#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/65/2216522.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216522_Fobs loop_ _publ_author_name 'Yuan, Chun-Lan' _publ_section_title ; catena-Poly[{di-\m-azido-bis[azido(N,N-diethylethane-1,2-diamine)copper(II)]} [[azido(N,N-diethylethane-1,2-diamine)copper(II)]-\m-azido]] ; _journal_coeditor_code HG2329 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3148 _journal_page_last m3149 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.478 _cell_angle_gamma 90.000 _cell_length_a 22.7220 _cell_length_b 13.2010 _cell_length_c 11.6488 _exptl_crystal_F_000 1644.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file hg2329Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 294.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 41427.76 46535.27 836.16 o 4 0 0 181.13 208.91 11.32 o 5 0 0 55.60 61.14 5.47 o 6 0 0 7577.26 7810.94 149.17 o 7 0 0 393.08 388.46 25.33 o 8 0 0 4758.08 4915.72 98.00 o 9 0 0 70057.88 72468.38 1304.33 o 10 0 0 0.26 9.60 6.64 o 11 0 0 3568.06 3565.18 77.69 o 12 0 0 72285.10 77536.11 1398.59 o 13 0 0 1554.03 1657.02 53.96 o 14 0 0 0.58 -7.38 8.26 o 15 0 0 4286.23 4174.86 99.70 o 16 0 0 1621.74 1520.08 46.30 o 17 0 0 494.12 487.29 26.85 o 18 0 0 394.50 317.47 27.33 o 19 0 0 146.26 187.31 20.53 o 20 0 0 852.39 975.21 83.08 o 21 0 0 587.88 653.37 44.74 o 22 0 0 0.46 3.29 25.23 o 23 0 0 1197.01 1271.37 91.03 o 24 0 0 1758.02 1749.11 113.52 o 25 0 0 317.87 322.09 57.12 o 26 0 0 96.30 127.50 45.24 o 27 0 0 852.15 658.72 80.52 o 28 0 0 92.29 97.34 46.07 o 29 0 0 92.97 205.92 54.66 o 1 1 0 25285.68 27179.65 423.66 o 2 1 0 22388.60 24316.70 310.79 o 3 1 0 9819.16 10705.35 138.56 o 4 1 0 1811.25 1940.36 31.23 o 5 1 0 79.37 76.85 13.05 o 6 1 0 3271.41 3310.70 47.70 o 7 1 0 628.21 625.97 13.75 o 8 1 0 6641.26 6952.94 95.32 o 9 1 0 19716.35 21290.78 277.08 o 10 1 0 9060.41 9801.96 133.00 o 11 1 0 4068.60 4157.84 62.57 o 12 1 0 38.38 70.71 8.19 o 13 1 0 1513.09 1501.01 30.05 o 14 1 0 90.73 147.93 10.65 o 15 1 0 2230.04 2202.54 47.83 o 16 1 0 28.13 23.27 8.14 o 17 1 0 2060.23 2135.66 41.83 o 18 1 0 1151.64 1227.79 33.80 o 19 1 0 53.65 77.17 12.82 o 20 1 0 26.28 22.06 11.44 o 21 1 0 839.41 917.92 41.60 o 22 1 0 769.10 786.91 52.54 o 23 1 0 27.61 20.85 22.75 o 24 1 0 197.67 160.72 30.57 o 25 1 0 277.29 301.97 39.32 o 26 1 0 187.90 183.09 35.63 o 27 1 0 74.13 117.09 31.50 o 28 1 0 21.95 41.66 28.71 o 0 2 0 86625.87 88895.02 1604.81 o 1 2 0 19054.47 20518.81 262.96 o 2 2 0 0.94 5.11 2.22 o 3 2 0 137.02 175.15 6.82 o 4 2 0 16031.98 17378.62 224.36 o 5 2 0 214.87 193.17 6.89 o 6 2 0 760.24 831.21 18.24 o 7 2 0 14686.13 15026.27 196.85 o 8 2 0 7437.55 7775.61 106.19 o 9 2 0 5430.17 5418.56 77.20 o 10 2 0 57.41 84.23 7.11 o 11 2 0 375.77 391.04 16.26 o 12 2 0 18233.70 18654.45 246.96 o 13 2 0 6333.81 5981.08 87.80 o 14 2 0 287.64 282.78 13.65 o 15 2 0 2819.86 2785.21 75.59 o 16 2 0 8105.77 8124.27 117.93 o 17 2 0 46.02 82.56 20.31 o 18 2 0 299.00 262.96 17.84 o 19 2 0 2333.22 2452.01 54.03 o 20 2 0 1.31 7.71 10.91 o 21 2 0 744.62 694.46 50.75 o 22 2 0 206.62 181.91 24.76 o 23 2 0 19.93 15.40 21.99 o 24 2 0 669.33 728.04 53.64 o 25 2 0 1216.54 1134.80 80.16 o 26 2 0 0.31 18.06 26.28 o 27 2 0 150.93 194.82 58.08 o 28 2 0 1038.15 1087.68 71.88 o 1 3 0 1671.90 1789.18 29.38 o 2 3 0 728.35 890.18 15.90 o 3 3 0 1922.85 2081.13 34.21 o 4 3 0 1931.52 1851.66 29.08 o 5 3 0 8754.39 9334.84 124.36 o 6 3 0 196.34 271.59 9.62 o 7 3 0 388.19 499.16 14.47 o 8 3 0 2213.75 2292.02 38.12 o 9 3 0 6561.38 7010.99 98.10 o 10 3 0 1347.61 1570.80 29.53 o 11 3 0 1549.80 1650.84 31.28 o 12 3 0 1056.81 1118.89 25.00 o 13 3 0 151.99 164.59 13.80 o 14 3 0 43.59 70.34 11.50 o 15 3 0 1297.79 1329.37 30.14 o 16 3 0 318.11 336.59 16.18 o 17 3 0 234.95 221.44 16.74 o 18 3 0 393.15 385.28 20.70 o 19 3 0 82.96 89.67 13.77 o 20 3 0 415.59 467.91 24.05 o 21 3 0 1041.56 1006.48 38.87 o 22 3 0 12.75 10.91 14.22 o 23 3 0 56.97 58.08 23.93 o 24 3 0 276.50 239.16 35.93 o 25 3 0 51.02 24.43 24.30 o 26 3 0 76.04 68.20 40.72 o 27 3 0 5.18 42.12 27.77 o 28 3 0 7.27 39.33 26.52 o 0 4 0 52971.00 58375.63 1051.18 o 1 4 0 13192.76 14290.20 186.64 o 2 4 0 297.51 308.49 10.93 o 3 4 0 1062.46 1181.64 21.18 o 4 4 0 6586.00 6483.61 89.09 o 5 4 0 8155.15 8577.69 116.04 o 6 4 0 2171.60 2359.62 37.85 o 7 4 0 5905.26 5853.32 82.98 o 8 4 0 8559.09 8605.25 118.45 o 9 4 0 13.30 10.11 5.44 o 10 4 0 41.47 44.10 7.66 o 11 4 0 1624.94 1595.40 33.99 o 12 4 0 3438.86 3333.55 54.55 o 13 4 0 9174.62 9187.95 129.78 o 14 4 0 53.31 68.98 9.49 o 15 4 0 5026.76 5054.97 78.82 o 16 4 0 7742.47 7790.36 126.93 o 17 4 0 612.94 593.41 24.47 o 18 4 0 94.19 94.33 13.70 o 19 4 0 3152.37 3125.19 106.33 o 20 4 0 1.32 24.03 14.13 o 21 4 0 1469.45 1386.95 45.82 o 22 4 0 0.31 13.70 15.44 o 23 4 0 67.40 72.82 29.11 o 24 4 0 707.18 802.88 56.53 o 25 4 0 1604.49 1644.08 79.98 o 26 4 0 5.41 -29.85 21.39 o 27 4 0 58.18 77.89 28.04 o 28 4 0 1114.69 1122.89 147.98 o 1 5 0 20384.85 21907.38 311.37 o 2 5 0 5260.29 5178.61 73.23 o 3 5 0 18.16 50.08 20.33 o 4 5 0 1762.90 1782.68 30.57 o 5 5 0 3720.58 3617.49 59.17 o 6 5 0 1885.77 2239.01 37.44 o 7 5 0 5368.16 5116.68 74.78 o 8 5 0 494.54 647.69 17.46 o 9 5 0 1.47 1.39 5.15 o 10 5 0 10143.28 10523.72 145.40 o 11 5 0 8.94 24.73 10.21 o 12 5 0 2949.91 2930.05 50.34 o 13 5 0 1755.24 1796.51 36.13 o 14 5 0 195.24 189.01 12.93 o 15 5 0 96.15 119.92 13.47 o 16 5 0 212.51 215.94 17.64 o 17 5 0 1158.49 1273.46 35.63 o 18 5 0 660.39 637.81 26.58 o 19 5 0 383.33 436.63 23.60 o 20 5 0 1630.59 1629.82 89.34 o 21 5 0 22.98 28.00 15.02 o 22 5 0 2057.88 2063.74 59.74 o 23 5 0 141.84 156.89 21.85 o 24 5 0 215.32 258.14 54.89 o 25 5 0 1289.44 1133.65 66.95 o 26 5 0 2.61 -31.52 21.02 o 27 5 0 103.85 163.70 50.00 o 0 6 0 71904.19 74708.41 1346.07 o 1 6 0 942.11 951.37 20.42 o 2 6 0 835.96 860.40 18.86 o 3 6 0 20632.05 20976.06 274.42 o 4 6 0 160.04 180.51 9.20 o 5 6 0 1485.29 1575.82 29.49 o 6 6 0 589.90 661.48 19.00 o 7 6 0 1338.54 1247.60 26.09 o 8 6 0 1212.55 1364.04 35.82 o 9 6 0 12902.07 13110.66 178.48 o 10 6 0 36.29 39.68 7.78 o 11 6 0 595.03 550.25 18.63 o 12 6 0 16322.57 16079.03 218.19 o 13 6 0 1680.24 1715.53 72.11 o 14 6 0 606.95 603.23 23.82 o 15 6 0 3156.55 3226.91 63.84 o 16 6 0 11.47 8.30 10.18 o 17 6 0 160.10 199.04 17.49 o 18 6 0 61.58 77.92 13.88 o 19 6 0 183.17 197.72 18.29 o 20 6 0 1023.08 1002.32 47.22 o 21 6 0 1416.80 1525.13 73.97 o 22 6 0 423.02 372.40 34.75 o 23 6 0 731.77 736.24 45.49 o 24 6 0 1072.49 1046.56 67.43 o 25 6 0 255.49 293.85 59.68 o 26 6 0 72.71 58.31 39.30 o 27 6 0 513.41 494.56 76.23 o 1 7 0 1858.40 1791.29 32.17 o 2 7 0 456.47 435.32 15.47 o 3 7 0 14125.50 14569.81 195.13 o 4 7 0 9212.22 9790.71 135.19 o 5 7 0 203.38 270.27 17.62 o 6 7 0 5636.82 5157.46 77.20 o 7 7 0 963.50 879.99 22.14 o 8 7 0 1162.24 1139.21 28.54 o 9 7 0 4418.46 4285.88 67.97 o 10 7 0 416.37 441.83 17.08 o 11 7 0 4460.59 4407.61 75.13 o 12 7 0 1110.30 1115.09 28.10 o 13 7 0 144.44 195.30 25.87 o 14 7 0 338.76 358.18 20.02 o 15 7 0 349.30 344.35 24.16 o 16 7 0 2741.77 2602.64 70.67 o 17 7 0 192.82 218.26 21.72 o 18 7 0 360.63 367.10 26.56 o 19 7 0 1.06 10.33 16.02 o 20 7 0 227.79 287.53 41.10 o 21 7 0 1181.23 1263.10 54.15 o 22 7 0 111.87 156.87 26.71 o 23 7 0 524.97 599.35 43.17 o 24 7 0 608.22 857.42 63.87 o 25 7 0 2.60 17.21 26.17 o 26 7 0 306.38 298.42 63.89 o 0 8 0 13018.89 13348.43 255.08 o 1 8 0 341.45 288.38 16.23 o 2 8 0 1801.19 1707.54 36.56 o 3 8 0 4676.77 4456.41 76.29 o 4 8 0 4326.53 4286.37 66.55 o 5 8 0 3025.19 3117.55 58.45 o 6 8 0 413.26 395.31 18.95 o 7 8 0 9158.72 9084.85 284.80 o 8 8 0 513.21 487.63 24.58 o 9 8 0 1814.17 1715.44 41.06 o 10 8 0 60.57 46.48 10.68 o 11 8 0 1193.42 1228.74 44.84 o 12 8 0 1499.34 1459.47 61.20 o 13 8 0 853.72 845.14 35.00 o 14 8 0 54.42 40.98 13.75 o 15 8 0 36.62 40.04 14.29 o 16 8 0 500.11 563.63 30.58 o 17 8 0 168.00 233.04 22.90 o 18 8 0 5.30 5.85 13.74 o 19 8 0 1467.80 1556.02 125.24 o 20 8 0 5.15 16.27 18.41 o 21 8 0 466.55 446.53 37.67 o 22 8 0 0.52 -15.69 18.59 o 23 8 0 195.19 257.67 55.15 o 24 8 0 8.85 14.11 24.77 o 25 8 0 60.28 106.58 30.96 o 1 9 0 4959.39 4952.21 158.53 o 2 9 0 803.53 880.36 26.09 o 3 9 0 1225.97 1249.36 31.88 o 4 9 0 1126.93 1020.82 28.89 o 5 9 0 1046.17 960.45 40.23 o 6 9 0 2938.14 2956.52 141.07 o 7 9 0 281.29 286.66 17.69 o 8 9 0 4053.87 4015.15 74.46 o 9 9 0 2891.65 2983.67 60.55 o 10 9 0 438.63 451.29 22.38 o 11 9 0 2657.80 2526.53 62.36 o 12 9 0 581.42 645.35 30.88 o 13 9 0 41.39 36.75 13.96 o 14 9 0 10.76 13.44 13.68 o 15 9 0 160.10 196.13 21.54 o 16 9 0 89.41 60.59 24.91 o 17 9 0 22.86 27.52 15.31 o 18 9 0 1141.47 1257.80 117.81 o 19 9 0 125.54 122.10 26.35 o 20 9 0 18.83 20.80 19.51 o 21 9 0 1286.67 1327.46 155.76 o 22 9 0 17.19 19.47 21.01 o 23 9 0 234.79 259.01 32.56 o 24 9 0 168.22 191.20 37.46 o 0 10 0 1183.48 1136.18 51.87 o 1 10 0 118.05 105.84 16.19 o 2 10 0 1340.55 1254.60 45.91 o 3 10 0 43.74 41.31 12.67 o 4 10 0 3319.37 3047.97 69.40 o 5 10 0 3310.87 3210.47 83.98 o 6 10 0 27.49 46.80 13.67 o 7 10 0 3611.88 3612.45 81.30 o 8 10 0 2046.96 2043.42 49.94 o 9 10 0 16.53 10.01 10.55 o 10 10 0 692.97 814.39 34.56 o 11 10 0 658.38 621.73 31.19 o 12 10 0 38.66 43.28 14.98 o 13 10 0 545.26 531.93 31.14 o 14 10 0 138.73 166.14 20.49 o 15 10 0 9.39 -0.27 13.06 o 16 10 0 961.63 1090.86 43.72 o 17 10 0 386.01 508.31 32.49 o 18 10 0 201.48 251.32 30.80 o 19 10 0 2003.40 1942.98 99.29 o 20 10 0 370.60 459.90 39.41 o 21 10 0 272.91 300.25 34.41 o 22 10 0 44.52 52.04 23.20 o 23 10 0 8.93 4.53 20.67 o 1 11 0 47.64 22.21 12.49 o 2 11 0 3317.03 3274.45 74.88 o 3 11 0 829.34 750.39 32.82 o 4 11 0 82.81 98.28 16.44 o 5 11 0 2592.33 2406.13 61.25 o 6 11 0 156.54 171.39 19.45 o 7 11 0 1927.22 1997.67 55.32 o 8 11 0 947.60 960.67 37.50 o 9 11 0 229.83 267.69 28.64 o 10 11 0 2220.17 2340.07 73.29 o 11 11 0 15.96 34.18 17.54 o 12 11 0 448.59 450.06 34.79 o 13 11 0 240.44 249.47 30.80 o 14 11 0 502.48 504.51 38.00 o 15 11 0 21.41 -1.44 15.06 o 16 11 0 64.11 59.78 18.24 o 17 11 0 1562.19 1661.77 123.52 o 18 11 0 65.10 72.18 25.02 o 19 11 0 445.40 492.30 40.51 o 20 11 0 247.78 299.01 34.10 o 21 11 0 32.57 22.52 21.10 o 0 12 0 732.80 694.57 46.98 o 1 12 0 2171.69 2071.26 57.68 o 2 12 0 1542.89 1560.50 48.91 o 3 12 0 157.55 179.66 20.09 o 4 12 0 67.65 67.28 15.84 o 5 12 0 138.22 160.26 19.73 o 6 12 0 197.69 204.55 21.26 o 7 12 0 75.88 107.98 18.25 o 8 12 0 9.14 -4.51 15.90 o 9 12 0 1150.64 1296.42 54.18 o 10 12 0 695.22 737.97 43.46 o 11 12 0 408.36 392.90 40.19 o 12 12 0 1145.78 1223.27 70.57 o 13 12 0 197.24 192.38 27.09 o 14 12 0 829.31 839.63 47.48 o 15 12 0 121.60 157.07 27.38 o 16 12 0 87.61 107.76 24.63 o 17 12 0 298.83 266.41 41.51 o 18 12 0 608.70 686.51 59.78 o 19 12 0 35.67 12.68 33.32 o 20 12 0 84.08 93.57 32.67 o 1 13 0 582.06 488.86 30.62 o 2 13 0 128.41 77.98 18.07 o 3 13 0 1479.93 1503.13 49.62 o 4 13 0 293.74 329.64 26.92 o 5 13 0 165.34 197.92 21.92 o 6 13 0 1105.80 1141.05 69.87 o 7 13 0 225.35 228.81 29.07 o 8 13 0 226.23 292.95 31.76 o 9 13 0 140.80 124.25 53.42 o 10 13 0 19.98 44.71 21.07 o 11 13 0 261.45 263.10 42.37 o 12 13 0 20.38 11.91 20.15 o 13 13 0 181.59 175.82 42.88 o 14 13 0 0.17 -0.18 19.80 o 15 13 0 347.90 385.09 37.90 o 16 13 0 115.39 139.98 36.39 o 17 13 0 284.05 283.25 43.32 o 18 13 0 151.62 180.34 37.00 o 0 14 0 236.31 272.78 36.50 o 1 14 0 500.03 481.06 39.18 o 2 14 0 1069.06 1072.50 43.82 o 3 14 0 6.53 5.33 14.57 o 4 14 0 0.26 14.66 15.41 o 5 14 0 366.74 431.07 30.92 o 6 14 0 92.42 124.90 37.52 o 7 14 0 151.86 187.05 28.37 o 8 14 0 135.50 145.03 27.82 o 9 14 0 179.79 250.18 38.19 o 10 14 0 184.21 198.96 29.63 o 11 14 0 302.95 366.52 36.84 o 12 14 0 1.18 -2.81 19.83 o 13 14 0 179.39 192.34 30.65 o 14 14 0 883.65 957.48 71.78 o 15 14 0 82.92 120.90 36.31 o 16 14 0 13.42 36.29 28.56 o 1 15 0 259.44 212.14 24.97 o 2 15 0 0.25 -16.18 15.61 o 3 15 0 704.64 698.63 39.08 o 4 15 0 306.50 293.10 27.63 o 5 15 0 62.24 28.26 20.30 o 6 15 0 429.10 456.25 39.89 o 7 15 0 114.54 129.75 27.00 o 8 15 0 302.23 317.66 42.82 o 9 15 0 202.81 248.17 32.88 o 10 15 0 9.95 -6.20 29.21 o 11 15 0 72.10 67.50 24.80 o 12 15 0 3.87 4.73 22.24 o 13 15 0 125.45 201.34 63.14 o 0 16 0 104.87 91.68 30.53 o 1 16 0 37.08 46.05 19.34 o 2 16 0 805.58 741.34 41.85 o 3 16 0 253.32 286.87 28.71 o 4 16 0 305.19 368.59 37.98 o 5 16 0 328.03 402.24 61.25 o 6 16 0 5.10 5.14 21.20 o 7 16 0 255.94 241.83 33.90 o 8 16 0 128.59 135.26 30.38 o 9 16 0 3.12 10.69 24.43 o -28 1 1 14.33 15.65 26.78 o -27 1 1 826.41 927.13 75.27 o -26 1 1 6.27 10.49 23.29 o -25 1 1 70.73 86.58 27.75 o -24 1 1 236.64 222.65 35.58 o -23 1 1 43.18 28.14 16.08 o -22 1 1 121.48 146.65 19.71 o -21 1 1 2913.45 2840.34 81.12 o -20 1 1 145.10 149.16 18.27 o -19 1 1 150.82 178.94 16.19 o -18 1 1 6802.43 6585.54 138.62 o -17 1 1 910.33 948.87 29.31 o -16 1 1 3.76 7.95 7.61 o -15 1 1 6124.85 5784.96 86.87 o -14 1 1 480.44 426.83 15.73 o -13 1 1 491.69 505.68 16.18 o -12 1 1 1875.72 1864.99 34.08 o -11 1 1 7730.86 7911.58 110.10 o -10 1 1 198.13 261.46 19.61 o -9 1 1 41463.32 44969.85 575.69 o -8 1 1 9597.73 9694.80 129.81 o -7 1 1 24.60 27.96 3.89 o -6 1 1 7299.83 7006.27 94.35 o -5 1 1 3406.79 3424.84 48.15 o -4 1 1 264.77 263.02 9.71 o -3 1 1 58865.54 59940.52 933.65 o -2 1 1 33828.45 37333.23 583.92 o -1 1 1 13093.15 14619.44 205.57 o 0 1 1 101.03 142.90 6.34 o 1 1 1 48391.53 51283.72 653.20 o 2 1 1 22310.75 24409.53 341.82 o 3 1 1 47737.14 50596.73 783.94 o 4 1 1 2054.74 2226.68 32.79 o 5 1 1 7191.23 7354.30 97.99 o 6 1 1 1130.81 1053.01 20.25 o 7 1 1 1971.63 1873.46 30.16 o 8 1 1 440.57 385.68 11.36 o 9 1 1 20913.31 23349.68 303.38 o 10 1 1 31798.17 34167.75 481.17 o 11 1 1 11418.69 12298.45 165.87 o 12 1 1 40.84 32.63 6.78 o 13 1 1 5894.73 6029.55 88.39 o 14 1 1 7207.18 7213.01 104.43 o 15 1 1 1118.61 1112.04 34.00 o 16 1 1 170.82 190.58 12.82 o 17 1 1 4773.97 4729.95 75.59 o 18 1 1 1424.22 1486.98 36.80 o 19 1 1 429.39 473.15 22.59 o 20 1 1 97.58 109.34 19.24 o 21 1 1 322.89 378.49 30.72 o 22 1 1 2522.74 2538.56 187.41 o 23 1 1 1023.29 1029.71 58.61 o 24 1 1 105.55 128.37 29.14 o 25 1 1 483.27 422.16 45.84 o 26 1 1 1938.91 2137.06 105.02 o 27 1 1 37.42 43.41 27.79 o 28 1 1 9.46 38.22 29.19 o -28 2 1 6.68 17.79 26.52 o -27 2 1 442.72 462.02 48.91 o -26 2 1 22.10 29.32 26.83 o -25 2 1 21.78 14.58 23.44 o -24 2 1 697.30 757.72 44.50 o -23 2 1 428.87 373.71 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