#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216418.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216418_Fobs loop_ _publ_author_name 'Wang, Fu-Min' _publ_section_title ; [6-Phenyl-2,4-bis(2-pyridylamino)-1,3,5-triazine]sulfatonickel(II) dihydrate ; _journal_coeditor_code DN2269 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2996 _journal_page_last m2997 _journal_volume 63 _journal_year 2007 _space_group_IT_number 58 _symmetry_space_group_name_Hall '-P 2 2n' _symmetry_space_group_name_H-M 'P n n m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.9120 _cell_length_b 11.4246 _cell_length_c 12.2370 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.8347 _[local]_cod_data_source_file dn2269Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xb0738 in Pnnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 276.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' '-x-1/2, y-1/2, z-1/2' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11169.41 11753.26 1371.02 o 4 0 0 17121.94 16771.34 1959.87 o 6 0 0 583.33 473.11 56.88 o 8 0 0 43539.76 43893.82 3654.50 o 10 0 0 1679.49 1793.67 150.29 o 12 0 0 4731.25 4888.11 408.20 o 14 0 0 3242.37 3177.99 265.83 o 16 0 0 971.37 1240.53 147.37 o 18 0 0 440.09 381.12 51.20 o 1 1 0 1011.44 642.22 45.62 o 2 1 0 4408.42 5364.66 427.96 o 3 1 0 13909.50 13677.82 794.53 o 4 1 0 225.99 211.27 12.52 o 5 1 0 6444.26 6867.34 398.97 o 6 1 0 7923.08 8420.54 570.40 o 7 1 0 42.62 54.61 5.26 o 8 1 0 160.27 102.17 18.73 o 9 1 0 25.01 29.05 5.21 o 10 1 0 3833.19 4247.65 288.12 o 11 1 0 2538.73 2418.05 142.92 o 12 1 0 244.67 217.34 14.47 o 13 1 0 974.79 959.98 57.62 o 14 1 0 8.19 12.93 8.08 o 15 1 0 123.67 131.40 13.53 o 16 1 0 1.54 -2.32 10.04 o 17 1 0 931.04 926.56 138.97 o 18 1 0 14.75 25.46 21.99 o 19 1 0 355.79 320.34 46.59 o 0 2 0 8054.31 8832.74 715.80 o 1 2 0 3625.09 3487.52 230.63 o 2 2 0 34897.29 33364.29 2195.08 o 3 2 0 11.46 6.63 4.03 o 4 2 0 505.12 392.45 20.59 o 5 2 0 1183.47 1293.19 67.03 o 6 2 0 5178.45 5247.02 271.74 o 7 2 0 8253.37 8302.17 429.00 o 8 2 0 59.25 36.44 6.29 o 9 2 0 3920.66 4167.58 283.13 o 10 2 0 211.80 199.39 17.64 o 11 2 0 23.15 18.20 7.47 o 12 2 0 33.72 26.52 5.67 o 13 2 0 1.48 2.02 6.16 o 14 2 0 1073.65 1058.79 72.84 o 15 2 0 81.65 123.75 18.54 o 16 2 0 1691.13 1804.90 182.41 o 17 2 0 1024.71 1032.01 88.65 o 18 2 0 53.47 25.96 20.07 o 1 3 0 5477.19 5576.35 370.10 o 2 3 0 76227.41 68167.42 4483.41 o 3 3 0 939.31 827.26 54.61 o 4 3 0 7142.60 6895.69 396.61 o 5 3 0 114.70 127.65 7.07 o 6 3 0 157.11 181.33 10.05 o 7 3 0 1179.87 1436.61 74.49 o 8 3 0 1236.12 1246.21 64.42 o 9 3 0 532.38 550.57 32.26 o 10 3 0 180.75 174.74 10.22 o 11 3 0 2.74 -8.72 5.81 o 12 3 0 299.44 347.95 24.86 o 13 3 0 271.39 267.62 20.02 o 14 3 0 1793.76 1713.95 140.27 o 15 3 0 130.69 112.99 16.04 o 16 3 0 19.70 18.73 13.56 o 17 3 0 187.07 217.21 27.52 o 18 3 0 529.91 458.12 43.26 o 0 4 0 2915.54 3579.44 289.43 o 1 4 0 15779.41 15187.20 866.76 o 2 4 0 8907.96 8929.26 587.93 o 3 4 0 5642.70 5778.03 380.46 o 4 4 0 416.54 459.80 30.49 o 5 4 0 1180.90 1157.55 66.87 o 6 4 0 973.31 1054.47 61.38 o 7 4 0 13997.90 14303.00 820.46 o 8 4 0 813.02 855.95 44.85 o 9 4 0 5514.68 5787.01 332.54 o 10 4 0 462.10 472.93 27.70 o 11 4 0 19.54 18.83 13.85 o 12 4 0 1182.62 1249.92 102.72 o 13 4 0 194.90 186.10 18.81 o 14 4 0 482.83 366.01 63.15 o 15 4 0 931.66 1051.53 125.81 o 16 4 0 26.36 54.91 15.12 o 17 4 0 436.27 431.75 40.41 o 18 4 0 33.49 33.58 18.30 o 1 5 0 1540.03 1801.64 118.77 o 2 5 0 4106.44 3682.25 211.96 o 3 5 0 598.95 643.40 43.14 o 4 5 0 869.09 1210.44 80.26 o 5 5 0 543.93 592.67 39.77 o 6 5 0 1055.31 1017.36 58.11 o 7 5 0 484.76 462.98 31.56 o 8 5 0 1.45 -0.55 4.96 o 9 5 0 88.79 69.69 12.30 o 10 5 0 2255.27 2022.13 134.08 o 11 5 0 113.37 124.11 11.01 o 12 5 0 1911.88 2065.20 168.66 o 13 5 0 343.44 257.14 24.48 o 14 5 0 25.90 13.12 18.83 o 15 5 0 0.86 -15.53 17.87 o 16 5 0 13.39 -0.85 20.21 o 17 5 0 21.05 11.26 15.33 o 0 6 0 15893.50 15453.50 1252.49 o 1 6 0 1759.69 1801.31 104.04 o 2 6 0 966.62 1098.06 63.75 o 3 6 0 5855.17 5711.60 376.18 o 4 6 0 3054.50 2845.24 187.26 o 5 6 0 9787.55 9837.70 647.69 o 6 6 0 156.79 184.02 13.67 o 7 6 0 2321.19 2458.20 162.29 o 8 6 0 1755.51 1815.74 120.22 o 9 6 0 1085.49 1159.71 77.45 o 10 6 0 1473.58 1306.92 86.75 o 11 6 0 254.43 286.29 21.00 o 12 6 0 644.89 621.94 52.66 o 13 6 0 308.11 315.01 28.84 o 14 6 0 25.06 29.52 12.03 o 15 6 0 129.48 83.12 21.35 o 16 6 0 9.56 2.13 19.43 o 17 6 0 143.00 127.92 21.38 o 1 7 0 460.52 491.84 28.54 o 2 7 0 324.03 450.63 30.23 o 3 7 0 19.41 27.13 9.37 o 4 7 0 958.62 948.44 63.11 o 5 7 0 933.38 939.00 62.70 o 6 7 0 0.51 -0.76 5.63 o 7 7 0 83.08 62.04 19.21 o 8 7 0 252.15 271.49 28.92 o 9 7 0 18.52 31.71 7.83 o 10 7 0 249.44 323.42 23.39 o 11 7 0 165.07 188.69 15.54 o 12 7 0 107.87 90.26 14.13 o 13 7 0 439.66 460.22 40.37 o 14 7 0 279.66 295.75 28.71 o 15 7 0 47.63 62.64 33.58 o 16 7 0 19.77 22.20 20.92 o 0 8 0 207.25 225.03 28.94 o 1 8 0 74.68 46.91 8.35 o 2 8 0 1224.25 1110.01 74.28 o 3 8 0 76.76 147.32 12.02 o 4 8 0 29.02 29.12 10.01 o 5 8 0 5.04 -6.68 6.20 o 6 8 0 1641.38 1629.73 108.21 o 7 8 0 1.10 4.45 10.51 o 8 8 0 231.93 265.84 19.76 o 9 8 0 2.42 -1.86 7.37 o 10 8 0 160.07 117.60 12.78 o 11 8 0 73.36 82.64 13.81 o 12 8 0 566.09 580.88 50.10 o 13 8 0 71.88 75.89 27.13 o 14 8 0 180.75 151.23 35.42 o 15 8 0 11.39 -2.72 15.47 o 1 9 0 69.21 35.95 9.64 o 2 9 0 4.80 25.26 8.99 o 3 9 0 6.88 6.03 7.15 o 4 9 0 65.51 49.38 8.18 o 5 9 0 4.31 -0.84 6.88 o 6 9 0 862.88 857.21 57.55 o 7 9 0 86.74 49.71 9.03 o 8 9 0 94.60 79.70 10.30 o 9 9 0 6.39 5.60 8.58 o 10 9 0 6.21 11.14 9.32 o 11 9 0 229.57 201.25 21.41 o 12 9 0 110.30 96.80 15.70 o 13 9 0 240.09 217.94 37.66 o 14 9 0 261.74 237.43 26.29 o 0 10 0 894.89 1177.13 135.32 o 1 10 0 583.13 517.14 43.54 o 2 10 0 532.20 475.20 49.22 o 3 10 0 368.15 406.15 57.69 o 4 10 0 190.81 235.41 33.65 o 5 10 0 1027.17 995.03 66.94 o 6 10 0 783.07 762.44 80.80 o 7 10 0 214.66 297.24 27.48 o 8 10 0 490.65 542.15 37.72 o 9 10 0 84.44 55.38 13.10 o 10 10 0 543.38 575.88 40.52 o 11 10 0 35.13 31.95 15.14 o 12 10 0 92.22 94.83 17.72 o 13 10 0 221.53 140.05 24.36 o 1 11 0 12.84 -16.36 10.90 o 2 11 0 358.34 438.03 37.94 o 3 11 0 0.42 -1.37 12.02 o 4 11 0 346.77 311.17 28.70 o 5 11 0 32.64 3.09 12.33 o 6 11 0 210.08 222.89 22.62 o 7 11 0 7.09 10.81 13.29 o 8 11 0 5.13 -0.11 10.85 o 9 11 0 33.11 32.43 15.25 o 10 11 0 708.18 749.42 64.09 o 11 11 0 1.36 12.10 14.73 o 0 12 0 44.17 32.20 17.80 o 1 12 0 792.18 689.49 57.90 o 2 12 0 131.93 176.61 19.89 o 3 12 0 102.08 92.83 15.74 o 4 12 0 13.95 -15.72 13.01 o 5 12 0 94.38 82.50 16.15 o 6 12 0 1.10 -13.11 14.52 o 7 12 0 665.88 682.81 58.14 o 8 12 0 39.19 38.31 21.56 o 9 12 0 62.51 44.69 18.51 o 1 13 0 74.17 90.35 17.53 o 2 13 0 7.08 -1.41 15.31 o 3 13 0 28.26 39.97 25.96 o 4 13 0 102.93 120.18 23.97 o 5 13 0 56.79 16.48 30.18 o 1 0 1 3745.64 4571.64 309.96 o 3 0 1 857.88 819.27 55.91 o 5 0 1 162.82 88.96 10.87 o 7 0 1 3600.78 3578.08 242.56 o 9 0 1 495.90 562.00 38.80 o 11 0 1 6588.57 6428.04 436.00 o 13 0 1 1050.53 1034.51 61.27 o 15 0 1 0.27 -5.64 9.29 o 17 0 1 468.08 461.68 41.72 o 19 0 1 843.82 814.70 70.76 o 0 1 1 46867.22 41746.19 2155.92 o 1 1 1 7018.77 7076.90 365.33 o 2 1 1 3904.99 4427.90 230.04 o 3 1 1 4008.88 3640.76 148.82 o 4 1 1 698.75 665.65 27.30 o 5 1 1 1220.11 1014.16 44.54 o 6 1 1 6982.27 7141.54 314.48 o 7 1 1 4524.60 4573.71 240.71 o 8 1 1 11778.41 12391.28 593.48 o 9 1 1 1517.09 1555.07 69.32 o 10 1 1 574.41 559.86 25.32 o 11 1 1 663.38 752.49 33.86 o 12 1 1 206.77 265.40 13.42 o 13 1 1 122.63 120.24 8.19 o 14 1 1 846.77 851.87 38.76 o 15 1 1 13.79 16.66 7.25 o 16 1 1 1333.62 1393.52 73.55 o 17 1 1 482.38 539.25 30.15 o 18 1 1 244.04 229.25 35.13 o 1 2 1 148.10 170.96 7.56 o 2 2 1 980.71 1180.40 51.24 o 3 2 1 5532.17 5747.09 220.23 o 4 2 1 1934.68 1848.47 75.36 o 5 2 1 3415.98 3156.70 122.27 o 6 2 1 3.67 3.84 1.64 o 7 2 1 41.89 50.10 2.82 o 8 2 1 547.32 544.95 22.80 o 9 2 1 63.61 63.08 4.15 o 10 2 1 1334.88 1202.82 49.65 o 11 2 1 1007.51 1072.21 47.79 o 12 2 1 1099.87 1191.65 57.20 o 13 2 1 1138.16 1184.11 57.18 o 14 2 1 51.55 46.45 7.38 o 15 2 1 9.84 5.02 7.32 o 16 2 1 57.96 51.29 13.67 o 17 2 1 504.20 542.64 34.55 o 18 2 1 242.51 298.14 26.11 o 0 3 1 5053.45 5434.39 312.85 o 1 3 1 20126.85 20887.35 846.20 o 2 3 1 12260.48 11555.65 499.44 o 3 3 1 5101.65 4858.31 209.90 o 4 3 1 53.92 34.36 2.26 o 5 3 1 2008.83 2039.83 78.37 o 6 3 1 7214.49 7481.29 273.76 o 7 3 1 10973.60 10923.74 399.54 o 8 3 1 669.57 702.90 26.04 o 9 3 1 1052.04 1090.18 40.09 o 10 3 1 261.82 251.66 10.32 o 11 3 1 24.04 14.82 3.96 o 12 3 1 1.51 4.26 4.35 o 13 3 1 6.36 3.06 6.03 o 14 3 1 656.45 740.41 44.16 o 15 3 1 854.21 909.46 54.22 o 16 3 1 194.09 145.19 15.16 o 17 3 1 471.97 473.45 34.91 o 18 3 1 0.14 -5.89 11.07 o 1 4 1 4218.98 3691.29 150.07 o 2 4 1 240.55 338.20 14.82 o 3 4 1 3.87 -2.01 1.84 o 4 4 1 2215.62 2172.79 93.46 o 5 4 1 46.45 36.62 2.84 o 6 4 1 3382.65 3265.55 132.86 o 7 4 1 279.71 218.00 9.28 o 8 4 1 25.92 30.04 2.89 o 9 4 1 655.40 688.53 26.58 o 10 4 1 690.62 699.25 28.82 o 11 4 1 264.23 275.34 15.34 o 12 4 1 1261.48 1247.64 64.39 o 13 4 1 97.71 125.82 10.23 o 14 4 1 265.54 273.85 18.41 o 15 4 1 63.85 54.46 9.48 o 16 4 1 114.01 97.41 13.41 o 17 4 1 51.99 59.05 20.12 o 18 4 1 331.96 308.15 32.73 o 0 5 1 3993.92 3746.65 215.24 o 1 5 1 6614.89 6474.24 262.91 o 2 5 1 159.70 130.87 6.27 o 3 5 1 1166.44 1216.82 51.47 o 4 5 1 52.23 58.13 3.78 o 5 5 1 1884.83 1965.67 84.60 o 6 5 1 173.93 153.39 7.46 o 7 5 1 2228.70 2285.47 98.68 o 8 5 1 1827.97 1813.01 84.61 o 9 5 1 2483.87 2354.30 109.98 o 10 5 1 46.67 40.42 5.65 o 11 5 1 35.34 46.80 5.96 o 12 5 1 113.75 84.84 7.45 o 13 5 1 552.24 614.65 36.65 o 14 5 1 38.78 36.01 9.74 o 15 5 1 287.97 310.89 20.91 o 16 5 1 162.03 145.90 26.95 o 17 5 1 429.68 437.40 33.44 o 1 6 1 1295.52 1210.22 49.22 o 2 6 1 40.88 42.79 3.72 o 3 6 1 156.70 167.11 8.09 o 4 6 1 86.23 124.65 20.85 o 5 6 1 13.12 8.82 5.74 o 6 6 1 141.19 158.91 10.06 o 7 6 1 1012.61 909.99 42.92 o 8 6 1 80.85 107.32 9.58 o 9 6 1 1.11 1.38 4.18 o 10 6 1 357.30 430.50 21.06 o 11 6 1 1670.27 1782.56 91.78 o 12 6 1 282.30 284.06 16.48 o 13 6 1 349.76 319.56 23.22 o 14 6 1 0.99 -5.02 9.83 o 15 6 1 8.15 2.17 10.63 o 16 6 1 1.24 3.37 12.50 o 17 6 1 0.50 15.28 13.36 o 0 7 1 1341.73 1386.78 79.67 o 1 7 1 21.05 22.38 4.33 o 2 7 1 1349.22 1385.17 59.72 o 3 7 1 3253.92 3316.51 154.89 o 4 7 1 1001.36 1049.52 49.30 o 5 7 1 1503.01 1570.61 73.58 o 6 7 1 1223.38 1245.50 58.53 o 7 7 1 644.59 647.54 30.85 o 8 7 1 687.21 697.85 33.21 o 9 7 1 159.11 175.80 11.71 o 10 7 1 690.17 750.87 39.49 o 11 7 1 401.74 410.05 22.50 o 12 7 1 67.34 62.08 7.92 o 13 7 1 1.90 5.14 8.42 o 14 7 1 120.78 160.90 25.86 o 15 7 1 353.86 423.02 31.77 o 16 7 1 250.81 197.71 25.13 o 1 8 1 9.43 9.07 3.84 o 2 8 1 3.14 8.60 4.06 o 3 8 1 148.41 147.03 8.38 o 4 8 1 15.47 -2.41 4.34 o 5 8 1 1356.31 1469.21 68.74 o 6 8 1 3.84 -2.18 4.60 o 7 8 1 16.63 4.85 4.88 o 8 8 1 88.45 52.54 8.83 o 9 8 1 171.63 188.40 17.02 o 10 8 1 14.12 6.72 6.55 o 11 8 1 75.79 61.96 11.27 o 12 8 1 65.52 74.72 10.57 o 13 8 1 699.24 663.27 40.11 o 14 8 1 3.11 3.36 10.37 o 15 8 1 0.19 -10.83 12.54 o 0 9 1 951.24 946.14 77.00 o 1 9 1 16.01 27.97 6.53 o 2 9 1 1481.19 1559.27 79.99 o 3 9 1 1098.80 1036.31 49.00 o 4 9 1 13.69 18.04 5.21 o 5 9 1 429.78 404.47 20.03 o 6 9 1 2287.47 2408.34 112.59 o 7 9 1 356.52 304.93 15.89 o 8 9 1 368.49 356.45 18.29 o 9 9 1 128.80 120.22 8.82 o 10 9 1 204.19 213.99 13.85 o 11 9 1 0.57 2.14 7.77 o 12 9 1 31.02 30.50 9.67 o 13 9 1 39.36 46.42 10.77 o 14 9 1 399.48 434.48 34.67 o 1 10 1 359.85 454.27 27.09 o 2 10 1 103.86 77.47 9.25 o 3 10 1 144.58 127.65 13.03 o 4 10 1 464.48 455.55 27.55 o 5 10 1 141.36 167.36 10.29 o 6 10 1 655.84 766.73 36.80 o 7 10 1 291.67 311.69 16.48 o 8 10 1 20.25 20.68 7.09 o 9 10 1 4.07 8.05 7.20 o 10 10 1 66.21 46.32 15.78 o 11 10 1 503.90 515.04 28.54 o 12 10 1 284.30 262.69 19.35 o 0 11 1 44.79 14.50 11.26 o 1 11 1 1244.47 1384.07 79.43 o 2 11 1 4.84 0.91 8.05 o 3 11 1 45.97 23.03 8.48 o 4 11 1 0.52 7.59 8.40 o 5 11 1 235.73 250.78 22.58 o 6 11 1 0.26 -5.55 8.97 o 7 11 1 134.39 84.37 13.28 o 8 11 1 62.41 74.33 13.07 o 9 11 1 487.25 481.67 26.78 o 10 11 1 25.19 1.48 9.54 o 11 11 1 20.01 14.84 11.08 o 1 12 1 168.59 123.75 19.14 o 2 12 1 37.41 23.34 9.05 o 3 12 1 28.77 53.77 10.50 o 4 12 1 113.88 105.35 11.69 o 5 12 1 18.00 6.52 9.56 o 6 12 1 78.67 72.36 11.08 o 7 12 1 173.62 117.13 12.77 o 8 12 1 20.51 19.80 10.66 o 9 12 1 13.40 2.80 13.27 o 0 13 1 4.97 9.02 21.74 o 1 13 1 158.72 114.35 17.56 o 2 13 1 45.07 38.64 11.07 o 3 13 1 178.77 226.21 37.17 o 4 13 1 6.47 19.98 11.07 o 5 13 1 65.21 98.46 13.08 o 0 0 2 30542.34 31601.93 2116.26 o 2 0 2 2975.49 2578.98 175.13 o 4 0 2 1217.38 1123.62 76.69 o 6 0 2 2145.75 2296.59 133.26 o 8 0 2 22689.40 22751.94 1541.29 o 10 0 2 1415.29 1434.89 97.61 o 12 0 2 114.84 128.87 11.65 o 14 0 2 71.48 92.76 11.02 o 16 0 2 394.68 380.07 28.67 o 18 0 2 454.50 465.77 42.95 o 1 1 2 1365.52 1338.36 52.18 o 2 1 2 31728.85 29526.58 1295.13 o 3 1 2 3314.71 3483.73 143.30 o 4 1 2 2.67 2.13 1.65 o 5 1 2 7522.91 7552.21 310.22 o 6 1 2 1910.61 1825.93 80.75 o 7 1 2 112.57 103.69 5.66 o 8 1 2 1279.69 1235.07 54.71 o 9 1 2 2252.64 2321.30 102.46 o 10 1 2 3324.85 3486.45 153.69 o 11 1 2 2899.26 3070.50 147.30 o 12 1 2 765.09 766.31 34.75 o 13 1 2 796.89 813.74 39.86 o 14 1 2 27.54 24.05 6.22 o 15 1 2 266.10 305.30 16.52 o 16 1 2 9.78 3.82 7.89 o 17 1 2 234.87 198.53 16.01 o 18 1 2 48.74 44.25 11.52 o 0 2 2 19103.51 17979.35 927.77 o 1 2 2 22789.62 22725.09 791.33 o 2 2 2 7.59 13.20 1.74 o 3 2 2 608.71 607.41 23.51 o 4 2 2 104.54 128.88 6.76 o 5 2 2 2.82 4.96 1.73 o 6 2 2 6663.80 6511.78 251.39 o 7 2 2 509.13 563.92 21.76 o 8 2 2 360.15 444.40 17.66 o 9 2 2 1905.30 1807.39 74.95 o 10 2 2 163.96 166.81 13.68 o 11 2 2 20.48 19.42 3.98 o 12 2 2 635.26 628.52 30.79 o 13 2 2 306.97 304.94 16.24 o 14 2 2 39.09 54.06 6.85 o 15 2 2 327.46 360.30 23.62 o 16 2 2 551.74 544.95 34.01 o 17 2 2 357.58 352.40 27.49 o 18 2 2 3.71 -6.52 12.42 o 1 3 2 3616.82 3738.40 143.55 o 2 3 2 220.61 209.01 8.16 o 3 3 2 124.75 101.19 4.62 o 4 3 2 6955.83 6959.49 282.24 o 5 3 2 119.42 130.46 5.84 o 6 3 2 420.16 424.25 17.62 o 7 3 2 1.11 7.99 2.63 o 8 3 2 125.14 105.54 5.92 o 9 3 2 669.24 643.55 25.34 o 10 3 2 325.95 337.51 20.37 o 11 3 2 279.13 280.17 13.21 o 12 3 2 1070.97 1090.23 52.66 o 13 3 2 662.13 680.32 41.16 o 14 3 2 726.80 721.20 50.65 o 15 3 2 25.89 35.57 8.80 o 16 3 2 270.11 283.40 19.37 o 17 3 2 29.92 33.84 12.74 o 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1 8 154.72 177.92 10.81 o 2 1 8 1774.15 1691.19 88.92 o 3 1 8 2314.56 2274.19 109.42 o 4 1 8 38.48 54.61 5.52 o 5 1 8 2376.76 2450.32 117.98 o 6 1 8 394.37 327.00 16.78 o 7 1 8 30.26 40.47 5.83 o 8 1 8 94.10 102.95 8.57 o 9 1 8 952.37 964.17 47.16 o 10 1 8 839.81 878.47 43.24 o 11 1 8 990.72 1051.09 51.11 o 12 1 8 50.16 37.44 7.38 o 13 1 8 382.20 363.20 21.92 o 14 1 8 2.98 4.72 9.01 o 15 1 8 45.33 33.36 9.97 o 0 2 8 29.40 33.77 10.24 o 1 2 8 2047.49 2139.12 88.35 o 2 2 8 628.78 657.22 29.17 o 3 2 8 19.01 8.37 4.36 o 4 2 8 35.67 34.20 5.16 o 5 2 8 1.24 4.14 4.86 o 6 2 8 1717.36 1669.61 80.30 o 7 2 8 280.97 270.62 17.02 o 8 2 8 473.40 480.84 23.97 o 9 2 8 426.89 411.26 31.36 o 10 2 8 66.47 50.78 6.69 o 11 2 8 12.23 6.06 6.70 o 12 2 8 72.61 53.76 8.42 o 13 2 8 125.46 102.67 10.44 o 14 2 8 107.06 95.36 16.97 o 15 2 8 128.34 149.55 15.40 o 1 3 8 60.77 82.85 5.27 o 2 3 8 29.01 35.03 5.46 o 3 3 8 554.07 572.01 25.61 o 4 3 8 3489.78 3470.19 152.25 o 5 3 8 804.95 791.14 42.17 o 6 3 8 472.64 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6 1 9 631.73 600.10 29.80 o 7 1 9 99.95 101.15 9.44 o 8 1 9 1010.47 1064.29 51.82 o 9 1 9 714.66 707.93 34.55 o 10 1 9 3.00 -4.58 6.62 o 11 1 9 5.68 8.27 7.61 o 12 1 9 37.85 33.70 7.91 o 13 1 9 68.76 42.06 10.14 o 14 1 9 65.21 39.56 10.22 o 1 2 9 158.39 154.92 13.64 o 2 2 9 628.80 632.18 28.35 o 3 2 9 264.92 251.02 13.25 o 4 2 9 90.74 103.48 13.98 o 5 2 9 949.10 954.60 46.67 o 6 2 9 4.04 0.12 5.45 o 7 2 9 4.09 12.48 7.44 o 8 2 9 105.88 135.34 9.60 o 9 2 9 8.71 12.18 6.52 o 10 2 9 219.96 198.67 17.45 o 11 2 9 3.08 8.29 7.44 o 12 2 9 505.89 550.18 30.71 o 13 2 9 106.19 97.03 11.22 o 14 2 9 69.88 56.61 11.26 o 0 3 9 176.90 239.22 15.91 o 1 3 9 605.68 575.48 24.49 o 2 3 9 403.48 426.77 19.49 o 3 3 9 242.55 243.02 12.01 o 4 3 9 93.41 69.22 8.82 o 5 3 9 509.96 544.63 29.35 o 6 3 9 3.86 -5.37 5.71 o 7 3 9 1005.90 1019.35 48.87 o 8 3 9 8.10 3.56 6.14 o 9 3 9 262.71 228.44 14.89 o 10 3 9 9.34 8.14 7.95 o 11 3 9 109.21 100.54 10.55 o 12 3 9 5.72 5.28 8.55 o 13 3 9 4.17 -4.20 9.48 o 14 3 9 60.38 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25.19 o 5 10 9 3.58 7.25 11.42 o 0 0 10 9029.26 9049.16 1054.93 o 2 0 10 133.49 121.62 12.29 o 4 0 10 22.38 0.72 8.17 o 6 0 10 31.09 44.29 9.50 o 8 0 10 1807.77 1697.47 116.53 o 10 0 10 154.00 148.15 15.48 o 12 0 10 215.62 207.77 19.44 o 1 1 10 104.16 78.31 13.74 o 2 1 10 961.49 1036.57 55.22 o 3 1 10 16.65 19.54 6.61 o 4 1 10 32.35 28.01 6.22 o 5 1 10 256.91 250.75 14.00 o 6 1 10 141.37 128.67 9.26 o 7 1 10 46.01 43.18 6.99 o 8 1 10 46.00 34.02 7.19 o 9 1 10 2.72 7.65 7.13 o 10 1 10 358.96 380.44 20.57 o 11 1 10 103.95 111.33 14.49 o 12 1 10 76.38 102.14 15.51 o 13 1 10 80.40 55.45 10.75 o 0 2 10 74.71 78.52 10.02 o 1 2 10 1587.02 1396.75 222.87 o 2 2 10 1126.22 1151.32 55.46 o 3 2 10 22.25 5.22 6.31 o 4 2 10 64.36 96.52 8.78 o 5 2 10 403.97 384.02 23.02 o 6 2 10 494.29 500.42 25.29 o 7 2 10 654.97 622.45 30.90 o 8 2 10 18.55 25.90 6.99 o 9 2 10 579.18 635.58 40.79 o 10 2 10 21.99 10.05 7.77 o 11 2 10 4.29 11.50 9.19 o 12 2 10 13.94 13.85 9.27 o 13 2 10 42.58 63.13 15.51 o 1 3 10 115.60 119.11 10.72 o 2 3 10 75.78 71.32 8.48 o 3 3 10 9.73 13.54 5.77 o 4 3 10 1341.46 1387.54 66.64 o 5 3 10 5.89 1.66 6.97 o 6 3 10 98.61 106.84 14.32 o 7 3 10 16.86 19.89 7.72 o 8 3 10 125.69 116.29 9.53 o 9 3 10 2.44 3.81 7.82 o 10 3 10 22.28 24.84 11.19 o 11 3 10 3.55 3.11 9.15 o 12 3 10 178.20 184.31 19.20 o 13 3 10 13.41 27.45 10.76 o 0 4 10 153.47 147.77 11.95 o 1 4 10 1840.21 1933.63 80.07 o 2 4 10 0.03 -5.20 5.36 o 3 4 10 1.80 8.44 5.63 o 4 4 10 39.45 31.86 6.60 o 5 4 10 307.53 313.17 16.78 o 6 4 10 63.83 74.18 10.16 o 7 4 10 1464.33 1431.13 75.03 o 8 4 10 2.02 1.76 9.15 o 9 4 10 692.23 694.89 42.92 o 10 4 10 41.64 77.42 25.04 o 11 4 10 16.27 5.02 10.84 o 12 4 10 63.61 53.59 10.85 o 1 5 10 50.32 53.15 5.99 o 2 5 10 358.03 434.83 26.61 o 3 5 10 41.96 25.42 6.78 o 4 5 10 53.32 49.28 7.83 o 5 5 10 190.97 190.65 13.07 o 6 5 10 157.17 181.75 13.11 o 7 5 10 68.78 32.41 8.29 o 8 5 10 13.80 15.10 8.63 o 9 5 10 74.35 69.50 9.91 o 10 5 10 308.45 296.82 21.33 o 11 5 10 79.95 74.97 18.85 o 12 5 10 235.97 251.86 39.97 o 0 6 10 1962.02 1990.78 115.18 o 1 6 10 211.14 225.94 12.91 o 2 6 10 213.58 203.61 13.26 o 3 6 10 371.61 371.71 19.32 o 4 6 10 146.31 151.47 10.49 o 5 6 10 445.58 448.35 22.78 o 6 6 10 85.52 58.11 13.75 o 7 6 10 317.05 322.29 17.46 o 8 6 10 537.16 592.95 29.76 o 9 6 10 208.99 231.51 14.36 o 10 6 10 219.84 188.47 15.67 o 11 6 10 46.25 49.83 19.51 o 1 7 10 15.40 24.03 7.88 o 2 7 10 39.13 30.44 7.92 o 3 7 10 288.56 303.48 15.15 o 4 7 10 17.46 19.63 7.82 o 5 7 10 284.34 284.96 16.03 o 6 7 10 17.57 12.00 7.98 o 7 7 10 23.22 11.03 8.55 o 8 7 10 57.63 55.56 11.52 o 9 7 10 50.15 32.99 10.55 o 0 8 10 412.70 404.25 58.51 o 1 8 10 8.50 17.88 8.21 o 2 8 10 537.75 572.24 51.22 o 3 8 10 5.31 6.59 8.38 o 4 8 10 0.04 4.54 8.67 o 5 8 10 0.31 1.53 8.77 o 6 8 10 801.30 864.74 84.97 o 7 8 10 26.76 13.00 10.87 o 8 8 10 252.85 302.37 24.35 o 1 9 10 44.12 52.68 9.83 o 2 9 10 24.60 28.87 9.56 o 3 9 10 119.60 107.82 12.81 o 4 9 10 20.30 25.04 11.13 o 5 9 10 94.18 103.28 15.08 o 6 9 10 54.64 36.13 13.05 o 0 10 10 320.15 337.79 46.67 o 1 0 11 444.65 570.38 49.32 o 3 0 11 123.66 130.42 14.21 o 5 0 11 35.37 9.45 9.41 o 7 0 11 171.65 153.62 23.15 o 9 0 11 11.21 7.14 10.59 o 11 0 11 624.22 657.07 47.64 o 0 1 11 1411.52 1395.58 116.64 o 1 1 11 728.08 802.15 48.00 o 2 1 11 45.26 44.00 9.97 o 3 1 11 94.33 94.69 11.34 o 4 1 11 340.93 337.91 22.89 o 5 1 11 50.33 26.80 7.15 o 6 1 11 472.16 412.18 30.20 o 7 1 11 192.74 167.76 11.53 o 8 1 11 891.37 873.56 43.27 o 9 1 11 270.73 297.60 17.35 o 10 1 11 221.23 236.94 20.96 o 11 1 11 57.77 71.69 10.11 o 12 1 11 4.43 -3.32 9.48 o 1 2 11 141.22 144.04 12.97 o 2 2 11 1.24 1.51 7.98 o 3 2 11 23.98 9.86 7.64 o 4 2 11 468.64 437.52 25.71 o 5 2 11 115.25 133.72 12.61 o 6 2 11 144.00 162.97 20.04 o 7 2 11 54.87 45.84 8.12 o 8 2 11 2.83 -4.93 7.50 o 9 2 11 0.65 -0.53 7.97 o 10 2 11 65.26 81.76 9.65 o 11 2 11 23.46 20.58 10.20 o 12 2 11 83.97 78.15 11.82 o 0 3 11 12.13 3.75 7.64 o 1 3 11 854.94 812.89 36.59 o 2 3 11 16.92 20.34 6.94 o 3 3 11 643.23 673.76 47.61 o 4 3 11 19.56 10.84 7.67 o 5 3 11 132.07 139.16 11.29 o 6 3 11 247.70 233.86 15.36 o 7 3 11 959.04 992.44 59.79 o 8 3 11 103.82 123.86 17.15 o 9 3 11 66.69 28.65 10.97 o 10 3 11 23.82 42.65 10.39 o 11 3 11 6.16 -1.23 10.32 o 1 4 11 58.10 59.38 7.43 o 2 4 11 50.79 49.11 8.44 o 3 4 11 45.51 29.87 7.17 o 4 4 11 280.05 274.76 15.64 o 5 4 11 100.21 89.04 8.62 o 6 4 11 359.99 342.90 22.96 o 7 4 11 23.73 34.25 10.21 o 8 4 11 0.82 7.71 10.94 o 9 4 11 1.95 -9.80 10.05 o 10 4 11 56.37 25.90 11.59 o 11 4 11 9.01 18.84 11.43 o 0 5 11 890.89 844.52 57.64 o 1 5 11 1378.27 1551.42 63.88 o 2 5 11 26.76 8.73 6.24 o 3 5 11 48.67 37.08 8.34 o 4 5 11 8.97 7.93 7.90 o 5 5 11 113.01 103.60 18.19 o 6 5 11 24.63 18.07 8.65 o 7 5 11 273.30 257.62 33.47 o 8 5 11 165.74 132.95 15.59 o 9 5 11 411.95 450.14 33.18 o 10 5 11 0.67 6.19 11.58 o 1 6 11 185.14 170.40 12.47 o 2 6 11 51.22 54.65 16.99 o 3 6 11 231.89 226.53 20.99 o 4 6 11 68.02 85.51 9.33 o 5 6 11 33.48 32.92 8.38 o 6 6 11 41.01 35.62 8.77 o 7 6 11 99.45 96.15 14.24 o 8 6 11 9.87 4.39 8.92 o 9 6 11 10.65 0.27 9.22 o 0 7 11 574.80 522.67 45.74 o 1 7 11 57.74 48.14 10.37 o 2 7 11 353.98 300.60 18.31 o 3 7 11 224.52 194.65 16.59 o 4 7 11 43.55 33.44 8.68 o 5 7 11 89.72 107.12 13.29 o 6 7 11 288.65 253.51 25.49 o 7 7 11 150.59 175.18 21.98 o 1 8 11 0.45 7.72 10.18 o 2 8 11 5.29 4.63 9.42 o 3 8 11 47.39 31.20 10.92 o 4 8 11 1.23 1.02 10.57 o 5 8 11 250.13 272.35 20.21 o 0 9 11 231.24 237.97 26.50 o 1 9 11 0.23 -2.49 11.38 o 0 0 12 2718.49 2759.56 323.82 o 2 0 12 51.38 93.69 38.08 o 4 0 12 243.27 235.43 20.59 o 6 0 12 202.38 193.29 18.17 o 8 0 12 873.05 923.84 80.24 o 10 0 12 161.67 192.00 19.32 o 1 1 12 105.93 142.42 20.12 o 2 1 12 190.70 256.15 35.51 o 3 1 12 496.50 501.71 28.06 o 4 1 12 13.41 31.61 12.05 o 5 1 12 216.65 233.16 15.60 o 6 1 12 52.94 27.84 8.43 o 7 1 12 70.19 81.94 9.45 o 8 1 12 55.55 66.39 9.35 o 9 1 12 23.62 13.19 8.66 o 10 1 12 164.45 168.29 17.75 o 0 2 12 3.20 17.68 13.31 o 1 2 12 197.83 174.04 15.61 o 2 2 12 214.69 221.60 27.54 o 3 2 12 34.39 31.25 8.76 o 4 2 12 1.67 -3.61 8.34 o 5 2 12 13.54 8.42 9.02 o 6 2 12 577.64 562.41 50.00 o 7 2 12 240.41 242.27 16.47 o 8 2 12 79.62 83.01 10.09 o 9 2 12 80.19 84.98 10.20 o 10 2 12 16.71 11.62 10.85 o 1 3 12 26.10 13.89 8.49 o 2 3 12 5.56 3.53 8.70 o 3 3 12 5.28 15.56 8.50 o 4 3 12 448.83 478.10 27.25 o 5 3 12 43.90 73.87 16.62 o 6 3 12 150.80 156.44 14.99 o 7 3 12 11.13 9.77 9.29 o 8 3 12 30.53 18.47 11.60 o 9 3 12 23.01 16.55 11.72 o 10 3 12 71.25 83.85 17.95 o 0 4 12 2.17 -14.34 9.56 o 1 4 12 520.67 510.09 26.22 o 2 4 12 13.03 17.80 7.89 o 3 4 12 43.61 52.97 9.27 o 4 4 12 39.23 37.46 10.54 o 5 4 12 86.70 75.86 11.47 o 6 4 12 12.08 -4.65 10.52 o 7 4 12 438.12 545.69 35.61 o 8 4 12 2.94 0.84 11.51 o 9 4 12 99.59 73.52 16.26 o 1 5 12 20.76 14.71 8.06 o 2 5 12 371.82 429.93 22.48 o 3 5 12 33.95 25.59 9.01 o 4 5 12 111.19 118.95 11.64 o 5 5 12 28.31 14.86 9.71 o 6 5 12 101.76 101.46 11.36 o 7 5 12 16.51 14.29 11.54 o 8 5 12 9.96 23.18 12.54 o 0 6 12 583.18 604.90 52.70 o 1 6 12 144.27 141.05 14.92 o 2 6 12 93.30 83.97 11.70 o 3 6 12 69.43 55.72 10.20 o 4 6 12 25.03 26.37 8.83 o 5 6 12 119.62 108.94 11.77 o 6 6 12 1.96 -1.20 9.41 o 7 6 12 80.22 50.47 13.54 o 1 7 12 14.86 25.88 10.59 o 2 7 12 2.30 11.95 12.57 o 3 7 12 64.90 46.20 18.47 o 4 7 12 60.27 66.69 11.13 o 1 0 13 146.19 123.79 21.28 o 3 0 13 497.00 534.51 119.96 o 5 0 13 291.69 294.71 30.46 o 7 0 13 140.55 160.40 34.33 o 0 1 13 630.97 701.42 153.29 o 1 1 13 194.01 200.21 30.50 o 2 1 13 216.68 206.99 17.08 o 3 1 13 111.09 123.36 14.06 o 4 1 13 11.14 8.77 9.55 o 5 1 13 2.87 2.78 9.60 o 6 1 13 52.25 40.18 11.28 o 7 1 13 9.70 3.78 10.33 o 8 1 13 173.02 162.32 18.93 o 1 2 13 0.41 0.42 10.42 o 2 2 13 167.07 174.54 15.46 o 3 2 13 235.06 278.31 26.69 o 4 2 13 175.28 161.67 13.45 o 5 2 13 506.94 510.54 33.12 o 6 2 13 52.45 50.17 11.01 o 7 2 13 2.86 3.40 10.53 o 8 2 13 1.12 6.12 10.57 o 0 3 13 137.38 118.08 18.44 o 1 3 13 113.00 117.05 15.21 o 2 3 13 92.27 78.75 12.81 o 3 3 13 16.13 16.43 10.03 o 4 3 13 0.58 14.99 9.86 o 5 3 13 91.44 79.78 12.64 o 6 3 13 32.92 38.69 10.75 o 7 3 13 299.89 335.44 24.38 o 1 4 13 100.23 90.08 11.27 o 2 4 13 123.78 95.18 13.23 o 3 4 13 74.35 106.54 13.91 o 4 4 13 301.28 296.58 21.42 o 5 4 13 3.11 2.05 11.83 o 6 4 13 94.00 97.25 19.97 o 0 5 13 11.27 -7.15 15.85 o 1 5 13 129.28 150.71 18.99 o 2 5 13 4.65 10.26 11.02 o 3 5 13 5.94 6.05 10.22 o 4 5 13 1.28 6.40 10.08 o 5 5 13 26.66 11.33 12.13 o 1 6 13 52.46 53.80 13.68 o 2 6 13 22.91 14.53 11.46 o 0 0 14 531.80 345.17 49.50 o 2 0 14 142.16 194.14 25.05 o 4 0 14 0.04 -12.21 16.67 o 1 1 14 84.20 92.75 13.82 o 2 1 14 156.69 222.10 24.40 o 3 1 14 271.99 268.18 43.96 o 4 1 14 1.99 -0.45 12.06 o 5 1 14 134.12 115.30 14.11 o 0 2 14 60.70 66.24 55.35 o 1 2 14 115.29 103.92 14.55 o 2 2 14 166.86 184.00 16.52 o 3 2 14 16.57 31.20 12.95 o 4 2 14 36.01 19.87 10.53 o 1 3 14 5.02 -1.46 11.72 o 2 3 14 58.17 38.17 12.86 o 3 3 14 73.70 79.35 12.22 o 0 4 14 95.92 136.79 25.35 o 1 4 14 129.65 122.26 14.75 o