#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/65/2216511.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216511_Fobs loop_ _publ_author_name 'Sun, Yanlong' 'Li, Yantuan' 'Cui, Xin' 'Lang, Xiuting' _publ_section_title ; Bromidobis(morpholine-4-dithiocarboxylato-\k^2^S,S')antimony(III) ; _journal_coeditor_code HB2665 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3132 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.060 _cell_angle_beta 81.796 _cell_angle_gamma 76.924 _cell_length_a 6.4280 _cell_length_b 11.1750 _cell_length_c 13.2410 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file hb2665Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 060219d in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13193.70 11413.37 241.35 o 2 0 0 1346.74 1356.78 54.23 o 3 0 0 412.50 336.66 16.90 o 4 0 0 2940.01 2933.26 76.78 o 5 0 0 2279.73 2241.77 65.68 o 6 0 0 2030.61 1927.76 92.87 o 7 0 0 2197.35 2180.29 106.72 o -7 1 0 1718.51 1606.36 90.67 o -6 1 0 873.63 792.61 56.92 o -5 1 0 165.11 199.70 18.73 o -4 1 0 365.08 353.58 19.69 o -3 1 0 4688.89 4551.01 106.09 o -2 1 0 5363.56 5228.82 116.17 o -1 1 0 13433.85 11402.74 389.54 o 1 1 0 29782.63 19798.30 416.21 o 2 1 0 876.35 921.99 27.31 o 3 1 0 1743.78 1697.47 47.37 o 4 1 0 6769.73 6373.07 148.48 o 5 1 0 4004.57 3733.54 97.82 o 6 1 0 1349.58 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