#------------------------------------------------------------------------------
#$Date: 2016-04-03 01:44:07 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181088 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/68/2216824.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2216824_Fobs
loop_
_publ_author_name
'Bibila Mayaya Bisseyou, Yvon'
'Soro, Adama P.'
'Sissouma, Drissa'
'Giorgi, Michel'
'Ebby, N'd\'ed\'e'
_publ_section_title
;
 3-(3-Chlorophenyl)-1-(2-methylimidazo[1,2-<i>a</i>]pyridin-3-yl)prop-2-en-1-one
;
_journal_coeditor_code           WN2207
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o4758
_journal_page_last               o4759
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_date             07-09-26
_audit_creation_method           CRYSTALS
_cell_angle_alpha                90
_cell_angle_beta                 93.425(4)
_cell_angle_gamma                90
_cell_length_a                   4.784(2)
_cell_length_b                   21.690(2)
_cell_length_c                   13.773(9)
_cod_data_source_file            wn2207Isup2.hkl
_cod_data_source_block           I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_calc
_refln_F_squared_sigma
_refln_observed_status
1 1 0 6266.31 6612.89 156.74 o
1 2 0 1887.90 2094.45 48.66 o
2 2 0 7152.08 8057.37 167.45 o
2 3 0 912.04 937.63 19.33 o
3 3 0 105.27 109.40 8.41 o
2 4 0 9194.89 8946.68 187.94 o
3 4 0 5872.16 5751.40 125.67 o
2 5 0 523.49 526.76 17.85 o
3 5 0 231.95 247.83 8.53 o
2 6 0 28577.90 29585.56 652.53 o
3 6 0 673.40 642.52 17.65 o
4 6 0 1792.68 1727.04 66.90 o
1 7 0 10096.23 9787.30 546.61 o
2 7 0 7803.96 8436.44 201.42 o
3 7 0 1811.35 1657.76 40.01 o
4 7 0 126.56 164.20 7.43 o
0 8 0 9221.76 10110.75 391.80 o
1 8 0 1592.81 1408.45 42.30 o
2 8 0 14774.40 13769.62 289.29 o
3 8 0 24.70 0.04 14.11 <
4 8 0 426.84 425.53 16.11 o
1 9 0 213.16 209.62 24.82 o
2 9 0 10939.07 10693.22 202.90 o
3 9 0 726.84 690.79 23.72 o
4 9 0 60.53 75.52 10.11 o
0 10 0 608.61 541.80 29.11 o
1 10 0 6997.32 6771.92 194.07 o
2 10 0 15505.23 15541.75 296.36 o
3 10 0 92.16 110.90 13.25 o
4 10 0 76.21 87.56 12.92 o
5 10 0 26.94 31.09 11.00 o
1 11 0 296.53 226.47 18.94 o
2 11 0 1122.92 1108.03 44.23 o
3 11 0 7226.70 7074.31 137.72 o
4 11 0 93.70 90.82 12.39 o
5 11 0 8.88 2.24 19.91 <
0 12 0 80.46 47.04 22.60 o
1 12 0 1359.40 1425.52 39.08 o
2 12 0 3846.48 3506.19 75.66 o
3 12 0 4148.65 4254.14 90.17 o
4 12 0 36.24 43.95 16.98 o
5 12 0 266.67 211.59 29.07 o
1 13 0 229.52 183.80 17.27 o
2 13 0 148.84 108.70 21.72 o
3 13 0 9759.46 9857.99 193.63 o
4 13 0 178.49 154.88 18.97 o
5 13 0 33.87 22.78 24.09 <
0 14 0 951.11 902.56 40.09 o
1 14 0 8390.56 8200.73 166.71 o
2 14 0 934.52 914.83 31.79 o
3 14 0 847.97 773.66 33.20 o
4 14 0 11.09 0.17 16.12 <
5 14 0 -29.27 6.52 24.78 <
1 15 0 761.21 733.31 27.59 o
2 15 0 57.30 20.09 17.87 o
3 15 0 125.66 138.14 21.97 o
4 15 0 165.38 233.16 21.86 o
0 16 0 1248.21 1303.62 59.35 o
1 16 0 244.61 203.45 20.96 o
2 16 0 49.42 42.80 22.64 o
3 16 0 871.43 881.15 40.15 o
4 16 0 1031.69 1043.97 46.25 o
1 17 0 689.59 677.87 31.51 o
2 17 0 70.06 0.10 29.46 o
3 17 0 218.15 234.92 20.09 o
4 17 0 426.42 480.93 26.43 o
0 18 0 62.57 65.54 25.63 o
1 18 0 2271.48 2137.34 56.24 o
2 18 0 2622.46 2677.16 71.69 o
3 18 0 301.72 302.86 26.75 o
4 18 0 828.86 1006.89 39.15 o
1 19 0 2796.29 2785.06 66.63 o
2 19 0 125.89 142.50 25.81 o
3 19 0 -33.76 0.47 21.15 <
4 19 0 82.45 54.99 34.87 o
0 20 0 175.56 195.41 33.39 o
1 20 0 6385.61 5911.02 137.45 o
2 20 0 430.98 481.37 34.88 o
3 20 0 38.94 20.87 32.32 <
1 21 0 205.64 225.04 27.53 o
2 21 0 78.68 80.82 25.37 o
3 21 0 -27.98 1.16 26.34 <
0 22 0 1128.29 1115.08 60.46 o
1 22 0 449.86 372.12 44.54 o
2 22 0 62.41 6.94 32.23 <
3 22 0 212.87 158.10 42.02 o
1 23 0 597.80 686.28 38.14 o
2 23 0 166.15 148.91 36.87 o
3 23 0 68.39 71.12 33.58 o
0 24 0 8003.09 7817.69 354.26 o
1 24 0 -57.30 0.75 31.95 <
2 24 0 73.44 87.36 36.51 o
1 25 0 11.90 9.79 37.88 <
2 25 0 286.96 406.27 32.86 o
0 26 0 17.64 91.46 48.55 <
1 26 0 144.72 114.75 57.74 o
-1 1 1 654.85 552.11 15.35 o
0 1 1 0.20 0.00 2.97 <
2 1 1 2992.09 3200.18 70.02 o
-2 2 1 127.69 115.59 6.78 o
-1 2 1 22377.17 24036.05 568.44 o
0 2 1 16837.66 0.00 539.80 x
2 2 1 13754.60 14194.82 286.16 o
-3 3 1 -16.00 9793.53 6.16 <
-2 3 1 1275.20 1141.85 41.42 o
-1 3 1 846.81 1048.12 19.21 o
0 3 1 31.02 0.00 5.90 x
2 3 1 1419.78 1317.89 42.96 o
3 3 1 46.24 47.67 5.44 o
-3 4 1 428.90 429.94 12.84 o
-2 4 1 7464.96 7571.60 203.90 o
2 4 1 8.82 6.75 8.43 <
3 4 1 28.84 26.80 5.16 o
-3 5 1 382.98 437.22 11.35 o
-2 5 1 749.66 792.07 25.74 o
0 5 1 19.10 64.70 6.64 o
2 5 1 499.52 376.97 15.20 o
3 5 1 5548.76 5691.30 110.25 o
-4 6 1 585.64 572.15 24.20 o
-3 6 1 314.35 281.69 12.06 o
-2 6 1 3504.64 2768.45 104.19 o
-1 6 1 11272.07 12307.60 227.20 o
0 6 1 4122.92 4262.21 84.76 o
1 6 1 263.09 215.06 15.25 o
2 6 1 10302.25 10360.89 249.69 o
3 6 1 0.20 2.80 6.65 <
4 6 1 219.93 229.40 13.94 o
-4 7 1 4209.41 4196.69 96.02 o
-3 7 1 2520.04 2428.88 52.21 o
-2 7 1 17580.11 17921.73 357.99 o
-1 7 1 13354.11 14086.20 369.79 o
0 7 1 713.42 708.65 18.16 o
1 7 1 2157.60 2190.88 65.96 o
3 7 1 879.12 829.73 23.13 o
4 7 1 240.56 223.70 9.62 o
-4 8 1 229.83 247.85 13.34 o
-3 8 1 431.39 410.42 16.62 o
-2 8 1 6052.84 5353.02 119.81 o
-1 8 1 536.85 511.86 42.17 o
0 8 1 216.38 232.98 13.53 o
1 8 1 15244.84 16340.36 442.02 o
3 8 1 278.22 247.25 15.35 o
4 8 1 79.39 55.74 8.55 o
-4 9 1 166.67 110.03 11.88 o
-3 9 1 477.86 472.06 20.55 o
-2 9 1 2311.69 2218.76 49.04 o
-1 9 1 56444.27 55463.96 1553.77 o
0 9 1 13579.24 13854.84 321.62 o
1 9 1 215.21 215.75 19.95 o
3 9 1 8804.07 8785.82 172.65 o
4 9 1 618.02 627.64 23.37 o
-5 10 1 32.26 13.80 12.61 o
-4 10 1 95.26 74.01 13.08 o
-3 10 1 199.37 209.98 16.94 o
-2 10 1 3960.19 3438.15 93.14 o
-1 10 1 955.43 942.10 59.35 o
0 10 1 3881.29 3698.48 92.20 o
1 10 1 2297.28 2223.23 69.02 o
3 10 1 4111.37 4062.46 84.64 o
4 10 1 78.32 34.76 14.87 o
5 10 1 208.22 227.57 18.18 o
-5 11 1 167.18 183.82 25.60 o
-4 11 1 372.10 357.68 18.90 o
-3 11 1 4668.99 4452.92 98.40 o
-2 11 1 919.30 892.07 29.11 o
-1 11 1 216.09 338.45 20.58 o
0 11 1 24077.73 24508.14 437.58 o
1 11 1 7714.11 8135.97 252.95 o
2 11 1 188.79 147.78 18.69 o
3 11 1 2401.98 2353.54 51.95 o
4 11 1 21.16 30.90 13.71 <
5 11 1 -16.16 0.64 14.39 <
-5 12 1 63.04 41.11 17.79 o
-4 12 1 17.64 1.61 18.23 <
-3 12 1 21.53 36.07 14.01 <
-2 12 1 484.00 462.59 22.44 o
-1 12 1 320.05 315.35 19.68 o
0 12 1 651.27 693.31 26.54 o
1 12 1 598.78 671.13 24.96 o
2 12 1 163.33 210.70 16.61 o
3 12 1 5105.10 5081.77 101.46 o
4 12 1 188.24 162.57 21.68 o
5 12 1 -6.40 15.97 19.38 <
-5 13 1 222.01 174.40 35.46 o
-4 13 1 152.77 153.52 16.07 o
-3 13 1 3717.34 3597.96 82.92 o
-2 13 1 1313.34 1397.24 39.86 o
-1 13 1 6012.45 5683.87 117.86 o
0 13 1 641.61 623.06 25.33 o
1 13 1 15.68 0.56 13.46 <
2 13 1 511.21 542.31 24.87 o
3 13 1 5835.43 5913.12 120.70 o
4 13 1 165.38 176.69 19.03 o
5 13 1 5.71 19.60 31.12 <
-5 14 1 176.62 184.52 34.55 o
-4 14 1 40.20 0.79 21.18 <
-3 14 1 949.26 893.26 38.20 o
-2 14 1 10102.26 9963.63 188.96 o
-1 14 1 13.47 0.40 14.75 <
0 14 1 1374.18 1278.73 37.07 o
1 14 1 43.96 3.99 18.70 o
2 14 1 2613.25 2544.59 60.32 o
3 14 1 2272.43 2233.07 77.23 o
4 14 1 290.02 352.39 23.16 o
-4 15 1 43.43 13.32 19.90 o
-3 15 1 629.01 673.06 33.61 o
-2 15 1 258.57 305.15 24.76 o
-1 15 1 1409.25 1295.67 36.04 o
0 15 1 4261.48 4023.70 84.86 o
1 15 1 642.12 601.75 24.83 o
2 15 1 15343.78 14938.16 299.77 o
3 15 1 1108.22 1014.78 40.61 o
4 15 1 138.77 152.95 24.50 o
-4 16 1 32.38 4.47 23.10 <
-3 16 1 921.73 951.91 35.82 o
-2 16 1 749.66 751.92 30.67 o
-1 16 1 1932.48 1890.83 51.87 o
0 16 1 5162.42 4942.12 109.21 o
1 16 1 2755.20 3035.05 65.09 o
2 16 1 5172.49 5198.77 113.63 o
3 16 1 27.46 16.80 18.76 <
4 16 1 535.00 768.32 31.92 o
-4 17 1 1077.15 1116.91 42.01 o
-3 17 1 272.58 296.00 24.76 o
-2 17 1 653.82 613.99 43.98 o
-1 17 1 710.76 586.99 31.99 o
0 17 1 1239.04 1255.86 42.94 o
1 17 1 64.64 7.78 26.05 o
2 17 1 1871.43 1688.96 63.16 o
3 17 1 1882.69 1879.13 59.88 o
4 17 1 1810.50 2015.04 60.42 o
-4 18 1 38.19 0.02 28.06 <
-3 18 1 -9.80 44.80 23.79 <
-2 18 1 558.38 623.47 32.61 o
-1 18 1 964.72 918.92 36.65 o
0 18 1 2213.70 2187.04 53.64 o
1 18 1 7.40 2.48 23.88 <
2 18 1 164.61 192.66 23.09 o
3 18 1 148.84 149.03 26.11 o
4 18 1 46.38 60.63 21.79 o
-4 19 1 52.85 64.15 34.75 <
-3 19 1 144.24 115.32 27.86 o
-2 19 1 21.81 14.26 18.77 <
-1 19 1 2493.00 2333.28 64.91 o
0 19 1 446.05 422.12 30.84 o
1 19 1 727.92 660.67 32.92 o
2 19 1 3.31 0.31 21.15 <
3 19 1 266.02 296.81 27.40 o
4 19 1 203.06 213.68 31.64 o
-3 20 1 28.20 14.54 21.98 <
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0 20 1 372.49 344.25 28.56 o
1 20 1 1112.89 1119.90 43.37 o
2 20 1 48.16 2.56 29.01 <
3 20 1 63.04 43.31 25.73 o
-3 21 1 167.96 170.39 27.99 o
-2 21 1 24.60 5.04 24.30 <
-1 21 1 97.61 109.22 25.89 o
0 21 1 865.54 826.11 37.07 o
1 21 1 71.40 26.82 26.03 o
2 21 1 271.92 272.49 34.96 o
3 21 1 93.12 41.23 34.55 o
-3 22 1 52.56 38.74 27.69 <
-2 22 1 16.00 6.65 20.40 <
-1 22 1 135.02 53.53 35.09 o
0 22 1 20.43 23.58 22.96 <
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2 22 1 906.61 1011.58 47.57 o
3 22 1 338.56 344.34 44.90 o
-3 23 1 62.88 103.38 39.97 <
-2 23 1 13.99 17.82 26.70 <
-1 23 1 184.69 154.21 27.45 o
0 23 1 239.01 190.12 35.87 o
1 23 1 10.82 28.07 27.11 <
2 23 1 299.64 232.84 39.12 o
-2 24 1 -7.62 18.52 19.60 <
-1 24 1 158.26 209.58 35.48 o
0 24 1 609.10 613.13 40.97 o
1 24 1 225.90 294.02 32.77 o
2 24 1 5.20 4.27 35.98 <
-2 25 1 89.11 180.02 33.61 o
-1 25 1 180.36 171.20 43.51 o
0 25 1 57.30 90.29 34.67 <
1 25 1 51.41 0.09 41.44 <
2 25 1 -60.06 0.41 27.43 <
-1 26 1 36.97 38.36 32.95 <
0 26 1 -4.08 118.04 38.30 <
1 26 1 5.62 21.46 57.69 <
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0 0 2 37.70 0.00 8.47 x
2 0 2 1748.08 1790.13 46.83 o
-3 1 2 2095.81 2341.16 65.01 o
-2 1 2 10621.36 10579.35 228.79 o
-1 1 2 1291.68 1540.20 26.60 o
0 1 2 8.70 0.00 5.90 <
2 1 2 2739.48 2511.39 54.43 o
3 1 2 4846.94 4746.59 136.46 o
-3 2 2 74.82 4300.20 10.73 o
-2 2 2 3306.25 3444.40 65.55 o
-1 2 2 3323.52 3619.45 70.33 o
0 2 2 69.72 0.00 6.18 x
1 2 2 2304.00 2016.72 45.12 o
2 2 2 4406.30 4159.25 84.97 o
3 2 2 333.06 312.31 10.22 o
-3 3 2 1352.03 1317.05 29.42 o
-2 3 2 15878.52 15910.30 312.50 o
-1 3 2 19332.12 20263.24 411.56 o
0 3 2 433.47 369.21 13.32 o
1 3 2 20612.35 21588.62 413.48 o
2 3 2 180.10 125.52 8.59 o
3 3 2 151.78 135.37 7.39 o
-3 4 2 882.09 1013.70 24.95 o
-2 4 2 28247.53 27523.33 1052.12 o
-1 4 2 18594.05 20463.76 365.44 o
0 4 2 791.86 784.51 18.57 o
2 4 2 956.66 857.13 22.27 o
3 4 2 205.92 179.79 9.47 o
-4 5 2 717.70 922.35 34.29 o
-3 5 2 182.25 189.84 9.18 o
-2 5 2 23448.80 22339.75 456.33 o
-1 5 2 4935.06 4912.84 95.54 o
2 5 2 31176.97 31742.36 653.31 o
3 5 2 980.94 900.92 24.43 o
4 5 2 1545.28 1487.18 54.25 o
-4 6 2 374.42 355.24 22.83 o
-3 6 2 1393.53 1430.70 32.10 o
-2 6 2 966.59 1106.32 23.63 o
-1 6 2 8779.69 9000.78 181.78 o
0 6 2 14747.67 15001.95 279.31 o
1 6 2 3728.32 3696.64 75.71 o
2 6 2 511.21 533.19 17.18 o
3 6 2 91.39 78.83 10.13 o
4 6 2 2619.39 2610.93 57.32 o
-4 7 2 48.72 51.45 6.56 o
-3 7 2 655.87 668.76 22.02 o
-2 7 2 161.29 173.67 14.73 o
-1 7 2 -5.29 7.87 8.37 <
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1 7 2 1.10 31.56 11.82 <
2 7 2 2876.18 2971.62 67.57 o
3 7 2 3316.61 3188.38 70.26 o
4 7 2 8179.39 7933.53 193.54 o
-4 8 2 229.22 251.03 16.65 o
-3 8 2 18.06 25.04 10.12 <
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-1 8 2 9410.94 9329.37 201.78 o
0 8 2 6760.13 7206.44 185.82 o
1 8 2 15732.68 15125.16 296.01 o
2 8 2 2270.52 2007.91 60.04 o
3 8 2 2150.18 2343.28 44.52 o
4 8 2 2646.07 2814.29 64.81 o
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-3 9 2 398.00 402.05 16.76 o
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-1 9 2 25924.22 24875.22 615.06 o
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1 9 2 8091.00 8215.94 187.10 o
2 9 2 57.15 2.70 19.66 o
3 9 2 2751.00 2766.72 61.89 o
4 9 2 69.06 71.61 12.63 o
5 9 2 212.58 208.25 13.71 o
-5 10 2 28.09 18.02 12.93 o
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-1 10 2 472.19 641.96 22.16 o
0 10 2 1080.44 1193.09 27.61 o
1 10 2 1720.59 1740.21 42.31 o
2 10 2 3866.35 3821.39 126.85 o
3 10 2 901.80 861.59 29.43 o
4 10 2 140.42 145.51 14.46 o
5 10 2 5.62 0.03 13.22 <
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-4 11 2 154.75 216.26 14.93 o
-3 11 2 2103.14 2185.14 48.61 o
-2 11 2 4296.80 4046.17 89.15 o
-1 11 2 1352.77 1317.23 41.19 o
0 11 2 4548.15 4625.03 91.72 o
1 11 2 7020.76 6719.84 169.26 o
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3 11 2 774.51 688.52 26.16 o
4 11 2 326.16 313.64 20.23 o
5 11 2 46.65 82.24 17.62 o
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0 12 2 1365.30 1366.90 35.47 o
1 12 2 8988.94 8448.85 227.54 o
2 12 2 7.62 1.29 12.92 <
3 12 2 14172.90 13964.01 283.34 o
4 12 2 570.25 610.89 21.49 o
5 12 2 110.25 108.08 18.69 o
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0 13 2 871.43 844.82 28.34 o
1 13 2 313.29 329.54 21.59 o
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3 13 2 5346.53 5375.80 112.60 o
4 13 2 219.63 253.76 19.56 o
5 13 2 273.24 234.17 29.09 o
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-1 14 2 429.73 380.71 21.56 o
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1 14 2 47.61 11.23 14.90 o
2 14 2 1741.39 1584.96 48.41 o
3 14 2 355.32 298.00 26.39 o
4 14 2 221.41 294.55 19.05 o
-4 15 2 466.99 480.69 28.53 o
-3 15 2 37.58 23.23 25.99 <
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-1 15 2 9874.40 9158.82 194.77 o
0 15 2 188.51 160.96 18.95 o
1 15 2 3134.88 2866.25 70.55 o
2 15 2 765.63 834.58 29.33 o
3 15 2 583.22 566.04 39.61 o
4 15 2 299.29 253.30 26.64 o
-4 16 2 -2.89 20.85 20.67 <
-3 16 2 16.48 28.67 19.08 <
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-1 16 2 271.26 263.80 23.72 o
0 16 2 3188.86 3051.99 70.02 o
1 16 2 464.83 456.34 28.03 o
2 16 2 1540.56 1640.56 42.39 o
3 16 2 22.28 31.44 17.37 <
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-4 17 2 230.13 255.26 24.88 o
-3 17 2 332.70 352.70 29.55 o
-2 17 2 1147.18 1196.86 54.19 o
-1 17 2 4165.41 3906.97 98.10 o
0 17 2 312.23 246.44 26.51 o
1 17 2 31.14 1.81 20.53 <
2 17 2 183.60 238.31 26.02 o
3 17 2 967.83 1017.34 40.44 o
4 17 2 2209.94 2499.40 62.99 o
-4 18 2 205.35 174.39 31.24 o
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-1 18 2 110.88 85.36 27.17 o
0 18 2 40.32 3.79 22.86 <
1 18 2 2322.28 2336.69 58.79 o
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3 18 2 99.40 120.47 30.91 o
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1 19 2 344.10 380.10 31.16 o
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