#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/64/2216436.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216436_Fobs loop_ _publ_author_name 'Wu, Ling-Yan' 'Zhu, Zhu' 'Jin, Chuan-Ming' _publ_section_title ; catena-Poly[[silver(I)-\m-1,1'-methylenediimidazole] hexafluoridophosphate] ; _journal_coeditor_code FJ2055 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2967 _journal_volume 63 _journal_year 2007 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.666 _cell_angle_gamma 90.000 _cell_length_a 8.3966 _cell_length_b 5.1604 _cell_length_c 13.6211 _exptl_crystal_F_000 388.00 _reflns_d_resolution_high 0.7829 _[local]_cod_data_source_file fj2055Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cd2731 in P2/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22153.38 6962.22 9290.99 o 4 0 0 3015.11 2995.18 213.89 o 6 0 0 3343.97 3352.08 174.18 o 8 0 0 1367.04 1334.15 69.41 o 10 0 0 126.14 144.59 14.28 o 0 1 0 5375.19 5528.94 393.39 o 1 1 0 244.67 246.93 8.73 o 2 1 0 7591.95 5545.98 1513.25 o 3 1 0 55.64 55.56 1.72 o 4 1 0 6205.99 5820.16 130.09 o 5 1 0 52.99 61.31 2.37 o 6 1 0 2044.84 1893.34 101.24 o 7 1 0 101.22 86.32 4.41 o 8 1 0 423.85 438.36 24.20 o 9 1 0 5.19 7.39 3.00 o 10 1 0 145.72 180.32 15.81 o 0 2 0 3040.20 3138.10 324.08 o 1 2 0 0.00 1.24 0.52 o 2 2 0 4577.71 4474.58 192.39 o 3 2 0 62.19 63.13 3.11 o 4 2 0 2872.13 2713.46 116.83 o 5 2 0 57.02 60.00 5.13 o 6 2 0 1340.62 1218.41 48.17 o 7 2 0 123.04 117.73 6.21 o 8 2 0 256.29 238.60 19.99 o 9 2 0 16.50 23.62 4.58 o 10 2 0 99.05 123.99 16.54 o 0 3 0 2269.48 2456.44 243.18 o 1 3 0 2.55 2.46 0.78 o 2 3 0 3994.93 4170.94 121.60 o 3 3 0 140.49 144.59 6.68 o 4 3 0 2503.11 2609.98 147.18 o 5 3 0 3.81 4.14 1.53 o 6 3 0 597.64 550.33 13.72 o 7 3 0 15.94 18.97 3.32 o 8 3 0 238.40 203.30 9.31 o 9 3 0 5.78 10.97 3.75 o 0 4 0 921.00 975.28 67.31 o 1 4 0 0.02 -1.09 0.97 o 2 4 0 1310.02 1308.61 49.30 o 3 4 0 7.68 9.08 1.89 o 4 4 0 1151.39 1159.06 56.91 o 5 4 0 14.00 12.18 2.80 o 6 4 0 231.66 236.66 19.58 o 7 4 0 6.25 7.40 2.52 o 8 4 0 133.45 148.43 8.60 o 0 5 0 1531.33 1596.38 42.44 o 1 5 0 3.00 3.59 1.99 o 2 5 0 578.11 547.51 27.84 o 3 5 0 5.11 4.33 1.93 o 4 5 0 168.26 158.97 6.75 o 5 5 0 14.70 15.02 3.08 o 6 5 0 188.45 198.79 14.68 o 0 6 0 234.16 240.03 18.20 o 1 6 0 12.94 12.10 3.85 o 2 6 0 398.28 401.20 16.84 o 3 6 0 2.00 2.84 2.82 o 4 6 0 286.29 307.77 22.71 o -9 0 1 110.80 131.31 12.09 o -7 0 1 54.95 49.96 4.91 o -5 0 1 267.95 209.04 11.69 o -3 0 1 2356.58 2138.19 126.00 o -1 0 1 4609.67 4778.72 38.99 o 1 0 1 130.35 164.31 4.98 o 3 0 1 5588.40 5257.97 333.78 o 5 0 1 1788.82 1647.45 61.18 o 7 0 1 181.29 169.45 8.10 o 9 0 1 1.00 8.43 5.25 o -10 1 1 0.50 -1.79 3.52 o -9 1 1 7.07 13.13 3.17 o -8 1 1 52.75 58.03 6.85 o -7 1 1 43.20 48.03 3.89 o -6 1 1 0.02 1.70 0.86 o -5 1 1 1254.81 1273.47 21.35 o -4 1 1 164.18 151.66 3.42 o -3 1 1 2985.08 3293.14 75.81 o -2 1 1 452.75 465.39 15.29 o -1 1 1 84.99 93.43 4.97 o 0 1 1 52.04 48.12 1.43 o 1 1 1 163.81 200.77 13.02 o 2 1 1 464.56 476.13 15.26 o 3 1 1 2901.22 3202.89 128.05 o 4 1 1 143.94 135.28 3.35 o 5 1 1 101.15 93.71 2.82 o 6 1 1 94.25 53.49 22.28 o 7 1 1 36.29 37.09 4.09 o 8 1 1 5.89 8.33 2.31 o 9 1 1 85.35 96.85 14.11 o 10 1 1 9.46 16.07 5.91 o -10 2 1 0.29 3.40 3.27 o -9 2 1 24.71 30.54 5.30 o -8 2 1 48.15 52.22 5.55 o -7 2 1 212.28 213.40 8.41 o -6 2 1 58.55 51.77 8.24 o -5 2 1 1.74 4.85 1.33 o -4 2 1 53.73 57.73 4.34 o -3 2 1 311.89 399.39 12.57 o -2 2 1 228.90 225.68 9.09 o -1 2 1 4262.21 4800.70 206.22 o 0 2 1 25.03 27.24 1.58 o 1 2 1 4422.57 4810.10 173.40 o 2 2 1 466.40 475.25 15.14 o 3 2 1 217.05 330.41 12.65 o 4 2 1 31.02 39.33 3.53 o 5 2 1 486.52 516.96 17.81 o 6 2 1 0.16 1.53 1.42 o 7 2 1 248.87 242.26 16.32 o 8 2 1 0.57 -0.55 2.04 o 9 2 1 58.04 65.71 7.93 o 10 2 1 1.14 3.07 3.43 o -9 3 1 46.43 48.26 6.90 o -8 3 1 7.59 8.58 2.59 o -7 3 1 271.60 256.75 9.91 o -6 3 1 20.79 19.06 3.23 o -5 3 1 422.38 383.73 22.31 o -4 3 1 14.28 18.12 2.87 o -3 3 1 898.04 924.27 32.37 o -2 3 1 48.99 56.86 5.11 o -1 3 1 3714.97 3591.10 232.29 o 0 3 1 6.33 6.31 1.22 o 1 3 1 3759.39 3729.23 182.69 o 2 3 1 45.43 58.83 4.08 o 3 3 1 550.45 600.56 32.30 o 4 3 1 28.55 22.51 4.66 o 5 3 1 553.10 488.25 28.51 o 6 3 1 17.44 15.26 2.91 o 7 3 1 265.93 259.67 13.98 o 8 3 1 0.77 0.10 2.21 o 9 3 1 25.99 33.29 6.11 o -8 4 1 8.28 9.20 3.08 o -7 4 1 91.92 91.78 6.77 o -6 4 1 2.21 1.44 1.73 o -5 4 1 691.01 637.10 27.35 o -4 4 1 0.52 1.83 1.37 o -3 4 1 411.25 403.64 18.64 o -2 4 1 9.07 14.74 2.63 o -1 4 1 562.06 473.18 26.48 o 0 4 1 17.42 23.46 2.58 o 1 4 1 674.32 597.28 26.90 o 2 4 1 9.18 10.57 1.97 o 3 4 1 668.38 646.15 30.98 o 4 4 1 48.11 45.04 4.08 o 5 4 1 203.80 183.39 14.91 o 6 4 1 1.97 2.26 1.83 o 7 4 1 69.46 67.51 6.67 o 8 4 1 0.44 1.33 2.54 o -6 5 1 7.51 7.57 2.81 o -5 5 1 24.14 25.03 3.82 o -4 5 1 10.97 9.20 2.59 o -3 5 1 115.36 120.86 6.66 o -2 5 1 7.92 12.36 4.09 o -1 5 1 341.26 318.82 13.31 o 0 5 1 0.24 2.91 2.19 o 1 5 1 129.40 131.14 8.39 o 2 5 1 0.42 2.06 1.97 o 3 5 1 167.79 173.48 8.95 o 4 5 1 46.11 46.03 5.31 o 5 5 1 182.18 165.66 14.41 o 6 5 1 0.62 -0.83 1.95 o -4 6 1 0.00 0.86 4.85 o -3 6 1 162.53 161.50 10.86 o -2 6 1 1.25 5.17 2.83 o -1 6 1 38.98 61.17 8.03 o 0 6 1 40.15 39.92 6.51 o 1 6 1 154.19 150.80 10.19 o 2 6 1 11.65 12.71 3.84 o 3 6 1 131.80 123.00 13.68 o 4 6 1 0.19 -2.41 3.05 o -8 0 2 899.37 959.25 20.91 o -6 0 2 2068.11 2057.18 44.82 o -4 0 2 2011.92 1986.79 58.69 o -2 0 2 13792.68 13401.44 1224.19 o 0 0 2 15246.38 14403.58 862.68 o 2 0 2 6162.44 6827.39 543.35 o 4 0 2 3567.28 3400.64 251.94 o 6 0 2 2750.71 2761.51 174.04 o 8 0 2 204.91 242.29 16.14 o 10 0 2 97.62 115.17 13.02 o -10 1 2 92.90 125.33 13.02 o -9 1 2 1.70 3.96 2.31 o -8 1 2 391.52 373.70 11.16 o -7 1 2 19.08 24.46 2.60 o -6 1 2 2376.99 2352.06 81.23 o -5 1 2 73.71 62.01 2.45 o -4 1 2 3917.14 3765.47 96.68 o -3 1 2 309.38 262.81 4.35 o -2 1 2 8170.71 8324.58 231.08 o -1 1 2 1.82 4.29 0.60 o 0 1 2 24608.69 26952.99 537.80 o 1 1 2 1059.19 1257.48 14.43 o 2 1 2 11807.28 13345.87 118.17 o 3 1 2 346.50 305.28 4.60 o 4 1 2 1807.17 1680.65 74.03 o 5 1 2 38.90 36.91 2.34 o 6 1 2 1683.65 1667.78 72.14 o 7 1 2 30.46 33.06 3.95 o 8 1 2 925.96 878.19 46.25 o 9 1 2 0.14 0.81 2.59 o 10 1 2 149.72 168.96 16.07 o -10 2 2 68.10 72.46 9.01 o -9 2 2 0.86 3.94 3.07 o -8 2 2 315.72 284.78 10.94 o -7 2 2 24.03 19.26 3.83 o -6 2 2 737.25 713.09 15.70 o -5 2 2 296.71 289.85 10.38 o -4 2 2 3473.71 3347.17 96.26 o -3 2 2 249.46 247.78 9.63 o -2 2 2 3512.07 3411.39 131.72 o -1 2 2 222.32 232.05 14.23 o 0 2 2 2838.99 3144.84 85.70 o 1 2 2 1074.19 1156.51 20.77 o 2 2 2 3680.64 3502.04 113.99 o 3 2 2 775.03 834.24 26.65 o 4 2 2 5875.15 6070.10 220.95 o 5 2 2 1.44 2.95 1.23 o 6 2 2 1299.30 1251.13 57.48 o 7 2 2 7.24 8.26 2.67 o 8 2 2 294.74 259.18 36.40 o 9 2 2 0.27 4.02 2.69 o 10 2 2 110.53 135.46 10.61 o -9 3 2 1.85 3.35 2.37 o -8 3 2 213.96 206.10 13.88 o -7 3 2 1.07 3.33 1.79 o -6 3 2 582.30 591.52 22.16 o -5 3 2 13.81 14.05 2.26 o -4 3 2 3067.33 3217.39 142.20 o -3 3 2 354.40 365.15 17.44 o -2 3 2 3155.38 3342.21 197.48 o -1 3 2 163.47 175.06 13.86 o 0 3 2 1713.45 1922.63 88.55 o 1 3 2 121.79 129.08 7.90 o 2 3 2 3105.36 3137.77 110.28 o 3 3 2 67.15 55.63 13.96 o 4 3 2 2547.65 2576.16 128.71 o 5 3 2 106.77 107.39 8.72 o 6 3 2 514.72 516.49 39.63 o 7 3 2 34.98 28.63 4.08 o 8 3 2 173.64 177.82 22.35 o 9 3 2 14.63 17.04 4.91 o -8 4 2 171.25 180.65 9.62 o -7 4 2 15.08 15.02 3.26 o -6 4 2 487.31 489.39 29.97 o -5 4 2 10.46 15.65 2.72 o -4 4 2 737.47 763.14 33.61 o -3 4 2 109.12 106.24 7.27 o -2 4 2 1932.33 1982.91 100.40 o -1 4 2 11.39 8.44 1.98 o 0 4 2 2319.68 2482.16 100.47 o 1 4 2 2.72 2.37 1.34 o 2 4 2 2210.24 2263.67 97.75 o 3 4 2 126.47 134.19 6.72 o 4 4 2 527.17 510.52 25.11 o 5 4 2 33.45 37.57 4.80 o 6 4 2 313.17 301.86 23.50 o 7 4 2 4.80 6.07 2.34 o 8 4 2 220.58 195.37 25.90 o -6 5 2 114.73 115.78 9.46 o -5 5 2 1.83 1.32 1.66 o -4 5 2 241.72 252.91 16.14 o -3 5 2 0.21 1.56 1.55 o -2 5 2 770.37 734.17 31.11 o -1 5 2 4.37 8.79 2.60 o 0 5 2 606.92 641.20 30.09 o 1 5 2 19.01 22.06 4.18 o 2 5 2 577.15 537.69 34.85 o 3 5 2 9.47 7.98 2.25 o 4 5 2 567.86 530.08 32.61 o 5 5 2 0.37 0.32 1.64 o 6 5 2 348.88 337.07 18.96 o -4 6 2 253.05 270.13 14.37 o -3 6 2 0.03 2.42 2.66 o -2 6 2 243.68 245.15 13.31 o -1 6 2 28.22 26.58 5.49 o 0 6 2 577.01 540.49 19.51 o 1 6 2 0.70 -0.50 3.42 o 2 6 2 383.39 327.28 15.05 o 3 6 2 0.05 -1.39 4.18 o 4 6 2 154.02 157.85 18.40 o -9 0 3 49.32 88.93 9.30 o -7 0 3 223.80 213.62 7.53 o -5 0 3 2139.47 2039.97 72.67 o -3 0 3 8375.11 8399.43 543.69 o -1 0 3 577.93 555.90 12.22 o 1 0 3 36.70 45.81 2.26 o 3 0 3 5900.47 6720.47 64.29 o 5 0 3 1348.30 1151.85 129.38 o 7 0 3 11.56 27.59 9.17 o 9 0 3 11.45 31.81 7.37 o -10 1 3 0.01 2.26 3.98 o -9 1 3 16.70 21.73 4.15 o -8 1 3 54.25 54.49 5.35 o -7 1 3 70.87 69.54 3.98 o -6 1 3 195.04 165.17 6.69 o -5 1 3 243.82 213.34 5.13 o -4 1 3 1189.34 1175.59 31.13 o -3 1 3 1795.47 1805.21 29.60 o -2 1 3 254.24 236.13 5.58 o -1 1 3 6174.06 6910.46 117.72 o 0 1 3 1573.62 1746.98 86.08 o 1 1 3 8766.28 10051.88 200.53 o 2 1 3 1313.05 1417.39 16.51 o 3 1 3 2043.78 2341.54 25.10 o 4 1 3 798.66 856.75 19.22 o 5 1 3 812.25 712.45 28.72 o 6 1 3 0.72 1.35 1.61 o 7 1 3 541.41 499.32 26.50 o 8 1 3 0.05 0.30 1.68 o 9 1 3 132.11 148.06 7.73 o 10 1 3 0.72 -0.40 5.38 o -10 2 3 3.30 11.50 4.46 o -9 2 3 37.29 43.97 5.37 o -8 2 3 64.68 60.22 5.94 o -7 2 3 100.86 97.20 4.88 o -6 2 3 93.51 82.18 4.52 o -5 2 3 281.46 251.58 6.94 o -4 2 3 402.22 421.89 18.44 o -3 2 3 644.31 745.57 35.71 o -2 2 3 176.42 173.54 14.00 o -1 2 3 3427.21 3794.20 112.84 o 0 2 3 945.58 1095.41 23.50 o 1 2 3 1803.82 1864.84 127.74 o 2 2 3 19.84 27.90 2.03 o 3 2 3 1627.80 1989.22 28.64 o 4 2 3 128.47 144.15 8.70 o 5 2 3 524.27 506.54 20.57 o 6 2 3 2.78 4.02 1.59 o 7 2 3 257.03 230.53 27.73 o 8 2 3 6.70 10.80 3.18 o 9 2 3 46.83 50.40 10.36 o -9 3 3 10.15 12.55 3.35 o -8 3 3 31.02 35.46 4.88 o -7 3 3 126.78 117.84 10.34 o -6 3 3 29.36 38.98 3.91 o -5 3 3 336.48 284.40 11.97 o -4 3 3 148.17 150.57 5.67 o -3 3 3 192.46 212.42 19.89 o -2 3 3 0.13 1.18 1.03 o -1 3 3 997.30 959.21 49.34 o 0 3 3 252.52 307.03 10.68 o 1 3 3 852.58 903.31 15.24 o 2 3 3 149.26 145.28 6.77 o 3 3 3 213.03 235.58 8.91 o 4 3 3 42.65 46.39 4.66 o 5 3 3 132.80 116.12 9.21 o 6 3 3 5.85 8.45 2.23 o 7 3 3 107.08 101.21 9.53 o 8 3 3 5.76 3.94 2.75 o 9 3 3 9.75 6.44 3.26 o -8 4 3 2.21 4.65 2.63 o -7 4 3 64.31 68.03 6.92 o -6 4 3 0.75 1.48 1.53 o -5 4 3 62.60 54.60 5.56 o -4 4 3 3.94 6.40 2.15 o -3 4 3 230.40 226.80 13.90 o -2 4 3 10.83 16.44 2.85 o -1 4 3 621.67 584.16 18.07 o 0 4 3 1.93 3.92 1.94 o 1 4 3 730.00 647.01 44.32 o 2 4 3 0.40 0.75 1.08 o 3 4 3 119.77 125.06 6.10 o 4 4 3 18.16 17.94 3.34 o 5 4 3 248.88 228.38 22.55 o 6 4 3 0.41 0.99 1.73 o 7 4 3 94.71 92.25 7.98 o 8 4 3 2.34 3.40 2.88 o -6 5 3 1.57 4.18 3.21 o -5 5 3 121.89 116.61 7.18 o -4 5 3 16.91 16.73 3.37 o -3 5 3 255.13 261.61 10.04 o -2 5 3 10.69 14.41 3.70 o -1 5 3 47.94 58.38 7.16 o 0 5 3 0.05 0.26 1.67 o 1 5 3 135.10 126.99 8.40 o 2 5 3 77.51 76.76 5.50 o 3 5 3 385.91 338.81 30.62 o 4 5 3 1.22 0.77 2.03 o 5 5 3 197.25 176.73 14.04 o 6 5 3 0.00 2.00 4.64 o -4 6 3 0.89 1.82 3.55 o -3 6 3 42.55 34.34 6.38 o -2 6 3 42.92 38.39 6.64 o -1 6 3 178.85 171.43 11.08 o 0 6 3 8.31 7.92 4.45 o 1 6 3 153.27 158.48 10.47 o 2 6 3 2.37 4.25 3.59 o 3 6 3 62.88 64.62 12.95 o -8 0 4 439.62 451.33 27.92 o -6 0 4 1644.99 1608.38 158.63 o -4 0 4 2803.79 3000.71 169.14 o -2 0 4 2920.93 2506.22 33.21 o 0 0 4 6831.39 6724.41 303.42 o 2 0 4 2666.58 2971.24 65.98 o 4 0 4 1118.67 1260.78 28.23 o 6 0 4 473.38 488.48 55.42 o 8 0 4 477.20 488.82 23.78 o 10 0 4 100.00 125.59 14.61 o -10 1 4 94.32 118.02 8.98 o -9 1 4 21.21 22.08 3.72 o -8 1 4 343.50 349.39 19.65 o -7 1 4 51.28 62.52 4.15 o -6 1 4 774.56 736.58 47.12 o -5 1 4 92.68 90.08 3.47 o -4 1 4 984.81 880.79 27.05 o -3 1 4 490.29 413.02 8.42 o -2 1 4 3774.70 3684.86 67.52 o -1 1 4 1900.58 2000.15 43.20 o 0 1 4 10815.84 11141.25 522.46 o 1 1 4 146.36 162.53 3.50 o 2 1 4 2983.94 3098.86 21.69 o 3 1 4 143.83 132.80 4.50 o 4 1 4 2596.81 2799.06 67.05 o 5 1 4 32.19 27.60 3.33 o 6 1 4 1894.63 1831.82 127.24 o 7 1 4 21.80 24.92 3.61 o 8 1 4 413.36 390.38 18.49 o 9 1 4 9.28 12.14 2.81 o 10 1 4 89.70 114.50 17.07 o -10 2 4 95.88 135.84 10.49 o -9 2 4 18.14 24.77 3.93 o -8 2 4 224.23 225.89 11.82 o -7 2 4 33.06 29.47 3.45 o -6 2 4 1247.22 1248.90 20.87 o -5 2 4 19.43 27.43 3.05 o -4 2 4 4036.75 4069.44 80.86 o -3 2 4 376.15 336.94 14.53 o -2 2 4 5937.58 6095.49 173.00 o -1 2 4 227.22 244.48 6.00 o 0 2 4 3448.90 4103.96 40.47 o 1 2 4 190.02 201.66 7.54 o 2 2 4 7428.02 8127.97 118.94 o 3 2 4 364.48 377.19 6.37 o 4 2 4 4053.80 4094.67 263.31 o 5 2 4 124.27 127.46 8.30 o 6 2 4 1284.67 1278.55 102.48 o 7 2 4 5.61 4.96 1.69 o 8 2 4 340.35 312.36 36.43 o 9 2 4 0.16 2.14 3.12 o -9 3 4 1.72 5.13 2.76 o -8 3 4 226.94 219.62 9.99 o -7 3 4 9.47 13.72 2.56 o -6 3 4 789.47 811.22 17.96 o -5 3 4 63.92 62.63 4.50 o -4 3 4 1928.12 1943.62 57.77 o -3 3 4 31.06 34.49 3.90 o -2 3 4 2775.74 2760.64 105.80 o -1 3 4 7.75 12.95 2.10 o 0 3 4 2481.74 2786.41 37.40 o 1 3 4 38.87 45.14 3.43 o 2 3 4 3364.77 3385.55 28.19 o 3 3 4 11.08 12.56 2.06 o 4 3 4 1491.04 1521.59 86.14 o 5 3 4 118.67 105.32 5.88 o 6 3 4 505.22 514.69 34.60 o 7 3 4 0.77 3.29 2.30 o 8 3 4 207.33 182.51 11.45 o -8 4 4 168.88 202.96 12.84 o -7 4 4 1.45 1.89 2.32 o -6 4 4 165.86 194.21 8.89 o -5 4 4 71.07 74.90 5.95 o -4 4 4 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