#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216424.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216424_Fobs loop_ _publ_author_name 'Singh, N. K.' 'Singh, Mamata' 'Srivastava, Ajay K.' 'Shrivastav, Anuraag' 'Sharma, R. K.' _publ_section_title ; 2-Methoxy-N'-(morpholin-4-ylcarbonothioyl)benzohydrazide hemihydrate ; _journal_coeditor_code DN2277 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4895 _journal_volume 63 _journal_year 2007 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.4864 _cell_length_b 24.6003 _cell_length_c 8.8726 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.8300 _[local]_cod_data_source_file dn2277Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 467 NKS-9 SMN with abs' _shelx_refln_list_code 4 _shelx_f_calc_maximum 328.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' 'x+1/2, -y, -z+1/2' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' '-x-1/2, y, z-1/2' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23299.54 17689.10 238.16 o 4 0 0 250.67 195.48 16.34 o 6 0 0 18357.19 17074.82 660.43 o 8 0 0 6430.41 6810.94 248.32 o 10 0 0 923.49 847.39 117.46 o 12 0 0 518.16 520.52 59.30 o 14 0 0 8056.03 8127.56 378.72 o 16 0 0 89.99 17.68 63.94 o 3 1 0 13443.08 12693.11 291.29 o 5 1 0 10728.46 10189.37 143.28 o 7 1 0 225.25 204.84 22.92 o 9 1 0 146.74 160.45 29.77 o 11 1 0 7155.55 6377.38 427.14 o 13 1 0 2.61 -24.90 24.90 o 15 1 0 346.32 236.65 48.11 o 2 2 0 11668.89 10064.39 191.55 o 4 2 0 4674.71 4013.54 97.11 o 6 2 0 1271.67 1164.55 14.11 o 8 2 0 3242.36 3294.76 88.33 o 10 2 0 3610.46 3352.96 143.75 o 12 2 0 262.60 152.17 24.93 o 14 2 0 792.01 836.59 78.79 o 16 2 0 5.85 62.79 54.13 o 1 3 0 1182.21 1002.76 33.28 o 3 3 0 817.82 719.82 13.41 o 5 3 0 587.00 600.03 13.09 o 7 3 0 637.17 704.24 10.21 o 9 3 0 2048.01 2262.10 116.66 o 11 3 0 2316.81 2091.93 99.41 o 13 3 0 3257.84 3272.64 127.95 o 15 3 0 185.21 182.85 51.25 o 0 4 0 2121.95 1945.96 79.98 o 2 4 0 13.76 8.15 2.98 o 4 4 0 9921.21 9361.49 148.59 o 6 4 0 147.40 112.51 6.22 o 8 4 0 5212.98 6085.49 101.07 o 10 4 0 524.29 580.13 41.03 o 12 4 0 488.59 457.11 32.56 o 14 4 0 382.49 285.50 54.78 o 16 4 0 243.49 188.28 55.92 o 1 5 0 85.85 71.09 8.66 o 3 5 0 407.42 462.35 17.31 o 5 5 0 1527.17 1557.55 36.63 o 7 5 0 4626.60 5133.93 69.13 o 9 5 0 537.83 555.19 14.78 o 11 5 0 42.20 7.75 15.35 o 13 5 0 21.57 44.68 62.08 o 15 5 0 569.52 649.08 105.19 o 2 6 0 79.26 46.20 7.28 o 4 6 0 17580.57 16489.53 234.44 o 6 6 0 17871.88 19464.75 207.62 o 8 6 0 3513.04 3759.26 78.90 o 10 6 0 2295.28 2321.96 46.91 o 12 6 0 357.27 366.03 31.00 o 14 6 0 1001.22 1140.45 127.43 o 1 7 0 4871.45 4677.96 90.98 o 3 7 0 333.14 313.53 15.34 o 5 7 0 13790.72 14172.32 186.08 o 7 7 0 5614.26 5691.26 79.07 o 9 7 0 83.79 89.04 6.64 o 11 7 0 2619.80 2573.96 56.92 o 13 7 0 1028.33 1058.50 60.83 o 15 7 0 893.89 1190.60 110.04 o 0 8 0 5552.31 5667.45 152.77 o 2 8 0 472.30 497.25 25.66 o 4 8 0 14843.95 14299.69 359.42 o 6 8 0 1542.12 1607.41 43.18 o 8 8 0 3.68 -1.06 4.11 o 10 8 0 4730.64 4762.94 100.91 o 12 8 0 43.48 49.13 6.20 o 14 8 0 739.03 710.14 56.28 o 1 9 0 4251.14 3938.52 146.25 o 3 9 0 271.54 267.60 12.37 o 5 9 0 361.24 390.00 17.23 o 7 9 0 7228.18 7448.88 148.81 o 9 9 0 103.65 125.42 9.09 o 11 9 0 1592.01 1462.42 38.35 o 13 9 0 2126.37 1958.83 66.54 o 15 9 0 225.33 295.90 66.11 o 0 10 0 6873.89 6967.66 371.50 o 2 10 0 9223.17 9044.37 337.02 o 4 10 0 5632.19 5679.94 146.38 o 6 10 0 1318.27 1401.34 25.47 o 8 10 0 366.27 365.02 13.15 o 10 10 0 710.86 658.23 23.00 o 12 10 0 30.40 34.76 8.25 o 14 10 0 80.04 104.85 44.95 o 1 11 0 10936.39 12205.06 215.81 o 3 11 0 105.91 146.81 12.31 o 5 11 0 9580.53 9365.31 252.30 o 7 11 0 94.39 155.62 11.87 o 9 11 0 2200.44 2233.51 43.68 o 11 11 0 169.83 156.96 10.38 o 13 11 0 208.39 227.66 18.65 o 15 11 0 555.14 664.83 58.40 o 0 12 0 7060.90 8817.94 239.15 o 2 12 0 5524.70 5973.94 209.53 o 4 12 0 0.49 21.29 8.53 o 6 12 0 1729.82 1651.36 46.40 o 8 12 0 855.79 988.31 26.01 o 10 12 0 23.10 9.09 6.82 o 12 12 0 5.18 6.45 10.85 o 14 12 0 63.55 134.68 37.68 o 1 13 0 6477.08 6731.23 201.28 o 3 13 0 8608.44 8157.22 239.35 o 5 13 0 611.84 577.06 23.24 o 7 13 0 42.53 38.68 7.23 o 9 13 0 108.58 122.15 10.70 o 11 13 0 394.45 390.95 16.99 o 13 13 0 1574.97 1560.67 48.67 o 0 14 0 677.02 461.30 26.04 o 2 14 0 9.52 23.97 7.87 o 4 14 0 3209.57 2901.79 95.09 o 6 14 0 7893.77 8082.92 193.89 o 8 14 0 19.90 12.98 6.95 o 10 14 0 204.73 262.10 13.38 o 12 14 0 402.36 370.17 34.87 o 14 14 0 1147.02 1372.39 96.43 o 1 15 0 521.52 408.51 15.94 o 3 15 0 4379.58 4124.43 74.05 o 5 15 0 1205.76 1208.38 50.80 o 7 15 0 4491.16 4499.44 72.95 o 9 15 0 7579.95 7691.04 99.71 o 11 15 0 980.01 1202.45 38.50 o 13 15 0 9.32 7.89 20.56 o 0 16 0 132.14 98.31 24.29 o 2 16 0 29.05 22.26 6.70 o 4 16 0 1269.45 1195.44 49.79 o 6 16 0 36.26 55.95 9.03 o 8 16 0 598.34 649.98 33.03 o 10 16 0 298.56 249.54 25.52 o 12 16 0 4.39 1.01 17.95 o 1 17 0 630.65 620.29 32.72 o 3 17 0 5.74 -3.69 8.07 o 5 17 0 196.13 175.75 12.46 o 7 17 0 10783.20 11027.47 298.45 o 9 17 0 25.20 11.74 9.28 o 11 17 0 694.31 731.83 56.29 o 13 17 0 52.95 98.37 31.44 o 0 18 0 13.80 18.33 22.89 o 2 18 0 841.97 876.98 29.25 o 4 18 0 5687.94 5970.62 117.04 o 6 18 0 1605.19 1658.59 58.18 o 8 18 0 587.66 599.07 26.65 o 10 18 0 354.11 417.06 24.81 o 12 18 0 167.13 178.16 37.19 o 1 19 0 750.12 749.67 28.16 o 3 19 0 172.19 195.60 16.92 o 5 19 0 6673.73 7281.89 169.99 o 7 19 0 1343.36 1319.24 37.22 o 9 19 0 591.75 620.72 41.95 o 11 19 0 50.35 31.92 28.51 o 0 20 0 0.99 -23.88 36.78 o 2 20 0 1898.17 1751.97 54.01 o 4 20 0 728.77 624.11 22.38 o 6 20 0 1173.51 1128.26 32.81 o 8 20 0 0.14 2.57 13.12 o 10 20 0 795.09 769.40 34.91 o 1 21 0 676.15 689.43 30.95 o 3 21 0 175.62 166.39 13.29 o 5 21 0 3.87 11.16 13.69 o 7 21 0 1142.75 1216.78 37.25 o 9 21 0 305.38 290.23 27.65 o 11 21 0 1476.97 1476.07 73.50 o 0 22 0 338.15 408.52 38.00 o 2 22 0 729.69 666.89 38.42 o 4 22 0 17.69 -5.62 15.08 o 6 22 0 365.75 348.39 39.77 o 8 22 0 275.91 241.42 22.79 o 10 22 0 612.30 616.61 49.41 o 1 23 0 2690.39 2392.27 60.05 o 3 23 0 74.55 66.10 24.20 o 5 23 0 117.81 125.69 17.71 o 7 23 0 3081.52 3096.78 139.60 o 9 23 0 29.16 32.97 20.47 o 0 24 0 3022.04 3338.40 134.17 o 2 24 0 2630.86 2567.44 71.64 o 4 24 0 735.38 909.67 50.37 o 6 24 0 8.17 -22.65 22.65 o 8 24 0 431.86 460.99 49.38 o 1 25 0 53.70 59.53 24.49 o 3 25 0 1204.65 1298.80 54.33 o 5 25 0 96.30 68.01 25.47 o 7 25 0 19.03 22.03 26.49 o 0 26 0 8.65 23.26 24.40 o 2 26 0 360.07 403.25 36.73 o 4 26 0 117.96 134.18 27.38 o 6 26 0 81.98 75.40 30.22 o 1 27 0 36.72 59.27 26.81 o 3 27 0 0.19 -7.85 27.30 o 5 27 0 5.03 -6.14 46.45 o 0 28 0 484.59 510.42 76.22 o 2 28 0 136.32 224.83 39.45 o 4 28 0 537.45 673.67 85.61 o 1 29 0 326.42 177.92 62.67 o 3 29 0 285.85 320.56 78.14 o 1 1 1 2866.44 2658.16 56.66 o 2 1 1 11416.37 10573.55 97.51 o 3 1 1 23052.28 21276.83 260.57 o 4 1 1 66.77 68.20 3.40 o 5 1 1 73.04 72.23 2.93 o 6 1 1 4.96 2.58 1.58 o 7 1 1 72.52 58.71 3.39 o 8 1 1 136.21 132.22 4.50 o 9 1 1 998.43 1073.76 22.28 o 10 1 1 1.14 25.45 9.83 o 11 1 1 1562.19 1679.26 75.64 o 12 1 1 25.35 19.04 22.03 o 13 1 1 3.40 16.19 20.66 o 14 1 1 11.20 36.79 30.33 o 15 1 1 973.40 974.57 50.74 o 16 1 1 0.71 54.55 28.10 o 1 2 1 1126.12 1097.28 12.48 o 2 2 1 8006.77 7385.36 91.64 o 3 2 1 537.11 553.52 7.35 o 4 2 1 1561.54 1583.24 21.30 o 5 2 1 1929.98 1821.68 21.71 o 6 2 1 328.27 286.43 6.32 o 7 2 1 37.61 24.91 5.37 o 8 2 1 0.39 8.22 3.83 o 9 2 1 2057.49 2189.05 38.12 o 10 2 1 75.86 71.08 12.05 o 11 2 1 1983.95 2097.64 107.48 o 12 2 1 1348.79 1265.42 74.16 o 13 2 1 228.56 268.07 27.78 o 14 2 1 494.26 500.50 40.46 o 15 2 1 1586.77 1661.04 112.36 o 16 2 1 119.69 99.11 35.92 o 1 3 1 1996.81 1884.61 20.68 o 2 3 1 247.79 332.04 9.46 o 3 3 1 930.56 804.81 13.11 o 4 3 1 218.37 248.88 5.11 o 5 3 1 56.68 40.18 3.05 o 6 3 1 508.85 434.03 9.21 o 7 3 1 1152.51 1220.95 18.90 o 8 3 1 1318.75 1290.26 23.82 o 9 3 1 1701.14 1672.32 35.40 o 10 3 1 289.78 304.59 8.80 o 11 3 1 144.25 139.82 20.77 o 12 3 1 969.43 913.44 44.86 o 13 3 1 493.46 631.37 69.90 o 14 3 1 18.87 23.62 21.79 o 15 3 1 564.67 600.18 65.48 o 16 3 1 594.18 760.26 72.41 o 1 4 1 1156.95 1012.11 12.45 o 2 4 1 143.62 167.99 4.07 o 3 4 1 4288.44 4144.66 56.58 o 4 4 1 3176.62 3091.41 31.33 o 5 4 1 8692.84 8526.93 68.50 o 6 4 1 85.25 67.01 3.56 o 7 4 1 586.21 715.99 11.64 o 8 4 1 664.92 776.48 18.24 o 9 4 1 2853.07 2948.10 66.92 o 10 4 1 1.34 4.11 6.55 o 11 4 1 1762.35 1927.56 46.03 o 12 4 1 161.85 156.63 25.20 o 13 4 1 12.54 -3.17 17.20 o 14 4 1 10.50 4.45 19.89 o 15 4 1 128.75 157.57 28.48 o 16 4 1 413.28 476.56 57.16 o 1 5 1 6211.95 5869.37 71.75 o 2 5 1 2074.16 2073.58 23.16 o 3 5 1 296.76 273.54 5.35 o 4 5 1 1896.47 1717.08 20.35 o 5 5 1 6237.30 6269.73 57.71 o 6 5 1 1029.57 1212.43 19.70 o 7 5 1 1155.14 1513.36 19.58 o 8 5 1 171.31 230.97 7.87 o 9 5 1 1486.19 1593.39 26.46 o 10 5 1 2.26 2.58 4.78 o 11 5 1 38.92 37.95 5.61 o 12 5 1 0.81 18.58 14.68 o 13 5 1 270.52 287.24 31.37 o 14 5 1 234.38 319.57 32.19 o 15 5 1 7.50 22.61 26.21 o 1 6 1 12914.59 12582.57 127.56 o 2 6 1 4515.20 4209.05 53.25 o 3 6 1 2200.37 2165.50 26.94 o 4 6 1 1663.89 1680.53 21.89 o 5 6 1 364.21 341.19 7.19 o 6 6 1 166.20 171.61 6.25 o 7 6 1 166.44 237.36 9.49 o 8 6 1 186.10 167.63 6.61 o 9 6 1 6.64 3.18 3.78 o 10 6 1 160.12 161.18 5.73 o 11 6 1 80.38 54.75 7.85 o 12 6 1 33.14 25.45 10.20 o 13 6 1 353.84 330.31 32.94 o 14 6 1 418.64 429.74 41.77 o 15 6 1 195.56 245.93 34.63 o 1 7 1 3330.44 2972.25 38.86 o 2 7 1 10.51 9.88 3.61 o 3 7 1 394.90 359.45 10.40 o 4 7 1 2054.88 2111.30 25.76 o 5 7 1 563.19 647.09 11.10 o 6 7 1 4533.14 5081.95 53.09 o 7 7 1 548.49 575.90 9.95 o 8 7 1 1368.40 1500.67 30.19 o 9 7 1 626.16 726.69 17.26 o 10 7 1 86.23 92.77 4.82 o 11 7 1 8.20 7.34 3.82 o 12 7 1 157.98 142.32 6.44 o 13 7 1 65.77 103.32 22.89 o 14 7 1 152.64 58.29 26.15 o 15 7 1 32.97 76.41 27.68 o 1 8 1 4524.19 4494.67 48.56 o 2 8 1 0.01 3.08 2.55 o 3 8 1 1948.18 2098.52 34.73 o 4 8 1 1580.58 1544.74 19.33 o 5 8 1 152.36 162.27 5.20 o 6 8 1 79.97 84.37 5.08 o 7 8 1 92.84 78.40 5.51 o 8 8 1 889.48 1031.56 16.96 o 9 8 1 31.97 37.07 5.09 o 10 8 1 822.77 853.88 18.83 o 11 8 1 14.58 17.52 3.67 o 12 8 1 453.32 491.47 12.82 o 13 8 1 707.99 647.88 36.85 o 14 8 1 351.54 321.63 35.70 o 15 8 1 799.80 936.07 105.41 o 1 9 1 4096.56 4182.78 53.56 o 2 9 1 2290.77 2174.79 35.46 o 3 9 1 283.44 308.28 7.32 o 4 9 1 984.77 960.42 19.28 o 5 9 1 559.14 653.50 11.77 o 6 9 1 388.72 324.92 10.31 o 7 9 1 1563.46 1596.98 31.17 o 8 9 1 1890.34 1773.54 28.12 o 9 9 1 237.36 260.22 7.89 o 10 9 1 238.69 238.15 8.18 o 11 9 1 65.26 41.50 4.42 o 12 9 1 0.36 3.56 3.81 o 13 9 1 65.36 45.62 10.30 o 14 9 1 3.58 -11.20 21.16 o 15 9 1 615.07 680.64 47.23 o 1 10 1 872.98 988.20 25.79 o 2 10 1 2177.83 2105.58 43.91 o 3 10 1 531.80 488.48 9.55 o 4 10 1 1458.75 1606.77 25.18 o 5 10 1 376.28 292.39 8.27 o 6 10 1 39.46 20.61 4.12 o 7 10 1 122.36 105.67 6.09 o 8 10 1 382.00 344.52 8.36 o 9 10 1 1327.44 1387.30 27.41 o 10 10 1 116.94 94.87 7.94 o 11 10 1 32.27 37.66 5.24 o 12 10 1 3.51 -3.74 5.35 o 13 10 1 750.66 738.26 27.53 o 14 10 1 2.66 -16.33 20.46 o 15 10 1 336.57 344.00 50.74 o 1 11 1 224.87 302.22 13.83 o 2 11 1 15829.76 15906.64 241.77 o 3 11 1 928.05 991.72 18.84 o 4 11 1 3570.20 3503.66 59.34 o 5 11 1 1065.26 986.03 21.19 o 6 11 1 427.84 390.79 10.87 o 7 11 1 556.62 520.60 11.58 o 8 11 1 346.60 303.96 13.48 o 9 11 1 336.70 309.47 11.27 o 10 11 1 224.66 236.73 8.40 o 11 11 1 41.49 35.30 6.14 o 12 11 1 1213.06 1273.25 27.82 o 13 11 1 410.45 418.48 32.84 o 14 11 1 16.55 24.68 24.31 o 15 11 1 2.41 -3.16 28.35 o 1 12 1 309.78 348.14 9.61 o 2 12 1 4200.70 4593.65 71.66 o 3 12 1 850.14 695.85 17.76 o 4 12 1 496.93 515.14 14.77 o 5 12 1 410.69 375.47 9.42 o 6 12 1 1813.24 1838.73 31.44 o 7 12 1 496.78 495.51 11.49 o 8 12 1 891.60 890.27 17.60 o 9 12 1 1325.43 1273.41 27.09 o 10 12 1 81.91 91.06 7.03 o 11 12 1 3.57 12.63 6.16 o 12 12 1 25.32 22.23 8.84 o 13 12 1 429.81 520.98 26.32 o 14 12 1 137.85 139.91 22.74 o 1 13 1 47.15 32.33 6.12 o 2 13 1 513.33 474.66 16.31 o 3 13 1 603.20 597.07 19.05 o 4 13 1 71.68 95.35 8.19 o 5 13 1 243.19 209.51 8.41 o 6 13 1 1256.17 1317.98 27.66 o 7 13 1 929.04 978.75 15.76 o 8 13 1 224.08 207.06 8.24 o 9 13 1 278.21 283.48 10.97 o 10 13 1 91.94 120.82 8.68 o 11 13 1 164.17 160.40 9.30 o 12 13 1 44.18 56.81 11.52 o 13 13 1 425.79 438.08 24.97 o 14 13 1 3.91 5.98 14.98 o 1 14 1 143.25 125.25 8.52 o 2 14 1 36.82 30.41 5.91 o 3 14 1 109.06 113.59 6.19 o 4 14 1 31.47 15.76 4.78 o 5 14 1 9.03 7.18 4.76 o 6 14 1 189.51 180.24 7.71 o 7 14 1 150.11 117.14 7.18 o 8 14 1 416.73 411.28 15.55 o 9 14 1 2.36 0.19 5.87 o 10 14 1 566.59 571.14 16.71 o 11 14 1 7.12 2.92 7.49 o 12 14 1 1.44 11.16 10.90 o 13 14 1 11.23 38.18 18.79 o 14 14 1 12.70 28.55 18.22 o 1 15 1 3.85 0.50 5.44 o 2 15 1 348.47 339.87 12.43 o 3 15 1 94.00 88.74 6.96 o 4 15 1 1.02 0.76 4.78 o 5 15 1 7.22 15.77 5.61 o 6 15 1 0.00 4.69 5.59 o 7 15 1 55.52 55.86 7.15 o 8 15 1 25.74 18.63 7.57 o 9 15 1 2227.30 2393.99 40.04 o 10 15 1 69.22 67.64 9.95 o 11 15 1 105.99 103.23 10.92 o 12 15 1 19.08 17.14 12.86 o 13 15 1 117.75 87.93 15.10 o 1 16 1 15.82 14.40 6.07 o 2 16 1 931.95 934.11 24.89 o 3 16 1 154.47 152.57 8.94 o 4 16 1 549.48 507.62 12.69 o 5 16 1 21.68 25.50 5.58 o 6 16 1 315.39 336.95 13.83 o 7 16 1 1234.60 1237.78 24.65 o 8 16 1 369.52 370.73 12.50 o 9 16 1 1800.95 1931.36 40.03 o 10 16 1 367.27 392.26 23.34 o 11 16 1 7.33 14.43 10.98 o 12 16 1 131.71 144.26 15.78 o 13 16 1 312.42 343.98 28.40 o 1 17 1 65.79 74.69 8.39 o 2 17 1 5526.78 5800.29 73.42 o 3 17 1 55.85 50.57 6.91 o 4 17 1 867.19 819.81 19.24 o 5 17 1 611.79 620.43 16.21 o 6 17 1 5091.47 5339.98 99.20 o 7 17 1 1758.47 1770.22 35.70 o 8 17 1 4728.29 5073.52 87.22 o 9 17 1 160.84 130.39 10.94 o 10 17 1 0.29 16.98 10.75 o 11 17 1 13.61 17.44 11.02 o 12 17 1 779.43 794.81 28.10 o 13 17 1 123.06 174.72 19.01 o 1 18 1 294.39 253.18 13.80 o 2 18 1 1025.45 1021.19 21.20 o 3 18 1 455.84 443.32 20.38 o 4 18 1 2373.53 2405.07 51.07 o 5 18 1 21.25 11.91 7.51 o 6 18 1 315.97 341.22 15.16 o 7 18 1 1003.55 1072.48 19.56 o 8 18 1 2542.93 2609.25 44.93 o 9 18 1 496.43 537.61 16.81 o 10 18 1 994.64 981.40 35.41 o 11 18 1 18.68 15.67 13.43 o 12 18 1 5.13 26.40 17.72 o 1 19 1 133.21 107.51 13.48 o 2 19 1 3845.09 3959.09 53.02 o 3 19 1 306.02 317.37 23.97 o 4 19 1 4092.11 3999.92 87.32 o 5 19 1 1130.81 1135.34 28.06 o 6 19 1 210.83 194.73 14.45 o 7 19 1 708.66 762.05 22.10 o 8 19 1 0.20 -6.72 8.48 o 9 19 1 11.54 33.70 10.36 o 10 19 1 194.89 198.08 14.86 o 11 19 1 100.29 79.83 15.61 o 12 19 1 257.33 331.32 32.57 o 1 20 1 55.64 64.42 10.84 o 2 20 1 1508.00 1436.11 28.05 o 3 20 1 216.64 183.60 16.12 o 4 20 1 195.14 187.95 12.32 o 5 20 1 481.99 455.12 21.24 o 6 20 1 725.20 689.85 18.29 o 7 20 1 41.14 40.82 8.29 o 8 20 1 3.68 11.88 9.22 o 9 20 1 675.28 629.34 23.31 o 10 20 1 12.40 29.35 11.85 o 11 20 1 49.78 68.00 18.29 o 1 21 1 46.92 23.97 12.09 o 2 21 1 332.04 333.46 14.93 o 3 21 1 50.92 36.16 15.77 o 4 21 1 27.80 32.94 9.72 o 5 21 1 74.52 46.54 11.90 o 6 21 1 115.50 121.58 14.13 o 7 21 1 118.64 123.19 13.09 o 8 21 1 178.11 166.86 13.93 o 9 21 1 7.24 6.51 11.04 o 10 21 1 34.34 25.51 16.49 o 11 21 1 0.01 -18.50 18.50 o 1 22 1 62.36 38.76 15.36 o 2 22 1 15.18 19.02 12.03 o 3 22 1 601.45 582.43 30.36 o 4 22 1 29.47 18.33 14.00 o 5 22 1 358.35 338.34 19.66 o 6 22 1 25.07 34.50 16.40 o 7 22 1 15.74 14.22 14.11 o 8 22 1 48.48 66.13 13.86 o 9 22 1 0.02 -11.11 12.41 o 10 22 1 155.48 147.58 21.57 o 1 23 1 6.00 8.57 13.64 o 2 23 1 1700.76 1651.90 57.27 o 3 23 1 23.60 26.60 11.96 o 4 23 1 460.14 426.44 19.76 o 5 23 1 18.49 -0.76 11.71 o 6 23 1 583.09 618.31 32.36 o 7 23 1 3.51 -6.87 12.59 o 8 23 1 734.53 749.50 26.24 o 9 23 1 249.50 250.95 19.20 o 10 23 1 0.91 17.92 21.73 o 1 24 1 340.02 408.36 49.98 o 2 24 1 1228.02 1167.96 48.64 o 3 24 1 30.03 39.53 15.74 o 4 24 1 116.62 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25.03 o 4 21 2 8.01 2.56 11.43 o 5 21 2 95.34 57.01 12.01 o 6 21 2 78.84 52.60 9.45 o 7 21 2 173.11 144.94 16.03 o 8 21 2 330.26 336.92 20.85 o 9 21 2 170.09 133.01 16.17 o 10 21 2 483.98 471.88 31.09 o 11 21 2 119.30 116.39 23.53 o 0 22 2 727.29 719.22 33.97 o 1 22 2 392.14 315.63 25.05 o 2 22 2 244.65 220.86 22.51 o 3 22 2 1018.01 963.09 33.47 o 4 22 2 294.36 258.05 16.29 o 5 22 2 448.65 403.27 22.66 o 6 22 2 41.40 39.86 11.54 o 7 22 2 1824.27 1927.75 47.19 o 8 22 2 201.36 173.07 18.14 o 9 22 2 119.21 122.74 17.77 o 10 22 2 374.75 533.13 47.54 o 0 23 2 1529.42 1777.60 63.63 o 1 23 2 0.73 6.47 14.34 o 2 23 2 143.75 126.34 15.18 o 3 23 2 703.44 643.17 24.81 o 4 23 2 143.70 98.92 15.20 o 5 23 2 80.58 90.20 17.56 o 6 23 2 8.06 9.80 13.22 o 7 23 2 485.78 480.35 26.00 o 8 23 2 831.96 967.57 35.29 o 9 23 2 14.85 12.01 17.65 o 0 24 2 1770.01 1526.38 102.84 o 1 24 2 30.03 29.24 18.40 o 2 24 2 135.32 142.82 22.35 o 3 24 2 297.98 308.70 26.82 o 4 24 2 32.84 41.84 18.78 o 5 24 2 127.61 124.86 19.42 o 6 24 2 0.69 0.33 14.93 o 7 24 2 1.58 27.19 17.17 o 8 24 2 51.46 36.02 20.16 o 9 24 2 8.94 26.76 25.15 o 0 25 2 1018.62 962.55 55.12 o 1 25 2 699.88 611.70 44.80 o 2 25 2 66.06 61.77 27.43 o 3 25 2 0.08 -6.79 17.99 o 4 25 2 163.02 193.08 29.69 o 5 25 2 72.58 29.76 17.89 o 6 25 2 68.15 77.20 22.61 o 7 25 2 23.93 64.84 22.93 o 8 25 2 50.17 51.75 21.79 o 0 26 2 244.17 206.28 39.30 o 1 26 2 50.87 44.53 26.04 o 2 26 2 77.87 79.14 21.70 o 3 26 2 293.07 271.34 26.83 o 4 26 2 569.17 595.77 39.15 o 5 26 2 67.78 86.77 23.91 o 6 26 2 100.01 106.34 25.14 o 7 26 2 388.73 528.39 36.66 o 0 27 2 238.62 322.66 47.18 o 1 27 2 2.67 -1.76 25.04 o 2 27 2 111.10 155.85 26.13 o 3 27 2 112.91 117.96 26.76 o 4 27 2 78.02 75.50 22.19 o 5 27 2 103.64 140.52 28.28 o 0 28 2 122.83 210.25 50.45 o 1 28 2 137.44 114.86 28.08 o 2 28 2 281.35 309.26 31.14 o 3 28 2 83.70 92.14 32.42 o 4 28 2 59.16 89.03 23.98 o 0 29 2 892.45 989.71 67.96 o 1 29 2 42.19 95.08 32.99 o 1 1 3 423.62 386.17 12.18 o 2 1 3 12362.60 12105.22 113.41 o 3 1 3 959.52 978.49 20.87 o 4 1 3 260.61 258.11 7.15 o 5 1 3 9611.90 9841.18 79.10 o 6 1 3 900.55 1046.04 15.82 o 7 1 3 184.69 205.31 7.33 o 8 1 3 299.32 310.43 11.81 o 9 1 3 2910.49 3023.10 46.19 o 10 1 3 649.44 666.32 11.19 o 11 1 3 856.15 900.34 23.64 o 12 1 3 52.32 39.46 9.10 o 13 1 3 225.97 198.78 20.17 o 14 1 3 0.84 7.49 20.01 o 15 1 3 266.28 325.56 50.16 o 1 2 3 2734.55 2547.35 38.20 o 2 2 3 146.41 155.25 7.13 o 3 2 3 3935.70 4130.93 41.48 o 4 2 3 2544.98 2578.95 40.28 o 5 2 3 23.30 29.62 4.37 o 6 2 3 715.41 648.00 10.64 o 7 2 3 172.65 184.93 6.53 o 8 2 3 1657.16 1787.55 34.67 o 9 2 3 47.52 56.55 4.94 o 10 2 3 50.49 52.90 4.88 o 11 2 3 1436.16 1483.25 31.60 o 12 2 3 12.31 7.40 6.55 o 13 2 3 450.37 397.58 16.88 o 14 2 3 143.76 132.75 15.71 o 15 2 3 27.85 72.61 32.69 o 1 3 3 2499.68 2281.08 37.63 o 2 3 3 35.55 66.62 6.29 o 3 3 3 99.08 85.40 5.22 o 4 3 3 14.40 13.92 3.27 o 5 3 3 4156.93 4196.20 40.51 o 6 3 3 123.04 88.56 4.70 o 7 3 3 17.75 11.29 4.51 o 8 3 3 12.11 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458.31 12.89 o 11 6 4 1738.25 1798.46 41.27 o 12 6 4 0.34 -5.52 7.63 o 13 6 4 4.12 -2.85 16.48 o 14 6 4 25.08 -15.53 17.75 o 0 7 4 13852.50 13619.78 365.62 o 1 7 4 0.39 3.26 4.53 o 2 7 4 83.15 101.91 7.42 o 3 7 4 3404.54 3696.41 50.06 o 4 7 4 2825.32 2811.30 57.89 o 5 7 4 1.03 -0.13 4.79 o 6 7 4 3321.91 3396.86 57.33 o 7 7 4 275.77 270.53 10.88 o 8 7 4 456.33 469.13 17.20 o 9 7 4 1014.46 1099.43 17.58 o 10 7 4 540.30 557.83 17.32 o 11 7 4 2.01 3.46 8.68 o 12 7 4 7.63 2.40 8.57 o 13 7 4 4.86 2.77 10.93 o 14 7 4 991.40 1150.63 58.98 o 0 8 4 4425.68 4504.38 118.89 o 1 8 4 205.75 210.38 10.55 o 2 8 4 68.52 70.33 7.26 o 3 8 4 365.53 342.87 10.59 o 4 8 4 18.82 19.48 5.03 o 5 8 4 2227.54 2247.07 36.78 o 6 8 4 12.66 23.64 5.89 o 7 8 4 2860.10 3128.57 43.66 o 8 8 4 4.88 16.63 5.43 o 9 8 4 531.52 502.42 13.42 o 10 8 4 27.61 17.80 6.32 o 11 8 4 855.09 916.41 20.20 o 12 8 4 101.40 103.15 13.46 o 13 8 4 146.22 99.32 15.68 o 14 8 4 234.48 245.85 32.24 o 0 9 4 6412.94 6238.91 86.38 o 1 9 4 637.38 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847.45 39.69 o 6 15 8 68.30 65.49 23.41 o 0 16 8 2348.54 2648.53 168.22 o 1 16 8 30.79 60.52 26.34 o 2 16 8 307.63 263.66 31.62 o 3 16 8 4.47 -21.66 21.66 o 4 16 8 760.89 805.32 47.80 o 5 16 8 52.37 40.59 22.89 o 6 16 8 333.30 339.10 29.39 o 0 17 8 511.31 564.22 107.74 o 1 17 8 34.46 -4.47 25.74 o 2 17 8 98.58 115.93 30.28 o 3 17 8 0.68 -21.38 21.38 o 4 17 8 80.70 62.22 23.15 o 5 17 8 5.23 -8.35 23.61 o 0 18 8 63.21 71.15 35.17 o 1 18 8 9.60 12.57 26.97 o 2 18 8 44.16 82.14 25.54 o 3 18 8 13.95 18.88 25.00 o 4 18 8 37.42 53.39 24.24 o 0 19 8 457.99 383.46 50.75 o 1 19 8 13.64 52.81 25.88 o 2 19 8 150.89 132.90 37.97 o 1 1 9 5.84 14.74 15.42 o 2 1 9 734.57 904.54 54.21 o 3 1 9 70.47 60.34 16.69 o 4 1 9 127.62 122.33 19.74 o 5 1 9 25.35 17.05 18.00 o 6 1 9 5.51 13.03 18.67 o 7 1 9 31.18 37.61 20.20 o 8 1 9 24.17 7.05 19.70 o 1 2 9 124.22 118.84 18.76 o 2 2 9 2.44 4.21 14.81 o 3 2 9 146.74 180.85 24.76 o 4 2 9 630.39 718.73 30.83 o 5 2 9 0.05 33.73 21.01 o 6 2 9 49.23 64.02 19.66 o 7 2 9 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23.17 o 5 7 9 0.43 7.06 19.64 o 6 7 9 13.97 48.37 21.39 o 7 7 9 2.75 13.31 23.45 o 1 8 9 2.85 22.72 17.06 o 2 8 9 17.14 31.02 16.29 o 3 8 9 13.20 3.34 15.94 o 4 8 9 50.07 30.53 20.24 o 5 8 9 208.85 187.39 24.85 o 6 8 9 50.29 33.58 21.77 o 7 8 9 0.58 -9.07 24.13 o 1 9 9 186.14 271.89 30.82 o 2 9 9 223.90 222.74 33.20 o 3 9 9 266.93 218.48 28.80 o 4 9 9 16.22 28.86 19.36 o 5 9 9 183.52 203.44 31.31 o 6 9 9 214.15 208.45 28.57 o 7 9 9 8.24 -1.58 21.19 o 1 10 9 175.95 203.97 36.67 o 2 10 9 162.88 157.95 25.91 o 3 10 9 43.98 34.79 22.77 o 4 10 9 1.26 4.22 20.37 o 5 10 9 519.69 475.60 54.70 o 6 10 9 98.11 85.92 21.77 o 1 11 9 57.26 73.43 27.45 o 2 11 9 56.43 76.94 22.10 o 3 11 9 0.24 2.57 23.61 o 4 11 9 69.85 54.50 25.49 o 5 11 9 113.77 108.77 26.60 o 6 11 9 45.27 66.47 24.37 o 1 12 9 218.58 165.09 35.10 o 2 12 9 252.50 364.12 63.23 o 3 12 9 13.16 -22.59 30.08 o 4 12 9 1.08 9.84 36.20 o 5 12 9 166.70 165.20 26.88 o 1 13 9 35.55 49.74 28.82 o 2 13 9 200.36 195.34 33.53 o 3 13 9 7.57 0.06 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