#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216435.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216435_Fobs loop_ _publ_author_name 'Fischer, Conrad' 'Gruber, Tobias' 'Seichter, Wilhelm' 'Weber, Edwin' _publ_section_title ; 5,11,17,23-Tetra-tert-butyl-25,26,27,28-tetramethoxycalix[4]arene tetrahydrofuran solvate ; _journal_coeditor_code FJ2051 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4572 _journal_page_last o4573 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.824 _cell_angle_gamma 90.000 _cell_length_a 16.9911 _cell_length_b 19.7724 _cell_length_c 28.5530 _exptl_crystal_F_000 3392.00 _reflns_d_resolution_high 0.7991 _[local]_cod_data_source_file fj2051Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Cofi_2_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 502.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 5744.17 4411.26 159.01 o 4 0 0 166109.34 165190.08 4225.25 o 5 0 0 7910.16 7618.20 267.52 o 6 0 0 5974.88 5968.11 245.76 o 7 0 0 5033.37 5215.81 230.76 o 8 0 0 408.85 336.52 104.01 o 9 0 0 421.33 510.28 128.76 o 10 0 0 235.79 133.76 109.01 o 11 0 0 267.61 427.53 143.01 o 12 0 0 483.62 341.12 42.92 o 13 0 0 574.27 595.74 49.84 o 14 0 0 7.61 -78.00 145.76 o 15 0 0 100.04 337.52 180.51 o 16 0 0 0.01 -116.26 148.26 o 17 0 0 18.83 -174.51 174.51 o 18 0 0 0.68 318.77 203.76 o 19 0 0 6.56 181.01 202.51 o 20 0 0 180.83 293.27 226.76 o 21 0 0 20.10 -0.50 200.76 o 2 1 0 3042.22 2599.52 51.71 o 3 1 0 29113.21 26150.44 317.40 o 4 1 0 12748.71 11509.49 191.70 o 5 1 0 1350.27 1427.34 51.20 o 6 1 0 899.05 742.08 43.93 o 7 1 0 6366.58 6523.31 112.32 o 8 1 0 3259.95 3412.78 77.01 o 9 1 0 8001.38 7866.76 135.80 o 10 1 0 1316.64 1260.18 56.31 o 11 1 0 561.40 584.76 60.47 o 12 1 0 2051.90 1870.77 82.02 o 13 1 0 728.26 714.49 66.34 o 14 1 0 2.67 9.94 74.74 o 15 1 0 251.96 162.96 56.48 o 16 1 0 2.61 17.61 65.50 o 17 1 0 988.70 927.78 82.28 o 18 1 0 2.77 63.20 65.69 o 19 1 0 46.99 -98.28 140.82 o 20 1 0 1.02 -144.03 144.03 o 21 1 0 4.20 44.57 152.55 o 1 2 0 37160.16 33432.87 1028.80 o 2 2 0 1504.60 1329.77 19.91 o 3 2 0 37562.70 39957.51 378.44 o 4 2 0 446.35 566.16 22.83 o 5 2 0 13714.42 12773.65 163.94 o 6 2 0 6099.29 5475.60 114.89 o 7 2 0 764.33 1040.95 52.91 o 8 2 0 2849.06 2532.99 72.48 o 9 2 0 1442.78 1393.38 59.44 o 10 2 0 1863.53 1783.39 68.20 o 11 2 0 23.72 -30.69 45.62 o 12 2 0 16.45 -52.98 71.38 o 13 2 0 17.41 -48.56 50.17 o 14 2 0 419.91 404.15 61.35 o 15 2 0 6.21 -24.70 59.05 o 16 2 0 334.88 236.70 60.89 o 17 2 0 140.08 26.60 73.69 o 18 2 0 47.20 -55.41 72.40 o 19 2 0 30.25 37.93 72.77 o 20 2 0 0.74 1.51 73.35 o 21 2 0 163.71 -2.54 162.73 o 1 3 0 30705.06 30985.05 228.71 o 2 3 0 15748.59 14472.99 112.08 o 3 3 0 18283.36 15482.90 133.36 o 4 3 0 5302.59 5445.47 56.09 o 5 3 0 1536.26 1946.82 45.46 o 6 3 0 14792.86 14779.05 172.85 o 7 3 0 0.71 42.43 23.69 o 8 3 0 1109.66 1041.40 39.30 o 9 3 0 4873.84 5523.81 102.73 o 10 3 0 2641.86 2440.54 82.84 o 11 3 0 9383.61 9911.56 179.37 o 12 3 0 510.80 656.58 60.98 o 13 3 0 818.81 944.88 70.38 o 14 3 0 1205.07 1456.65 81.36 o 15 3 0 3490.42 3503.44 141.03 o 16 3 0 397.79 384.66 81.93 o 17 3 0 2.17 -10.83 60.90 o 18 3 0 64.13 -77.18 77.18 o 19 3 0 74.37 -78.24 78.24 o 20 3 0 7.67 -68.85 79.06 o 21 3 0 204.69 64.47 163.61 o 0 4 0 10380.72 7837.08 97.51 o 1 4 0 13627.59 12288.87 99.34 o 2 4 0 37884.14 36664.61 271.74 o 3 4 0 0.09 -13.30 13.30 o 4 4 0 19040.18 18025.48 155.87 o 5 4 0 4948.34 4906.22 66.22 o 6 4 0 33515.63 31335.91 316.75 o 7 4 0 3988.88 4176.93 69.80 o 8 4 0 308.84 397.26 31.14 o 9 4 0 287.75 273.01 29.52 o 10 4 0 8.82 5.02 46.20 o 11 4 0 4922.61 4821.17 84.87 o 12 4 0 1532.12 1629.14 54.64 o 13 4 0 4160.69 4203.90 81.79 o 14 4 0 2190.27 2329.58 100.93 o 15 4 0 0.18 -1.38 128.67 o 16 4 0 65.84 -52.45 79.20 o 17 4 0 17.80 9.24 112.26 o 18 4 0 1.13 -67.42 67.42 o 19 4 0 14.97 -67.87 141.58 o 20 4 0 355.00 205.31 93.72 o 1 5 0 713.77 537.21 22.78 o 2 5 0 7181.90 6335.50 62.08 o 3 5 0 149.95 47.51 19.30 o 4 5 0 2727.45 2723.98 44.89 o 5 5 0 9491.95 9199.56 109.96 o 6 5 0 6721.27 7282.19 91.80 o 7 5 0 1966.65 2012.86 49.56 o 8 5 0 0.61 -23.64 23.64 o 9 5 0 5672.00 5180.47 85.77 o 10 5 0 709.09 840.77 40.22 o 11 5 0 10378.93 9619.47 148.99 o 12 5 0 8917.93 8630.17 131.51 o 13 5 0 3369.45 3179.68 78.05 o 14 5 0 48.02 -19.33 44.29 o 15 5 0 643.24 582.23 56.06 o 16 5 0 8.81 -83.96 83.96 o 17 5 0 51.11 13.96 86.97 o 18 5 0 643.94 742.11 105.56 o 19 5 0 85.97 98.35 73.42 o 20 5 0 89.61 -24.13 94.52 o 0 6 0 6641.33 5940.11 95.18 o 1 6 0 8092.85 7588.10 84.16 o 2 6 0 265.88 373.57 23.82 o 3 6 0 14321.67 15134.89 134.92 o 4 6 0 733.71 867.65 24.48 o 5 6 0 669.08 893.37 40.85 o 6 6 0 1448.84 1321.22 43.06 o 7 6 0 1377.42 1714.10 43.10 o 8 6 0 2756.82 2782.38 63.54 o 9 6 0 487.88 537.03 34.04 o 10 6 0 3055.46 3255.89 61.76 o 11 6 0 8.49 -17.86 41.14 o 12 6 0 1225.38 1295.32 49.66 o 13 6 0 181.83 242.94 67.95 o 14 6 0 14.20 -9.33 47.97 o 15 6 0 205.22 229.93 40.28 o 16 6 0 1.58 17.38 61.96 o 17 6 0 185.56 80.92 93.61 o 18 6 0 179.95 222.76 53.49 o 19 6 0 11.80 -49.15 49.15 o 20 6 0 219.84 223.55 60.70 o 1 7 0 764.98 715.75 32.30 o 2 7 0 549.24 451.81 26.98 o 3 7 0 2431.96 2620.30 46.82 o 4 7 0 5797.40 5569.63 64.66 o 5 7 0 872.92 765.44 34.26 o 6 7 0 3125.99 3385.90 65.95 o 7 7 0 4109.93 4163.07 67.15 o 8 7 0 7239.87 6740.02 114.62 o 9 7 0 3523.32 3581.74 78.01 o 10 7 0 223.97 278.54 36.73 o 11 7 0 1337.13 1273.93 64.01 o 12 7 0 358.11 508.96 45.32 o 13 7 0 71.79 99.15 63.86 o 14 7 0 784.12 899.45 58.47 o 15 7 0 299.23 369.61 59.49 o 16 7 0 63.35 60.30 47.65 o 17 7 0 511.69 530.96 56.54 o 18 7 0 1212.85 1150.14 62.73 o 19 7 0 4.43 -32.96 82.10 o 20 7 0 33.53 68.20 58.18 o 0 8 0 15314.55 14348.91 210.28 o 1 8 0 423.48 524.14 37.04 o 2 8 0 8937.67 8948.67 97.54 o 3 8 0 509.70 404.98 23.30 o 4 8 0 8075.37 8826.26 96.12 o 5 8 0 10846.85 13044.17 158.39 o 6 8 0 171.80 265.11 46.57 o 7 8 0 105.44 70.32 34.47 o 8 8 0 184.40 151.11 33.58 o 9 8 0 8.00 14.21 36.84 o 10 8 0 33.00 2.95 36.26 o 11 8 0 1453.56 1720.76 60.52 o 12 8 0 25.37 27.96 49.51 o 13 8 0 340.32 363.50 57.81 o 14 8 0 1207.92 1211.90 66.94 o 15 8 0 0.07 -49.56 49.56 o 16 8 0 7.14 -48.03 79.98 o 17 8 0 74.34 65.08 53.29 o 18 8 0 196.87 200.86 59.02 o 19 8 0 23.11 -54.38 54.38 o 20 8 0 67.04 92.25 72.89 o 1 9 0 15.57 -30.03 30.03 o 2 9 0 12052.37 12019.04 130.30 o 3 9 0 437.13 633.51 30.03 o 4 9 0 19.98 -9.43 25.60 o 5 9 0 93.92 84.32 27.20 o 6 9 0 6.02 -44.99 44.99 o 7 9 0 590.93 866.62 53.98 o 8 9 0 462.89 579.15 40.26 o 9 9 0 808.80 1053.73 46.25 o 10 9 0 4108.83 3644.15 95.28 o 11 9 0 1295.74 1478.65 68.01 o 12 9 0 209.52 181.73 78.25 o 13 9 0 287.98 337.46 68.79 o 14 9 0 1357.06 1165.04 118.51 o 15 9 0 82.54 28.92 59.81 o 16 9 0 172.07 -3.43 63.87 o 17 9 0 0.01 42.00 61.56 o 18 9 0 0.09 13.72 61.99 o 19 9 0 130.00 78.80 62.60 o 0 10 0 8452.07 8868.08 153.70 o 1 10 0 5392.09 5437.11 83.39 o 2 10 0 628.68 800.79 36.48 o 3 10 0 3793.21 4092.42 61.81 o 4 10 0 8.04 -11.62 27.74 o 5 10 0 93.48 118.36 27.92 o 6 10 0 840.44 1014.68 45.75 o 7 10 0 2523.85 2496.96 95.91 o 8 10 0 577.41 563.52 47.68 o 9 10 0 0.93 -40.46 46.45 o 10 10 0 2756.56 2461.43 82.47 o 11 10 0 1048.87 1138.68 84.17 o 12 10 0 807.14 740.57 78.70 o 13 10 0 331.47 372.50 79.97 o 14 10 0 31.08 29.96 69.34 o 15 10 0 6.15 -60.45 61.97 o 16 10 0 17.00 17.83 64.73 o 17 10 0 109.01 25.47 80.97 o 18 10 0 2.10 -62.67 62.67 o 19 10 0 102.64 64.51 69.50 o 1 11 0 2181.03 2327.22 55.37 o 2 11 0 3642.33 3816.55 86.14 o 3 11 0 587.94 644.27 33.34 o 4 11 0 634.62 694.74 38.48 o 5 11 0 2166.75 2208.20 54.73 o 6 11 0 1715.16 1964.18 63.29 o 7 11 0 1086.29 1565.17 73.84 o 8 11 0 1274.81 1261.29 57.95 o 9 11 0 1021.28 1010.15 94.64 o 10 11 0 708.31 511.54 82.69 o 11 11 0 16.25 -97.48 97.48 o 12 11 0 23.19 102.23 66.84 o 13 11 0 462.14 663.32 91.80 o 14 11 0 750.27 557.14 156.25 o 15 11 0 192.32 102.24 68.50 o 16 11 0 756.88 778.25 84.01 o 17 11 0 175.05 191.53 72.54 o 18 11 0 232.65 256.59 95.66 o 19 11 0 45.52 89.58 112.52 o 0 12 0 18.32 -58.94 58.97 o 1 12 0 6745.38 6774.90 95.98 o 2 12 0 693.23 690.68 44.04 o 3 12 0 136.88 166.42 30.50 o 4 12 0 2.30 -12.83 31.84 o 5 12 0 18.94 23.17 32.73 o 6 12 0 186.67 81.80 48.03 o 7 12 0 409.35 509.17 70.39 o 8 12 0 0.17 16.63 39.51 o 9 12 0 1175.68 1148.21 99.28 o 10 12 0 276.77 182.11 82.29 o 11 12 0 944.67 1200.92 133.36 o 12 12 0 7.00 24.82 103.48 o 13 12 0 42.44 56.49 129.01 o 14 12 0 1.47 -103.65 108.09 o 15 12 0 228.55 103.24 96.15 o 16 12 0 310.95 256.44 110.95 o 17 12 0 0.71 -92.10 92.10 o 18 12 0 0.91 1.57 103.20 o 1 13 0 58.57 27.18 35.04 o 2 13 0 56.81 77.89 35.22 o 3 13 0 1098.12 1242.60 44.24 o 4 13 0 687.17 582.57 42.75 o 5 13 0 157.44 138.19 35.94 o 6 13 0 1828.11 2056.56 69.18 o 7 13 0 101.55 76.57 42.79 o 8 13 0 240.71 304.85 70.39 o 9 13 0 806.52 778.54 96.60 o 10 13 0 492.58 554.49 135.76 o 11 13 0 80.06 47.81 108.52 o 12 13 0 51.13 -157.93 199.39 o 13 13 0 744.91 656.38 131.34 o 14 13 0 0.21 -83.13 111.19 o 15 13 0 2.38 -92.46 113.09 o 16 13 0 173.37 238.79 102.63 o 17 13 0 365.42 194.33 105.65 o 18 13 0 53.19 163.47 103.40 o 0 14 0 174.19 220.51 64.67 o 1 14 0 317.62 275.19 41.12 o 2 14 0 347.11 298.32 40.82 o 3 14 0 275.70 224.30 32.76 o 4 14 0 2705.42 2812.77 70.45 o 5 14 0 239.95 265.60 45.45 o 6 14 0 143.55 15.13 51.89 o 7 14 0 80.70 126.12 49.61 o 8 14 0 56.81 26.72 84.51 o 9 14 0 0.99 67.61 85.65 o 10 14 0 392.71 446.70 125.42 o 11 14 0 23.81 31.96 115.90 o 12 14 0 952.64 779.54 138.70 o 13 14 0 102.59 50.58 160.51 o 14 14 0 828.81 1041.36 159.88 o 15 14 0 8.11 -29.39 193.64 o 16 14 0 70.96 -51.69 102.57 o 17 14 0 0.51 -58.60 105.56 o 1 15 0 54.78 -39.12 39.12 o 2 15 0 200.79 155.83 37.38 o 3 15 0 2.33 7.09 31.27 o 4 15 0 315.65 409.95 44.96 o 5 15 0 1063.91 1322.06 92.43 o 6 15 0 103.59 -8.11 57.07 o 7 15 0 334.84 395.10 92.54 o 8 15 0 12.05 -25.40 87.18 o 9 15 0 28.95 -19.32 85.32 o 10 15 0 576.34 554.91 135.70 o 11 15 0 1249.60 1473.97 214.26 o 12 15 0 36.81 -72.49 119.07 o 13 15 0 6.60 -142.45 171.76 o 14 15 0 85.74 54.90 130.74 o 15 15 0 26.61 224.95 144.76 o 16 15 0 5.80 -137.94 137.94 o 0 16 0 8.87 -59.42 59.42 o 1 16 0 259.07 237.12 45.90 o 2 16 0 0.63 -16.63 51.28 o 3 16 0 230.85 147.73 44.56 o 4 16 0 10.39 -59.16 59.16 o 5 16 0 1129.18 1281.23 80.53 o 6 16 0 436.59 526.15 65.56 o 7 16 0 130.93 62.43 56.68 o 8 16 0 477.19 237.63 97.64 o 9 16 0 1227.05 1167.28 187.89 o 10 16 0 159.90 157.08 126.26 o 11 16 0 195.13 44.59 127.91 o 12 16 0 244.17 178.69 132.28 o 13 16 0 115.54 167.13 130.35 o 14 16 0 79.34 266.24 137.86 o 15 16 0 94.74 77.86 131.37 o 16 16 0 29.24 159.10 114.46 o 1 17 0 263.65 159.96 45.91 o 2 17 0 783.96 893.82 67.92 o 3 17 0 173.91 69.46 50.06 o 4 17 0 123.78 125.58 66.97 o 5 17 0 50.03 -21.55 79.53 o 6 17 0 40.40 -68.69 82.71 o 7 17 0 222.91 252.55 64.85 o 8 17 0 30.48 -174.29 199.89 o 9 17 0 216.04 48.24 131.71 o 10 17 0 69.53 -50.14 242.64 o 11 17 0 76.66 -134.95 134.95 o 12 17 0 130.80 -60.11 137.76 o 13 17 0 170.68 39.28 143.26 o 14 17 0 43.27 -91.72 140.31 o 15 17 0 0.85 -106.67 136.35 o 0 18 0 135.46 151.73 65.72 o 1 18 0 97.53 36.08 55.46 o 2 18 0 121.03 -5.10 52.04 o 3 18 0 157.97 118.11 51.06 o 4 18 0 35.15 -63.92 65.21 o 5 18 0 0.46 -70.64 70.64 o 6 18 0 772.85 961.68 152.00 o 7 18 0 40.45 54.80 66.44 o 8 18 0 234.49 136.10 71.15 o 9 18 0 111.67 -40.73 138.72 o 10 18 0 555.86 612.22 152.96 o 11 18 0 546.57 510.04 160.93 o 12 18 0 123.18 111.54 148.30 o 13 18 0 152.99 407.27 150.27 o 14 18 0 10.44 146.42 140.97 o 1 19 0 255.97 105.55 57.17 o 2 19 0 223.83 166.81 55.29 o 3 19 0 213.30 122.02 68.97 o 4 19 0 6.44 -44.54 68.90 o 5 19 0 30.64 -9.07 74.84 o 6 19 0 326.53 488.84 114.45 o 7 19 0 76.18 -41.86 70.59 o 8 19 0 85.51 94.90 60.36 o 9 19 0 9.17 -4.97 143.20 o 10 19 0 74.44 -72.88 137.01 o 11 19 0 48.81 20.37 145.57 o 12 19 0 20.46 -52.78 140.74 o 13 19 0 40.37 247.50 156.01 o 0 20 0 56.09 55.31 130.49 o 1 20 0 202.84 320.08 76.38 o 2 20 0 13.08 80.97 57.08 o 3 20 0 13.26 -5.15 52.66 o 4 20 0 192.89 245.30 111.00 o 5 20 0 2.72 -56.83 74.68 o 6 20 0 808.28 799.03 90.43 o 7 20 0 154.48 61.14 71.35 o 8 20 0 141.82 -31.84 60.76 o 9 20 0 71.03 -48.11 215.64 o 10 20 0 7.53 -44.35 150.01 o 11 20 0 16.23 -80.58 288.64 o 12 20 0 42.99 -108.60 145.37 o 1 21 0 5.13 -69.50 69.50 o 2 21 0 38.13 -48.61 57.88 o 3 21 0 49.83 80.52 59.73 o 4 21 0 96.86 -13.38 80.03 o 5 21 0 68.68 -53.23 142.07 o 6 21 0 364.53 536.66 121.50 o 7 21 0 28.00 48.28 121.22 o 8 21 0 0.07 -28.47 62.49 o 9 21 0 1.75 -148.15 148.15 o 10 21 0 9.11 81.05 149.33 o 11 21 0 7.83 234.87 158.54 o 0 22 0 147.60 250.67 158.76 o 1 22 0 256.53 243.64 79.10 o 2 22 0 1.44 -9.48 63.79 o 3 22 0 4.94 -54.80 54.80 o 4 22 0 296.66 364.39 149.25 o 5 22 0 99.16 110.15 109.67 o 6 22 0 56.50 -31.66 90.48 o 7 22 0 16.25 -81.79 81.79 o 8 22 0 0.26 -66.22 66.22 o 9 22 0 130.12 6.11 183.01 o 1 23 0 28.03 93.62 93.93 o 2 23 0 105.02 68.23 109.20 o 3 23 0 0.12 77.18 96.84 o 4 23 0 27.74 -30.75 91.32 o 5 23 0 3.56 -83.00 83.00 o 6 23 0 86.78 -8.36 94.56 o 7 23 0 67.49 43.29 85.83 o 0 24 0 298.16 107.76 235.51 o 1 24 0 12.61 -25.05 130.97 o 2 24 0 2.69 12.04 77.53 o 3 24 0 32.29 -37.00 98.59 o 4 24 0 1.01 -90.15 90.15 o 5 24 0 86.57 37.54 104.53 o -21 1 1 30.94 -73.46 159.39 o -20 1 1 76.87 162.18 152.64 o -19 1 1 78.64 52.67 137.83 o -18 1 1 568.73 548.40 153.73 o -17 1 1 926.33 897.38 103.99 o -16 1 1 594.50 687.77 95.70 o -15 1 1 764.14 820.17 60.09 o -14 1 1 2939.20 2671.54 128.61 o -13 1 1 921.99 733.39 55.22 o -12 1 1 113.44 225.20 46.84 o -11 1 1 7073.42 7380.31 135.62 o -10 1 1 116.09 176.83 54.06 o -9 1 1 264.40 271.60 37.87 o -8 1 1 1051.36 876.98 42.26 o -7 1 1 3153.13 3585.94 76.16 o -6 1 1 697.19 729.88 35.82 o -5 1 1 13425.55 12606.50 185.08 o -4 1 1 8797.42 8493.81 130.86 o -3 1 1 31035.00 29827.41 328.88 o -2 1 1 263.94 113.11 13.15 o 2 1 1 378.36 552.63 43.64 o 3 1 1 72184.86 69765.43 701.02 o 4 1 1 826.99 677.35 20.12 o 5 1 1 10800.43 10553.00 181.31 o 6 1 1 5683.79 5478.18 110.23 o 7 1 1 6234.75 5106.43 105.90 o 8 1 1 1005.08 1163.02 49.38 o 9 1 1 379.44 395.32 41.58 o 10 1 1 8.12 -10.96 29.69 o 11 1 1 5472.65 5228.55 92.34 o 12 1 1 2952.76 2593.25 65.75 o 13 1 1 18.53 113.98 46.15 o 14 1 1 1393.61 1293.93 66.96 o 15 1 1 467.97 683.88 59.74 o 16 1 1 546.07 541.99 76.03 o 17 1 1 133.58 111.30 67.99 o 18 1 1 196.04 213.58 69.46 o 19 1 1 16.89 40.00 68.15 o 20 1 1 14.46 -143.10 143.10 o 21 1 1 7.74 -47.21 146.30 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