#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216430.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216430_Fobs loop_ _publ_author_name 'Wojciechowska, A.' 'Daszkiewicz, M.' _publ_section_title ; Reinvestigation of bis(2,2'-bipyridine)(nitrato-\k^2^O,O')cobalt(III) hydroxide nitrate tetrahydrate ; _journal_coeditor_code EZ2106 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2975 _journal_page_last m2976 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.918 _cell_angle_gamma 90.000 _cell_length_a 10.9489 _cell_length_b 16.0468 _cell_length_c 14.4563 _exptl_crystal_F_000 1208.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file ez2106Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' co1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 322.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 37552.32 33917.30 90.63 o 4 0 0 33206.69 30913.64 626.10 o 6 0 0 9313.76 9942.81 138.56 o 8 0 0 3293.94 3485.28 81.77 o 10 0 0 109.28 93.97 16.75 o 12 0 0 644.87 660.82 26.44 o 3 1 0 5288.26 5035.25 72.12 o 5 1 0 7082.68 6764.71 83.08 o 7 1 0 2507.60 2568.22 31.06 o 9 1 0 2386.69 2518.44 46.84 o 11 1 0 6.46 8.25 6.47 o 13 1 0 402.58 427.90 27.19 o 2 2 0 915.82 1200.14 17.37 o 4 2 0 21.03 19.28 3.35 o 6 2 0 5330.01 5196.89 53.18 o 8 2 0 1033.46 979.47 16.42 o 10 2 0 56.46 46.50 9.35 o 12 2 0 516.38 546.20 20.83 o 1 3 0 5576.81 6004.68 76.33 o 3 3 0 7364.56 7241.50 53.89 o 5 3 0 30.56 44.50 4.58 o 7 3 0 1513.42 1574.93 22.05 o 9 3 0 1666.08 1649.98 22.35 o 11 3 0 13.18 25.13 9.54 o 13 3 0 322.87 315.02 23.91 o 0 4 0 5299.74 5863.60 49.49 o 2 4 0 7434.35 7521.15 44.94 o 4 4 0 1655.33 1414.25 21.74 o 6 4 0 4040.36 4011.22 44.65 o 8 4 0 4651.40 4988.20 75.74 o 10 4 0 304.82 261.20 15.19 o 12 4 0 157.69 115.41 20.71 o 1 5 0 462.12 324.83 7.54 o 3 5 0 13.98 14.81 2.64 o 5 5 0 547.89 442.18 8.75 o 7 5 0 4275.94 4402.37 54.27 o 9 5 0 2940.50 3116.38 31.78 o 11 5 0 62.94 50.24 14.56 o 0 6 0 4452.98 4521.22 83.03 o 2 6 0 3922.12 3710.56 47.70 o 6 6 0 8469.68 8710.79 81.45 o 8 6 0 2373.14 2377.66 54.14 o 10 6 0 1168.51 1287.11 41.87 o 12 6 0 89.95 75.67 20.69 o 1 7 0 431.58 353.38 7.47 o 3 7 0 1975.45 1509.44 16.02 o 5 7 0 4532.98 4451.50 47.05 o 7 7 0 5466.19 5596.16 68.28 o 9 7 0 652.31 631.30 18.84 o 11 7 0 302.15 361.73 28.70 o 0 8 0 4773.62 4178.03 40.34 o 2 8 0 5601.92 5406.11 70.51 o 4 8 0 1488.78 1598.97 28.35 o 6 8 0 3423.99 3783.55 64.98 o 8 8 0 639.92 660.85 15.38 o 10 8 0 305.22 362.46 16.58 o 12 8 0 352.61 368.36 27.55 o 1 9 0 10058.92 10297.43 88.38 o 3 9 0 4487.03 4371.71 42.33 o 5 9 0 1839.86 1778.31 33.45 o 7 9 0 2979.30 3179.28 28.41 o 9 9 0 27.54 43.08 8.70 o 11 9 0 262.22 265.71 20.53 o 0 10 0 526.06 676.28 30.00 o 2 10 0 2130.66 2386.58 22.10 o 4 10 0 6.38 5.92 4.12 o 6 10 0 1386.59 1416.72 21.70 o 8 10 0 25.76 23.36 6.85 o 10 10 0 219.16 248.03 16.89 o 1 11 0 4167.31 4672.13 121.86 o 3 11 0 1444.48 1577.63 34.45 o 5 11 0 323.80 354.94 13.62 o 7 11 0 466.22 437.02 14.09 o 9 11 0 35.73 31.95 8.48 o 11 11 0 103.27 85.16 16.05 o 0 12 0 2948.52 2630.46 68.35 o 2 12 0 4546.98 4606.53 69.39 o 4 12 0 1971.75 2074.12 42.58 o 6 12 0 981.15 999.47 23.46 o 8 12 0 112.96 163.43 13.70 o 10 12 0 215.62 245.89 18.62 o 1 13 0 1483.53 1574.87 72.62 o 3 13 0 3592.68 3936.76 35.67 o 5 13 0 718.97 723.87 18.91 o 7 13 0 653.40 657.68 21.58 o 9 13 0 168.92 159.56 16.73 o 0 14 0 377.61 407.38 38.11 o 2 14 0 1135.65 1250.26 32.67 o 4 14 0 274.34 268.30 21.92 o 6 14 0 550.60 579.48 23.64 o 8 14 0 199.79 238.71 17.71 o 1 15 0 337.73 329.15 25.38 o 3 15 0 387.52 361.45 23.84 o 5 15 0 72.05 87.75 17.63 o 7 15 0 374.16 385.60 18.76 o 0 16 0 220.57 202.12 41.81 o 2 16 0 51.64 19.28 10.56 o 4 16 0 11.06 14.64 11.25 o 6 16 0 224.13 205.06 35.08 o 8 16 0 23.89 23.45 11.26 o 1 17 0 21.06 16.12 11.03 o 3 17 0 1.94 8.66 9.19 o 5 17 0 56.32 29.26 13.32 o 7 17 0 37.48 28.19 12.27 o 0 18 0 653.37 743.05 47.12 o 2 18 0 40.17 18.84 11.28 o 4 18 0 148.04 158.04 39.17 o 1 19 0 125.94 86.09 19.82 o 3 19 0 126.31 143.06 23.96 o 0 20 0 393.62 373.15 64.18 o -13 1 1 0.79 14.10 9.57 o -11 1 1 6.61 6.86 5.88 o -9 1 1 20.93 30.15 6.23 o -7 1 1 54.72 41.50 4.94 o -5 1 1 3592.60 3520.29 35.58 o -3 1 1 8114.45 7949.14 96.69 o 1 1 1 493.28 664.82 8.96 o 3 1 1 3987.11 3347.36 51.25 o 5 1 1 2670.02 2589.11 47.61 o 7 1 1 25.09 25.41 5.35 o 9 1 1 2.22 9.18 6.21 o 11 1 1 18.98 16.15 7.55 o 13 1 1 0.97 10.47 9.00 o -12 2 1 9.67 17.09 9.80 o -10 2 1 12.40 12.02 6.09 o -8 2 1 159.78 197.41 7.95 o -6 2 1 98.77 173.28 5.96 o -4 2 1 2752.82 2458.87 27.93 o -2 2 1 5957.90 5443.57 52.12 o 2 2 1 581.48 592.72 12.12 o 4 2 1 151.95 138.57 8.76 o 6 2 1 563.09 756.13 13.27 o 8 2 1 235.68 218.13 10.52 o 10 2 1 0.05 9.81 6.50 o 12 2 1 4.98 10.36 9.26 o -13 3 1 26.87 30.40 12.25 o -11 3 1 563.01 605.74 21.41 o -9 3 1 104.13 93.25 10.61 o -7 3 1 28.98 19.91 3.77 o -5 3 1 429.21 412.06 10.17 o -3 3 1 310.39 413.17 6.87 o -1 3 1 328.07 316.36 9.07 o 1 3 1 2747.96 3124.42 26.12 o 3 3 1 7615.95 7026.45 81.65 o 5 3 1 2.07 3.84 1.94 o 7 3 1 8.49 9.53 3.80 o 9 3 1 90.51 67.28 9.18 o 11 3 1 219.20 221.58 17.09 o 13 3 1 54.56 32.56 12.02 o -12 4 1 8.12 16.90 9.98 o -10 4 1 312.67 296.85 15.22 o -8 4 1 79.45 79.05 10.65 o -6 4 1 586.98 494.43 10.13 o -4 4 1 1136.49 1232.12 16.65 o -2 4 1 49867.57 47924.84 175.19 o 0 4 1 669.40 473.21 9.73 o 2 4 1 281.42 293.43 6.25 o 4 4 1 400.46 552.07 8.30 o 6 4 1 157.05 133.38 10.91 o 8 4 1 102.45 120.85 8.63 o 10 4 1 97.92 84.47 12.74 o 12 4 1 43.67 39.42 12.61 o -13 5 1 64.62 61.04 18.17 o -11 5 1 120.19 85.41 13.98 o -9 5 1 112.41 151.43 13.06 o -7 5 1 629.67 662.72 14.95 o -5 5 1 619.72 751.20 16.44 o -3 5 1 1532.21 2121.10 25.21 o 3 5 1 2895.21 2443.45 31.05 o 5 5 1 955.59 1107.93 19.20 o 7 5 1 2.83 4.18 3.64 o 9 5 1 394.23 393.12 13.86 o 11 5 1 678.44 632.31 25.67 o -12 6 1 239.49 239.63 25.78 o -10 6 1 2.52 9.90 7.09 o -8 6 1 165.92 131.80 10.53 o -6 6 1 850.62 855.69 14.77 o -4 6 1 3005.46 3033.23 43.93 o -2 6 1 4476.01 4340.15 27.33 o 0 6 1 291.17 240.64 11.03 o 2 6 1 9.16 5.14 1.71 o 4 6 1 20.67 18.31 3.24 o 6 6 1 1490.59 1551.10 19.60 o 8 6 1 334.24 309.77 10.97 o 10 6 1 11.71 13.60 6.87 o 12 6 1 150.27 128.33 16.26 o -11 7 1 53.20 43.32 10.87 o -9 7 1 151.90 120.24 13.92 o -7 7 1 504.09 531.06 20.90 o -5 7 1 991.03 1034.29 13.96 o -3 7 1 259.77 215.09 7.03 o -1 7 1 4210.27 3911.50 33.41 o 1 7 1 8.29 4.23 1.99 o 3 7 1 1366.52 1528.65 26.20 o 5 7 1 277.19 263.98 8.43 o 7 7 1 98.10 95.27 7.90 o 9 7 1 0.42 5.78 4.23 o 11 7 1 178.42 224.69 18.47 o -12 8 1 295.71 272.10 24.26 o -10 8 1 150.27 191.43 16.25 o -8 8 1 730.34 788.95 17.39 o -6 8 1 1388.24 1469.72 21.94 o -4 8 1 2101.69 2466.41 37.36 o -2 8 1 851.25 842.61 23.59 o 0 8 1 134.91 122.21 10.90 o 2 8 1 0.98 4.32 2.04 o 4 8 1 158.07 166.42 6.80 o 6 8 1 1.13 6.41 3.96 o 8 8 1 181.73 225.35 10.43 o 10 8 1 18.34 39.85 10.53 o 12 8 1 25.89 33.38 16.08 o -11 9 1 37.19 39.14 10.64 o -9 9 1 200.49 146.87 11.73 o -7 9 1 817.91 727.93 17.12 o -5 9 1 508.61 394.12 11.13 o -3 9 1 843.44 849.02 26.18 o -1 9 1 23.24 14.10 4.67 o 1 9 1 4219.37 4557.13 24.72 o 3 9 1 1087.31 1020.26 21.38 o 5 9 1 801.31 779.19 18.22 o 7 9 1 24.71 18.61 5.21 o 9 9 1 28.61 29.41 7.89 o 11 9 1 39.69 37.52 10.88 o -10 10 1 12.34 12.33 8.13 o -8 10 1 66.66 49.26 8.85 o -6 10 1 16.91 8.03 5.34 o -4 10 1 660.51 697.33 13.62 o -2 10 1 1954.66 2137.86 30.73 o 0 10 1 3005.78 3472.82 25.34 o 2 10 1 5265.94 6026.89 105.47 o 4 10 1 535.47 627.31 12.83 o 6 10 1 155.08 154.19 8.95 o 8 10 1 19.15 14.97 6.89 o 10 10 1 86.67 71.71 15.94 o -11 11 1 6.39 10.82 10.09 o -9 11 1 6.86 9.58 5.91 o -7 11 1 5.66 10.62 6.30 o -5 11 1 1.68 5.19 4.72 o -3 11 1 1058.32 1124.83 18.78 o -1 11 1 1490.52 1551.06 24.26 o 1 11 1 1056.93 1140.28 22.15 o 3 11 1 779.41 812.81 14.94 o 5 11 1 504.21 509.26 13.73 o 7 11 1 38.47 36.23 7.53 o 9 11 1 32.32 22.61 7.19 o 11 11 1 0.99 10.19 9.64 o -10 12 1 5.27 10.90 8.57 o -8 12 1 5.10 16.22 7.22 o -6 12 1 214.46 210.56 14.75 o -4 12 1 175.35 165.58 11.85 o -2 12 1 932.27 1090.61 29.38 o 0 12 1 87.58 104.18 12.57 o 2 12 1 473.59 560.08 17.61 o 4 12 1 435.97 467.60 14.31 o 6 12 1 51.56 42.06 9.16 o 8 12 1 2.04 9.40 6.80 o 10 12 1 0.34 6.79 7.02 o -9 13 1 80.08 53.93 9.31 o -7 13 1 32.90 22.24 9.48 o -5 13 1 189.44 171.38 20.08 o -3 13 1 1.17 6.55 5.80 o -1 13 1 292.32 323.81 15.40 o 1 13 1 358.81 416.27 19.81 o 3 13 1 19.96 15.62 6.48 o 5 13 1 32.96 22.18 7.65 o 7 13 1 112.89 70.79 11.24 o 9 13 1 14.14 15.70 8.19 o -8 14 1 97.23 97.40 12.66 o -6 14 1 557.20 637.11 25.23 o -4 14 1 44.25 28.80 9.61 o -2 14 1 875.83 803.48 39.86 o 0 14 1 660.73 623.18 33.42 o 2 14 1 458.40 443.49 22.88 o 4 14 1 69.15 57.79 13.64 o 6 14 1 522.66 532.79 19.02 o 8 14 1 86.08 56.37 12.66 o -9 15 1 45.38 38.66 10.76 o -7 15 1 249.94 227.73 19.62 o -5 15 1 267.96 293.43 25.89 o -3 15 1 40.74 46.28 12.44 o -1 15 1 388.49 376.47 22.37 o 1 15 1 336.39 322.27 21.62 o 3 15 1 23.82 11.66 10.23 o 5 15 1 246.38 271.05 17.63 o 7 15 1 299.44 286.73 18.68 o -8 16 1 128.62 133.83 18.88 o -6 16 1 132.67 162.73 23.54 o -4 16 1 32.09 21.21 11.89 o -2 16 1 143.22 157.88 20.53 o 0 16 1 15.62 21.29 9.28 o 2 16 1 114.42 79.62 18.07 o 4 16 1 1.76 9.82 11.51 o 6 16 1 403.44 391.35 28.26 o -7 17 1 257.87 200.74 31.63 o -5 17 1 43.56 41.50 15.48 o -3 17 1 85.42 78.34 19.58 o -1 17 1 122.26 106.24 21.49 o 1 17 1 150.78 119.54 25.31 o 3 17 1 44.00 20.32 13.13 o 5 17 1 153.99 135.31 17.54 o -6 18 1 132.17 104.67 20.36 o -4 18 1 40.08 33.22 15.10 o -2 18 1 489.45 407.33 45.35 o 0 18 1 78.50 45.93 20.81 o 2 18 1 23.80 30.04 12.81 o 4 18 1 86.36 72.93 16.37 o -3 19 1 95.94 63.84 20.19 o -1 19 1 432.15 364.38 37.22 o 1 19 1 12.55 12.16 11.46 o 3 19 1 96.75 72.28 19.63 o 0 20 1 198.50 187.48 24.16 o -12 0 2 576.72 579.09 35.79 o -10 0 2 1836.63 1922.41 29.12 o -8 0 2 405.59 358.95 19.83 o -6 0 2 625.55 715.35 13.79 o -4 0 2 7982.15 8420.95 36.68 o -2 0 2 48822.36 46824.75 564.61 o 2 0 2 103952.52 88423.98 1624.99 o 4 0 2 25224.71 24014.05 487.18 o 6 0 2 9487.97 10137.73 191.86 o 8 0 2 477.03 422.35 36.78 o 10 0 2 18.23 7.51 9.95 o 12 0 2 387.77 388.27 46.83 o -13 1 2 495.56 509.97 30.73 o -11 1 2 802.09 847.60 23.26 o -9 1 2 913.07 1003.26 15.98 o -7 1 2 340.74 290.32 8.05 o -5 1 2 666.84 499.40 9.30 o 1 1 2 1863.92 1866.91 37.64 o 3 1 2 2122.84 1892.82 31.37 o 5 1 2 9414.99 9423.32 129.39 o 7 1 2 3761.13 3726.88 41.99 o 9 1 2 1719.10 1712.10 35.91 o 11 1 2 872.37 892.35 25.74 o -12 2 2 304.22 311.42 23.05 o -10 2 2 1311.12 1367.08 20.76 o -8 2 2 3261.69 3249.68 34.63 o -4 2 2 2104.83 1875.70 13.20 o -2 2 2 33838.36 32611.45 303.90 o 2 2 2 1518.43 1751.69 19.65 o 4 2 2 6756.52 7217.53 144.32 o 6 2 2 1873.23 1759.48 27.80 o 8 2 2 1086.94 1091.52 36.37 o 10 2 2 4.40 4.90 5.89 o 12 2 2 224.49 239.48 20.99 o -13 3 2 118.14 116.95 21.87 o -11 3 2 776.87 827.74 21.12 o -9 3 2 2116.57 2132.13 35.31 o -7 3 2 3978.45 3942.68 42.17 o -5 3 2 20.40 19.23 3.41 o -3 3 2 4284.77 5091.63 44.68 o -1 3 2 65343.70 61224.06 866.70 o 1 3 2 1194.15 1157.51 14.14 o 3 3 2 2746.61 3101.46 41.42 o 5 3 2 9539.55 9908.02 141.47 o 7 3 2 4725.01 4724.01 80.10 o 9 3 2 189.86 187.77 14.73 o 11 3 2 892.01 952.08 23.67 o -12 4 2 33.75 19.33 10.01 o -10 4 2 1110.86 1139.05 36.23 o -8 4 2 5827.82 6238.23 48.78 o -6 4 2 6438.56 6375.49 84.30 o -4 4 2 10290.37 10264.26 115.40 o -2 4 2 62521.75 59607.96 356.84 o 0 4 2 857.55 756.74 6.89 o 2 4 2 3946.87 4265.40 45.64 o 4 4 2 11020.32 11055.30 95.20 o 6 4 2 3600.04 3806.09 46.18 o 8 4 2 2225.75 2108.74 25.97 o 10 4 2 1100.47 1118.20 24.49 o 12 4 2 556.94 582.04 21.41 o -13 5 2 27.58 39.52 12.59 o -11 5 2 128.16 163.85 17.05 o -9 5 2 1958.93 1998.43 47.44 o -7 5 2 4152.50 4228.15 50.91 o -5 5 2 8150.69 8171.32 91.29 o -3 5 2 14589.70 15179.86 48.87 o -1 5 2 5674.57 5574.05 69.95 o 1 5 2 187.07 192.42 4.77 o 3 5 2 360.25 324.40 6.60 o 5 5 2 3571.80 3916.04 44.08 o 7 5 2 2489.07 2475.69 36.20 o 9 5 2 882.72 889.52 18.56 o 11 5 2 1937.49 2090.31 37.82 o -12 6 2 17.92 14.32 8.12 o -10 6 2 243.83 271.31 15.97 o -8 6 2 4048.93 4352.62 72.68 o -6 6 2 961.27 901.10 14.75 o -4 6 2 3358.81 3243.44 33.67 o -2 6 2 4660.23 4465.08 52.63 o 0 6 2 225.10 163.33 6.87 o 2 6 2 19.26 44.09 3.64 o 4 6 2 2668.50 2373.04 24.84 o 6 6 2 5321.36 5108.71 38.31 o 8 6 2 1910.28 1990.24 33.11 o 10 6 2 1812.69 1880.76 27.86 o 12 6 2 719.03 690.97 30.14 o -11 7 2 194.09 176.04 16.07 o -9 7 2 669.55 656.84 19.19 o -7 7 2 2767.80 2776.12 55.38 o -5 7 2 2778.41 2523.38 36.61 o -3 7 2 4312.76 3923.84 44.16 o -1 7 2 1451.51 1262.08 19.93 o 1 7 2 3896.33 3569.67 49.93 o 3 7 2 865.85 1052.61 26.82 o 5 7 2 4223.04 4280.79 56.84 o 7 7 2 1578.19 1543.20 18.69 o 9 7 2 1068.95 1055.40 18.14 o 11 7 2 452.98 404.18 26.60 o -12 8 2 36.64 44.22 11.50 o -10 8 2 205.65 267.59 17.01 o -8 8 2 1277.90 1359.26 31.19 o -6 8 2 2250.22 2413.79 34.60 o -4 8 2 265.27 229.94 7.32 o -2 8 2 12828.28 13022.20 73.14 o 0 8 2 11407.22 10741.30 118.52 o 2 8 2 298.99 210.82 6.94 o 4 8 2 927.15 858.53 12.63 o 6 8 2 1935.19 2136.08 21.00 o 8 8 2 793.56 789.13 22.11 o 10 8 2 321.93 328.92 16.92 o -11 9 2 463.20 515.09 23.62 o -9 9 2 467.20 468.07 15.34 o -7 9 2 1036.69 1090.94 19.00 o -5 9 2 2456.72 2523.70 24.05 o -3 9 2 1063.19 1012.92 12.58 o -1 9 2 8029.63 8103.77 85.15 o 1 9 2 11731.12 12120.30 106.23 o 3 9 2 3791.10 3516.02 43.47 o 5 9 2 4553.73 4537.92 39.56 o 7 9 2 1296.86 1326.17 18.77 o 9 9 2 496.34 560.80 17.24 o 11 9 2 41.24 37.49 12.97 o -10 10 2 125.81 113.21 13.83 o -8 10 2 780.75 698.14 19.34 o -6 10 2 666.32 618.94 14.72 o -4 10 2 653.27 636.21 13.44 o -2 10 2 832.35 898.06 25.99 o 0 10 2 3887.73 4528.11 74.53 o 2 10 2 710.25 827.20 21.85 o 4 10 2 1696.44 1808.24 31.35 o 6 10 2 460.28 382.74 11.68 o 8 10 2 13.20 9.97 6.02 o 10 10 2 65.36 58.56 11.55 o -11 11 2 152.18 117.26 17.17 o -9 11 2 506.56 542.24 18.49 o -7 11 2 230.10 203.39 13.84 o -5 11 2 224.24 208.75 11.70 o -3 11 2 1183.18 1280.81 24.63 o -1 11 2 1019.30 968.86 29.39 o 1 11 2 6856.65 7319.42 206.15 o 3 11 2 278.03 269.26 15.02 o 5 11 2 1521.56 1618.69 22.48 o 7 11 2 5.25 10.56 5.60 o 9 11 2 166.92 173.05 14.61 o -10 12 2 154.82 130.43 15.29 o -8 12 2 1202.90 1281.37 35.96 o -6 12 2 37.91 48.58 9.54 o -4 12 2 34.38 38.79 8.38 o -2 12 2 1033.84 941.75 24.25 o 0 12 2 1970.11 1863.65 43.19 o 2 12 2 1046.20 984.85 50.41 o 4 12 2 1727.28 1732.59 24.49 o 6 12 2 632.63 687.94 19.89 o 8 12 2 146.50 209.30 14.98 o 10 12 2 110.39 113.16 16.88 o -9 13 2 419.41 383.60 19.56 o -7 13 2 531.71 551.63 19.35 o -5 13 2 178.95 217.13 15.60 o -3 13 2 359.43 352.46 15.40 o -1 13 2 2524.70 2589.79 32.34 o 1 13 2 983.82 969.35 47.63 o 3 13 2 363.26 388.73 17.57 o 5 13 2 652.69 647.32 17.67 o 7 13 2 107.45 119.41 12.88 o 9 13 2 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