#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/65/2216572.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2216572_Fobs
loop_
_publ_author_name
'Yousefi, Mohammad'
'Ahmadi, Roya'
'Amani, Vahid'
'Khavasi, Hamid Reza'
_publ_section_title
;
 Bis(2,9-dimethyl-1,10-phenanthrolinium) hexachloridoplatinate(IV)
;
_journal_coeditor_code           HK2386
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m3114
_journal_page_last               m3115
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                78.427
_cell_angle_beta                 66.464
_cell_angle_gamma                79.540
_cell_length_a                   8.9617
_cell_length_b                   9.2179
_cell_length_c                   9.9930
_exptl_crystal_F_000             2340.00
_reflns_d_resolution_high        0.7296
_[local]_cod_data_source_file    hk2386Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' W7'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            91.84
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 579.52 405.73 4.49 o
3 0 0 3591.36 3164.84 121.45 o
4 0 0 5647.82 5093.99 425.73 o
5 0 0 3382.65 2833.46 106.54 o
6 0 0 1777.07 1463.35 228.04 o
7 0 0 2746.72 2242.69 382.72 o
8 0 0 2423.96 2317.86 37.04 o
9 0 0 445.19 382.04 38.41 o
10 0 0 72.40 65.31 1.74 o
11 0 0 286.95 263.29 17.50 o
-11 1 0 323.28 326.82 38.17 o
-10 1 0 459.00 425.50 15.95 o
-9 1 0 1848.19 1799.00 110.10 o
-8 1 0 2525.04 2845.08 385.37 o
-7 1 0 2615.11 2488.22 70.18 o
-6 1 0 1578.01 1371.65 44.31 o
-5 1 0 2801.59 2354.14 74.83 o
-2 1 0 4926.75 3116.42 17.12 o
0 1 0 1740.11 2439.17 48.78 o
3 1 0 148.87 125.71 2.74 o
4 1 0 2263.59 2142.18 6.12 o
5 1 0 1149.47 819.58 42.81 o
6 1 0 738.64 615.02 53.15 o
7 1 0 1092.52 1003.51 87.39 o
8 1 0 1077.19 962.50 82.23 o
9 1 0 606.00 580.80 6.77 o
10 1 0 101.63 89.37 1.77 o
11 1 0 57.83 63.72 7.83 o
-10 2 0 530.74 471.84 4.38 o
-9 2 0 325.68 278.53 34.02 o
-8 2 0 2382.74 2346.69 5.62 o
-7 2 0 2836.05 2583.36 7.58 o
-6 2 0 586.40 589.36 91.02 o
-5 2 0 293.22 231.89 20.62 o
-4 2 0 731.06 740.95 168.24 o
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-1 2 0 2688.24 2756.71 76.46 o
0 2 0 3820.57 4790.49 15.57 o
2 2 0 57.90 74.75 3.50 o
3 2 0 147.22 149.80 22.41 o
4 2 0 717.62 690.24 35.59 o
5 2 0 3255.30 2847.38 78.94 o
6 2 0 2523.17 2471.92 18.65 o
7 2 0 735.29 622.75 49.94 o
8 2 0 1270.13 1284.44 26.13 o
9 2 0 776.46 722.87 21.25 o
10 2 0 349.59 351.64 5.25 o
11 2 0 195.94 191.11 2.18 o
-10 3 0 315.55 342.65 40.68 o
-9 3 0 275.73 260.37 5.98 o
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-6 3 0 1147.75 1074.04 120.42 o
-5 3 0 56.33 70.36 9.59 o
-4 3 0 489.52 514.31 55.45 o
-2 3 0 4163.87 4477.38 10.50 o
-1 3 0 3678.14 4036.64 59.69 o
0 3 0 5039.69 6030.82 183.61 o
1 3 0 4231.67 4488.17 144.81 o
2 3 0 1341.96 1388.87 18.26 o
3 3 0 1869.24 1791.58 43.77 o
4 3 0 3013.11 3172.58 127.96 o
5 3 0 6787.18 6425.35 9.14 o
6 3 0 3907.48 3768.18 9.69 o
7 3 0 1639.08 1531.17 4.33 o
8 3 0 1114.22 1079.67 28.59 o
9 3 0 1427.04 1455.08 60.44 o
10 3 0 728.73 722.14 20.17 o
11 3 0 266.37 268.94 13.11 o
-10 4 0 439.65 436.22 18.88 o
-9 4 0 508.16 510.98 46.55 o
-8 4 0 508.11 540.20 26.49 o
-7 4 0 1217.80 1258.51 97.66 o
-6 4 0 1273.89 1277.04 100.00 o
-5 4 0 824.30 886.53 96.17 o
-4 4 0 1647.28 1803.22 94.41 o
-3 4 0 4359.39 4951.79 9.87 o
0 4 0 3630.07 3897.84 19.45 o
3 4 0 1316.86 1274.85 32.09 o
4 4 0 3925.14 4105.59 27.95 o
5 4 0 6818.69 6956.28 124.54 o
6 4 0 3675.38 3441.33 175.26 o
7 4 0 1585.02 1448.15 15.01 o
8 4 0 517.87 521.01 2.68 o
9 4 0 638.91 627.43 22.82 o
10 4 0 523.64 547.83 26.00 o
-9 5 0 883.75 925.09 62.11 o
-8 5 0 473.75 498.45 45.32 o
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-6 5 0 1967.56 2078.08 249.40 o
-5 5 0 3100.27 3027.15 888.64 o
-4 5 0 1413.35 1747.58 257.01 o
-3 5 0 3863.66 4436.99 8.94 o
-1 5 0 3708.88 3848.42 68.34 o
0 5 0 1322.61 1250.84 25.02 o
1 5 0 3188.88 3555.84 88.45 o
2 5 0 4668.36 4946.49 107.94 o
3 5 0 1547.10 1526.96 82.73 o
4 5 0 431.99 341.93 9.85 o
5 5 0 1541.85 1461.77 48.63 o
6 5 0 4056.06 3964.31 69.40 o
7 5 0 529.81 476.23 8.96 o
8 5 0 32.88 42.96 1.89 o
9 5 0 217.51 210.69 14.25 o
10 5 0 298.91 332.27 2.60 o
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-7 6 0 743.95 719.56 104.66 o
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-5 6 0 126.55 153.55 34.60 o
-4 6 0 708.98 680.59 136.58 o
-3 6 0 6634.28 6676.57 957.24 o
-2 6 0 3076.15 3296.91 111.62 o
-1 6 0 840.92 851.65 19.85 o
0 6 0 135.10 114.98 12.73 o
1 6 0 169.46 198.00 4.37 o
2 6 0 1007.76 941.51 20.22 o
3 6 0 1573.94 1452.58 8.80 o
4 6 0 1857.25 1843.47 65.44 o
5 6 0 1450.36 1420.54 6.70 o
6 6 0 594.56 524.94 16.62 o
7 6 0 460.09 424.83 11.65 o
8 6 0 306.86 314.22 2.01 o
9 6 0 153.70 143.47 9.02 o
10 6 0 569.19 603.20 41.16 o
-8 7 0 186.84 194.29 9.82 o
-7 7 0 57.96 63.70 2.88 o
-6 7 0 379.97 432.64 42.93 o
-5 7 0 1755.21 1766.59 168.72 o
-4 7 0 926.01 879.45 5.50 o
-3 7 0 51.29 55.90 3.50 o
-2 7 0 1931.65 1948.11 44.75 o
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0 7 0 378.32 358.78 8.88 o
1 7 0 319.03 325.47 4.62 o
2 7 0 908.58 918.16 25.29 o
3 7 0 3365.32 3432.69 112.21 o
4 7 0 2293.86 2240.54 57.01 o
5 7 0 1208.33 1169.33 45.14 o
6 7 0 1883.48 1830.70 63.21 o
7 7 0 1568.81 1547.61 13.28 o
8 7 0 445.83 456.39 6.99 o
9 7 0 340.69 352.02 10.61 o
-7 8 0 60.15 62.74 3.07 o
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-3 8 0 1845.74 1733.34 87.64 o
-2 8 0 1523.91 1652.61 109.93 o
-1 8 0 1739.11 1761.53 48.91 o
0 8 0 2403.75 2462.01 114.69 o
1 8 0 578.85 595.71 26.48 o
2 8 0 2274.62 2295.60 72.67 o
3 8 0 5328.89 5657.14 176.72 o
4 8 0 2795.19 2876.89 137.65 o
5 8 0 1509.29 1237.75 228.60 o
6 8 0 1009.78 983.68 45.49 o
7 8 0 1090.83 1020.62 35.22 o
8 8 0 561.26 521.14 16.50 o
9 8 0 301.36 296.45 16.95 o
-6 9 0 493.84 507.49 17.90 o
-5 9 0 1640.78 1503.31 205.85 o
-4 9 0 2635.01 2516.20 225.56 o
-3 9 0 1549.97 1419.20 58.09 o
-2 9 0 1054.30 1110.04 35.17 o
-1 9 0 1584.63 1572.48 76.39 o
0 9 0 1333.86 1319.49 44.50 o
1 9 0 1078.22 1071.52 53.84 o
2 9 0 1679.43 1673.93 80.32 o
3 9 0 2056.12 2067.57 26.60 o
4 9 0 2055.39 2126.79 94.08 o
5 9 0 414.60 437.40 13.82 o
6 9 0 201.49 218.66 12.81 o
7 9 0 391.04 370.01 18.05 o
8 9 0 342.83 340.81 12.23 o
-5 10 0 1057.76 1059.67 48.20 o
-4 10 0 1377.13 1314.87 70.28 o
-3 10 0 673.90 628.78 18.60 o
-2 10 0 307.84 287.42 11.00 o
-1 10 0 479.33 466.51 8.36 o
0 10 0 467.52 484.26 26.71 o
1 10 0 429.45 396.81 15.98 o
2 10 0 447.97 461.73 25.53 o
3 10 0 924.86 977.49 75.85 o
4 10 0 963.29 1032.57 33.44 o
5 10 0 237.92 227.61 8.61 o
6 10 0 80.36 80.94 4.79 o
7 10 0 137.08 149.27 7.81 o
-4 11 0 433.96 392.10 3.13 o
-3 11 0 314.09 278.14 11.11 o
-2 11 0 96.47 98.39 9.89 o
-1 11 0 261.05 259.50 11.09 o
0 11 0 591.98 588.67 15.07 o
1 11 0 395.27 358.98 18.98 o
2 11 0 419.61 414.37 23.86 o
3 11 0 1064.83 1098.46 63.03 o
4 11 0 772.96 772.51 40.34 o
5 11 0 444.65 446.96 53.32 o
6 11 0 189.20 177.19 9.44 o
-1 12 0 127.56 112.31 6.20 o
0 12 0 743.65 781.36 39.78 o
1 12 0 2121.18 2080.11 188.83 o
2 12 0 1249.35 1256.93 108.44 o
3 12 0 356.55 321.91 29.72 o
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-1 -12 1 887.82 850.40 86.67 o
0 -12 1 912.47 832.92 69.38 o
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-4 -11 1 285.77 271.67 10.47 o
-3 -11 1 198.12 197.95 25.77 o
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-1 -11 1 913.97 917.94 101.73 o
0 -11 1 950.68 1028.19 97.58 o
1 -11 1 309.50 346.73 30.46 o
2 -11 1 39.64 37.67 2.59 o
3 -11 1 180.91 157.04 5.07 o
-6 -10 1 92.95 105.73 7.25 o
-5 -10 1 174.08 179.03 7.32 o
-4 -10 1 338.66 360.34 26.35 o
-3 -10 1 338.99 337.70 19.00 o
-2 -10 1 288.90 293.16 17.82 o
-1 -10 1 1205.19 1236.25 110.80 o
0 -10 1 1729.32 1717.76 131.81 o
1 -10 1 569.22 616.29 35.04 o
2 -10 1 117.47 117.84 7.38 o
3 -10 1 539.73 546.01 39.13 o
4 -10 1 888.46 820.26 102.30 o
5 -10 1 909.20 808.99 119.26 o
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-7 -9 1 506.86 539.18 19.56 o
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-3 -9 1 1876.43 1928.21 74.54 o
-2 -9 1 1155.61 1186.01 53.44 o
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4 -9 1 1543.42 1452.95 33.59 o
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6 -9 1 883.18 952.60 4.48 o
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2 -8 1 671.14 725.26 36.93 o
3 -8 1 307.55 298.63 7.55 o
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5 -8 1 1442.38 1364.89 195.77 o
6 -8 1 553.77 613.05 3.76 o
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-6 -7 1 543.24 505.90 12.10 o
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-1 -7 1 3274.58 3355.37 129.41 o
0 -7 1 569.61 535.41 9.37 o
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2 -7 1 860.67 915.69 46.33 o
3 -7 1 1333.39 1281.37 34.59 o
4 -7 1 951.26 897.91 71.74 o
5 -7 1 1265.61 1299.70 174.97 o
6 -7 1 785.58 724.22 31.71 o
7 -7 1 116.54 138.92 2.19 o
8 -7 1 106.32 107.59 2.10 o
-9 -6 1 236.71 276.04 16.76 o
-8 -6 1 35.29 44.00 3.82 o
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-6 -6 1 1033.38 1022.21 4.99 o
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-3 -6 1 1996.80 1778.94 48.82 o
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0 -6 1 63.79 66.24 3.03 o
1 -6 1 4189.24 4367.70 322.27 o
2 -6 1 1753.97 1808.20 75.76 o
3 -6 1 209.37 197.64 10.76 o
4 -6 1 1197.71 1082.14 186.13 o
5 -6 1 2985.13 3075.81 225.87 o
6 -6 1 2807.96 2852.20 196.35 o
7 -6 1 497.86 539.88 36.53 o
8 -6 1 295.40 291.03 11.88 o
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-10 -5 1 398.38 430.36 13.45 o
-9 -5 1 285.73 328.02 24.53 o
-8 -5 1 297.17 293.46 2.67 o
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-6 -5 1 808.65 711.63 6.93 o
-5 -5 1 1297.01 1242.47 33.16 o
-4 -5 1 1602.69 1448.80 51.30 o
-3 -5 1 4976.13 4890.61 112.74 o
-2 -5 1 6356.94 6229.90 13.00 o
-1 -5 1 1607.45 1564.99 47.47 o
0 -5 1 909.29 723.73 137.91 o
1 -5 1 3066.37 3062.25 61.68 o
2 -5 1 5259.99 5654.78 79.10 o
3 -5 1 5361.10 5914.96 10.14 o
4 -5 1 2616.38 2656.95 149.52 o
5 -5 1 3925.39 4059.92 596.17 o
6 -5 1 2623.32 2934.64 469.26 o
7 -5 1 1007.29 1081.71 108.13 o
8 -5 1 442.13 475.09 35.67 o
9 -5 1 604.65 613.20 16.42 o
-10 -4 1 779.43 877.94 32.22 o
-9 -4 1 878.86 925.69 5.98 o
-8 -4 1 328.76 341.00 9.08 o
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-6 -4 1 2549.80 2312.12 33.88 o
-5 -4 1 2900.69 2669.60 39.35 o
-4 -4 1 5021.05 4781.73 166.23 o
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0 -4 1 2303.90 2374.30 65.96 o
1 -4 1 1226.95 1149.70 11.72 o
4 -4 1 2170.92 2173.65 375.31 o
5 -4 1 1596.69 1616.78 217.34 o
6 -4 1 1507.82 1710.00 164.80 o
7 -4 1 1011.24 1059.29 53.83 o
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9 -4 1 309.30 331.67 19.94 o
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-10 -3 1 885.51 1021.85 38.95 o
-9 -3 1 1255.10 1262.23 22.82 o
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-7 -3 1 817.95 821.00 26.81 o
-6 -3 1 2668.51 2462.90 6.80 o
-5 -3 1 5641.03 5566.82 45.22 o
-4 -3 1 3342.47 2938.95 29.69 o
-3 -3 1 2219.17 2000.93 58.32 o
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0 -3 1 306.48 287.80 7.50 o
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4 -3 1 3572.63 4070.44 8.67 o
5 -3 1 133.40 127.24 7.04 o
6 -3 1 427.43 442.04 57.53 o
7 -3 1 1010.76 940.41 22.32 o
8 -3 1 232.63 210.18 5.36 o
9 -3 1 205.10 189.09 5.88 o
10 -3 1 577.22 544.64 8.18 o
-10 -2 1 465.74 519.24 4.09 o
-9 -2 1 455.33 447.80 12.28 o
-8 -2 1 604.58 582.79 25.49 o
-7 -2 1 318.71 309.80 23.88 o
-6 -2 1 1294.08 1143.69 53.20 o
-5 -2 1 4076.25 3708.80 30.43 o
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-2 -2 1 1227.43 1013.60 26.67 o
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1 -2 1 1015.76 1069.09 27.22 o
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0 0 1 4242.60 5607.16 215.49 o
5 0 1 1793.76 1750.37 97.87 o
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8 0 1 1739.55 1590.60 4.62 o
9 0 1 1226.49 1240.96 66.21 o
10 0 1 334.64 422.12 76.07 o
11 0 1 334.05 370.89 85.90 o
-10 1 1 162.04 170.93 2.33 o
-9 1 1 474.43 490.79 2.97 o
-8 1 1 1779.51 1841.79 69.30 o
-7 1 1 3066.57 2926.69 11.84 o
-6 1 1 3100.05 2836.25 100.01 o
-5 1 1 3317.01 2629.58 147.41 o
-4 1 1 5360.92 4324.76 12.40 o
-3 1 1 4568.70 4057.22 205.14 o
-2 1 1 59.16 59.39 2.16 o
-1 1 1 3478.97 3945.60 197.74 o
3 1 1 715.12 735.85 5.80 o
4 1 1 1690.85 1640.06 23.63 o
5 1 1 1101.40 1139.79 85.03 o
6 1 1 133.24 101.10 3.13 o
7 1 1 595.89 557.76 45.37 o
8 1 1 1566.35 1340.46 99.72 o
9 1 1 1093.75 1037.13 32.46 o
10 1 1 194.69 198.33 14.56 o
11 1 1 115.99 106.03 2.14 o
-10 2 1 379.34 370.72 20.01 o
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-6 2 1 1258.50 1096.66 151.92 o
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4 4 13 241.18 236.91 3.26 o
5 4 13 291.52 242.44 3.42 o
6 4 13 359.20 333.17 3.05 o
7 4 13 296.13 273.54 14.71 o
8 4 13 1104.36 1153.63 5.78 o
3 5 13 94.64 90.72 2.25 o
4 5 13 269.23 258.38 3.41 o
5 5 13 919.14 1053.21 4.94 o
6 5 13 1011.60 1092.21 5.10 o
7 5 13 630.41 620.30 16.00 o
4 6 13 494.42 484.98 3.84 o
5 6 13 1123.26 1188.95 5.32 o
6 6 13 1180.65 1078.35 5.00 o