#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/66/2216600.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216600_Fobs loop_ _publ_author_name 'Jing, Zuo-Liang' 'Yu, Ming' 'Chen, Xin' _publ_section_title ; (E)-N'-(5-Bromo-2-hydroxybenzylidene)-4-hydroxybenzohydrazide ethanol solvate ; _journal_coeditor_code IS2249 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4902 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 129.479 _cell_angle_gamma 90.000 _cell_length_a 17.8726 _cell_length_b 17.8342 _cell_length_c 12.9547 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file is2249Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R070411E in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 326.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2481.39 2851.72 82.95 o 6 0 0 29408.43 29790.27 1084.53 o 8 0 0 8948.75 7178.14 259.36 o 10 0 0 19908.98 18911.44 834.13 o 12 0 0 1883.38 1700.25 205.92 o 14 0 0 2946.29 2704.00 345.25 o 16 0 0 723.92 1160.54 585.89 o 1 1 0 6436.55 5814.69 253.87 o 3 1 0 5228.03 4965.04 100.79 o 5 1 0 2958.39 2649.48 79.40 o 7 1 0 5528.00 4880.89 92.75 o 9 1 0 1949.82 1650.24 90.90 o 11 1 0 1890.45 1560.44 98.26 o 13 1 0 0.42 12.19 61.40 o 15 1 0 1107.86 1000.94 340.69 o 0 2 0 10358.37 10952.70 177.50 o 2 2 0 9923.67 8931.04 74.39 o 4 2 0 1777.57 1487.76 64.79 o 6 2 0 4995.23 4976.96 116.38 o 8 2 0 1950.28 1510.68 84.88 o 10 2 0 42.51 60.57 26.68 o 12 2 0 865.31 601.98 83.05 o 14 2 0 343.91 244.79 143.01 o 16 2 0 678.87 692.94 328.35 o 1 3 0 9375.37 9631.26 109.01 o 3 3 0 27344.94 25252.11 451.92 o 5 3 0 8327.49 7442.03 128.18 o 7 3 0 8507.50 8096.38 130.71 o 9 3 0 13315.78 11984.92 328.81 o 11 3 0 336.65 258.21 71.05 o 13 3 0 191.65 210.35 97.94 o 15 3 0 4898.63 5022.99 244.45 o 0 4 0 10019.22 10262.20 212.67 o 2 4 0 36510.89 37088.47 626.05 o 4 4 0 1093.49 992.07 40.26 o 6 4 0 14714.24 14446.18 271.72 o 8 4 0 26829.50 26582.67 454.30 o 10 4 0 6367.87 5827.49 194.17 o 12 4 0 2300.66 1946.73 113.29 o 14 4 0 215.36 93.82 86.96 o 16 4 0 1116.25 1340.55 476.66 o 1 5 0 2459.39 2274.42 41.56 o 3 5 0 3406.74 3340.99 64.28 o 5 5 0 0.41 2.75 17.33 o 7 5 0 286.11 322.68 37.20 o 9 5 0 1753.69 1700.96 99.37 o 11 5 0 384.02 371.43 75.35 o 13 5 0 1926.25 1958.12 156.50 o 15 5 0 0.99 31.18 57.50 o 0 6 0 47463.33 47406.00 960.98 o 2 6 0 11101.68 11082.82 119.51 o 4 6 0 656.23 661.56 43.44 o 6 6 0 839.68 650.23 40.95 o 8 6 0 7698.04 7130.98 160.22 o 10 6 0 6672.12 6467.63 241.37 o 12 6 0 4353.48 4053.18 173.47 o 14 6 0 110.84 116.87 65.72 o 1 7 0 32309.24 31700.46 425.54 o 3 7 0 12138.55 14111.11 169.73 o 5 7 0 7507.63 7760.00 185.12 o 7 7 0 21744.32 21064.70 330.69 o 9 7 0 11287.16 10898.25 345.25 o 11 7 0 7000.67 6918.75 158.03 o 13 7 0 1686.53 1677.17 112.71 o 15 7 0 1233.25 1027.22 175.73 o 0 8 0 19239.23 16829.11 230.09 o 2 8 0 15022.38 17804.35 195.73 o 4 8 0 12985.75 14350.80 343.80 o 6 8 0 1374.49 1208.17 63.19 o 8 8 0 203.13 149.31 35.20 o 10 8 0 224.63 225.99 35.82 o 12 8 0 7.53 26.93 28.68 o 14 8 0 41.65 37.36 49.79 o 1 9 0 909.55 881.90 36.85 o 3 9 0 1297.01 1121.99 70.32 o 5 9 0 1093.18 1246.71 66.79 o 7 9 0 2980.25 2731.18 123.31 o 9 9 0 2991.34 2887.14 96.81 o 11 9 0 446.88 512.63 87.89 o 13 9 0 203.82 240.72 62.34 o 0 10 0 35977.45 34728.26 714.20 o 2 10 0 30375.48 31249.83 584.10 o 4 10 0 79.36 82.79 25.29 o 6 10 0 8112.59 7973.71 219.43 o 8 10 0 15022.06 14694.85 384.73 o 10 10 0 11281.51 11330.24 240.45 o 12 10 0 339.24 344.62 86.48 o 14 10 0 483.56 555.48 124.00 o 1 11 0 10943.38 10553.28 292.57 o 3 11 0 3587.71 3607.96 151.73 o 5 11 0 167.20 181.13 39.91 o 7 11 0 6601.97 6165.29 158.69 o 9 11 0 3379.91 3560.78 119.96 o 11 11 0 297.07 288.38 53.33 o 13 11 0 85.73 45.94 61.48 o 0 12 0 6.45 37.49 23.46 o 2 12 0 178.48 210.37 34.55 o 4 12 0 300.82 278.40 37.92 o 6 12 0 94.60 93.49 24.38 o 8 12 0 399.67 412.77 45.11 o 10 12 0 12.24 18.22 32.23 o 12 12 0 14.49 5.70 68.27 o 1 13 0 21170.84 21185.91 423.54 o 3 13 0 268.52 220.41 61.57 o 5 13 0 953.51 922.40 92.30 o 7 13 0 4294.26 4250.42 123.53 o 9 13 0 1803.34 1822.69 100.53 o 11 13 0 891.82 961.07 176.79 o 0 14 0 19907.66 18813.59 1029.60 o 2 14 0 28587.06 29880.30 1321.93 o 4 14 0 11.39 30.22 27.86 o 6 14 0 3627.72 3414.49 197.09 o 8 14 0 15537.95 15284.38 457.09 o 10 14 0 6255.28 6087.49 222.65 o 12 14 0 398.47 274.22 95.57 o 1 15 0 7597.83 7039.35 223.79 o 3 15 0 96.96 120.61 36.64 o 5 15 0 8.73 20.87 28.79 o 7 15 0 582.72 627.84 134.54 o 9 15 0 978.73 1037.06 174.38 o 11 15 0 172.41 148.21 65.28 o 0 16 0 189.29 171.94 68.33 o 2 16 0 53.44 58.64 33.38 o 4 16 0 149.57 150.16 45.85 o 6 16 0 3123.44 3141.03 217.05 o 8 16 0 2342.23 2330.74 156.67 o 10 16 0 1428.84 1551.09 108.38 o 1 17 0 9227.17 8917.58 604.78 o 3 17 0 565.32 534.03 148.75 o 5 17 0 368.73 379.33 80.31 o 7 17 0 2823.91 2919.60 194.53 o 9 17 0 4856.88 4739.92 253.25 o 0 18 0 5360.99 5115.06 463.58 o 2 18 0 2242.20 2113.70 152.09 o 4 18 0 124.96 129.06 57.54 o 6 18 0 580.43 596.36 121.18 o 8 18 0 2063.17 2282.20 94.31 o 1 19 0 6.31 64.34 36.22 o 3 19 0 225.24 236.54 67.46 o 5 19 0 199.72 54.99 68.55 o 7 19 0 112.86 138.89 89.75 o 0 20 0 7431.85 7543.02 550.15 o 2 20 0 2868.14 3293.45 216.21 o 4 20 0 142.19 81.47 88.72 o 1 21 0 2368.45 2484.64 254.33 o -17 1 1 2129.15 2555.42 292.32 o -15 1 1 3263.09 3215.97 268.77 o -13 1 1 11186.97 10443.39 372.04 o -11 1 1 35.94 11.49 29.18 o -9 1 1 5462.18 5055.51 109.64 o -7 1 1 11357.32 9853.94 346.99 o -5 1 1 37022.31 34847.07 815.58 o -3 1 1 34681.33 32771.23 325.09 o -1 1 1 1881.22 2170.20 35.56 o 1 1 1 17058.30 15642.40 134.06 o 3 1 1 8921.11 8889.60 119.19 o 5 1 1 38020.57 39322.80 399.19 o 7 1 1 28.54 161.02 34.71 o 9 1 1 6074.10 5212.19 235.91 o 11 1 1 4824.40 4560.32 143.69 o 13 1 1 930.00 1084.78 247.25 o 15 1 1 108.68 36.46 52.64 o -16 2 1 806.00 1071.34 331.72 o -14 2 1 772.62 1131.60 359.34 o -12 2 1 150.32 174.98 45.89 o -10 2 1 2786.91 2556.28 146.63 o -8 2 1 40296.10 40167.31 733.35 o -6 2 1 9301.67 8573.12 301.36 o -4 2 1 5789.29 4939.89 109.07 o -2 2 1 1570.60 1589.06 41.09 o 0 2 1 24298.54 26332.96 279.87 o 4 2 1 8349.31 7446.10 106.56 o 6 2 1 8639.11 9569.65 153.80 o 8 2 1 14822.89 14138.32 436.26 o 10 2 1 12865.31 11952.17 326.35 o 12 2 1 1926.20 1910.49 128.28 o 14 2 1 2.33 76.84 56.80 o -17 3 1 824.96 770.94 143.20 o -15 3 1 1882.28 1920.02 142.40 o -13 3 1 1824.54 1844.30 93.47 o -11 3 1 1294.05 1070.43 72.24 o -9 3 1 111.21 72.78 34.99 o -7 3 1 7383.66 7344.11 317.29 o -5 3 1 6342.87 5749.23 186.51 o -3 3 1 2782.96 2619.90 53.96 o -1 3 1 1470.89 1476.74 36.12 o 1 3 1 5411.07 5268.50 75.80 o 3 3 1 1702.23 1608.14 80.18 o 5 3 1 5904.08 6073.12 117.73 o 7 3 1 4635.81 4240.81 162.41 o 9 3 1 456.50 440.96 48.60 o 11 3 1 763.10 741.39 133.80 o 13 3 1 527.56 475.52 115.93 o 15 3 1 31.70 -2.81 78.00 o -16 4 1 1121.04 1117.85 374.84 o -14 4 1 116.52 183.20 57.05 o -12 4 1 31.58 11.04 44.35 o -10 4 1 287.60 410.69 70.93 o -8 4 1 3784.17 3617.92 149.02 o -6 4 1 4228.60 3802.08 127.76 o -4 4 1 511.96 465.54 27.10 o -2 4 1 6880.29 6953.34 115.68 o 0 4 1 6883.11 7191.52 104.77 o 2 4 1 2603.77 2295.37 54.70 o 4 4 1 327.40 309.18 33.40 o 6 4 1 822.87 659.65 33.69 o 8 4 1 5405.13 5125.40 193.58 o 10 4 1 2236.57 2124.42 83.26 o 12 4 1 1561.30 1521.72 137.13 o 14 4 1 24.54 47.95 43.90 o -15 5 1 4936.26 5086.21 327.92 o -13 5 1 5798.19 5897.29 202.00 o -11 5 1 4358.64 4027.06 201.32 o -9 5 1 17132.20 16231.27 311.09 o -7 5 1 30053.56 28863.61 734.18 o -5 5 1 32142.61 31044.36 396.43 o -3 5 1 5304.27 5297.92 101.88 o -1 5 1 2288.44 2324.02 47.92 o 1 5 1 46375.63 44812.51 427.57 o 3 5 1 53290.19 51979.21 572.88 o 5 5 1 26.78 33.38 15.66 o 7 5 1 72.41 79.95 24.88 o 9 5 1 15714.00 14246.65 298.50 o 11 5 1 1845.64 1825.67 103.78 o 13 5 1 442.71 485.64 142.63 o 15 5 1 1630.54 1798.02 144.67 o -16 6 1 3248.42 3579.33 174.26 o -14 6 1 1580.58 1814.47 159.66 o -12 6 1 1386.74 1395.51 67.52 o -10 6 1 12227.69 12280.27 417.36 o -8 6 1 17528.52 17832.91 383.20 o -6 6 1 12225.13 12381.20 149.94 o -4 6 1 20004.01 19523.85 194.74 o -2 6 1 22604.32 22840.64 442.66 o 0 6 1 7385.76 7439.06 140.57 o 2 6 1 37628.29 37206.73 471.09 o 4 6 1 13581.81 13833.67 237.32 o 6 6 1 130.03 143.37 29.14 o 8 6 1 17599.14 17398.88 362.12 o 10 6 1 20587.01 20673.94 376.21 o 12 6 1 781.90 900.02 133.07 o 14 6 1 823.66 917.22 194.83 o -15 7 1 1264.72 1360.70 143.66 o -13 7 1 47.96 66.46 52.34 o -11 7 1 3523.16 3663.05 101.05 o -9 7 1 3465.62 3231.39 121.42 o -7 7 1 785.25 917.50 43.82 o -5 7 1 8938.55 10037.85 121.84 o -3 7 1 778.46 945.51 46.97 o -1 7 1 81.22 115.54 16.72 o 1 7 1 1901.65 2201.02 65.68 o 3 7 1 16117.53 17348.54 418.94 o 5 7 1 271.61 248.94 35.98 o 7 7 1 1748.51 1514.15 69.47 o 9 7 1 8341.19 7868.88 203.86 o 11 7 1 309.98 273.21 66.78 o 13 7 1 539.58 415.51 157.91 o -16 8 1 1768.41 1837.62 238.67 o -14 8 1 1530.49 1769.25 127.74 o -12 8 1 1094.37 1179.84 67.36 o -10 8 1 16650.09 16737.48 384.31 o -8 8 1 10334.06 9508.15 226.67 o -6 8 1 32402.73 34752.35 672.15 o -4 8 1 3419.18 3832.76 109.25 o -2 8 1 151.68 150.36 27.82 o 0 8 1 31973.91 34013.49 629.85 o 2 8 1 35107.97 35473.93 761.79 o 4 8 1 18968.10 20129.82 380.34 o 6 8 1 443.34 417.83 34.49 o 8 8 1 14419.11 13865.34 440.95 o 10 8 1 6931.98 7090.39 192.11 o 12 8 1 3220.81 3364.72 162.46 o 14 8 1 40.40 17.91 53.04 o -15 9 1 2935.46 3554.91 227.92 o -13 9 1 7898.66 8159.69 315.19 o -11 9 1 4060.09 4167.79 118.39 o -9 9 1 388.08 469.08 48.97 o -7 9 1 24846.90 25997.06 522.37 o -5 9 1 7576.94 7462.84 125.20 o -3 9 1 1578.20 1487.99 89.14 o -1 9 1 5514.82 5583.96 151.58 o 1 9 1 24946.68 26818.96 414.21 o 3 9 1 5323.29 4634.27 149.85 o 5 9 1 1526.93 1522.74 74.31 o 7 9 1 4076.85 4279.05 132.30 o 9 9 1 332.78 269.44 56.07 o 11 9 1 4866.41 5262.93 223.28 o 13 9 1 154.46 80.77 56.86 o -14 10 1 221.48 180.88 54.39 o -12 10 1 3259.80 3000.40 113.24 o -10 10 1 805.90 897.23 57.26 o -8 10 1 13.43 18.06 24.10 o -6 10 1 385.19 325.64 47.78 o -4 10 1 38.23 98.62 25.89 o -2 10 1 150.70 124.33 25.79 o 0 10 1 2279.86 2344.56 59.44 o 2 10 1 51.93 52.27 10.48 o 4 10 1 4988.86 5391.60 193.32 o 6 10 1 50.04 49.04 23.08 o 8 10 1 46.80 87.99 27.92 o 10 10 1 31.75 62.36 42.25 o 12 10 1 452.22 448.26 117.22 o -13 11 1 55.70 95.85 55.27 o -11 11 1 1116.43 1112.03 77.01 o -9 11 1 3594.42 3413.75 87.75 o -7 11 1 3076.49 2865.79 113.87 o -5 11 1 7303.99 7004.34 230.84 o -3 11 1 429.58 364.72 27.57 o -1 11 1 4015.15 3989.88 142.20 o 1 11 1 4582.50 4670.08 248.24 o 3 11 1 9099.38 8807.00 215.70 o 5 11 1 1104.14 1005.35 54.50 o 7 11 1 71.51 85.22 22.42 o 9 11 1 4657.58 4757.76 243.54 o 11 11 1 925.17 1050.50 228.59 o 13 11 1 310.57 267.68 110.87 o -14 12 1 967.33 1092.95 172.48 o -12 12 1 919.41 1000.52 108.84 o -10 12 1 1725.57 1760.17 73.93 o -8 12 1 12353.05 12173.71 321.53 o -6 12 1 11371.29 10908.05 344.29 o -4 12 1 1663.19 1560.20 68.56 o -2 12 1 6098.04 6374.99 228.24 o 0 12 1 16332.65 16351.17 415.41 o 2 12 1 27040.62 29916.26 1172.23 o 4 12 1 1704.06 1469.14 65.10 o 6 12 1 2.96 16.41 25.48 o 8 12 1 5880.68 5595.09 219.26 o 10 12 1 8738.37 8997.68 329.40 o 12 12 1 2268.18 2455.31 165.00 o -13 13 1 125.31 155.84 76.30 o -11 13 1 1.06 7.93 53.30 o -9 13 1 1796.93 1977.45 63.13 o -7 13 1 2157.95 2106.78 71.26 o -5 13 1 4217.60 4279.30 105.27 o -3 13 1 1105.51 958.06 59.99 o -1 13 1 5418.40 5595.31 206.84 o 1 13 1 792.04 811.19 83.92 o 3 13 1 7956.19 7888.36 283.21 o 5 13 1 411.17 438.15 82.17 o 7 13 1 1051.53 869.39 84.75 o 9 13 1 3712.29 3781.59 171.56 o 11 13 1 450.24 444.29 113.87 o -12 14 1 320.90 386.51 103.16 o -10 14 1 572.86 541.91 105.68 o -8 14 1 287.48 307.13 71.21 o -6 14 1 1477.69 1511.19 85.20 o -4 14 1 143.17 116.71 32.34 o -2 14 1 7813.35 7483.15 234.05 o 0 14 1 402.18 439.81 60.89 o 2 14 1 1453.93 1448.87 123.34 o 4 14 1 3588.95 3529.53 170.80 o 6 14 1 1492.87 1230.41 89.03 o 8 14 1 703.00 876.38 184.51 o 10 14 1 384.79 391.72 107.04 o -11 15 1 1.50 42.19 38.33 o -9 15 1 2960.00 2941.27 173.22 o -7 15 1 8686.78 8865.09 307.05 o -5 15 1 2967.61 3189.19 123.91 o -3 15 1 3350.47 3289.31 223.61 o -1 15 1 117.74 124.49 29.71 o 1 15 1 5501.43 5421.30 187.51 o 3 15 1 8430.80 8101.67 216.13 o 5 15 1 149.51 210.13 42.59 o 7 15 1 2288.76 2190.84 151.65 o 9 15 1 2252.55 2243.70 108.79 o -10 16 1 1731.94 1797.44 109.31 o -8 16 1 2888.82 2896.63 154.56 o -6 16 1 13063.09 12537.16 737.08 o -4 16 1 666.03 734.46 62.04 o -2 16 1 19.35 41.06 54.63 o 0 16 1 23236.88 23708.36 437.34 o 2 16 1 6401.25 6181.46 268.44 o 4 16 1 6198.06 6251.68 193.56 o 6 16 1 1979.17 1670.12 79.65 o 8 16 1 3714.85 4217.70 272.19 o -9 17 1 123.93 124.13 45.48 o -7 17 1 18.59 53.20 32.11 o -5 17 1 129.97 130.89 60.27 o -3 17 1 47.02 45.08 46.27 o -1 17 1 776.94 903.36 199.25 o 1 17 1 181.41 189.02 65.39 o 3 17 1 13.92 33.84 36.40 o 5 17 1 0.12 -13.74 46.33 o 7 17 1 56.41 56.48 38.92 o -8 18 1 3059.89 3379.53 272.55 o -6 18 1 2497.81 2418.48 161.80 o -4 18 1 1229.50 1260.45 162.08 o -2 18 1 727.47 773.56 207.73 o 0 18 1 3577.98 3756.32 331.26 o 2 18 1 2834.84 2864.01 203.26 o 4 18 1 997.08 1026.97 217.10 o 6 18 1 162.63 124.71 49.55 o -7 19 1 6691.09 6440.63 552.69 o -5 19 1 6118.89 6189.24 465.81 o -3 19 1 460.30 390.12 117.99 o -1 19 1 2481.85 2505.51 229.87 o 1 19 1 10362.03 11496.76 464.78 o 3 19 1 7097.31 7433.57 266.14 o 5 19 1 734.03 778.73 244.87 o -6 20 1 400.87 470.98 131.81 o -4 20 1 144.41 96.94 72.80 o -2 20 1 588.38 645.88 185.45 o 0 20 1 2027.72 2387.23 390.09 o 2 20 1 420.31 421.90 106.31 o 4 20 1 96.05 124.69 71.72 o -3 21 1 53.26 67.33 56.70 o -1 21 1 122.08 44.38 73.40 o 1 21 1 1009.22 1179.36 317.78 o -18 0 2 179.11 216.93 156.00 o -16 0 2 7446.68 6573.65 444.63 o -14 0 2 2950.76 2643.19 390.06 o -12 0 2 9954.36 9105.31 458.59 o -10 0 2 2235.34 2202.18 178.92 o -8 0 2 22357.47 22466.80 333.70 o -4 0 2 10401.48 10768.37 386.49 o -2 0 2 17508.76 18277.40 717.16 o 0 0 2 17693.62 16445.80 279.67 o 4 0 2 99407.22 93380.88 5176.21 o 6 0 2 1184.22 770.87 101.15 o 8 0 2 2462.06 2265.61 232.70 o 10 0 2 2196.17 2197.76 169.96 o 12 0 2 16851.39 16750.44 424.21 o 14 0 2 83.70 120.83 73.41 o -17 1 2 952.18 1029.44 280.69 o -15 1 2 951.51 844.00 302.71 o -13 1 2 6333.72 6226.90 272.53 o -11 1 2 978.48 989.10 64.91 o -9 1 2 364.12 513.28 77.05 o -7 1 2 7705.03 7343.54 256.05 o -5 1 2 209.97 262.54 45.19 o -3 1 2 15965.88 16958.86 182.81 o -1 1 2 4.18 27.26 7.15 o 1 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8885.12 511.74 o -16 2 15 971.38 592.39 247.57 o -14 2 15 556.16 318.51 123.82 o -12 2 15 390.51 489.07 143.56 o -10 2 15 570.23 591.47 213.67 o -15 3 15 4.38 31.90 64.74 o -13 3 15 15.22 37.02 61.70 o -11 3 15 97.04 135.95 102.51 o -14 4 15 1.82 79.93 57.81 o -12 4 15 422.73 433.97 181.91 o