#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2216447.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216447_Fobs loop_ _publ_author_name 'Kallamadi, Ramnath' 'Jackson, John A.' 'Zeller, Matthias' _publ_section_title ; Triethynylphosphine oxide ; _journal_coeditor_code FL2164 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4563 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8646 _cell_length_b 9.7823 _cell_length_c 9.3277 _exptl_crystal_F_000 248.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file fl2164Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 07rk001m1 in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 721.79 890.33 8.68 o 4 0 0 2001.91 2371.57 22.66 o 6 0 0 4.16 5.11 0.65 o 8 0 0 147.03 148.12 4.04 o 2 1 0 5770.89 6152.29 47.72 o 4 1 0 333.81 312.16 2.63 o 6 1 0 3.50 2.40 0.38 o 8 1 0 231.57 253.94 3.97 o 0 2 0 5129.16 5298.66 117.78 o 2 2 0 46.56 23.13 0.34 o 4 2 0 6.91 5.03 0.23 o 6 2 0 402.42 436.58 5.17 o 8 2 0 283.86 290.24 4.34 o 2 3 0 358.51 285.29 2.52 o 4 3 0 284.61 276.69 2.53 o 6 3 0 339.18 341.59 4.32 o 8 3 0 200.97 215.18 3.58 o 0 4 0 7808.89 8137.19 91.08 o 2 4 0 202.55 218.55 1.67 o 4 4 0 80.04 77.77 1.04 o 6 4 0 0.07 0.07 0.17 o 8 4 0 557.15 579.35 11.83 o 2 5 0 1292.25 1285.34 8.24 o 4 5 0 153.15 135.05 1.34 o 6 5 0 73.74 72.51 1.60 o 8 5 0 93.99 105.13 2.78 o 0 6 0 3450.96 3604.88 29.26 o 2 6 0 19.18 15.05 0.45 o 4 6 0 167.40 166.27 1.74 o 6 6 0 264.80 274.28 3.76 o 8 6 0 90.37 87.16 3.39 o 2 7 0 1151.30 1125.79 7.57 o 4 7 0 401.85 390.52 3.29 o 6 7 0 1.10 0.93 0.27 o 0 8 0 3744.11 3931.98 36.45 o 2 8 0 1.68 2.11 0.27 o 4 8 0 431.40 462.50 3.85 o 6 8 0 14.32 11.35 0.70 o 2 9 0 678.87 682.50 5.62 o 4 9 0 60.70 57.69 1.09 o 6 9 0 20.02 18.78 0.82 o 0 10 0 464.03 446.74 5.94 o 2 10 0 9.65 11.45 0.55 o 4 10 0 0.11 0.01 0.32 o 2 11 0 11.78 9.37 0.54 o 4 11 0 178.47 179.57 3.12 o 0 12 0 653.89 672.46 10.19 o 2 12 0 0.01 0.25 0.39 o 1 0 1 5005.48 5111.34 44.67 o 2 0 1 3046.36 3381.72 25.49 o 3 0 1 624.87 754.05 6.11 o 4 0 1 0.98 0.50 0.22 o 5 0 1 277.91 320.36 2.90 o 6 0 1 186.44 200.33 2.99 o 7 0 1 417.84 440.16 5.48 o 8 0 1 12.02 8.89 0.68 o 9 0 1 0.50 1.42 0.40 o 0 1 1 185.41 156.74 1.28 o 1 1 1 556.89 594.66 2.75 o 2 1 1 313.15 338.02 2.00 o 3 1 1 1014.25 1089.55 5.43 o 4 1 1 219.44 246.19 1.57 o 5 1 1 592.64 548.46 3.00 o 6 1 1 49.77 51.09 0.81 o 7 1 1 206.38 216.98 2.39 o 8 1 1 11.64 9.16 0.49 o 9 1 1 216.26 252.80 2.96 o 1 2 1 1361.77 1394.00 5.87 o 2 2 1 1098.67 1209.92 7.15 o 3 2 1 26.13 29.96 0.34 o 4 2 1 750.45 815.04 4.22 o 5 2 1 100.19 113.78 1.00 o 6 2 1 0.09 0.05 0.13 o 7 2 1 651.09 673.28 5.33 o 8 2 1 52.56 50.71 1.11 o 9 2 1 1.74 2.76 0.40 o 0 3 1 1083.02 1274.07 9.70 o 1 3 1 0.92 3.68 0.11 o 2 3 1 171.02 184.30 1.21 o 3 3 1 233.29 215.53 1.31 o 4 3 1 76.57 82.63 0.66 o 5 3 1 924.01 920.55 5.69 o 6 3 1 53.35 53.82 0.88 o 7 3 1 55.08 54.53 1.07 o 8 3 1 23.63 19.48 0.72 o 1 4 1 710.88 725.86 3.50 o 2 4 1 0.97 0.29 0.07 o 3 4 1 22.76 20.80 0.29 o 4 4 1 0.98 0.61 0.09 o 5 4 1 17.85 17.05 0.35 o 6 4 1 5.20 5.01 0.29 o 7 4 1 557.34 584.64 5.17 o 8 4 1 28.02 25.90 1.27 o 0 5 1 5.54 3.47 0.20 o 1 5 1 114.32 96.46 0.71 o 2 5 1 72.15 65.93 0.59 o 3 5 1 364.71 337.60 1.84 o 4 5 1 19.26 16.98 0.31 o 5 5 1 529.27 531.39 3.05 o 6 5 1 3.89 4.30 0.28 o 7 5 1 69.53 68.78 1.46 o 8 5 1 4.52 6.29 0.55 o 1 6 1 906.45 918.02 4.36 o 2 6 1 11.19 12.42 0.26 o 3 6 1 39.44 36.21 0.49 o 4 6 1 286.93 287.98 1.75 o 5 6 1 164.15 162.91 1.59 o 6 6 1 21.45 17.93 0.52 o 7 6 1 338.63 348.93 4.46 o 8 6 1 39.51 39.57 1.33 o 0 7 1 4.81 3.16 0.25 o 1 7 1 184.58 162.11 1.19 o 2 7 1 120.96 106.78 0.93 o 3 7 1 571.29 552.61 2.99 o 4 7 1 56.07 51.91 0.65 o 5 7 1 281.67 283.67 2.37 o 6 7 1 98.33 96.42 1.38 o 7 7 1 159.50 153.39 2.71 o 1 8 1 706.91 721.73 3.87 o 2 8 1 173.11 167.37 1.30 o 3 8 1 63.92 58.97 0.72 o 4 8 1 13.62 10.20 0.35 o 5 8 1 110.24 107.60 1.33 o 6 8 1 47.53 47.70 1.00 o 7 8 1 193.79 194.22 3.19 o 0 9 1 36.35 29.95 0.81 o 1 9 1 59.55 57.38 0.80 o 2 9 1 6.48 6.11 0.30 o 3 9 1 231.06 224.92 1.74 o 4 9 1 23.18 22.22 0.52 o 5 9 1 225.38 230.56 2.33 o 6 9 1 0.13 0.16 0.21 o 1 10 1 185.21 185.80 1.67 o 2 10 1 76.26 78.14 1.01 o 3 10 1 0.68 0.80 0.22 o 4 10 1 68.04 72.78 1.30 o 5 10 1 17.15 15.90 0.61 o 0 11 1 135.15 137.62 2.06 o 1 11 1 1.25 1.65 0.23 o 2 11 1 41.20 37.21 0.72 o 3 11 1 82.43 75.24 1.18 o 4 11 1 35.58 34.57 0.97 o 1 12 1 153.63 159.32 1.66 o 2 12 1 2.22 1.98 0.27 o 3 12 1 2.73 2.79 0.34 o 0 13 1 59.15 59.55 1.43 o 0 0 2 2066.70 2134.91 22.21 o 1 0 2 570.43 592.62 3.82 o 2 0 2 272.37 228.98 2.13 o 3 0 2 1921.78 2152.61 22.84 o 4 0 2 17.71 12.74 0.39 o 5 0 2 54.43 53.29 0.94 o 6 0 2 355.94 379.16 3.52 o 7 0 2 98.57 98.94 2.11 o 8 0 2 192.55 188.37 3.30 o 9 0 2 3.07 1.98 0.57 o 1 1 2 954.75 972.09 4.49 o 2 1 2 963.81 919.67 5.51 o 3 1 2 3.05 2.93 0.13 o 4 1 2 527.72 514.57 2.90 o 5 1 2 554.91 619.09 3.70 o 6 1 2 31.57 26.36 0.52 o 7 1 2 1.88 1.02 0.23 o 8 1 2 135.89 140.74 1.96 o 9 1 2 0.12 0.85 0.28 o 0 2 2 14696.98 14510.27 82.32 o 1 2 2 461.32 540.63 2.44 o 2 2 2 96.06 113.37 0.70 o 3 2 2 422.29 435.43 2.32 o 4 2 2 660.82 717.32 3.86 o 5 2 2 98.12 104.73 1.04 o 6 2 2 1.13 1.68 0.17 o 7 2 2 29.77 29.60 0.77 o 8 2 2 214.50 210.10 2.71 o 1 3 2 42.18 57.62 0.43 o 2 3 2 1583.30 1656.48 6.84 o 3 3 2 494.71 546.07 2.72 o 4 3 2 420.81 399.14 2.28 o 5 3 2 72.88 72.98 0.75 o 6 3 2 0.10 0.27 0.15 o 7 3 2 37.83 36.00 0.85 o 8 3 2 93.82 102.70 1.94 o 0 4 2 2396.51 2552.68 14.66 o 1 4 2 177.22 197.72 1.13 o 2 4 2 122.37 108.79 0.76 o 3 4 2 101.38 87.06 0.65 o 4 4 2 119.48 121.28 1.02 o 5 4 2 44.03 45.03 0.59 o 6 4 2 290.79 299.94 2.76 o 7 4 2 13.27 10.39 0.45 o 8 4 2 94.82 87.57 2.00 o 1 5 2 63.15 50.75 0.50 o 2 5 2 492.17 453.63 2.30 o 3 5 2 50.40 45.96 0.50 o 4 5 2 501.09 493.12 2.81 o 5 5 2 113.92 111.85 1.08 o 6 5 2 10.88 8.38 0.49 o 7 5 2 4.84 6.07 0.50 o 8 5 2 149.53 152.96 2.78 o 0 6 2 3122.42 3266.32 19.97 o 1 6 2 4.47 4.30 0.17 o 2 6 2 0.02 0.25 0.10 o 3 6 2 471.89 442.51 2.36 o 4 6 2 267.75 273.40 1.94 o 5 6 2 10.39 9.57 0.33 o 6 6 2 4.65 2.92 0.36 o 7 6 2 74.35 71.60 1.49 o 1 7 2 246.58 218.42 1.40 o 2 7 2 544.85 535.77 2.89 o 3 7 2 0.63 0.82 0.14 o 4 7 2 160.07 158.11 1.40 o 5 7 2 355.19 355.82 2.60 o 6 7 2 11.13 10.57 0.55 o 7 7 2 1.10 1.12 0.28 o 0 8 2 732.12 742.70 5.85 o 1 8 2 43.77 35.84 0.56 o 2 8 2 43.99 45.29 0.61 o 3 8 2 330.61 326.33 2.08 o 4 8 2 30.12 28.65 0.57 o 5 8 2 4.13 4.66 0.29 o 6 8 2 117.37 119.62 2.02 o 7 8 2 28.98 27.33 0.89 o 1 9 2 52.22 47.52 0.73 o 2 9 2 126.18 121.69 1.18 o 3 9 2 4.08 4.04 0.25 o 4 9 2 322.56 330.40 2.57 o 5 9 2 57.61 54.91 1.03 o 6 9 2 5.41 6.06 0.46 o 0 10 2 1118.10 1186.77 10.53 o 1 10 2 45.89 44.65 0.75 o 2 10 2 3.64 3.86 0.28 o 3 10 2 25.09 21.96 0.55 o 4 10 2 151.76 157.64 1.84 o 5 10 2 47.18 46.54 1.04 o 1 11 2 0.72 1.06 0.22 o 2 11 2 353.23 367.52 2.84 o 3 11 2 71.48 69.35 1.19 o 4 11 2 55.79 54.89 1.17 o 0 12 2 333.74 328.41 3.68 o 1 12 2 0.42 0.83 0.23 o 2 12 2 14.24 16.70 0.55 o 3 12 2 34.64 32.59 0.85 o 1 0 3 1.46 6.69 0.19 o 2 0 3 61.29 59.77 0.63 o 3 0 3 574.97 651.97 4.53 o 4 0 3 1727.67 1853.36 13.01 o 5 0 3 87.84 88.22 1.29 o 6 0 3 57.04 51.99 1.03 o 7 0 3 467.48 471.33 5.72 o 8 0 3 131.34 129.99 3.17 o 0 1 3 5.18 1.41 0.11 o 1 1 3 699.89 821.87 3.88 o 2 1 3 820.15 898.39 4.31 o 3 1 3 374.21 341.14 2.01 o 4 1 3 174.45 187.56 1.45 o 5 1 3 713.64 712.60 4.21 o 6 1 3 311.74 324.77 2.27 o 7 1 3 77.75 75.95 1.25 o 8 1 3 0.94 0.79 0.24 o 1 2 3 1205.96 1273.97 6.47 o 2 2 3 366.21 358.84 1.92 o 3 2 3 60.66 66.09 0.60 o 4 2 3 329.99 329.37 1.94 o 5 2 3 253.79 257.90 1.93 o 6 2 3 26.01 23.36 0.50 o 7 2 3 109.39 110.13 1.45 o 8 2 3 0.25 0.84 0.27 o 0 3 3 71.51 77.15 0.77 o 1 3 3 60.90 57.35 0.46 o 2 3 3 574.92 610.56 2.84 o 3 3 3 1267.21 1323.86 6.67 o 4 3 3 41.84 40.70 0.55 o 5 3 3 183.34 169.98 1.47 o 6 3 3 178.64 184.49 1.72 o 7 3 3 274.35 278.39 2.98 o 8 3 3 27.63 27.00 0.94 o 1 4 3 785.68 827.28 3.64 o 2 4 3 207.21 229.32 1.27 o 3 4 3 3.54 3.09 0.14 o 4 4 3 1013.82 1057.54 5.30 o 5 4 3 567.93 594.75 3.31 o 6 4 3 0.77 0.79 0.17 o 7 4 3 139.05 135.87 1.92 o 8 4 3 81.42 82.88 1.91 o 0 5 3 31.06 41.06 0.63 o 1 5 3 41.98 48.95 0.50 o 2 5 3 438.45 425.57 2.27 o 3 5 3 621.38 619.76 3.15 o 4 5 3 15.69 11.50 0.34 o 5 5 3 355.66 356.36 2.50 o 6 5 3 272.10 275.35 2.91 o 7 5 3 186.04 186.21 2.59 o 8 5 3 7.99 6.70 0.57 o 1 6 3 264.53 277.87 1.62 o 2 6 3 245.06 210.75 1.35 o 3 6 3 0.14 0.61 0.11 o 4 6 3 250.01 233.35 1.84 o 5 6 3 50.58 51.38 0.82 o 6 6 3 37.97 35.03 0.99 o 7 6 3 133.02 125.37 2.08 o 0 7 3 191.54 164.40 1.74 o 1 7 3 42.73 35.33 0.48 o 2 7 3 177.65 175.48 1.25 o 3 7 3 132.33 127.63 1.08 o 4 7 3 168.05 156.65 1.50 o 5 7 3 312.78 327.48 2.61 o 6 7 3 83.93 79.22 1.57 o 7 7 3 8.53 7.91 0.51 o 1 8 3 63.57 65.18 0.78 o 2 8 3 8.00 5.41 0.25 o 3 8 3 81.93 81.11 0.91 o 4 8 3 421.17 431.10 3.04 o 5 8 3 58.84 55.43 0.93 o 6 8 3 11.14 9.87 0.55 o 0 9 3 3.35 2.54 0.40 o 1 9 3 11.71 9.29 0.34 o 2 9 3 193.13 190.36 1.64 o 3 9 3 241.92 234.72 2.13 o 4 9 3 4.46 4.00 0.31 o 5 9 3 209.56 220.10 2.14 o 6 9 3 167.28 168.94 2.57 o 1 10 3 330.53 346.21 2.50 o 2 10 3 26.47 25.91 0.61 o 3 10 3 27.00 26.29 0.70 o 4 10 3 105.16 98.39 1.35 o 5 10 3 126.69 129.09 2.06 o 0 11 3 35.73 34.96 1.03 o 1 11 3 36.15 40.83 0.80 o 2 11 3 40.69 37.23 0.77 o 3 11 3 266.18 272.58 2.67 o 4 11 3 15.24 13.99 0.56 o 1 12 3 100.15 105.89 1.39 o 2 12 3 0.33 0.35 0.23 o 0 0 4 1007.69 965.90 9.02 o 1 0 4 160.81 195.78 1.48 o 2 0 4 23.49 16.54 0.31 o 3 0 4 500.39 507.42 4.08 o 4 0 4 98.88 85.13 1.21 o 5 0 4 315.64 331.94 3.17 o 6 0 4 2.49 3.24 0.31 o 7 0 4 27.65 28.98 0.93 o 8 0 4 182.99 171.14 3.69 o 1 1 4 391.47 379.62 2.01 o 2 1 4 0.05 3.09 0.21 o 3 1 4 80.84 86.52 0.71 o 4 1 4 619.57 599.00 3.62 o 5 1 4 269.68 285.59 2.10 o 6 1 4 0.10 0.29 0.15 o 7 1 4 85.17 82.31 1.32 o 8 1 4 13.21 13.49 0.71 o 0 2 4 289.54 298.25 2.25 o 1 2 4 355.23 354.85 2.01 o 2 2 4 398.68 383.93 2.09 o 3 2 4 988.79 1024.64 5.24 o 4 2 4 151.16 142.74 1.07 o 5 2 4 0.10 0.48 0.16 o 6 2 4 157.91 155.50 1.58 o 7 2 4 3.22 3.66 0.32 o 8 2 4 18.83 14.05 0.77 o 1 3 4 990.96 1017.64 4.89 o 2 3 4 453.92 439.92 2.39 o 3 3 4 13.75 13.44 0.31 o 4 3 4 691.88 687.20 3.80 o 5 3 4 402.39 423.85 3.02 o 6 3 4 112.73 113.84 1.32 o 7 3 4 23.59 24.45 0.79 o 8 3 4 49.05 47.72 1.43 o 0 4 4 2658.21 2836.70 17.57 o 1 4 4 4.11 3.19 0.14 o 2 4 4 60.09 55.33 0.58 o 3 4 4 866.72 851.46 4.31 o 4 4 4 778.64 818.40 4.46 o 5 4 4 102.01 99.70 1.25 o 6 4 4 3.12 2.85 0.31 o 7 4 4 107.02 106.54 1.69 o 8 4 4 3.37 2.30 0.36 o 1 5 4 334.99 295.52 1.61 o 2 5 4 249.19 254.73 1.49 o 3 5 4 37.28 37.87 0.51 o 4 5 4 373.04 372.42 2.55 o 5 5 4 317.01 321.97 2.69 o 6 5 4 41.35 39.67 0.81 o 7 5 4 55.33 49.23 1.23 o 0 6 4 60.18 77.17 0.99 o 1 6 4 104.90 83.91 0.75 o 2 6 4 135.01 141.38 1.11 o 3 6 4 385.14 369.33 2.54 o 4 6 4 10.80 11.50 0.37 o 5 6 4 9.64 8.01 0.40 o 6 6 4 71.17 70.99 1.20 o 7 6 4 0.16 -0.01 0.24 o 1 7 4 219.35 209.75 1.47 o 2 7 4 23.28 17.36 0.37 o 3 7 4 1.07 1.20 0.19 o 4 7 4 368.52 377.12 2.85 o 5 7 4 76.44 76.05 1.07 o 6 7 4 13.77 11.59 0.61 o 7 7 4 35.81 35.57 1.08 o 0 8 4 267.15 287.23 2.68 o 1 8 4 1.89 1.50 0.16 o 2 8 4 25.58 24.31 0.51 o 3 8 4 228.63 221.45 1.91 o 4 8 4 52.78 52.22 0.89 o 5 8 4 96.77 100.61 1.31 o 6 8 4 0.21 0.53 0.28 o 1 9 4 129.43 123.08 1.33 o 2 9 4 132.24 131.43 1.33 o 3 9 4 22.53 20.93 0.57 o 4 9 4 127.50 126.51 1.60 o 5 9 4 145.94 142.95 1.75 o 0 10 4 290.36 281.05 4.88 o 1 10 4 91.13 91.11 1.17 o 2 10 4 47.51 50.75 0.86 o 3 10 4 261.23 270.33 2.60 o 4 10 4 114.19 116.68 1.59 o 5 10 4 0.33 0.21 0.28 o 1 11 4 203.06 205.37 2.08 o 2 11 4 55.22 54.58 1.00 o 3 11 4 16.79 15.22 0.68 o 0 12 4 222.68 224.59 3.22 o 1 12 4 6.88 6.10 0.45 o 2 12 4 10.55 11.85 0.60 o 1 0 5 214.24 201.47 1.59 o 2 0 5 80.28 62.32 0.72 o 3 0 5 1.02 0.90 0.12 o 4 0 5 288.51 284.90 3.33 o 5 0 5 102.52 88.56 1.55 o 6 0 5 98.00 95.36 2.61 o 7 0 5 0.67 1.02 0.30 o 8 0 5 38.05 40.05 2.19 o 0 1 5 68.59 54.46 0.70 o 1 1 5 418.73 468.03 2.38 o 2 1 5 264.97 282.87 1.59 o 3 1 5 356.55 316.23 1.96 o 4 1 5 0.55 0.57 0.16 o 5 1 5 177.46 171.28 1.64 o 6 1 5 323.21 330.59 2.65 o 7 1 5 88.52 85.12 1.21 o 8 1 5 134.57 134.32 3.19 o 1 2 5 8.23 4.88 0.17 o 2 2 5 111.13 97.18 0.85 o 3 2 5 293.12 306.42 1.95 o 4 2 5 846.67 871.76 5.28 o 5 2 5 259.81 258.90 2.14 o 6 2 5 2.12 3.39 0.29 o 7 2 5 55.31 47.12 0.88 o 8 2 5 194.34 204.60 3.28 o 0 3 5 1035.72 1065.00 7.01 o 1 3 5 414.64 445.00 2.44 o 2 3 5 278.94 280.43 1.72 o 3 3 5 406.04 379.93 2.36 o 4 3 5 258.37 253.19 2.05 o 5 3 5 186.98 181.89 1.72 o 6 3 5 428.04 448.98 3.34 o 7 3 5 143.90 135.89 2.15 o 8 3 5 3.92 4.80 0.54 o 1 4 5 258.87 273.19 1.70 o 2 4 5 1107.01 1118.68 5.49 o 3 4 5 15.51 13.16 0.33 o 4 4 5 343.93 335.28 2.24 o 5 4 5 115.01 109.55 1.36 o 6 4 5 38.68 34.31 0.76 o 7 4 5 0.04 0.09 0.21 o 0 5 5 557.08 523.19 3.90 o 1 5 5 65.17 55.30 0.63 o 2 5 5 175.10 182.78 1.33 o 3 5 5 273.16 275.90 2.05 o 4 5 5 117.39 114.18 1.19 o 5 5 5 67.45 69.41 1.08 o 6 5 5 232.75 233.10 2.71 o 7 5 5 57.87 55.89 1.33 o 1 6 5 9.47 13.84 0.34 o 2 6 5 6.93 5.61 0.24 o 3 6 5 148.18 139.98 1.35 o 4 6 5 447.89 461.92 3.12 o 5 6 5 139.51 137.05 1.63 o 6 6 5 44.60 41.75 0.93 o 7 6 5 36.80 36.21 1.43 o 0 7 5 3.78 4.49 0.35 o 1 7 5 227.82 211.06 1.65 o 2 7 5 151.14 148.80 1.27 o 3 7 5 140.18 134.32 1.36 o 4 7 5 18.14 16.92 0.52 o 5 7 5 184.33 184.75 2.14 o 6 7 5 221.37 228.92 2.53 o 1 8 5 82.50 88.63 0.97 o 2 8 5 67.90 64.10 0.90 o 3 8 5 0.98 1.53 0.24 o 4 8 5 164.12 162.31 1.72 o 5 8 5 35.96 35.85 0.89 o 6 8 5 24.42 25.00 0.85 o 0 9 5 293.02 310.57 3.58 o 1 9 5 10.01 6.99 0.33 o 2 9 5 65.95 62.27 0.89 o 3 9 5 117.74 115.55 1.52 o 4 9 5 49.61 46.08 0.94 o 5 9 5 23.44 23.47 0.81 o 1 10 5 20.45 19.08 0.58 o 2 10 5 162.87 167.00 2.06 o 3 10 5 24.31 25.09 0.71 o 4 10 5 208.89 217.31 2.38 o 0 11 5 172.05 196.11 4.34 o 1 11 5 62.16 53.69 0.99 o 2 11 5 79.07 80.06 1.54 o 3 11 5 71.26 71.12 1.44 o 0 0 6 161.54 158.98 2.00 o 1 0 6 666.22 664.89 4.33 o 2 0 6 100.78 90.59 1.09 o 3 0 6 295.73 275.72 2.59 o 4 0 6 203.71 189.02 2.44 o 5 0 6 29.34 29.60 0.90 o 6 0 6 11.89 10.24 0.59 o 7 0 6 40.53 35.26 1.11 o 8 0 6 3.38 3.17 0.63 o 1 1 6 662.79 657.49 3.41 o 2 1 6 18.46 12.18 0.24 o 3 1 6 17.53 13.01 0.30 o 4 1 6 243.22 223.60 1.93 o 5 1 6 50.49 49.54 0.83 o 6 1 6 75.10 71.30 1.07 o 7 1 6 220.83 225.02 2.20 o 0 2 6 172.36 173.91 1.63 o 1 2 6 193.44 172.55 1.22 o 2 2 6 14.28 10.88 0.25 o 3 2 6 491.23 474.80 2.82 o 4 2 6 109.88 104.00 1.26 o 5 2 6 221.01 220.98 2.11 o 6 2 6 13.45 15.05 0.50 o 7 2 6 48.51 48.49 0.93 o 1 3 6 1026.16 1036.12 5.12 o 2 3 6 58.15 60.87 0.66 o 3 3 6 55.01 51.75 0.74 o 4 3 6 157.91 146.55 1.48 o 5 3 6 267.50 269.84 2.44 o 6 3 6 0.52 0.69 0.20 o 7 3 6 124.07 119.47 1.52 o 0 4 6 17.90 10.22 0.42 o 1 4 6 1169.80 1191.69 5.85 o 2 4 6 45.39 46.45 0.59 o 3 4 6 718.35 728.85 4.11 o 4 4 6 0.03 0.47 0.17 o 5 4 6 3.63 3.13 0.31 o 6 4 6 0.99 0.61 0.19 o 7 4 6 4.06 3.70 0.32 o 1 5 6 816.06 859.32 4.45 o 2 5 6 14.12 10.72 0.31 o 3 5 6 113.14 103.96 1.12 o 4 5 6 165.07 159.83 1.72 o 5 5 6 94.86 97.06 1.53 o 6 5 6 7.56 5.72 0.46 o 7 5 6 87.65 88.18 2.06 o 0 6 6 227.92 248.77 2.85 o 1 6 6 43.14 42.11 0.66 o 2 6 6 11.48 11.30 0.33 o 3 6 6 214.60 210.75 2.25 o 4 6 6 151.48 151.22 1.50 o 5 6 6 191.96 199.41 2.11 o 6 6 6 4.18 4.39 0.38 o 1 7 6 160.31 164.41 1.60 o 2 7 6 60.47 61.77 0.82 o 3 7 6 18.62 15.10 0.44 o 4 7 6 92.63 87.47 1.18 o 5 7 6 33.17 30.18 0.81 o 6 7 6 67.99 64.06 1.50 o 0 8 6 71.35 72.23 1.45 o 1 8 6 230.20 237.85 2.11 o 2 8 6 18.50 19.05 0.65 o 3 8 6 152.01 152.07 1.75 o 4 8 6 60.04 64.84 1.10 o 5 8 6 16.88 14.69 0.57 o 1 9 6 363.47 382.09 3.15 o 2 9 6 6.49 5.14 0.39 o 3 9 6 59.01 54.52 1.10 o 4 9 6 90.08 97.37 1.43 o 0 10 6 10.71 10.38 0.69 o 1 10 6 99.46 95.34 1.48 o 2 10 6 2.42 3.10 0.35 o 3 10 6 214.22 230.00 2.74 o 1 11 6 179.27 194.88 2.33 o 2 11 6 4.02 4.01 0.44 o 1 0 7 26.09 20.41 0.51 o 2 0 7 350.81 315.92 2.68 o 3 0 7 6.04 4.86 0.39 o 4 0 7 327.78 326.92 3.66 o 5 0 7 112.44 101.89 1.82 o 6 0 7 50.68 56.43 1.40 o 7 0 7 0.25 0.88 0.34 o 0 1 7 891.85 896.33 6.14 o 1 1 7 55.76 55.17 0.58 o 2 1 7 61.93 61.96 0.66 o 3 1 7 87.90 71.08 0.95 o 4 1 7 21.38 16.43 0.48 o 5 1 7 8.43 7.79 0.39 o 6 1 7 314.25 329.05 2.78 o 7 1 7 75.34 69.20 1.15 o 1 2 7 32.77 30.24 0.44 o 2 2 7 474.80 457.32 2.52 o 3 2 7 60.90 59.14 0.77 o 4 2 7 211.42 200.29 2.28 o 5 2 7 6.11 6.86 0.35 o 6 2 7 41.88 39.64 0.89 o 7 2 7 15.12 13.40 0.54 o 0 3 7 724.58 723.62 5.64 o 1 3 7 201.97 202.40 1.52 o 2 3 7 56.86 59.74 0.66 o 3 3 7 9.11 10.12 0.37 o 4 3 7 14.63 13.14 0.45 o 5 3 7 56.55 55.58 1.00 o 6 3 7 260.06 258.22 2.71 o 7 3 7 1.22 1.13 0.25 o 1 4 7 109.51 100.93 1.00 o 2 4 7 237.05 232.05 1.64 o 3 4 7 183.52 179.66 1.50 o 4 4 7 256.64 254.92 2.52 o 5 4 7 5.34 4.53 0.34 o 6 4 7 54.44 56.56 1.13 o 7 4 7 29.53 26.26 0.78 o 0 5 7 549.68 578.68 4.83 o 1 5 7 221.58 211.97 1.64 o 2 5 7 56.18 57.05 0.85 o 3 5 7 1.61 1.01 0.19 o 4 5 7 10.35 7.80 0.38 o 5 5 7 74.01 69.13 1.22 o 6 5 7 239.59 250.85 3.31 o 1 6 7 86.04 85.30 1.02 o 2 6 7 312.11 317.23 2.52 o 3 6 7 101.08 101.26 1.18 o 4 6 7 158.61 159.21 2.00 o 5 6 7 3.94 2.75 0.30 o 6 6 7 21.62 25.67 0.81 o 0 7 7 488.71 533.33 5.20 o 1 7 7 6.18 5.20 0.32 o 2 7 7 40.14 36.08 0.77 o 3 7 7 78.13 69.59 1.04 o 4 7 7 20.84 19.56 0.70 o 5 7 7 8.10 6.34 0.41 o 1 8 7 5.44 5.87 0.32 o 2 8 7 148.79 162.90 1.85 o 3 8 7 1.59 0.99 0.24 o 4 8 7 144.44 147.20 2.27 o 5 8 7 28.98 29.32 0.89 o 0 9 7 226.68 257.29 3.32 o 1 9 7 104.95 95.10 1.37 o 2 9 7 35.10 34.39 0.88 o 3 9 7 1.45 0.90 0.35 o 4 9 7 3.59 4.17 0.53 o 1 10 7 0.61 0.36 0.35 o 2 10 7 108.69 127.41 1.96 o 0 0 8 121.43 128.18 2.32 o 1 0 8 399.38 377.24 3.14 o 2 0 8 35.09 35.25 0.78 o 3 0 8 461.26 449.87 4.59 o 4 0 8 44.34 42.71 1.12 o 5 0 8 104.41 104.71 1.93 o 6 0 8 44.71 54.32 1.40 o 7 0 8 79.33 79.60 1.80 o 1 1 8 795.83 805.85 4.22 o 2 1 8 1.78 1.98 0.17 o 3 1 8 102.99 94.26 1.17 o 4 1 8 0.07 0.69 0.19 o 5 1 8 107.40 107.94 1.38 o 6 1 8 9.66 8.51 0.41 o 0 2 8 9.32 9.13 0.39 o 1 2 8 761.04 776.83 4.49 o 2 2 8 36.84 32.24 0.49 o 3 2 8 256.17 252.49 2.17 o 4 2 8 0.08 -0.06 0.18 o 5 2 8 2.95 3.07 0.29 o 6 2 8 48.70 48.19 0.94 o 1 3 8 377.41 385.53 2.39 o 2 3 8 84.05 82.79 1.04 o 3 3 8 33.45 27.15 0.63 o 4 3 8 0.95 1.19 0.19 o 5 3 8 1.66 2.27 0.26 o 6 3 8 6.01 6.46 0.41 o 0 4 8 0.28 0.15 0.22 o 1 4 8 48.38 43.86 0.65 o 2 4 8 32.02 29.39 0.60 o 3 4 8 87.56 83.97 1.26 o 4 4 8 4.55 3.27 0.30 o 5 4 8 238.89 240.21 2.59 o 6 4 8 50.31 51.15 1.10 o 1 5 8 295.21 304.54 2.28 o 2 5 8 30.64 25.95 0.59 o 3 5 8 3.22 2.97 0.25 o 4 5 8 0.23 0.63 0.24 o 5 5 8 34.97 32.58 0.84 o 6 5 8 0.02 -0.21 0.21 o 0 6 8 32.62 34.61 0.97 o 1 6 8 611.72 646.66 4.44 o 2 6 8 21.80 18.97 0.52 o 3 6 8 278.15 289.19 2.47 o 4 6 8 8.62 8.49 0.57 o 5 6 8 0.16 0.16 0.22 o 1 7 8 593.85 644.44 4.34 o 2 7 8 0.02 0.33 0.19 o 3 7 8 165.09 161.55 1.94 o 4 7 8 0.01 0.50 0.22 o 0 8 8 34.16 29.33 0.97 o 1 8 8 134.59 139.80 1.72 o 2 8 8 14.15 11.98 0.47 o 3 8 8 187.37 208.04 2.68 o 4 8 8 12.87 12.91 0.71 o 1 9 8 131.18 151.98 1.99 o 2 9 8 9.98 8.21 0.45 o 3 9 8 0.01 -0.09 0.24 o 1 0 9 0.52 0.36 0.19 o 2 0 9 419.87 421.66 4.96 o 3 0 9 153.14 159.28 2.35 o 4 0 9 237.27 228.96 3.06 o 5 0 9 168.56 174.91 2.70 o 6 0 9 0.61 0.95 0.31 o 0 1 9 622.78 625.69 6.48 o 1 1 9 20.10 17.79 0.43 o 2 1 9 53.90 53.78 0.80 o 3 1 9 90.28 97.76 1.24 o 4 1 9 50.73 46.35 0.86 o 5 1 9 0.17 0.11 0.19 o 6 1 9 208.40 212.98 2.52 o 1 2 9 43.59 42.64 0.64 o 2 2 9 155.77 145.67 1.44 o 3 2 9 0.00 0.34 0.17 o 4 2 9 142.21 142.08 1.95 o 5 2 9 45.90 46.66 1.03 o 6 2 9 38.84 40.43 0.95 o 0 3 9 134.12 132.08 1.81 o 1 3 9 19.70 17.10 0.41 o 2 3 9 37.55 37.56 0.69 o 3 3 9 36.26 39.68 0.78 o 4 3 9 10.47 10.42 0.50 o 5 3 9 0.33 0.61 0.21 o 1 4 9 8.05 6.76 0.28 o 2 4 9 17.61 15.94 0.45 o 3 4 9 190.51 194.83 2.36 o 4 4 9 155.22 155.18 2.27 o 5 4 9 73.91 74.22 1.35 o 0 5 9 193.95 218.56 2.55 o 1 5 9 0.18 0.41 0.14 o 2 5 9 39.99 38.22 0.79 o 3 5 9 40.74 38.48 0.95 o 4 5 9 0.22 -0.01 0.20 o 5 5 9 4.99 3.75 0.37 o 1 6 9 43.79 41.81 0.85 o 2 6 9 222.73 236.74 2.87 o 3 6 9 0.51 0.59 0.37 o 4 6 9 109.50 109.80 1.79 o 0 7 9 445.10 484.49 6.08 o 1 7 9 64.64 58.46 1.05 o 2 7 9 29.23 29.83 0.78 o 3 7 9 60.83 64.57 1.44 o 1 8 9 0.45 0.54 0.24 o 2 8 9 148.77 164.08 1.96 o 0 9 9 107.09 135.34 2.34 o 0 0 10 24.41 23.94 1.03 o 1 0 10 320.04 323.44 4.19 o 2 0 10 171.04 164.24 2.76 o 3 0 10 228.04 236.11 3.55 o 4 0 10 70.18 66.85 1.76 o 5 0 10 2.07 2.20 0.44 o 1 1 10 267.80 268.82 2.26 o 2 1 10 149.20 153.50 1.88 o 3 1 10 23.30 19.58 0.64 o 4 1 10 74.74 74.60 1.23 o 5 1 10 53.78 55.05 1.09 o 0 2 10 1.42 1.39 0.24 o 1 2 10 20.83 15.38 0.42 o 2 2 10 93.84 88.80 1.38 o 3 2 10 124.16 122.84 1.69 o 4 2 10 8.19 6.20 0.36 o 5 2 10 85.69 88.05 1.53 o 1 3 10 132.92 133.42 1.34 o 2 3 10 4.16 4.08 0.45 o 3 3 10 0.00 0.01 0.20 o 4 3 10 41.86 43.37 1.00 o 5 3 10 30.82 29.69 0.86 o 0 4 10 68.19 64.27 1.28 o 1 4 10 166.21 165.04 1.74 o 2 4 10 116.67 115.87 1.34 o 3 4 10 109.04 114.02 1.68 o 4 4 10 10.46 8.55 0.46 o 1 5 10 183.38 194.93 2.05 o 2 5 10 19.99 21.58 0.59 o 3 5 10 22.21 19.78 0.68 o 4 5 10 52.38 49.59 1.23 o 0 6 10 29.63 29.41 1.40 o 1 6 10 23.74 23.96 0.69 o 2 6 10 67.72 66.58 1.43 o 3 6 10 104.68 114.54 1.83 o 1 7 10 112.24 122.04 1.74 o 2 7 10 152.65 152.15 2.52 o 1 0 11 169.80 180.84 2.62 o 2 0 11 11.99 10.58 0.74 o 3 0 11 1.46 1.45 0.35 o 4 0 11 73.81 73.15 1.91 o 0 1 11 15.46 14.09 0.59 o 1 1 11 47.24 47.16 0.91 o 2 1 11 51.05 49.14 1.04 o 3 1 11 194.78 215.80 2.48 o 4 1 11 0.11 -0.01 0.22 o 1 2 11 6.01 5.82 0.30 o 2 2 11 4.91 4.27 0.32 o 3 2 11 140.12 145.78 1.97 o 4 2 11 180.83 190.22 2.74 o 0 3 11 66.74 66.85 1.34 o 1 3 11 0.57 0.82 0.19 o 2 3 11 57.55 59.40 1.15 o 3 3 11 55.49 60.45 1.31 o 1 4 11 20.20 21.72 0.74 o 2 4 11 83.99 84.42 1.54 o 3 4 11 24.48 23.76 0.81 o 0 5 11 51.90 55.21 1.78 o 1 5 11 18.98 19.69 0.78 o 2 5 11 34.25 36.25 1.00 o 0 0 12 107.41 107.68 4.91 o 1 0 12 28.14 29.98 1.14 o 2 0 12 47.31 43.88 1.44 o 1 1 12 11.12 9.49 0.44 o 2 1 12 122.01 130.36 2.16 o 0 2 12 5.95 6.92 0.41 o 1 2 12 32.55 28.58 0.78 o 1 3 12 100.35 106.83 2.01 o