#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216432.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216432_Fobs loop_ _publ_author_name 'Grimminger, Philipp' 'Kl\"ufers, Peter' _publ_section_title ; Triethylammonium bis(oxalato)oxido(triphenylphosphane)rhenate(V) ; _journal_coeditor_code EZ2113 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3188 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.4146 _cell_length_b 15.3531 _cell_length_c 30.3448 _exptl_crystal_F_000 2944.00 _reflns_d_resolution_high 0.7657 _[local]_cod_data_source_file ez2113Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kn056 in P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 682.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 360872.56 365042.34 18792.43 o 4 0 0 279644.69 289210.44 10140.08 o 6 0 0 465271.59 532280.56 17428.80 o 8 0 0 192684.84 190033.06 7013.63 o 10 0 0 93783.23 91786.30 3764.32 o 12 0 0 42083.45 44308.14 2944.81 o 14 0 0 20735.21 21595.76 1522.58 o 16 0 0 12098.21 10667.31 1756.32 o 2 1 0 2345.93 1988.77 125.97 o 4 1 0 12069.96 12028.81 334.08 o 6 1 0 279.17 157.45 176.24 o 8 1 0 8190.03 8388.84 534.69 o 10 1 0 16554.39 15124.04 939.30 o 12 1 0 3.76 -220.93 313.89 o 14 1 0 34.14 -0.19 613.89 o 16 1 0 767.51 378.73 719.64 o 2 2 0 302218.06 314903.69 5901.70 o 4 2 0 319626.66 335532.84 8305.27 o 6 2 0 159483.69 165651.98 4120.17 o 8 2 0 62265.59 61240.02 1416.77 o 10 2 0 77908.68 78118.05 1925.78 o 12 2 0 25653.45 25797.18 1033.52 o 14 2 0 32033.78 32231.54 1599.71 o 16 2 0 13570.04 14080.03 2938.03 o 2 3 0 36371.32 37424.99 724.78 o 4 3 0 1677.47 1839.09 99.76 o 6 3 0 129.33 199.71 129.12 o 8 3 0 1475.65 1312.90 194.43 o 10 3 0 3349.56 3561.49 527.39 o 12 3 0 3531.63 3312.54 888.88 o 14 3 0 1691.28 1703.16 525.15 o 0 4 0 63951.46 66040.64 1641.32 o 2 4 0 70435.90 70884.59 1622.86 o 4 4 0 31657.25 29712.34 599.28 o 6 4 0 78419.04 81100.78 1567.43 o 8 4 0 21597.24 20878.75 567.94 o 10 4 0 22317.98 20805.47 885.50 o 12 4 0 26399.61 26725.47 912.82 o 14 4 0 13704.32 14495.90 1314.08 o 2 5 0 17897.36 18722.71 474.26 o 4 5 0 5080.77 5307.50 170.20 o 6 5 0 1295.66 1657.63 133.00 o 8 5 0 2748.84 2965.77 254.46 o 10 5 0 402.66 1214.42 215.88 o 12 5 0 87.57 189.57 350.93 o 14 5 0 38.26 554.53 560.90 o 0 6 0 27702.43 28260.92 978.80 o 2 6 0 7176.36 6595.50 225.02 o 4 6 0 51716.60 54114.32 1090.90 o 6 6 0 2817.80 7073.64 638.25 o 8 6 0 4880.15 4792.05 258.36 o 10 6 0 2608.16 2779.16 303.46 o 12 6 0 41.40 2421.98 933.18 o 14 6 0 11.84 831.17 613.38 o 2 7 0 6119.32 6496.05 194.20 o 4 7 0 598.54 457.89 82.96 o 6 7 0 3617.17 3446.45 185.42 o 8 7 0 4978.68 4965.05 332.72 o 10 7 0 2044.85 2267.32 290.30 o 12 7 0 3331.99 3091.26 470.22 o 14 7 0 5752.59 8248.44 1092.39 o 0 8 0 17616.93 17190.99 505.84 o 2 8 0 14694.19 13784.54 299.88 o 4 8 0 13275.20 13095.08 350.39 o 6 8 0 10274.06 9393.18 317.72 o 8 8 0 11360.42 10879.18 414.93 o 10 8 0 3584.17 3508.96 485.71 o 12 8 0 4066.45 4055.57 655.34 o 14 8 0 2663.23 2227.05 968.63 o 2 9 0 443.82 412.68 122.45 o 4 9 0 3451.38 3748.71 191.69 o 6 9 0 2454.91 2620.80 199.14 o 8 9 0 1381.68 1689.14 238.33 o 10 9 0 3828.65 3949.84 401.89 o 12 9 0 2144.50 2500.69 672.33 o 14 9 0 545.98 -503.74 630.41 o 0 10 0 127684.46 123400.66 3605.14 o 2 10 0 136361.30 133710.94 2923.63 o 4 10 0 98154.05 96693.20 2056.49 o 6 10 0 74161.96 72332.20 1525.21 o 8 10 0 37913.13 36184.34 963.21 o 10 10 0 21424.39 23434.55 1031.37 o 12 10 0 17364.21 17998.36 1323.20 o 2 11 0 2243.94 2427.44 194.82 o 4 11 0 4245.60 4411.24 223.21 o 6 11 0 14.11 -245.71 245.71 o 8 11 0 2061.37 2437.15 500.77 o 10 11 0 785.84 697.85 384.12 o 12 11 0 233.05 733.17 808.90 o 0 12 0 98683.76 98572.33 2948.57 o 2 12 0 105540.66 102293.31 2063.98 o 4 12 0 47170.73 47861.34 1105.35 o 6 12 0 55804.95 55957.62 1384.08 o 8 12 0 57654.75 58474.82 1643.37 o 10 12 0 21392.49 22099.72 1666.32 o 12 12 0 22856.30 22098.51 1714.46 o 2 13 0 111.24 82.17 173.78 o 4 13 0 10.57 71.61 177.61 o 6 13 0 39.71 -114.15 260.54 o 8 13 0 334.73 377.42 296.79 o 10 13 0 208.75 -519.08 519.08 o 12 13 0 152.85 587.76 720.53 o 0 14 0 57802.32 56827.32 2533.29 o 2 14 0 81922.23 83288.73 2066.18 o 4 14 0 61576.57 61214.33 1667.18 o 6 14 0 45815.59 48086.71 1659.23 o 8 14 0 38284.49 40271.72 1461.12 o 10 14 0 20445.53 21844.62 1148.16 o 2 15 0 548.17 629.84 236.37 o 4 15 0 100.41 306.46 292.09 o 6 15 0 17.14 294.28 266.38 o 8 15 0 35.89 -288.40 288.40 o 10 15 0 145.88 -240.05 906.66 o 0 16 0 29983.47 30207.13 1242.11 o 2 16 0 38123.46 40301.28 1270.02 o 4 16 0 26670.63 26792.33 928.51 o 6 16 0 28247.56 29626.35 1184.16 o 8 16 0 17025.99 18887.66 1274.09 o 2 17 0 683.36 336.74 311.52 o 4 17 0 160.94 -0.71 309.71 o 6 17 0 445.31 163.73 356.70 o 8 17 0 829.86 1101.21 722.43 o 0 18 0 7547.41 7164.08 727.95 o 2 18 0 1370.17 661.14 553.14 o 4 18 0 2437.92 1881.74 410.41 o 6 18 0 2281.41 1708.60 459.61 o 2 19 0 392.55 215.29 324.51 o 4 19 0 2.14 161.33 407.09 o 2 1 1 5532.13 6009.87 108.79 o 3 1 1 62901.49 67980.55 1325.03 o 4 1 1 266.26 259.23 60.36 o 5 1 1 115385.34 123008.04 2056.38 o 6 1 1 2927.65 3102.18 157.56 o 7 1 1 136038.25 142784.25 2246.64 o 8 1 1 3161.99 2973.95 177.05 o 9 1 1 32345.42 30575.18 860.82 o 10 1 1 4403.66 4312.62 387.24 o 11 1 1 26235.01 25457.89 597.22 o 12 1 1 3738.46 3766.08 375.91 o 13 1 1 19988.11 19169.71 677.68 o 14 1 1 2112.41 1228.04 356.49 o 15 1 1 8119.57 8768.02 833.33 o 16 1 1 493.36 835.04 641.58 o 1 2 1 19380.12 20972.33 303.96 o 2 2 1 157571.20 166908.28 2279.53 o 3 2 1 7044.83 6936.43 126.16 o 4 2 1 29457.48 31039.99 505.23 o 5 2 1 105.41 121.10 59.17 o 6 2 1 41611.45 41657.93 637.59 o 7 2 1 122.47 35.40 72.05 o 8 2 1 17131.39 17116.73 389.32 o 9 2 1 3678.33 3332.52 188.03 o 10 2 1 6543.55 5900.91 274.26 o 11 2 1 1822.46 1900.96 347.94 o 12 2 1 2492.82 2625.34 275.56 o 13 2 1 738.20 573.53 248.19 o 14 2 1 2141.69 2382.59 682.33 o 15 2 1 354.21 0.68 424.63 o 16 2 1 778.45 1219.21 682.69 o 1 3 1 107114.60 111047.82 1512.17 o 2 3 1 25996.93 28082.28 398.35 o 3 3 1 88423.48 94429.83 1328.31 o 4 3 1 3716.31 3973.38 109.48 o 5 3 1 26552.26 27234.39 420.52 o 6 3 1 1544.19 1560.53 128.82 o 7 3 1 41190.61 41677.63 647.36 o 8 3 1 1786.99 1624.43 133.79 o 9 3 1 31089.72 31656.05 578.89 o 10 3 1 1229.39 1160.28 286.54 o 11 3 1 18748.05 18348.39 487.31 o 12 3 1 690.35 873.21 284.41 o 13 3 1 9348.90 9804.80 429.27 o 14 3 1 9.90 420.76 354.85 o 15 3 1 4392.14 4802.10 525.94 o 0 4 1 177674.92 189078.11 3359.60 o 1 4 1 1218.06 1192.90 46.32 o 2 4 1 29350.94 29485.24 464.59 o 3 4 1 6.28 -36.53 39.40 o 4 4 1 43049.43 44503.49 648.53 o 5 4 1 336.84 352.20 72.28 o 6 4 1 37290.36 37594.06 569.16 o 7 4 1 1705.64 1891.43 140.41 o 8 4 1 15572.36 15122.08 332.32 o 9 4 1 1287.63 1272.57 154.99 o 10 4 1 20989.40 20552.43 486.04 o 11 4 1 972.41 705.34 243.86 o 12 4 1 12177.95 11533.46 446.65 o 13 4 1 5.77 -42.95 250.05 o 14 4 1 10296.66 9830.40 773.92 o 15 4 1 23.37 -533.92 533.92 o 1 5 1 19594.74 20448.63 285.48 o 2 5 1 416.40 378.95 44.87 o 3 5 1 9577.45 9356.66 169.60 o 4 5 1 1840.33 2017.79 77.53 o 5 5 1 22115.16 21479.83 323.61 o 6 5 1 1669.01 1610.09 100.14 o 7 5 1 9030.31 8748.09 221.99 o 8 5 1 565.70 420.01 109.02 o 9 5 1 2004.38 1679.34 158.60 o 10 5 1 19.43 143.27 227.44 o 11 5 1 8934.36 9354.72 378.74 o 12 5 1 10.47 197.33 284.37 o 13 5 1 2980.60 3115.87 338.85 o 14 5 1 676.22 1187.02 430.40 o 15 5 1 777.17 292.99 641.70 o 0 6 1 151740.25 154046.98 2933.20 o 1 6 1 2547.49 2676.33 105.26 o 2 6 1 40325.02 38783.86 625.70 o 3 6 1 252.19 232.82 63.72 o 4 6 1 80265.05 79632.46 1199.82 o 5 6 1 210.30 306.00 68.43 o 6 6 1 74804.98 73747.98 1050.02 o 7 6 1 14.58 -90.69 90.69 o 8 6 1 27527.07 27313.60 551.70 o 9 6 1 40.91 -8.70 115.41 o 10 6 1 18166.57 18075.87 448.33 o 11 6 1 241.44 -46.34 211.94 o 12 6 1 28017.76 28229.46 739.73 o 13 6 1 260.80 -44.58 367.99 o 14 6 1 15866.60 16709.54 923.18 o 15 6 1 50.24 -24.10 740.48 o 1 7 1 103.66 92.17 59.67 o 2 7 1 7019.62 7669.48 149.10 o 3 7 1 811.54 874.21 71.01 o 4 7 1 578.39 626.53 73.66 o 5 7 1 252.57 206.77 77.98 o 6 7 1 1272.46 1303.99 137.66 o 7 7 1 438.10 147.69 103.97 o 8 7 1 3777.73 3844.09 174.26 o 9 7 1 9.85 150.26 156.20 o 10 7 1 756.79 837.78 207.22 o 11 7 1 62.70 -192.25 206.30 o 12 7 1 1092.64 1531.67 310.69 o 13 7 1 1687.41 1821.44 403.80 o 14 7 1 166.60 316.14 561.45 o 15 7 1 14.53 -660.73 660.73 o 0 8 1 90935.83 86401.37 1770.54 o 1 8 1 3614.06 3578.92 109.26 o 2 8 1 129499.03 127388.65 1630.23 o 3 8 1 2592.44 2366.65 106.36 o 4 8 1 74194.75 72055.18 1090.44 o 5 8 1 1264.85 1070.13 96.01 o 6 8 1 60440.61 59771.91 842.24 o 7 8 1 578.98 540.39 119.53 o 8 8 1 38559.96 37916.80 592.17 o 9 8 1 3033.79 3245.66 198.07 o 10 8 1 20878.72 21968.17 542.93 o 11 8 1 300.68 312.20 267.11 o 12 8 1 14461.32 16402.61 743.21 o 13 8 1 1971.32 2023.80 504.29 o 14 8 1 7425.00 7204.09 924.57 o 1 9 1 38161.44 36951.66 514.70 o 2 9 1 775.77 669.74 105.25 o 3 9 1 24113.17 22517.47 357.81 o 4 9 1 178.25 -17.89 94.45 o 5 9 1 17247.29 16183.61 304.10 o 6 9 1 2003.87 2233.84 133.33 o 7 9 1 16511.15 15991.61 413.08 o 8 9 1 674.17 535.82 167.43 o 9 9 1 16202.23 16608.07 447.91 o 10 9 1 79.30 152.98 232.26 o 11 9 1 7910.93 8259.91 411.55 o 12 9 1 1434.55 1523.32 442.66 o 13 9 1 3178.69 2256.53 532.47 o 14 9 1 529.22 592.20 544.45 o 0 10 1 31681.72 29553.57 589.16 o 1 10 1 9.56 -76.68 81.48 o 2 10 1 19953.65 18841.85 322.16 o 3 10 1 4087.21 4197.12 166.26 o 4 10 1 9331.48 9033.24 197.69 o 5 10 1 72.59 166.27 145.66 o 6 10 1 17800.44 16827.88 348.74 o 7 10 1 520.58 316.77 152.81 o 8 10 1 10227.22 9918.73 316.21 o 9 10 1 2554.50 2488.92 237.75 o 10 10 1 7208.52 6252.65 336.57 o 11 10 1 9.95 -257.94 257.94 o 12 10 1 4798.38 5030.91 590.43 o 13 10 1 735.36 440.29 537.17 o 1 11 1 54515.99 52211.21 884.57 o 2 11 1 249.90 222.22 122.22 o 3 11 1 29355.35 28142.43 509.21 o 4 11 1 321.22 187.69 93.64 o 5 11 1 26107.72 25666.75 600.99 o 6 11 1 101.18 97.33 150.68 o 7 11 1 25797.33 26415.18 558.41 o 8 11 1 1192.05 1117.72 198.70 o 9 11 1 15834.60 15952.78 508.63 o 10 11 1 487.88 633.71 235.13 o 11 11 1 8739.72 9539.85 563.50 o 12 11 1 233.59 27.16 381.26 o 13 11 1 5673.55 5121.98 842.74 o 0 12 1 62.68 84.87 276.22 o 1 12 1 166.54 462.93 125.00 o 2 12 1 77.25 92.76 123.74 o 3 12 1 41.51 34.94 108.34 o 4 12 1 3890.09 3760.83 167.75 o 5 12 1 125.77 -17.09 139.42 o 6 12 1 402.00 293.23 200.79 o 7 12 1 1.93 155.97 164.00 o 8 12 1 475.18 416.35 186.63 o 9 12 1 5.96 -200.36 216.67 o 10 12 1 901.15 1031.38 390.45 o 11 12 1 689.89 531.89 372.02 o 12 12 1 708.45 1792.82 445.28 o 1 13 1 27147.90 25119.55 472.98 o 2 13 1 70.95 263.96 143.13 o 3 13 1 28089.87 26819.32 787.72 o 4 13 1 131.15 253.20 161.30 o 5 13 1 33546.42 33102.21 917.19 o 6 13 1 699.47 671.07 178.49 o 7 13 1 19770.36 20373.94 790.46 o 8 13 1 14.15 -206.07 206.07 o 9 13 1 11641.77 12765.57 466.96 o 10 13 1 198.50 138.87 309.90 o 11 13 1 11038.58 11057.09 1005.46 o 12 13 1 10.30 876.15 559.92 o 0 14 1 242.91 120.01 194.84 o 1 14 1 127.28 62.28 123.05 o 2 14 1 553.48 419.28 169.61 o 3 14 1 41.17 -34.89 152.55 o 4 14 1 1286.04 1093.13 202.68 o 5 14 1 55.75 41.85 174.92 o 6 14 1 330.55 49.80 176.66 o 7 14 1 686.55 244.10 325.91 o 8 14 1 281.76 179.63 248.07 o 9 14 1 338.15 770.62 263.72 o 10 14 1 114.73 67.64 339.76 o 11 14 1 3.36 -188.20 468.45 o 1 15 1 22148.27 22341.84 509.13 o 2 15 1 135.26 191.09 155.50 o 3 15 1 17276.52 17412.61 458.29 o 4 15 1 70.69 153.03 155.21 o 5 15 1 13147.19 13515.93 449.05 o 6 15 1 353.59 433.16 229.72 o 7 15 1 13109.61 14160.46 486.74 o 8 15 1 1527.17 2156.48 331.50 o 9 15 1 11582.35 11762.61 617.97 o 10 15 1 926.00 1220.66 390.50 o 0 16 1 13962.17 14350.68 661.61 o 1 16 1 39.07 252.91 171.52 o 2 16 1 12918.97 12850.01 387.43 o 3 16 1 24.51 319.26 166.26 o 4 16 1 9398.31 9326.93 394.54 o 5 16 1 11.84 14.61 237.44 o 6 16 1 8148.20 7707.94 368.90 o 7 16 1 0.22 -265.12 265.12 o 8 16 1 6848.64 6400.64 412.45 o 9 16 1 13.72 112.94 450.72 o 1 17 1 8391.36 8668.18 365.69 o 2 17 1 731.95 1201.31 249.57 o 3 17 1 5924.84 5462.63 317.45 o 4 17 1 22.45 -106.22 196.19 o 5 17 1 6722.34 6817.30 374.42 o 6 17 1 19.73 -200.62 241.03 o 7 17 1 4663.33 4392.10 350.55 o 8 17 1 237.07 422.51 377.09 o 0 18 1 10574.15 10535.08 643.33 o 1 18 1 82.46 15.11 196.34 o 2 18 1 15155.24 14435.16 513.43 o 3 18 1 283.53 827.19 233.06 o 4 18 1 12501.68 12491.25 507.75 o 5 18 1 91.55 -80.78 231.89 o 6 18 1 11620.43 11534.25 550.17 o 1 19 1 38.54 -155.01 240.94 o 2 19 1 2.89 163.98 239.24 o 3 19 1 93.13 110.46 277.75 o 4 19 1 336.87 269.31 288.93 o 2 0 2 29327.92 30655.03 820.26 o 3 0 2 99.95 -99.65 99.65 o 4 0 2 22888.96 23787.58 577.13 o 5 0 2 283.03 334.37 131.72 o 6 0 2 393.88 549.46 135.25 o 7 0 2 14268.27 15086.80 508.82 o 8 0 2 4355.32 4577.04 354.64 o 9 0 2 3612.49 3523.81 415.36 o 10 0 2 103.79 431.16 226.76 o 11 0 2 3115.67 2294.77 315.02 o 12 0 2 2369.59 2384.69 327.19 o 13 0 2 1648.38 1778.82 392.83 o 14 0 2 32.51 67.87 498.76 o 15 0 2 899.66 71.48 788.03 o 16 0 2 385.66 -78.96 726.04 o 2 1 2 494.31 196.00 40.89 o 3 1 2 5328.43 5388.07 139.75 o 4 1 2 66.33 7.90 88.85 o 5 1 2 14804.38 14750.10 265.69 o 6 1 2 187.34 41.05 69.16 o 7 1 2 18074.48 18038.66 366.75 o 8 1 2 26.56 140.86 129.22 o 9 1 2 8235.67 7879.75 322.92 o 10 1 2 4032.23 3947.88 278.21 o 11 1 2 993.10 1400.39 282.73 o 12 1 2 1528.86 1722.09 283.16 o 13 1 2 4806.06 4821.97 361.76 o 14 1 2 100.41 -94.30 319.57 o 15 1 2 663.46 599.08 386.35 o 16 1 2 135.13 -478.38 529.17 o 1 2 2 16815.05 17553.57 255.40 o 2 2 2 45566.66 48942.03 660.51 o 3 2 2 99.24 -8.92 33.09 o 4 2 2 6235.89 6451.66 133.78 o 5 2 2 3239.31 3379.83 113.66 o 6 2 2 8043.32 8229.47 181.12 o 7 2 2 12.39 -22.10 101.08 o 8 2 2 1090.94 1151.12 117.65 o 9 2 2 341.09 478.97 215.66 o 10 2 2 27.96 62.42 193.78 o 11 2 2 169.69 394.25 219.88 o 12 2 2 574.23 607.71 339.44 o 13 2 2 751.30 725.34 368.48 o 14 2 2 202.50 242.31 390.79 o 15 2 2 231.47 488.45 616.42 o 16 2 2 432.48 651.71 727.54 o 1 3 2 70581.23 72523.30 1013.97 o 2 3 2 227.33 212.69 28.93 o 3 3 2 117633.80 123620.05 1780.20 o 4 3 2 112.64 152.95 57.43 o 5 3 2 118970.59 124479.80 2003.26 o 6 3 2 255.26 335.13 87.67 o 7 3 2 56900.68 55466.46 931.83 o 8 3 2 1154.96 1166.18 176.86 o 9 3 2 26694.92 26031.34 491.99 o 10 3 2 357.48 243.84 201.19 o 11 3 2 27305.16 27702.55 635.62 o 12 3 2 992.33 857.53 205.45 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