4599.77 97.05 o -13 1 1 283.65 224.00 11.74 o -11 1 1 20536.57 18891.99 503.88 o -9 1 1 67147.28 59829.31 3064.10 o -7 1 1 13828.70 12960.26 590.02 o -5 1 1 19346.35 18910.98 434.74 o -3 1 1 731.33 656.32 25.43 o -1 1 1 18305.76 19784.43 793.06 o 1 1 1 11960.32 7143.10 292.55 o 3 1 1 14198.12 14823.85 289.58 o 5 1 1 49445.64 47774.55 914.93 o 7 1 1 53349.04 50805.42 975.86 o 9 1 1 9879.64 10284.06 205.10 o 11 1 1 492.79 469.59 25.35 o 13 1 1 801.65 958.66 29.22 o 15 1 1 4650.79 4130.63 91.21 o 17 1 1 1626.43 1583.78 43.45 o 19 1 1 13895.76 13399.00 270.26 o 21 1 1 8296.16 8192.78 197.59 o 23 1 1 6294.33 6135.37 154.77 o 25 1 1 5668.50 5172.34 135.98 o 27 1 1 5222.57 4794.36 126.24 o 29 1 1 4995.20 4890.53 115.10 o 31 1 1 1041.23 1004.45 48.82 o 33 1 1 2219.33 2276.62 80.80 o 35 1 1 513.09 545.03 51.30 o 37 1 1 1641.59 1666.54 88.10 o 39 1 1 378.29 422.49 50.14 o 41 1 1 3.60 -20.80 74.45 o 43 1 1 593.75 538.88 59.34 o 45 1 1 174.87 253.49 48.45 o 47 1 1 245.00 267.10 77.37 o 49 1 1 262.67 243.52 53.12 o 51 1 1 117.69 126.13 69.52 o -52 2 1 213.62 322.39 87.06 o -50 2 1 66.87 92.59 50.14 o -48 2 1 419.70 435.75 59.43 o -46 2 1 212.31 291.64 51.47 o -44 2 1 733.78 830.01 151.97 o -42 2 1 1130.33 1286.74 61.11 o -40 2 1 1344.92 1311.46 53.09 o -38 2 1 668.58 778.97 57.21 o -36 2 1 2295.55 2539.81 93.73 o -34 2 1 9068.88 9427.81 207.32 o -32 2 1 6241.33 6601.59 151.49 o -30 2 1 3056.54 3032.29 80.42 o -28 2 1 459.40 476.39 27.24 o -26 2 1 4405.17 4516.97 106.62 o -24 2 1 3416.80 3276.83 81.37 o -22 2 1 3847.82 3618.84 87.14 o -20 2 1 12480.24 12307.15 226.50 o -18 2 1 29622.96 27980.94 491.11 o -16 2 1 31328.75 29453.25 596.19 o -14 2 1 16116.51 15049.97 367.76 o -12 2 1 26167.91 24492.58 532.38 o -10 2 1 16627.03 16065.61 316.49 o -8 2 1 19642.09 17994.90 352.36 o -6 2 1 9487.97 8905.91 179.93 o -4 2 1 13003.28 12579.66 293.77 o -2 2 1 5569.49 5367.40 135.88 o 0 2 1 1309.20 1089.28 38.43 o 2 2 1 9962.14 9412.32 227.34 o 4 2 1 5682.14 5085.94 109.44 o 6 2 1 6918.29 6103.97 127.77 o 8 2 1 16847.07 16597.96 328.49 o 10 2 1 43977.36 44706.49 777.23 o 12 2 1 53604.73 53556.60 928.12 o 14 2 1 23823.55 23079.99 454.75 o 16 2 1 26.20 20.09 14.87 o 18 2 1 4392.92 4138.89 95.43 o 20 2 1 9645.84 9482.47 198.97 o 22 2 1 1994.17 1827.13 52.79 o 24 2 1 8616.25 8506.03 182.96 o 26 2 1 1721.00 1819.04 55.40 o 28 2 1 9210.90 9289.55 201.10 o 30 2 1 4226.43 4375.82 108.05 o 32 2 1 754.07 842.09 39.27 o 34 2 1 5123.27 5064.27 124.64 o 36 2 1 1901.95 2091.56 68.12 o 38 2 1 1861.60 1882.15 139.96 o 40 2 1 1063.26 1154.31 58.14 o 42 2 1 853.09 893.23 74.60 o 44 2 1 273.69 310.48 51.01 o 46 2 1 269.69 299.51 62.29 o 48 2 1 346.42 322.28 70.91 o 50 2 1 135.76 104.29 76.29 o -49 3 1 652.92 765.38 107.98 o -47 3 1 221.43 154.81 42.92 o -45 3 1 702.51 672.71 52.41 o -43 3 1 726.63 812.02 47.63 o -41 3 1 193.94 131.63 25.98 o -39 3 1 774.45 779.31 77.08 o -37 3 1 249.29 262.09 27.49 o -35 3 1 1213.47 1315.36 51.91 o -33 3 1 1122.03 1123.77 46.84 o -31 3 1 2453.99 2418.88 111.32 o -29 3 1 211.92 190.54 27.71 o -27 3 1 6871.38 6897.99 156.64 o -25 3 1 24898.25 24887.43 499.44 o -23 3 1 6613.77 6349.39 164.90 o -21 3 1 7058.80 7006.15 178.39 o -19 3 1 1630.08 1707.56 51.27 o -17 3 1 4939.19 4745.11 109.47 o -15 3 1 2373.86 2238.54 53.28 o -13 3 1 4697.76 4655.87 94.83 o -11 3 1 4431.14 4242.01 87.56 o -9 3 1 4815.34 4573.25 92.93 o -7 3 1 10144.67 9841.76 183.15 o -5 3 1 5476.75 5290.97 117.90 o -3 3 1 23526.48 22840.10 535.98 o -1 3 1 8172.27 8460.95 214.18 o 1 3 1 34824.96 35114.57 814.06 o 3 3 1 26554.19 27803.93 648.70 o 5 3 1 12494.82 11984.89 291.58 o 7 3 1 11910.17 11681.83 241.87 o 9 3 1 4847.18 4735.76 95.74 o 11 3 1 18098.44 17483.55 314.92 o 13 3 1 4271.47 4379.91 143.26 o 15 3 1 9669.52 9725.76 235.71 o 17 3 1 4889.63 4783.64 111.64 o 19 3 1 14486.50 14499.10 298.69 o 21 3 1 18388.54 18720.25 379.96 o 23 3 1 592.85 626.87 32.44 o 25 3 1 2162.72 2278.25 66.73 o 27 3 1 2316.08 2441.75 71.23 o 29 3 1 1013.26 1056.48 44.07 o 31 3 1 1098.93 1142.48 53.25 o 33 3 1 1141.06 1106.19 70.33 o 35 3 1 557.38 638.70 77.96 o 37 3 1 880.17 889.99 52.67 o 39 3 1 586.24 641.31 47.20 o 41 3 1 912.22 1000.00 64.58 o 43 3 1 659.11 652.72 95.98 o 45 3 1 746.80 885.00 71.40 o -44 4 1 236.98 321.78 80.60 o -42 4 1 394.04 431.88 52.82 o -40 4 1 488.24 492.64 52.18 o -38 4 1 133.34 134.15 41.68 o -36 4 1 571.81 511.58 49.06 o -34 4 1 1009.22 972.98 63.45 o -32 4 1 225.28 223.92 35.12 o -30 4 1 317.28 427.79 131.97 o -28 4 1 218.84 219.13 33.03 o -26 4 1 231.21 230.81 34.08 o -24 4 1 51.72 31.50 31.53 o -22 4 1 860.95 931.08 58.25 o -20 4 1 733.96 716.09 52.24 o -18 4 1 2424.98 2461.43 101.97 o -16 4 1 7446.04 7632.96 242.69 o -14 4 1 458.98 500.03 43.83 o -12 4 1 4489.75 4465.55 127.36 o -10 4 1 34.42 47.16 21.15 o -8 4 1 6051.20 6233.97 167.28 o -6 4 1 4348.95 4144.80 151.50 o -4 4 1 1764.87 1745.92 82.22 o -2 4 1 2505.97 2351.20 163.35 o 0 4 1 1257.34 1302.17 69.46 o 2 4 1 7129.30 6993.81 231.09 o 4 4 1 2078.91 2211.09 95.52 o 6 4 1 6914.59 6861.16 179.75 o 8 4 1 1526.26 1447.06 58.40 o 10 4 1 5043.98 5062.86 172.83 o 12 4 1 5865.82 5770.30 156.18 o 14 4 1 244.21 269.63 28.45 o 16 4 1 1799.44 1825.48 67.79 o 18 4 1 1538.11 1483.65 60.14 o 20 4 1 374.98 374.40 32.51 o 22 4 1 95.51 52.48 20.07 o 24 4 1 489.83 534.50 56.45 o 26 4 1 267.96 198.58 34.33 o 28 4 1 1726.23 1658.50 68.02 o 30 4 1 593.90 404.23 42.13 o 32 4 1 418.27 384.52 37.92 o 34 4 1 140.14 127.21 29.19 o 36 4 1 252.37 315.35 52.92 o 38 4 1 577.60 599.09 48.80 o 40 4 1 123.95 74.02 43.90 o 42 4 1 137.24 136.74 35.42 o -35 5 1 26.51 64.57 29.99 o -33 5 1 0.06 -6.99 25.54 o -31 5 1 8.38 -7.72 24.26 o -29 5 1 34.85 60.29 32.15 o -27 5 1 53.09 7.88 26.11 o -25 5 1 11.29 14.79 47.22 o -23 5 1 429.38 384.31 46.25 o -21 5 1 28.89 10.44 35.22 o -19 5 1 161.08 142.63 35.45 o -17 5 1 1.88 -16.27 26.30 o -15 5 1 66.48 62.29 30.61 o -13 5 1 80.77 71.01 31.18 o -11 5 1 1298.71 1442.23 81.64 o -9 5 1 287.95 342.61 45.17 o -7 5 1 844.30 998.11 74.35 o -5 5 1 28.49 21.23 23.88 o -3 5 1 135.39 144.14 52.30 o -1 5 1 509.43 436.79 47.32 o 1 5 1 34.73 23.96 24.79 o 3 5 1 1.44 26.63 24.53 o 5 5 1 119.94 159.90 36.61 o 7 5 1 216.97 200.11 38.61 o 9 5 1 2.30 -35.72 36.92 o 11 5 1 0.55 -52.30 52.30 o 13 5 1 683.89 636.81 55.79 o 15 5 1 12.27 11.85 26.09 o 17 5 1 240.73 244.29 37.94 o 19 5 1 73.89 64.78 30.28 o 21 5 1 197.16 187.90 36.98 o 23 5 1 9.37 -8.60 28.15 o 25 5 1 6.02 36.79 30.09 o 27 5 1 28.18 12.78 25.05 o 29 5 1 63.69 68.29 31.16 o 31 5 1 22.77 -0.24 29.53 o 33 5 1 3.18 2.50 29.07 o 35 5 1 203.20 269.48 54.45 o -24 6 1 32.84 25.33 35.16 o -22 6 1 164.89 184.77 42.87 o -20 6 1 456.71 447.85 72.75 o -18 6 1 1018.57 953.52 74.88 o -16 6 1 547.69 489.56 57.27 o -14 6 1 1550.37 1644.75 95.75 o -12 6 1 878.89 802.16 103.98 o -10 6 1 1319.30 1455.86 127.82 o -8 6 1 1259.86 1329.78 90.21 o -6 6 1 774.06 906.56 115.67 o -4 6 1 1453.95 1542.66 91.70 o -2 6 1 2129.39 2033.42 156.89 o 0 6 1 199.03 155.35 59.99 o 2 6 1 510.08 501.43 80.60 o 4 6 1 2409.80 2566.59 292.09 o 6 6 1 1039.34 1114.26 80.50 o 8 6 1 1900.32 1855.11 101.52 o 10 6 1 740.63 722.14 66.88 o 12 6 1 2000.60 1965.46 105.12 o 14 6 1 965.22 979.82 91.37 o 16 6 1 713.96 667.91 87.98 o 18 6 1 468.25 492.64 61.83 o 20 6 1 67.94 144.58 40.76 o 22 6 1 485.67 478.55 147.97 o 24 6 1 74.40 17.23 39.38 o -9 7 1 1301.09 1182.83 145.51 o 5 7 1 1757.57 1505.22 155.66 o 7 7 1 999.19 893.35 127.97 o -52 0 2 1067.62 1007.79 120.59 o -50 0 2 3171.97 3543.25 223.34 o -48 0 2 629.91 588.18 87.06 o -46 0 2 1703.52 2033.42 151.04 o -44 0 2 357.91 431.91 73.52 o -42 0 2 1414.94 1486.45 121.21 o -40 0 2 979.42 1059.16 99.98 o -38 0 2 2522.94 2489.93 156.27 o -36 0 2 1850.02 1992.81 132.89 o -34 0 2 3409.09 3099.04 173.50 o -32 0 2 2110.96 1975.89 127.36 o -30 0 2 6703.24 6767.49 314.39 o -28 0 2 11212.67 9701.33 424.83 o -26 0 2 60.57 19.07 23.69 o -24 0 2 45326.86 45366.08 1802.70 o -22 0 2 4817.90 5177.37 236.87 o -20 0 2 18563.85 18061.71 735.23 o -18 0 2 979.49 891.50 61.83 o -16 0 2 175.97 145.20 27.07 o -14 0 2 11523.04 10552.53 434.06 o -12 0 2 11564.76 10729.73 436.52 o -10 0 2 30807.95 28986.06 1005.74 o -8 0 2 303.20 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